DTA measure 1Pb_updown Date: 2026225:98 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.05 s Mass = 1163.600 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3343 1.5405 234.9523 233.4118 272.9730 2.1313 1.5402 235.2097 233.6695 272.9444 2.9175 1.5402 235.4887 233.9485 272.8852 3.7550 1.5365 235.7651 234.2286 272.8683 4.5110 1.5344 235.9989 234.4645 272.8679 5.3688 1.5319 236.2994 234.7674 272.8949 6.1348 1.5370 236.5496 235.0126 272.9299 6.9623 1.5373 236.8162 235.2789 272.9820 7.7585 1.5383 237.0936 235.5553 273.0266 8.5555 1.5389 237.3401 235.8012 273.0941 9.3828 1.5375 237.5863 236.0488 273.2144 10.1485 1.5373 237.8255 236.2882 273.3673 11.0070 1.5360 238.1341 236.5981 273.5265 11.7315 1.5371 238.3861 236.8490 273.6969 12.6000 1.5301 238.6832 237.1531 273.9464 13.3660 1.5279 238.9434 237.4155 274.1560 14.1930 1.5296 239.2172 237.6876 274.3769 14.9795 1.5274 239.4788 237.9513 274.6532 15.7865 1.5245 239.7348 238.2103 274.9273 16.6033 1.5207 239.9759 238.4552 275.2299 17.3693 1.5199 240.2164 238.6965 275.5125 18.2275 1.5190 240.4737 238.9548 275.8456 18.9933 1.5153 240.7073 239.1920 276.0995 19.8208 1.5114 240.9634 239.4520 276.4118 20.6070 1.5095 241.2015 239.6921 276.6998 21.4140 1.5057 241.4686 239.9629 276.9972 22.2313 1.5023 241.7374 240.2352 277.2931 23.0073 1.4973 241.9830 240.4856 277.5396 23.8553 1.4894 242.2724 240.7829 277.7907 24.6313 1.4840 242.5350 241.0510 278.0012 25.4485 1.4785 242.8072 241.3287 278.2180 26.2453 1.4745 243.0392 241.5646 278.3890 27.0415 1.4661 243.2972 241.8311 278.5716 27.8693 1.4592 243.5653 242.1062 278.7237 28.6350 1.4574 243.7867 242.3293 278.8481 29.4830 1.4524 244.0499 242.5975 278.9968 30.2593 1.4473 244.3190 242.8718 279.0831 31.0760 1.4408 244.5612 243.1204 279.1628 31.8728 1.4353 244.8124 243.3771 279.2522 32.6695 1.4347 245.0434 243.6087 279.3342 33.4968 1.4326 245.2661 243.8335 279.3664 34.2628 1.4307 245.5059 244.0752 279.3966 35.1208 1.4234 245.7592 244.3358 279.4236 35.8865 1.4181 246.0036 244.5855 279.4455 36.7140 1.4095 246.2568 244.8473 279.4536 37.5105 1.4034 246.4862 245.0827 279.4820 38.3070 1.3972 246.7407 245.3434 279.4864 39.1345 1.4246 246.9826 245.5580 279.4934 39.9003 1.4602 247.2234 245.7632 279.4853 40.7583 1.4408 247.5061 246.0652 279.4543 41.5243 1.4266 247.7459 246.3192 279.4648 42.3515 1.4127 247.9588 246.5461 279.4852 43.1480 1.3983 248.1762 246.7779 279.4886 43.9450 1.3873 248.4077 247.0204 279.5234 44.7618 1.3846 248.6688 247.2843 279.5963 45.5380 1.3818 248.9054 247.5236 279.6678 46.3553 1.3811 249.1056 247.7245 279.7438 47.1208 1.3760 249.3311 247.9552 279.8104 47.9790 1.3733 249.5624 248.1891 279.9244 48.7348 1.3681 249.7823 248.4142 280.0496 49.5515 1.3627 250.0149 248.6522 280.1851 50.3588 1.3545 250.2578 248.9033 280.3235 51.1450 1.3455 250.5225 249.1770 280.4872 51.9620 1.3358 250.7522 249.4164 280.6698 52.7385 1.3294 250.9801 249.6507 280.8379 53.5860 1.3261 251.2226 249.8965 281.0924 54.3523 1.3204 251.4533 250.1329 281.3105 55.1795 1.3168 251.6994 250.3825 281.5696 55.9760 1.3082 251.9360 250.6278 281.8314 56.7625 1.2985 252.1743 250.8757 282.0784 57.5898 1.2882 252.4452 251.1571 282.3563 58.3558 1.2826 252.6461 251.3636 282.5983 59.2140 1.2763 252.8923 251.6160 282.8617 59.9695 1.2729 253.0898 251.8169 283.1455 60.8073 1.2670 253.3289 252.0619 283.4088 61.5628 1.2570 253.5619 252.3049 283.6336 62.3900 1.2481 253.7778 252.5296 283.8833 63.1868 1.2391 254.0150 252.7759 284.1155 63.9833 1.2312 254.2407 253.0095 284.3579 64.8105 1.2225 254.4422 253.2197 284.5768 65.5665 1.2138 254.6476 253.4338 284.7683 66.4345 1.2025 254.9118 253.7093 284.9871 67.1903 1.1984 255.1260 253.9276 285.1460 68.0178 1.1881 255.3443 254.1562 285.2945 68.8140 1.1789 255.5854 254.4065 285.4227 69.6110 1.1755 255.8170 254.6414 285.5149 70.4383 1.1691 256.0136 254.8445 285.6217 71.2040 1.1620 256.2233 255.0613 285.7317 72.0623 1.1506 256.4498 255.2992 285.8345 72.8280 1.1427 256.6700 255.5273 285.9061 73.6555 1.1334 256.9051 255.7717 285.9656 74.4420 1.1271 257.1256 255.9986 286.0011 75.2485 1.1168 257.3601 256.2433 286.0098 76.0660 1.1092 257.6011 256.4919 286.0412 76.8318 1.1068 257.8016 256.6948 286.0433 77.6900 1.1033 258.0017 256.8984 286.0391 78.4663 1.0966 258.1996 257.1030 286.0303 79.2830 1.0852 258.4438 257.3585 285.9811 80.0798 1.0782 258.6777 257.5995 285.9869 80.8765 1.0707 258.8973 257.8266 285.9913 81.7140 1.0677 259.1117 258.0440 286.0009 82.4698 1.0597 259.3145 258.2548 286.0318 83.2970 1.0509 259.5292 258.4783 286.0740 84.0630 1.0473 259.7184 258.6711 286.1175 84.9213 1.0441 259.9663 258.9222 286.1724 85.6868 1.0352 260.2001 259.1649 286.2376 86.5143 1.0265 260.4142 259.3877 286.3213 87.3110 1.0223 260.6197 259.5974 286.4220 88.1073 1.0200 260.8209 259.8009 286.5611 88.9350 1.0128 261.0427 260.0298 286.7085 89.6905 1.0074 261.2420 260.2345 286.8538 90.5588 1.0011 261.4548 260.4537 287.0466 91.3145 0.9972 261.6622 260.6650 287.2238 92.1520 0.9907 261.8523 260.8617 287.4272 92.9383 0.9853 262.0735 261.0883 287.6444 93.7453 0.9797 262.3129 261.3332 287.8582 94.5623 0.9698 262.5327 261.5629 288.1348 95.3383 0.9577 262.7100 261.7523 288.3814 96.1558 0.9500 262.9204 261.9704 288.6625 96.9315 0.9461 263.1046 262.1585 288.9254 97.7795 0.9381 263.2873 262.3493 289.2116 98.5558 0.9302 263.5190 262.5888 289.4872 99.3725 0.9223 263.7437 262.8214 289.7481 100.1798 0.9189 263.9757 263.0568 290.0161 100.9660 0.9075 264.1557 263.2482 290.2684 101.7728 0.8968 264.3347 263.4378 290.4898 102.5593 0.8889 264.5149 263.6260 290.7277 103.3968 0.8815 264.7333 263.8518 290.9502 104.1523 0.8771 264.9209 264.0438 291.1178 105.0208 0.8675 265.1603 264.2928 291.3311 105.7763 0.8598 265.3434 264.4836 291.4925 106.6138 0.8546 265.5637 264.7091 291.6374 107.4003 0.8471 265.7676 264.9206 291.7680 108.2070 0.8386 265.9885 265.1499 291.8831 109.0243 0.8310 266.2009 265.3699 292.0059 109.7903 0.8269 266.4212 265.5943 292.1114 110.6380 0.8162 266.6490 265.8328 292.1896 111.4043 0.8052 266.8121 266.0069 292.2734 112.2210 0.7972 267.0331 266.2359 292.3275 113.0178 0.7883 267.2587 266.4704 292.3658 113.8145 0.7835 267.4521 266.6685 292.3995 114.6315 0.7760 267.6571 266.8811 292.4274 115.3975 0.7691 267.8460 267.0769 292.4441 116.2248 0.7590 268.0183 267.2592 292.4390 116.9805 0.7492 268.2004 267.4513 292.4372 117.8388 0.7402 268.4127 267.6725 292.4527 118.6043 0.7349 268.6200 267.8850 292.4634 119.4215 0.7319 268.8240 268.0921 292.4723 120.2183 0.7249 269.0171 268.2923 292.4826 121.0148 0.7178 269.2171 268.4993 292.5028 121.8423 0.7139 269.4322 268.7183 292.5576 122.6080 0.7067 269.6408 268.9341 292.6098 123.4558 0.6989 269.8756 269.1767 292.6601 124.2320 0.6932 270.0861 269.3929 292.7145 125.0490 0.6891 270.2959 269.6068 292.7755 125.8458 0.6888 270.4908 269.8020 292.8659 126.6425 0.6827 270.6856 270.0029 292.9779 127.4695 0.6774 270.8753 270.1979 293.1324 128.2358 0.6731 271.0603 270.3873 293.2875 129.0528 0.6654 271.2438 270.5784 293.4611 129.8288 0.6588 271.4192 270.7603 293.6413 130.6770 0.6480 271.6358 270.9878 293.8532 131.4425 0.6375 271.8412 271.2038 294.0736 132.2700 0.6269 272.0513 271.4244 294.3161 133.0668 0.6188 272.2275 271.6087 294.5692 133.8630 0.6135 272.4034 271.7899 294.8048 134.6805 0.6067 272.6185 272.0118 295.0564 135.4565 0.5982 272.7887 272.1906 295.3064 136.3043 0.5880 272.9728 272.3848 295.5782 137.0703 0.5788 273.1695 272.5907 295.8249 137.8975 0.5721 273.3521 272.7800 296.1064 138.6943 0.5674 273.5233 272.9559 296.3380 139.4910 0.5586 273.7335 273.1748 296.5660 140.3080 0.5563 273.8828 273.3265 296.8086 141.0843 0.5485 274.0654 273.5169 297.0119 141.9320 0.5415 274.2844 273.7429 297.2262 142.6978 0.5316 274.4900 273.9584 297.4142 143.5253 0.5183 274.6899 274.1715 297.6354 144.3218 0.5124 274.8681 274.3557 297.8113 145.1183 0.5099 275.0792 274.5694 297.9857 145.9355 0.5037 275.2899 274.7862 298.1357 146.7115 0.5010 275.4815 274.9805 298.2754 147.5695 0.4945 275.7135 275.2190 298.3884 148.3355 0.4897 275.9114 275.4217 298.4824 149.1525 0.4831 276.0870 275.6040 298.5794 149.9593 0.4764 276.2701 275.7936 298.6585 150.7460 0.4670 276.4680 276.0010 298.7045 151.5730 0.4625 276.6632 276.2007 298.7305 152.3390 0.4585 276.8407 276.3822 298.7610 153.1973 0.4536 277.0258 276.5722 298.7941 153.9628 0.4455 277.2163 276.7708 298.7935 154.7903 0.4362 277.4216 276.9854 298.7934 155.5870 0.4282 277.6107 277.1825 298.8296 156.3833 0.4244 277.7945 277.3701 298.8507 157.2108 0.4171 277.9852 277.5681 298.8653 157.9665 0.4123 278.1628 277.7504 298.8780 158.8348 0.4030 278.3703 277.9674 298.8914 159.5908 0.3996 278.5252 278.1256 298.8978 160.4178 0.3945 278.6909 278.2964 298.9400 161.2453 0.3882 278.8962 278.5081 298.9775 162.0113 0.3837 279.0814 278.6977 299.0491 162.8690 0.3776 279.2800 278.9024 299.1617 163.6353 0.3697 279.4452 279.0755 299.2322 164.4625 0.3586 279.6499 279.2914 299.3355 165.2283 0.3530 279.8381 279.4851 299.4603 166.0558 0.3506 280.0307 279.6801 299.5837 166.8728 0.3452 280.2328 279.8876 299.7551 167.6490 0.3399 280.4100 280.0701 299.9123 168.4970 0.3301 280.6208 280.2907 300.1007 169.2628 0.3257 280.7846 280.4589 300.2999 170.0903 0.3226 280.9690 280.6464 300.5318 170.8868 0.3138 281.1319 280.8181 300.7585 171.6835 0.3058 281.2883 280.9826 301.0140 172.5110 0.3028 281.4743 281.1715 301.2552 173.2765 0.2980 281.6754 281.3774 301.5039 174.1248 0.2883 281.8779 281.5896 301.7293 174.8905 0.2847 282.0493 281.7646 301.9601 175.7178 0.2813 282.2621 281.9808 302.2383 176.5043 0.2702 282.4316 282.1614 302.5096 177.2905 0.2650 282.6040 282.3391 302.7492 178.1280 0.2562 282.7795 282.5233 303.0120 178.8838 0.2499 282.9344 282.6845 303.2112 179.7008 0.2430 283.1324 282.8894 303.4515 180.4768 0.2396 283.2936 283.0540 303.6560 181.3248 0.2351 283.4932 283.2580 303.8533 182.0905 0.2264 283.6380 283.4116 304.0216 182.9180 0.2166 283.8400 283.6234 304.1954 183.7148 0.2092 284.0020 283.7929 304.3377 184.5110 0.2017 284.1677 283.9660 304.4793 185.2975 0.1917 284.3616 284.1699 304.5935 186.1045 0.1849 284.5734 284.3885 304.7102 186.9213 0.1810 284.7563 284.5753 304.8034 187.6873 0.1787 284.9378 284.7591 304.8806 188.5455 0.1718 285.1548 284.9830 304.9307 189.3110 0.1644 285.3396 285.1752 304.9788 190.1283 0.1581 285.5195 285.3614 305.0256 190.9250 0.1533 285.7019 285.5486 305.0495 191.7215 0.1494 285.8844 285.7350 305.0852 192.5493 0.1432 286.0709 285.9277 305.1052 193.3045 0.1381 286.2302 286.0921 305.1136 194.1423 0.1297 286.4164 286.2868 305.1447 194.8980 0.1238 286.5900 286.4663 305.1456 195.7558 0.1143 286.7650 286.6507 305.1874 196.5220 0.1091 286.9494 286.8404 305.2061 197.3493 0.1016 287.1085 287.0069 305.2425 198.1458 0.0942 287.2835 287.1893 305.2826 198.9325 0.0933 287.4791 287.3858 305.3201 199.7698 0.0870 287.6628 287.5758 305.3808 200.5358 0.0816 287.8501 287.7685 305.4428 201.3633 0.0740 288.0824 288.0084 305.5496 202.1185 0.0641 288.2549 288.1908 305.6432 202.9870 0.0620 288.4529 288.3910 305.8041 203.7428 0.0622 288.6148 288.5526 305.9579 204.5700 0.0553 288.7945 288.7392 306.0866 205.3670 0.0522 288.9768 288.9247 306.2398 206.1735 0.0462 289.1377 289.0915 306.3996 206.9908 0.0414 289.3332 289.2918 306.5660 207.7568 0.0325 289.4670 289.4345 306.7652 208.6145 0.0278 289.6369 289.6091 306.9912 209.3805 0.0236 289.8135 289.7899 307.1941 210.2078 0.0212 290.0003 289.9791 307.4239 210.9940 0.0156 290.1724 290.1568 307.6269 211.8010 0.0087 290.3703 290.3616 307.8901 212.6183 0.0019 290.5708 290.5689 308.1535 213.3838 -0.0045 290.7094 290.7139 308.4024 214.2420 -0.0126 290.8776 290.8902 308.6565 215.0080 -0.0226 291.0458 291.0684 308.8753 215.8353 -0.0233 291.2218 291.2451 309.1188 216.6320 -0.0297 291.3637 291.3934 309.3172 217.4285 -0.0360 291.5152 291.5512 309.5112 218.2558 -0.0395 291.6941 291.7336 309.7457 219.0218 -0.0437 291.8811 291.9248 309.9367 219.8388 -0.0547 292.0447 292.0994 310.1260 220.6148 -0.0621 292.2085 292.2707 310.2921 221.4730 -0.0710 292.3936 292.4646 310.4587 222.2388 -0.0786 292.5706 292.6492 310.5891 223.0660 -0.0844 292.7623 292.8467 310.7322 223.8628 -0.0890 292.9329 293.0220 310.8524 224.6695 -0.0968 293.0894 293.1862 310.9655 225.4868 -0.1054 293.2903 293.3957 311.0766 226.2528 -0.1138 293.4480 293.5618 311.1616 227.0798 -0.1191 293.6210 293.7402 311.2299 227.8560 -0.1225 293.7940 293.9165 311.2871 228.7040 -0.1299 293.9894 294.1192 311.3427 229.4698 -0.1358 294.1373 294.2731 311.4068 230.2973 -0.1408 294.3184 294.4592 311.4612 231.0938 -0.1502 294.4972 294.6474 311.4974 231.8903 -0.1549 294.6848 294.8396 311.5256 232.7178 -0.1555 294.8577 295.0132 311.5480 233.4835 -0.1578 294.9841 295.1419 311.6005 234.3418 -0.1665 295.1676 295.3341 311.6029 235.1078 -0.1687 295.3276 295.4964 311.6514 235.9348 -0.1694 295.4932 295.6626 311.6850 236.7318 -0.1709 295.6854 295.8563 311.7182 237.5283 -0.1741 295.8846 296.0587 311.7709 238.3555 -0.1819 296.0534 296.2353 311.8377 239.1115 -0.1871 296.2176 296.4047 311.9071 239.9693 -0.1944 296.4053 296.5997 311.9908 240.7250 -0.1983 296.5667 296.7650 312.0894 241.5525 -0.2035 296.7777 296.9811 312.1857 242.3285 -0.2081 296.9340 297.1421 312.3395 243.1458 -0.2166 297.0850 297.3016 312.5052 243.9320 -0.2224 297.2413 297.4637 312.6656 244.7285 -0.2280 297.4136 297.6416 312.8462 245.5458 -0.2356 297.6000 297.8355 313.0405 246.3115 -0.2419 297.7848 298.0267 313.2018 247.1695 -0.2439 297.9651 298.2090 313.4079 247.9253 -0.2472 298.1249 298.3721 313.6071 248.7525 -0.2540 298.3041 298.5581 313.8449 249.5490 -0.2605 298.4850 298.7455 314.0734 250.3458 -0.2649 298.6802 298.9452 314.3294 251.1628 -0.2720 298.8427 299.1148 314.5841 251.9388 -0.2756 298.9810 299.2566 314.8423 252.7868 -0.2792 299.1357 299.4149 315.0902 253.5525 -0.2857 299.2936 299.5793 315.3038 254.3800 -0.2928 299.4801 299.7729 315.5403 255.1460 -0.2944 299.6372 299.9316 315.7521 255.9730 -0.3002 299.7884 300.0886 315.9843 256.7595 -0.3040 299.9761 300.2801 316.1621 257.5665 -0.3076 300.1676 300.4752 316.3617 258.3835 -0.3129 300.3257 300.6386 316.5526 259.1495 -0.3193 300.4783 300.7976 316.6957 260.0075 -0.3257 300.6484 300.9740 316.8328 260.7838 -0.3300 300.8324 301.1624 316.9884 261.6010 -0.3342 300.9882 301.3224 317.1342 262.3973 -0.3188 301.1612 301.4800 317.2626 263.1943 -0.3172 301.3433 301.6605 317.3426 264.0215 -0.3067 301.4940 301.8007 317.4150 264.7875 -0.2887 301.6298 301.9185 317.4665 265.6355 -0.3073 301.8126 302.1199 317.5093 266.4113 -0.3229 301.9803 302.3032 317.5497 267.2285 -0.3169 302.1278 302.4446 317.6230 268.0355 -0.2948 302.2964 302.5912 317.6683 268.8218 -0.2591 302.5034 302.7625 317.7143 269.6598 -0.2592 302.7004 302.9596 317.7598 270.4150 -0.2864 302.8416 303.1280 317.7754 271.2733 -0.3104 303.0164 303.3268 317.7917 272.0393 -0.3294 303.2004 303.5298 317.8328 272.8663 -0.3473 303.3523 303.6996 317.8790 273.6630 -0.3609 303.5152 303.8761 317.9382 274.4598 -0.3741 303.6738 304.0480 317.9887 275.2868 -0.3865 303.8539 304.2404 318.0413 276.0528 -0.3972 304.0484 304.4456 318.1187 276.9110 -0.4044 304.2408 304.6452 318.1834 277.6665 -0.4165 304.3922 304.8088 318.2853 278.5043 -0.4253 304.5500 304.9753 318.4172 279.2905 -0.4316 304.6756 305.1072 318.5270 280.0873 -0.4358 304.8615 305.2973 318.6451 280.9148 -0.4391 305.0174 305.4565 318.7827 281.6803 -0.4407 305.1861 305.6267 318.9306 282.5385 -0.4438 305.3767 305.8204 319.1049 283.2738 -0.4478 305.5357 305.9834 319.2753 284.1318 -0.4501 305.7312 306.1813 319.4821 284.9080 -0.4556 305.8926 306.3482 319.6627 285.7250 -0.4624 306.0481 306.5105 319.8736 286.5218 -0.4698 306.1869 306.6567 320.0783 287.3185 -0.4790 306.3711 306.8501 320.2803 288.1455 -0.4871 306.5362 307.0232 320.4960 288.9118 -0.4909 306.7137 307.2046 320.7001 289.7595 -0.4953 306.8864 307.3818 320.9654 290.5355 -0.5031 307.0583 307.5614 321.1918 291.3630 -0.5078 307.2193 307.7271 321.4316 292.1595 -0.5152 307.4089 307.9241 321.6628 292.9458 -0.5228 307.5641 308.0869 321.8981 293.7838 -0.5259 307.7102 308.2361 322.1291 294.5493 -0.5281 307.8424 308.3705 322.3379 295.3768 -0.5330 307.9881 308.5211 322.5381 296.1428 -0.5377 308.1457 308.6834 322.7270 297.0005 -0.5434 308.3126 308.8559 322.9020 297.7668 -0.5503 308.4659 309.0162 323.0362 298.5940 -0.5536 308.6159 309.1695 323.1871 299.3803 -0.5566 308.8044 309.3610 323.3328 300.1875 -0.5607 308.9875 309.5482 323.4838 301.0043 -0.5659 309.1818 309.7478 323.6062 301.7803 -0.5728 309.3220 309.8948 323.7145 302.5975 -0.5797 309.5077 310.0874 323.7948 303.3633 -0.5844 309.6540 310.2384 323.8775 304.2110 -0.5876 309.8346 310.4222 323.9474 304.9773 -0.5882 309.9854 310.5736 324.0102 305.7940 -0.5895 310.1301 310.7197 324.0760 306.5908 -0.5938 310.3090 310.9028 324.1283 307.3875 -0.6002 310.4778 311.0780 324.1711 308.2043 -0.6051 310.6651 311.2702 324.2154 308.9703 -0.6109 310.8217 311.4326 324.2426 309.8285 -0.6166 310.9807 311.5972 324.2731 310.5530 -0.6215 311.1343 311.7558 324.3360 311.4113 -0.6318 311.3195 311.9513 324.3819 312.1773 -0.6381 311.4749 312.1131 324.4032 312.9940 -0.6396 311.6430 312.2826 324.4468 313.7910 -0.6454 311.7954 312.4409 324.4824 314.5875 -0.6514 311.9659 312.6174 324.5385 315.4148 -0.6548 312.1311 312.7859 324.5985 316.1810 -0.6582 312.2741 312.9323 324.6675 317.0285 -0.6605 312.4283 313.0888 324.7689 317.8050 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