DTA measure 2VFGHE) Pb(3) Date: 2024925:953 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1649.00 s Mass = 958.800 mg data_number = 1024 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4289 -4.2757 431.7851 436.0609 424.0015 4.0213 -4.2834 431.9092 436.1926 423.9983 5.6293 -4.2900 432.0407 436.3307 423.9999 7.2250 -4.2992 432.1796 436.4788 423.9650 8.8238 -4.3067 432.3076 436.6142 423.9333 10.4528 -4.3163 432.4336 436.7499 423.8531 12.0519 -4.2628 432.5568 436.8196 423.7459 13.6506 -4.3019 432.6729 436.9747 423.6095 15.2646 -4.3272 432.7997 437.1269 423.4542 16.8704 -4.3377 432.9197 437.2574 423.2915 18.4696 -4.3390 433.0234 437.3624 423.1162 20.0836 -4.3429 433.1428 437.4857 422.9198 21.6976 -4.3547 433.2482 437.6029 422.7098 23.3115 -4.3639 433.3565 437.7204 422.4702 24.9105 -4.3668 433.4730 437.8398 422.2460 26.5103 -4.3711 433.5663 437.9374 422.0382 28.1253 -4.3765 433.6654 438.0418 421.8067 29.7395 -4.3806 433.7606 438.1412 421.5637 31.3531 -4.3814 433.8439 438.2252 421.3281 32.9466 -4.3920 433.9457 438.3377 421.1029 34.5376 -4.3958 434.0251 438.4209 420.9033 36.1489 -4.4016 434.0930 438.4946 420.6754 37.7384 -4.4083 434.1823 438.5906 420.4697 39.3621 -4.4123 434.2535 438.6659 420.2469 40.9589 -4.4159 434.3360 438.7518 420.0399 42.5575 -4.4202 434.4078 438.8280 419.8116 44.1583 -4.4220 434.4815 438.9036 419.5957 45.7735 -4.4228 434.5493 438.9721 419.4223 47.3725 -4.4244 434.6016 439.0260 419.2153 49.0015 -4.4298 434.6515 439.0813 419.0167 50.6003 -4.4307 434.7150 439.1457 418.8421 52.1988 -4.4370 434.7702 439.2072 418.6411 53.7978 -4.4429 434.8064 439.2493 418.4493 55.4123 -4.4446 434.8560 439.3005 418.2774 57.0250 -4.4497 434.9143 439.3640 418.1019 58.6396 -4.4533 434.9549 439.4082 417.9178 60.2396 -4.4585 434.9856 439.4440 417.7522 61.8546 -4.4563 435.0185 439.4748 417.5808 63.4535 -4.4569 435.0446 439.5014 417.4096 65.0470 -4.4625 435.0741 439.5366 417.2364 66.6695 -4.4670 435.0995 439.5665 417.0450 68.2675 -4.4728 435.1211 439.5938 416.8654 69.8764 -4.4756 435.1335 439.6092 416.6838 71.4735 -4.4804 435.1466 439.6270 416.4894 73.0716 -4.4861 435.1724 439.6585 416.3116 74.6858 -4.4923 435.1684 439.6607 416.1259 76.2998 -4.4964 435.1978 439.6942 415.9393 77.8966 -4.5038 435.2046 439.7084 415.7415 79.5156 -4.5065 435.1961 439.7026 415.5318 81.1145 -4.5108 435.2042 439.7149 415.3143 82.7136 -4.5173 435.2143 439.7315 415.1101 84.3425 -4.5312 435.1977 439.7290 414.8964 85.9565 -4.5344 435.1952 439.7296 414.6829 87.5555 -4.5382 435.1819 439.7201 414.4724 89.1544 -4.5433 435.1753 439.7185 414.2594 90.7703 -4.5483 435.1563 439.7045 414.0502 92.3856 -4.5517 435.1331 439.6847 413.8498 93.9999 -4.5557 435.1241 439.6797 413.6473 95.5991 -4.5576 435.1029 439.6605 413.4372 97.2074 -4.5624 435.0746 439.6369 413.2405 98.7961 -4.5665 435.0472 439.6138 413.0493 100.4051 -4.5716 435.0230 439.5946 412.8657 102.0000 -4.5774 435.0036 439.5810 412.6686 103.6268 -4.5811 434.9585 439.5396 412.4788 105.2239 -4.5897 434.9116 439.5013 412.2989 106.8219 -4.5948 434.8742 439.4690 412.1213 108.4209 -4.5974 434.8358 439.4332 411.9513 110.0198 -4.5998 434.7928 439.3927 411.7402 111.6486 -4.6039 434.7539 439.3578 411.5403 113.2478 -4.6043 434.7026 439.3069 411.3262 114.8618 -4.6089 434.6642 439.2731 411.1224 116.4606 -4.6113 434.6099 439.2212 410.9174 118.0658 -4.6171 434.5505 439.1675 410.7060 119.6676 -4.6195 434.5008 439.1203 410.5243 121.2966 -4.6238 434.4483 439.0721 410.3140 122.8965 -4.6290 434.3890 439.0180 410.1219 124.5105 -4.6334 434.3242 438.9576 409.9117 126.1099 -4.6351 434.2615 438.8966 409.7303 127.7085 -4.6396 434.2007 438.8402 409.5498 129.3318 -4.6455 434.1310 438.7765 409.3582 130.9260 -4.6491 434.0697 438.7188 409.1513 132.5345 -4.6523 433.9791 438.6314 408.9605 134.1293 -4.6564 433.9105 438.5668 408.7620 135.7268 -4.6581 433.8575 438.5156 408.5549 137.3404 -4.6644 433.7800 438.4444 408.3311 138.9368 -4.6660 433.7010 438.3670 408.1196 140.5645 -4.6695 433.6177 438.2872 407.9127 142.1635 -4.6701 433.5250 438.1951 407.7016 143.7625 -4.6741 433.4348 438.1090 407.4783 145.3615 -4.6827 433.3519 438.0346 407.2938 146.9751 -4.6836 433.2793 437.9629 407.0767 148.6051 -4.6783 433.1924 437.8707 406.8650 150.2080 -4.6823 433.0838 437.7662 406.6592 151.8218 -4.6884 433.0141 437.7025 406.4668 153.4206 -4.6887 432.9160 437.6047 406.2552 155.0346 -4.6905 432.8081 437.4986 406.0577 156.6488 -4.6894 432.7222 437.4117 405.8453 158.2493 -4.6927 432.6197 437.3124 405.6459 159.8498 -4.6984 432.5334 437.2318 405.4495 161.4700 -4.6974 432.4255 437.1229 405.2700 163.0610 -4.7020 432.3286 437.0306 405.0737 164.6539 -4.7036 432.2110 436.9146 404.8795 166.2764 -4.7030 432.1159 436.8190 404.6977 167.8711 -4.7033 432.0106 436.7140 404.5192 169.4671 -4.7058 431.8894 436.5951 404.3288 171.0799 -4.7097 431.7833 436.4930 404.1283 172.6796 -4.7095 431.6852 436.3947 403.9097 174.2935 -4.7086 431.5793 436.2879 403.7125 175.9096 -4.7122 431.4697 436.1820 403.5180 177.5091 -4.7038 431.3418 436.0456 403.3121 179.1115 -4.7065 431.2233 435.9297 403.1142 180.7123 -4.7012 431.1119 435.8131 402.9221 182.3285 -4.6964 430.9897 435.6861 402.7046 183.9425 -4.6984 430.8708 435.5692 402.4887 185.5564 -4.7043 430.7389 435.4432 402.2923 187.1553 -4.7036 430.6204 435.3239 402.0919 188.7538 -4.6945 430.5003 435.1948 401.8886 190.3684 -4.6977 430.3702 435.0679 401.7044 191.9826 -4.7033 430.2677 434.9710 401.5023 193.5930 -4.7019 430.1393 434.8412 401.3079 195.1856 -4.7034 429.9954 434.6988 401.0991 196.7826 -4.7020 429.8712 434.5732 400.9167 198.3750 -4.6919 429.7558 434.4477 400.7001 199.9883 -4.6966 429.6204 434.3170 400.4894 201.5988 -4.7000 429.4975 434.1975 400.2863 203.2109 -4.6934 429.3545 434.0479 400.0589 204.8089 -4.6965 429.2219 433.9184 399.8541 206.4078 -4.6973 429.0865 433.7838 399.6492 208.0216 -4.6954 428.9527 433.6481 399.4159 209.6206 -4.6952 428.8166 433.5118 399.2081 211.2346 -4.6929 428.6857 433.3786 398.9844 212.8506 -4.6939 428.5273 433.2211 398.7723 214.4506 -4.6925 428.4064 433.0989 398.5646 216.0496 -4.6926 428.2610 432.9536 398.3390 217.6635 -4.7003 428.1160 432.8163 398.1380 219.2926 -4.7055 427.9811 432.6866 397.9209 220.8750 -4.7073 427.8266 432.5339 397.7281 222.4935 -4.7056 427.6865 432.3921 397.5136 224.1075 -4.7032 427.5535 432.2567 397.3237 225.7016 -4.6961 427.4066 432.1026 397.1267 227.3086 -4.6973 427.2410 431.9383 396.9037 228.9309 -4.6968 427.1080 431.8049 396.6986 230.5245 -4.6955 426.9605 431.6560 396.5231 232.1194 -4.6938 426.8092 431.5029 396.3150 233.7293 -4.6940 426.6593 431.3533 396.1180 235.3275 -4.6945 426.5050 431.1995 395.9310 236.9565 -4.6927 426.3377 431.0304 395.7227 238.5558 -4.6918 426.1983 430.8901 395.5387 240.1555 -4.6885 426.0562 430.7446 395.3461 241.7695 -4.6883 425.8905 430.5788 395.1401 243.3685 -4.6846 425.7362 430.4208 394.9459 244.9975 -4.6831 425.5773 430.2605 394.7280 246.5965 -4.6833 425.4240 430.1073 394.5236 248.1956 -4.6819 425.2649 429.9468 394.3108 249.7946 -4.6793 425.1149 429.7942 394.1016 251.4088 -4.6789 424.9522 429.6311 393.8874 253.0378 -4.6738 424.7833 429.4571 393.6621 254.6366 -4.6711 424.6364 429.3075 393.4630 256.2355 -4.6700 424.4666 429.1366 393.2559 257.8290 -4.6657 424.3144 428.9801 393.0461 259.4350 -4.6643 424.1507 428.8150 392.8224 261.0419 -4.6602 423.9736 428.6338 392.6098 262.6493 -4.6589 423.8158 428.4747 392.4029 264.2445 -4.6556 423.6567 428.3123 392.2075 265.8426 -4.6513 423.4870 428.1383 392.0025 267.4418 -4.6478 423.3407 427.9884 391.7992 269.0706 -4.6481 423.1563 427.8044 391.5923 270.6698 -4.6429 422.9901 427.6330 391.3878 272.2994 -4.6383 422.8196 427.4578 391.1887 273.8986 -4.6407 422.6689 427.3096 390.9988 275.5125 -4.6386 422.5175 427.1561 390.7838 277.1266 -4.6365 422.3249 426.9613 390.5757 278.7255 -4.6310 422.1664 426.7974 390.3933 280.3426 -4.6242 421.9872 426.6115 390.2029 281.9435 -4.6215 421.8268 426.4483 390.0106 283.5575 -4.6206 421.6363 426.2569 389.8050 285.1714 -4.6189 421.4887 426.1076 389.6131 286.7704 -4.6191 421.3055 425.9246 389.4042 288.3851 -4.6106 421.1399 425.7505 389.2328 289.9833 -4.6067 420.9606 425.5673 389.0199 291.5915 -4.6006 420.7967 425.3973 388.8126 293.1978 -4.5994 420.6271 425.2265 388.6149 294.7888 -4.5973 420.4562 425.0536 388.3829 296.3974 -4.5944 420.2796 424.8739 388.1715 297.9929 -4.5934 420.0948 424.6882 387.9589 299.6064 -4.5885 419.9190 424.5075 387.7446 301.2205 -4.5840 419.7566 424.3406 387.5381 302.8206 -4.5816 419.5756 424.1572 387.3313 304.4210 -4.5768 419.4080 423.9848 387.1182 306.0346 -4.5699 419.2280 423.7980 386.9035 307.6338 -4.5708 419.0548 423.6257 386.6894 309.2628 -4.5681 418.8713 423.4394 386.4795 310.8616 -4.5627 418.6882 423.2509 386.2708 312.4756 -4.5584 418.5205 423.0789 386.0566 314.0746 -4.5547 418.3427 422.8974 385.8730 315.6885 -4.5518 418.1765 422.7282 385.6579 317.3028 -4.5483 417.9894 422.5376 385.4455 318.9025 -4.5456 417.8130 422.3586 385.2345 320.5169 -4.5408 417.6198 422.1605 385.0308 322.1146 -4.5381 417.4466 421.9848 384.8362 323.7060 -4.5329 417.2776 421.8104 384.6283 325.3270 -4.5313 417.0763 421.6076 384.4157 326.9191 -4.5280 416.8999 421.4280 384.2309 328.5125 -4.5217 416.7090 421.2307 384.0109 330.1226 -4.5196 416.5395 421.0592 383.8042 331.7201 -4.5181 416.3621 420.8802 383.6160 333.3335 -4.5127 416.1763 420.6890 383.4300 334.9475 -4.5073 415.9868 420.4940 383.2169 336.5465 -4.5087 415.8106 420.3193 383.0204 338.1455 -4.5114 415.6297 420.1411 382.8208 339.7445 -4.5068 415.4469 419.9536 382.6059 341.3735 -4.5017 415.2653 419.7669 382.4053 342.9725 -4.4952 415.0715 419.5667 382.1919 344.5861 -4.4904 414.8864 419.3767 381.9843 346.1848 -4.4880 414.7133 419.2013 381.7832 347.7838 -4.4868 414.5267 419.0135 381.5629 349.4126 -4.4785 414.3425 418.8210 381.3503 351.0126 -4.4714 414.1457 418.6171 381.1390 352.6280 -4.4700 413.9684 418.4384 380.9209 354.2270 -4.4684 413.7864 418.2548 380.7096 355.8200 -4.4601 413.5960 418.0561 380.4993 357.4260 -4.4569 413.3994 417.8563 380.2979 359.0330 -4.4559 413.2204 417.6763 380.0965 360.6400 -4.4487 413.0222 417.4708 379.8886 362.2353 -4.4422 412.8475 417.2897 379.6714 363.8336 -4.4377 412.6577 417.0954 379.4763 365.4478 -4.4314 412.4754 416.9067 379.2624 367.0618 -4.4277 412.2843 416.7120 379.0363 368.6756 -4.4256 412.0959 416.5215 378.8294 370.2746 -4.4217 411.9115 416.3331 378.6244 371.8736 -4.4154 411.7170 416.1324 378.4144 373.5026 -4.4128 411.5184 415.9311 378.1921 375.1018 -4.4081 411.3396 415.7476 377.9943 376.7169 -4.4022 411.1458 415.5480 377.7937 378.3165 -4.3973 410.9616 415.3589 377.5817 379.9155 -4.3926 410.7615 415.1541 377.3686 381.5445 -4.3895 410.5584 414.9479 377.1653 383.1585 -4.3850 410.3730 414.7580 376.9649 384.7574 -4.3799 410.1907 414.5707 376.7762 386.3549 -4.3741 409.9996 414.3738 376.5695 387.9470 -4.3700 409.8108 414.1808 376.3745 389.5694 -4.3606 409.6207 413.9814 376.1658 391.1619 -4.3604 409.4279 413.7883 375.9713 392.7693 -4.3564 409.2387 413.5951 375.7678 394.3641 -4.3457 409.0491 413.3948 375.5846 395.9625 -4.3413 408.8624 413.2037 375.3968 397.5765 -4.3386 408.6831 413.0218 375.1886 399.1905 -4.3343 408.4773 412.8116 374.9846 400.7895 -4.3293 408.2693 412.5986 374.7868 402.3880 -4.3232 408.0767 412.4000 374.5716 404.0019 -4.3201 407.8815 412.2016 374.3611 405.6008 -4.3145 407.6931 412.0076 374.1559 407.2299 -4.3119 407.5097 411.8216 373.9413 408.8288 -4.3061 407.3159 411.6220 373.7151 410.4440 -4.2998 407.1089 411.4087 373.5069 412.0436 -4.2931 406.9291 411.2222 373.2915 413.6576 -4.2924 406.7285 411.0209 373.0864 415.2743 -4.2903 406.5255 410.8158 372.8504 416.8816 -4.2864 406.3366 410.6230 372.6573 418.4811 -4.2792 406.1407 410.4198 372.4336 420.0890 -4.2715 405.9425 410.2141 372.2259 421.6806 -4.2658 405.7584 410.0242 372.0167 423.3026 -4.2631 405.5554 409.8185 371.8082 424.8975 -4.2579 405.3641 409.6220 371.5970 426.5089 -4.2523 405.1663 409.4186 371.3937 428.1075 -4.2477 404.9567 409.2044 371.1897 429.7215 -4.2426 404.7737 409.0163 370.9906 431.3355 -4.2351 404.5814 408.8165 370.7823 432.9345 -4.2302 404.3797 408.6099 370.5792 434.5485 -4.2258 404.1912 408.4171 370.3676 436.2758 -4.2194 403.9861 408.2055 370.1614 437.9665 -4.2142 403.7695 407.9837 369.9393 439.5805 -4.2074 403.5786 407.7860 369.7468 441.1795 -4.2035 403.3722 407.5757 369.5500 442.7939 -4.2001 403.1761 407.3762 369.3456 444.3929 -4.1931 402.9825 407.1756 369.1457 446.0218 -4.1896 402.7844 406.9740 368.9401 447.6359 -4.1842 402.6014 406.7856 368.7639 449.2359 -4.1783 402.4000 406.5783 368.5615 450.8348 -4.1733 402.2001 406.3734 368.3703 452.4420 -4.1681 401.9991 406.1672 368.1342 454.0488 -4.1553 401.8002 405.9555 367.9228 455.6563 -4.1495 401.6063 405.7558 367.7176 457.2505 -4.1444 401.4126 405.5570 367.5048 458.8464 -4.1402 401.2054 405.3456 367.2957 460.4588 -4.1355 401.0094 405.1449 367.0652 462.0726 -4.1290 400.8111 404.9402 366.8500 463.6718 -4.1236 400.6204 404.7440 366.6331 465.2858 -4.1197 400.4262 404.5459 366.4251 466.8846 -4.1159 400.2322 404.3481 366.1941 468.4836 -4.1194 400.0378 404.1572 365.9938 470.1126 -4.1176 399.8293 403.9469 365.7761 471.7266 -4.1091 399.6142 403.7233 365.5583 473.3256 -4.1027 399.4193 403.5221 365.3369 474.9245 -4.0999 399.2264 403.3263 365.1363 476.5391 -4.0951 399.0270 403.1222 364.9230 478.1535 -4.0891 398.8326 402.9217 364.7199 479.7676 -4.0855 398.6253 402.7108 364.5105 481.3675 -4.0803 398.4251 402.5054 364.3092 482.9796 -4.0758 398.2180 402.2938 364.1084 484.5719 -4.0697 398.0297 402.0994 363.8939 486.1938 -4.0640 397.8141 401.8781 363.6855 487.9670 -4.0590 397.6198 401.6788 363.4542 489.5870 -4.0532 397.4085 401.4617 363.2440 491.1838 -4.0477 397.2061 401.2538 363.0502 492.7975 -4.0426 397.0207 401.0632 362.8327 494.4115 -4.0375 396.8063 400.8438 362.6350 496.0105 -4.0321 396.6102 400.6423 362.4210 497.6249 -4.0243 396.4061 400.4303 362.2218 499.2244 -4.0191 396.2045 400.2235 362.0145 500.8229 -4.0129 395.9920 400.0049 361.8174 502.4519 -4.0094 395.8006 399.8100 361.6109 504.0516 -4.0045 395.6041 399.6086 361.4197 505.6665 -3.9968 395.4064 399.4033 361.2147 507.2656 -3.9932 395.1992 399.1924 361.0225 508.8646 -3.9881 395.0116 398.9997 360.8266 510.4936 -3.9825 394.8116 398.7941 360.6178 512.0926 -3.9752 394.6015 398.5767 360.4344 513.7065 -3.9681 394.4001 398.3682 360.2278 515.3029 -3.9613 394.2033 398.1646 360.0226 516.8945 -3.9521 393.9949 397.9470 359.8084 518.6935 -3.9475 393.7671 397.7146 359.5666 520.3074 -3.9419 393.5686 397.5105 359.3374 521.9173 -3.9366 393.3741 397.3107 359.1096 523.5145 -3.9328 393.1598 397.0926 358.9057 525.1285 -3.9263 392.9650 396.8913 358.6859 526.7426 -3.9203 392.7599 396.6801 358.4581 528.3421 -3.9164 392.5477 396.4641 358.2471 529.9415 -3.9100 392.3596 396.2696 358.0279 531.5555 -3.9035 392.1579 396.0615 357.8124 533.1695 -3.8977 391.9579 395.8557 357.5909 534.7835 -3.8922 391.7533 395.6456 357.3824 536.3825 -3.8848 391.5529 395.4376 357.1648 537.9815 -3.8811 391.3528 395.2339 356.9629 539.5960 -3.8743 391.1516 395.0260 356.7525 541.2253 -3.8678 390.9334 394.8011 356.5389 542.8239 -3.8637 390.7376 394.6014 356.3336 544.4236 -3.8595 390.5387 394.3982 356.1138 546.0376 -3.8520 390.3343 394.1863 355.9074 547.6365 -3.8453 390.1373 393.9826 355.7034 549.4275 -3.8408 389.8975 393.7382 355.4634 551.0418 -3.8326 389.7048 393.5374 355.2594 552.6510 -3.8284 389.5084 393.3368 355.0554 554.2456 -3.8212 389.3085 393.1297 354.8455 555.8698 -3.8184 389.1016 392.9200 354.6394 557.4679 -3.8124 388.8990 392.7114 354.4423 559.0688 -3.8054 388.6837 392.4891 354.2337 560.6698 -3.8011 388.4867 392.2878 354.0285 562.2836 -3.7962 388.2765 392.0727 353.8398 563.8978 -3.7888 388.0742 391.8630 353.6349 565.5128 -3.7841 387.8737 391.6577 353.4269 567.1126 -3.7767 387.6747 391.4514 353.2400 568.7608 -3.7725 387.4660 391.2385 353.0335 570.5243 -3.7657 387.2487 391.0144 352.8143 572.1536 -3.7600 387.0418 390.8017 352.6071 573.7535 -3.7554 386.8347 390.5901 352.4182 575.3525 -3.7496 386.6359 390.3855 352.2119 576.9670 -3.7452 386.4350 390.1802 352.0138 578.5815 -3.7410 386.2209 389.9619 351.8127 580.3823 -3.7339 385.9825 389.7165 351.5950 581.9750 -3.7295 385.7852 389.5147 351.3894 583.5978 -3.7231 385.5906 389.3137 351.1845 585.2054 -3.7181 385.3938 389.1119 350.9798 586.7999 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