DTA measure 1VFGHE9Pb(4) Date: 2024925:1116 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1135.79 s Mass = 958.800 mg data_number = 1413 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2115 0.6148 229.6449 229.0301 265.9785 2.0635 0.6190 229.9086 229.2896 266.0037 2.8555 0.6201 230.1531 229.5330 266.0244 3.6485 0.6227 230.3875 229.7648 266.0350 4.4708 0.6244 230.6309 230.0065 266.0647 5.2335 0.6260 230.8536 230.2276 266.0777 6.0855 0.6287 231.1034 230.4747 266.0866 6.8475 0.6270 231.3312 230.7042 266.1236 7.6695 0.6300 231.5757 230.9456 266.1532 8.4915 0.6295 231.8123 231.1828 266.1841 9.2530 0.6407 232.0431 231.4024 266.2326 10.1018 0.6780 232.3191 231.6411 266.3120 10.8898 0.7146 232.5560 231.8413 266.3655 11.6780 0.7148 232.7781 232.0633 266.4141 12.4958 0.6950 232.9932 232.2981 266.4570 13.2540 0.6553 233.1948 232.5395 266.5109 14.1025 0.6560 233.4352 232.7792 266.5998 14.8913 0.6883 233.6816 232.9933 266.7034 15.6823 0.6993 233.9184 233.2191 266.7803 16.5023 0.7023 234.1556 233.4533 266.8815 17.2625 0.6917 234.3510 233.6594 266.9577 18.1145 0.6553 234.5731 233.9179 267.0448 18.9065 0.6489 234.7896 234.1407 267.1289 19.6985 0.6739 235.0434 234.3695 267.2409 20.5205 0.6981 235.2847 234.5866 267.3725 21.2825 0.6810 235.4795 234.7986 267.4720 22.1345 0.6548 235.6946 235.0397 267.5812 22.8965 0.6479 235.9086 235.2607 267.7040 23.7185 0.6469 236.1392 235.4924 267.8217 24.5405 0.6734 236.3764 235.7031 267.9837 25.3025 0.7006 236.6033 235.9027 268.1294 26.1540 0.6953 236.8424 236.1470 268.2746 26.9460 0.6972 237.0528 236.3556 268.4189 27.7378 0.6797 237.2576 236.5780 268.5452 28.5600 0.6555 237.4791 236.8237 268.6710 29.3215 0.6807 237.6974 237.0167 268.8176 30.1740 0.6961 237.9280 237.2320 268.9673 30.9658 0.7026 238.1437 237.4411 269.1017 31.7575 0.7126 238.3582 237.6457 269.2311 32.5800 0.7056 238.5794 237.8738 269.3601 33.3425 0.7078 238.7871 238.0792 269.5047 34.1948 0.7072 239.0176 238.3104 269.6339 34.9868 0.7061 239.2155 238.5094 269.7660 35.7785 0.7055 239.4335 238.7280 269.8744 36.6008 0.6923 239.6473 238.9550 270.0036 37.3925 0.6905 239.8536 239.1631 270.1176 38.2148 0.6829 240.0763 239.3933 270.2334 39.0068 0.6515 240.2668 239.6154 270.3219 39.7995 0.6264 240.4658 239.8393 270.4256 40.6218 0.6255 240.6888 240.0633 270.5281 41.4133 0.6291 240.8796 240.2505 270.6324 42.2320 0.6447 241.1088 240.4641 270.7595 43.0200 0.7126 241.3501 240.6375 270.8896 43.8080 0.7636 241.5498 240.7862 271.0003 44.6273 0.7515 241.7535 241.0019 271.0906 45.4160 0.6463 241.9459 241.2995 271.1597 46.2355 0.6270 242.1497 241.5228 271.2521 47.0243 0.6484 242.3717 241.7233 271.3904 47.8130 0.6571 242.5759 241.9188 271.4785 48.6313 0.6550 242.7862 242.1313 271.5947 49.4210 0.6536 243.0051 242.3515 271.6986 50.2428 0.6452 243.2106 242.5654 271.7903 51.0345 0.6413 243.4097 242.7684 271.8772 51.8265 0.6348 243.5932 242.9584 271.9865 52.6485 0.6376 243.8178 243.1802 272.0977 53.4405 0.6381 244.0209 243.3828 272.2023 54.2628 0.6345 244.2162 243.5816 272.3328 55.0548 0.6272 244.4132 243.7860 272.4231 55.8465 0.6212 244.6074 243.9862 272.5037 56.6688 0.6120 244.8171 244.2050 272.6080 57.4605 0.5869 244.9984 244.4116 272.6919 58.2825 0.5783 245.2079 244.6296 272.7853 59.0745 0.5655 245.3914 244.8259 272.8787 59.8665 0.5556 245.5912 245.0355 272.9899 60.6885 0.5518 245.8035 245.2517 273.0930 61.4805 0.5471 245.9957 245.4486 273.2018 62.3033 0.5444 246.1830 245.6386 273.3186 63.0955 0.5460 246.3830 245.8371 273.4250 63.8885 0.5417 246.5738 246.0322 273.5012 64.7105 0.5357 246.7935 246.2577 273.6119 65.5025 0.5323 246.9793 246.4470 273.7206 66.3253 0.5313 247.1831 246.6518 273.8260 67.1175 0.5483 247.3903 246.8420 273.9316 67.9098 0.5559 247.5844 247.0285 274.0490 68.7320 0.5636 247.7994 247.2359 274.1484 69.5238 0.5559 247.9778 247.4220 274.2576 70.3465 0.5513 248.1637 247.6124 274.3602 71.1388 0.5444 248.3577 247.8133 274.4578 71.9315 0.5472 248.5519 248.0047 274.5573 72.7543 0.5454 248.7562 248.2108 274.6726 73.5450 0.5393 248.9412 248.4018 274.7738 74.3633 0.5366 249.1447 248.6081 274.8849 75.1515 0.5201 249.3239 248.8038 274.9913 75.9390 0.5576 249.5192 248.9616 275.0825 76.7573 0.5740 249.6929 249.1188 275.1658 77.5450 0.5821 249.8814 249.2993 275.2478 78.3640 0.5739 250.0715 249.4976 275.3566 79.1525 0.5673 250.2566 249.6893 275.4553 79.9420 0.5377 250.4314 249.8937 275.5408 80.7613 0.4764 250.6240 250.1476 275.6287 81.5525 0.4773 250.8214 250.3440 275.7415 82.3738 0.5242 251.0135 250.4894 275.8477 83.1660 0.5243 251.1970 250.6726 275.9732 83.9575 0.5206 251.3796 250.8589 276.0956 84.7800 0.5208 251.5742 251.0534 276.2116 85.5415 0.5196 251.7430 251.2235 276.3048 86.3940 0.5277 251.9382 251.4105 276.4452 87.1860 0.5384 252.1261 251.5877 276.5765 87.9775 0.5256 252.3037 251.7781 276.6935 88.7998 0.5167 252.5055 251.9887 276.8142 89.5615 0.4705 252.6826 252.2122 276.9296 90.4138 0.4209 252.8766 252.4557 277.0753 91.1758 0.4096 253.0414 252.6318 277.1978 91.9978 0.4041 253.2393 252.8352 277.3199 92.8198 0.4014 253.4333 253.0319 277.4552 93.5815 0.3954 253.6142 253.2188 277.5643 94.4343 0.3944 253.8167 253.4224 277.6853 95.1965 0.3875 253.9821 253.5947 277.8031 96.0188 0.3786 254.1627 253.7841 277.9037 96.8410 0.3736 254.3328 253.9592 278.0051 97.6035 0.4100 254.5104 254.1005 278.1124 98.4555 0.6140 254.6937 254.0797 278.2108 99.2175 0.5247 254.8421 254.3174 278.3022 100.0395 0.5110 255.0288 254.5177 278.4065 100.8315 0.5085 255.2011 254.6926 278.4974 101.6235 0.5063 255.3718 254.8655 278.6057 102.4760 0.5046 255.5449 255.0403 278.7149 103.2385 0.5014 255.7113 255.2099 278.7963 104.0613 0.4922 255.9168 255.4247 278.9159 104.8535 0.4865 256.0793 255.5928 279.0189 105.6425 0.4778 256.2595 255.7817 279.1120 106.4910 0.4758 256.4359 255.9602 279.2186 107.2490 0.4663 256.6078 256.1414 279.3236 108.0670 0.4644 256.7814 256.3170 279.4236 108.8573 0.4543 256.9616 256.5074 279.5397 109.6478 0.4450 257.1240 256.6790 279.6357 110.4965 0.4497 257.3137 256.8640 279.7369 111.2550 0.4396 257.4830 257.0434 279.8265 112.0750 0.4154 257.6545 257.2391 279.9324 112.8660 0.4117 257.8121 257.4004 280.0503 113.6575 0.4119 257.9875 257.5756 280.1405 114.5095 0.4089 258.1808 257.7719 280.2573 115.2710 0.4368 258.3443 257.9075 280.3512 116.0925 0.5104 258.5527 258.0422 280.4902 116.8845 0.6419 258.7394 258.0976 280.5979 117.6765 0.5923 258.8885 258.2962 280.6898 118.4985 0.4878 259.0539 258.5661 280.7742 119.2905 0.3873 259.2260 258.8386 280.8905 120.1125 0.3683 259.4221 259.0538 281.0000 120.9045 0.3055 259.5615 259.2560 281.0760 121.6965 0.2414 259.6957 259.4544 281.1426 122.5185 0.2217 259.8596 259.6379 281.2408 123.3105 0.2149 260.0290 259.8141 281.3363 124.1320 0.2100 260.2133 260.0034 281.4508 124.9245 0.2100 260.3603 260.1503 281.5375 125.7173 0.2341 260.5349 260.3008 281.6710 126.5390 0.2320 260.7171 260.4850 281.7886 127.3308 0.2286 260.8880 260.6594 281.8892 128.1528 0.2151 261.0467 260.8316 282.0034 128.9448 0.1891 261.1814 260.9923 282.0897 129.7365 0.2342 261.3715 261.1373 282.2180 130.5588 0.2055 261.5373 261.3318 282.3273 131.3505 0.1716 261.7023 261.5307 282.4343 132.1728 0.1628 261.8786 261.7157 282.5622 132.9648 0.1558 262.0377 261.8819 282.6998 133.7565 0.1501 262.1952 262.0451 282.8050 134.6093 0.1454 262.3770 262.2316 282.9370 135.3715 0.1411 262.5365 262.3954 283.0539 136.1945 0.1356 262.6906 262.5550 283.1688 136.9865 0.1301 262.8455 262.7154 283.3013 137.7785 0.1279 263.0171 262.8892 283.4219 138.5990 0.1227 263.1833 263.0606 283.5313 139.3868 0.1166 263.3337 263.2171 283.6535 140.2060 0.1109 263.5125 263.4016 283.7785 140.9943 0.1074 263.6727 263.5653 283.8852 141.7840 0.1024 263.8281 263.7257 283.9980 142.6025 0.0989 263.9972 263.8983 284.0943 143.3910 0.0927 264.1530 264.0603 284.1890 144.2100 0.0864 264.3191 264.2326 284.3156 144.9990 0.0803 264.4767 264.3963 284.4100 145.7900 0.0731 264.6389 264.5658 284.5137 146.6405 0.0695 264.8107 264.7413 284.6010 147.4025 0.0641 264.9651 264.9010 284.6909 148.2245 0.0599 265.1262 265.0663 284.8069 149.0168 0.0548 265.2873 265.2325 284.9237 149.8085 0.0516 265.4436 265.3920 285.0251 150.6608 0.0506 265.6138 265.5632 285.1231 151.4225 0.0442 265.7562 265.7120 285.2067 152.2448 0.0370 265.9051 265.8681 285.3044 153.0368 0.0327 266.0749 266.0422 285.3972 153.8285 0.0266 266.2307 266.2041 285.4970 154.6505 0.0228 266.3988 266.3760 285.6018 155.4425 0.0179 266.5538 266.5359 285.7035 156.2645 0.0136 266.7130 266.6994 285.7992 157.0565 0.0094 266.8646 266.8552 285.9082 157.8485 0.0030 267.0279 267.0249 285.9893 158.6705 -0.0020 267.1776 267.1797 286.0949 159.4625 -0.0060 267.3262 267.3321 286.1856 160.2845 -0.0093 267.4959 267.5052 286.2875 161.0765 -0.0161 267.6458 267.6619 286.3829 161.8695 -0.0203 267.7895 267.8098 286.4602 162.7210 -0.0240 267.9508 267.9748 286.5739 163.4835 -0.0289 268.1105 268.1394 286.6625 164.3053 -0.0353 268.2745 268.3098 286.7540 165.0975 -0.0374 268.4122 268.4496 286.8547 165.8885 -0.0432 268.5579 268.6011 286.9733 166.7415 -0.0477 268.7366 268.7843 287.0739 167.5035 -0.0514 268.8898 268.9412 287.1686 168.3258 -0.0569 269.0398 269.0967 287.2985 169.1480 -0.0627 269.1946 269.2573 287.4150 169.9108 -0.0670 269.3499 269.4169 287.5144 170.7600 -0.0699 269.5129 269.5827 287.6286 171.5180 -0.0739 269.6491 269.7230 287.7425 172.3363 -0.0783 269.8068 269.8851 287.8628 173.1540 -0.0850 269.9607 270.0457 287.9937 173.9128 -0.0882 270.0961 270.1843 288.0914 174.7618 -0.0887 270.2485 270.3372 288.2083 175.5203 -0.0926 270.3940 270.4865 288.3331 176.3405 -0.0978 270.5462 270.6440 288.4539 177.1605 -0.1033 270.6942 270.7974 288.5688 177.9213 -0.1106 270.8490 270.9596 288.6861 178.7720 -0.1212 271.0044 271.1256 288.8144 179.5340 -0.1291 271.1546 271.2837 288.9251 180.3555 -0.1372 271.3056 271.4427 289.0487 181.1463 -0.1424 271.4586 271.6010 289.1784 181.9375 -0.1467 271.5918 271.7386 289.2953 182.7900 -0.1491 271.7564 271.9055 289.4201 183.5518 -0.1537 271.9071 272.0609 289.5178 184.3738 -0.1608 272.0473 272.2080 289.6371 185.1660 -0.1664 272.2085 272.3749 289.7668 185.9575 -0.1690 272.3645 272.5335 289.8641 186.8098 -0.1757 272.5256 272.7013 289.9647 187.5715 -0.1801 272.6708 272.8509 290.0622 188.3938 -0.1843 272.8181 273.0024 290.1734 189.1860 -0.1866 272.9656 273.1522 290.2697 189.9775 -0.1914 273.1005 273.2920 290.3764 190.7998 -0.1947 273.2391 273.4338 290.4710 191.5915 -0.2018 273.3858 273.5876 290.5691 192.4145 -0.2089 273.5653 273.7742 290.6703 193.2068 -0.2111 273.6968 273.9079 290.7534 193.9985 -0.2161 273.8355 274.0516 290.8454 194.8210 -0.2214 273.9853 274.2067 290.9530 195.6135 -0.2268 274.1317 274.3584 291.0422 196.4365 -0.2326 274.2779 274.5106 291.1322 197.2285 -0.2379 274.4322 274.6701 291.2388 198.0205 -0.2405 274.5778 274.8183 291.3214 198.8730 -0.2462 274.7354 274.9816 291.4257 199.6355 -0.2511 274.8717 275.1228 291.5292 200.4583 -0.2538 275.0062 275.2600 291.6339 201.2505 -0.2576 275.1455 275.4032 291.7193 202.0433 -0.2608 275.2941 275.5549 291.8013 202.8620 -0.2647 275.4383 275.7031 291.9026 203.6200 -0.2676 275.5922 275.8598 292.0178 204.4690 -0.2747 275.7411 276.0158 292.1094 205.2570 -0.2835 275.8840 276.1676 292.2004 206.0450 -0.2895 276.0247 276.3142 292.3085 206.8635 -0.2915 276.1723 276.4638 292.4177 207.6520 -0.2938 276.3135 276.6073 292.5270 208.4725 -0.2987 276.4411 276.7398 292.6478 209.2630 -0.3049 276.5975 276.9024 292.7456 210.0543 -0.3059 276.7253 277.0312 292.8638 210.8748 -0.3086 276.8850 277.1935 292.9820 211.6365 -0.3146 277.0145 277.3291 293.0923 212.4885 -0.3209 277.1779 277.4988 293.2184 213.2805 -0.3241 277.3080 277.6321 293.3189 214.0725 -0.3290 277.4597 277.7888 293.4322 214.8945 -0.3331 277.6182 277.9513 293.5509 215.6565 -0.3377 277.7384 278.0761 293.6547 216.5085 -0.3432 277.8888 278.2320 293.7891 217.2705 -0.3442 278.0370 278.3812 293.8847 218.0925 -0.3469 278.1866 278.5335 294.0148 218.9145 -0.3549 278.3264 278.6813 294.1392 219.6765 -0.3582 278.4485 278.8067 294.2566 220.5285 -0.3627 278.5898 278.9526 294.3658 221.2905 -0.3676 278.7366 279.1042 294.4926 222.1123 -0.3731 278.8717 279.2449 294.6126 222.9045 -0.3747 279.0189 279.3935 294.7207 223.6955 -0.3774 279.1614 279.5388 294.8388 224.5485 -0.3792 279.3006 279.6799 294.9713 225.3108 -0.3862 279.4401 279.8263 295.0692 226.1328 -0.3876 279.5868 279.9744 295.1918 226.9250 -0.3863 279.7287 280.1150 295.2968 227.7165 -0.3954 279.8631 280.2585 295.3867 228.5693 -0.4036 280.0098 280.4134 295.4866 229.3315 -0.4105 280.1236 280.5342 295.5822 230.1545 -0.4167 280.2777 280.6944 295.6912 230.9468 -0.4209 280.4192 280.8401 295.7937 231.7405 -0.4247 280.5415 280.9663 295.8777 232.5933 -0.4283 280.7090 281.1373 295.9909 233.3555 -0.4329 280.8424 281.2753 296.0728 234.1778 -0.4355 280.9779 281.4134 296.1785 234.9660 -0.4402 281.1202 281.5605 296.2814 235.7540 -0.4433 281.2565 281.6999 296.3655 236.5728 -0.4437 281.4060 281.8497 296.4675 237.3610 -0.4408 281.5372 281.9780 296.5486 238.1800 -0.4407 281.6779 282.1186 296.6526 238.9680 -0.4420 281.8118 282.2538 296.7361 239.7578 -0.4542 281.9287 282.3828 296.7902 240.6070 -0.4628 282.0768 282.5396 296.8714 241.3668 -0.4692 282.2159 282.6852 296.9692 242.1888 -0.4736 282.3568 282.8304 297.0858 242.9800 -0.3881 282.4965 282.8847 297.2015 243.7715 -0.2818 282.6458 282.9277 297.3080 244.5938 -0.3534 282.7685 283.1218 297.4038 245.3855 -0.2747 282.9145 283.1891 297.5048 246.2078 -0.3460 283.0466 283.3926 297.6079 246.9998 -0.4270 283.1559 283.5829 297.7025 247.7915 -0.3508 283.2880 283.6389 297.8082 248.6138 -0.3291 283.4611 283.7902 297.9419 249.4055 -0.3313 283.6161 283.9474 298.0665 250.2278 -0.3409 283.7768 284.1177 298.1718 251.0198 -0.3508 283.8856 284.2364 298.2686 251.8115 -0.3858 284.0002 284.3860 298.3628 252.6335 -0.4002 284.1394 284.5396 298.4799 253.4255 -0.4136 284.2583 284.6718 298.5807 254.2475 -0.3117 284.4079 284.7195 298.7002 255.0395 -0.2492 284.5471 284.7964 298.8160 255.8315 -0.3615 284.6777 285.0392 298.9137 256.6535 -0.4096 284.8021 285.2117 299.0161 257.4455 -0.4208 284.9421 285.3629 299.1269 258.2683 -0.4343 285.0680 285.5024 299.2343 259.0605 -0.4282 285.2075 285.6357 299.3514 259.8525 -0.3706 285.3487 285.7193 299.4831 260.7050 -0.4046 285.4944 285.8990 299.5826 261.4675 -0.3817 285.6317 286.0134 299.6887 262.2955 -0.3739 285.7627 286.1366 299.8075 263.0883 -0.4057 285.8959 286.3016 299.8959 263.8805 -0.4074 286.0252 286.4325 300.0126 264.7028 -0.3818 286.1592 286.5410 300.1177 265.4945 -0.3886 286.2976 286.6862 300.2353 266.3175 -0.4006 286.4265 286.8271 300.3483 267.1095 -0.4660 286.5501 287.0162 300.4310 267.8990 -0.5413 286.6621 287.2034 300.5312 268.7173 -0.5827 286.7973 287.3799 300.6384 269.4750 -0.5917 286.9309 287.5227 300.7360 270.3233 -0.5951 287.0682 287.6634 300.8497 271.1123 -0.6021 287.2002 287.8023 300.9638 271.9015 -0.6069 287.3339 287.9408 301.0661 272.7270 -0.6094 287.4679 288.0772 301.1771 273.4865 -0.6156 287.6015 288.2171 301.2840 274.3360 -0.6187 287.7430 288.3617 301.3905 275.1263 -0.6214 287.8561 288.4775 301.4906 275.9173 -0.6258 287.9780 288.6038 301.5817 276.7390 -0.6214 288.1140 288.7354 301.6983 277.5005 -0.6239 288.2455 288.8694 301.8011 278.3530 -0.6328 288.4003 289.0331 301.9228 279.1150 -0.6405 288.5027 289.1431 302.0225 279.9368 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