DTA measure 1Pb_updown2 Date: 2026225:1010 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.68 s Mass = 1163.600 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5285 -0.2013 247.6600 247.8613 223.3880 4.1329 -0.1887 247.5924 247.7810 223.1312 5.7428 -0.1790 247.5745 247.7535 222.8777 7.3314 -0.1713 247.5159 247.6872 222.5888 8.9410 -0.1620 247.4804 247.6424 222.3378 10.5458 -0.1561 247.4330 247.5891 222.1058 12.1505 -0.1511 247.4137 247.5648 221.8772 13.7753 -0.1452 247.3886 247.5338 221.6135 15.3795 -0.1416 247.3383 247.4799 221.3559 16.9894 -0.1329 247.2560 247.3889 221.1163 18.5941 -0.1302 247.2032 247.3334 220.8555 20.2040 -0.1287 247.1239 247.2526 220.6156 21.7975 -0.1252 247.0753 247.2006 220.3991 23.4074 -0.1199 247.0231 247.1430 220.1447 25.0121 -0.1166 246.9402 247.0568 219.9103 26.6323 -0.1143 246.8271 246.9414 219.6704 28.2415 -0.1137 246.7694 246.8831 219.4362 29.8459 -0.1089 246.7098 246.8187 219.2216 31.4558 -0.1078 246.6523 246.7601 219.0263 33.0605 -0.1068 246.5852 246.6921 218.9005 34.6700 -0.1063 246.5416 246.6479 218.7742 36.2793 -0.1066 246.4726 246.5792 218.7065 37.9045 -0.1074 246.3588 246.4662 218.6854 39.5090 -0.1052 246.2712 246.3764 218.6990 41.1181 -0.1027 246.1837 246.2864 218.7976 42.7280 -0.1052 246.1086 246.2138 218.9339 44.3276 -0.1067 246.0281 246.1349 219.1738 45.9314 -0.1117 245.9397 246.0514 219.4820 47.5310 -0.1189 245.8676 245.9865 219.8081 49.1460 -0.1209 245.7900 245.9109 220.1642 50.7353 -0.1235 245.6918 245.8153 220.5809 52.3391 -0.1337 245.6061 245.7397 221.0890 53.9439 -0.1375 245.5305 245.6680 221.5582 55.5486 -0.1438 245.4376 245.5814 221.9844 57.1479 -0.1516 245.3550 245.5067 222.4004 58.7520 -0.1564 245.2650 245.4215 222.7880 60.3568 -0.1660 245.1354 245.3014 223.1599 61.9768 -0.1779 245.0537 245.2317 223.4681 63.5909 -0.1891 244.9603 245.1494 223.7376 65.1956 -0.1965 244.8821 245.0786 223.9750 66.8055 -0.2030 244.8262 245.0292 224.1731 68.3944 -0.2147 244.7407 244.9555 224.3657 70.0038 -0.2232 244.6616 244.8848 224.5009 71.6085 -0.2277 244.6098 244.8375 224.6285 73.2184 -0.2303 244.5580 244.7883 224.7153 74.8226 -0.2376 244.4621 244.6997 224.7705 76.4423 -0.2451 244.3810 244.6261 224.8008 78.0521 -0.2592 244.3250 244.5842 224.8651 79.6569 -0.2661 244.2821 244.5482 224.9200 81.2558 -0.2748 244.2062 244.4810 224.9837 82.8603 -0.2824 244.1456 244.4280 225.0540 84.4701 -0.2819 244.1111 244.3930 225.1423 86.0749 -0.2801 244.0528 244.3329 225.2795 87.6848 -0.2870 243.9830 244.2700 225.3543 89.3043 -0.2974 243.9266 244.2239 225.5015 90.9086 -0.3050 243.8566 244.1615 225.7117 92.5185 -0.3071 243.8065 244.1136 225.9519 94.1233 -0.3131 243.7846 244.0978 226.1940 95.7325 -0.3175 243.7404 244.0579 226.4774 97.3215 -0.3223 243.6863 244.0085 226.7947 98.9468 -0.3340 243.6066 243.9406 227.1093 100.5361 -0.3407 243.5159 243.8567 227.4192 102.1559 -0.3456 243.4757 243.8213 227.7503 103.7651 -0.3509 243.4408 243.7917 228.0731 105.3750 -0.3595 243.3713 243.7309 228.3925 106.9849 -0.3714 243.3172 243.6886 228.6912 108.5835 -0.3766 243.2683 243.6449 228.9921 110.1883 -0.3839 243.2449 243.6288 229.2715 111.7725 -0.3874 243.1944 243.5818 229.5341 113.3765 -0.3950 243.1771 243.5722 229.7582 114.9913 -0.4005 243.1480 243.5485 229.9666 116.5858 -0.4047 243.1094 243.5140 230.1481 118.1904 -0.4080 243.0512 243.4592 230.2985 119.7944 -0.4100 243.0355 243.4455 230.4333 121.3939 -0.4130 243.0244 243.4374 230.5488 122.9986 -0.4234 243.0105 243.4339 230.6608 124.6085 -0.4290 243.0295 243.4585 230.7390 126.2075 -0.4338 242.9947 243.4285 230.8541 127.8273 -0.4394 242.9574 243.3969 230.9571 129.4218 -0.4396 242.9455 243.3851 231.0482 131.0265 -0.4394 242.9290 243.3684 231.1694 132.6354 -0.4428 242.9039 243.3468 231.3541 134.2401 -0.4491 242.8781 243.3272 231.4859 135.8398 -0.4536 242.8671 243.3207 231.6554 137.4493 -0.4527 242.8709 243.3236 231.8835 139.0534 -0.4514 242.8109 243.2622 232.1461 140.6786 -0.4534 242.8040 243.2574 232.3359 142.2834 -0.4466 242.8218 243.2684 232.5919 143.8975 -0.4449 242.8049 243.2498 232.8676 145.5021 -0.4442 242.7863 243.2305 233.1608 147.1120 -0.4471 242.8194 243.2665 233.4675 148.7168 -0.4441 242.8111 243.2551 233.7456 150.3309 -0.4487 242.8135 243.2622 234.0316 151.9201 -0.4548 242.8105 243.2654 234.3476 153.5454 -0.4582 242.8011 243.2593 234.6254 155.1648 -0.4622 242.8278 243.2900 234.8914 156.7744 -0.4654 242.8450 243.3104 235.1184 158.3791 -0.4677 242.8301 243.2978 235.3211 159.9890 -0.4714 242.8500 243.3215 235.5166 161.5980 -0.4725 242.8659 243.3383 235.6789 163.2078 -0.4706 242.9023 243.3729 235.8677 164.7971 -0.4696 242.9362 243.4058 236.0536 166.4275 -0.4739 242.9865 243.4603 236.2293 168.0323 -0.4799 242.9993 243.4792 236.3837 169.6360 -0.4808 243.0207 243.5015 236.5689 171.2459 -0.4768 243.0532 243.5300 236.7199 172.8506 -0.4760 243.0666 243.5426 236.8349 174.4554 -0.4774 243.0834 243.5608 236.9850 176.0394 -0.4784 243.1053 243.5837 237.1446 177.6383 -0.4763 243.1378 243.6141 237.2845 179.2533 -0.4774 243.1378 243.6152 237.4770 180.8626 -0.4744 243.1610 243.6354 237.6804 182.4464 -0.4736 243.1995 243.6731 237.8608 184.0511 -0.4719 243.2211 243.6930 238.0824 185.6508 -0.4735 243.2693 243.7429 238.3013 187.2555 -0.4691 243.3437 243.8128 238.5429 188.8595 -0.4656 243.3950 243.8606 238.8148 190.4640 -0.4622 243.4415 243.9037 239.0844 192.0739 -0.4584 243.5124 243.9708 239.3504 193.6631 -0.4533 243.5584 244.0117 239.6442 195.2773 -0.4533 243.6035 244.0568 239.9200 196.8871 -0.4609 243.6584 244.1193 240.1794 198.4919 -0.4632 243.6812 244.1444 240.4126 200.1013 -0.4565 243.7204 244.1769 240.6542 201.7055 -0.4592 243.7469 244.2061 240.8906 203.3154 -0.4640 243.8389 244.3029 241.0773 204.9095 -0.4611 243.9479 244.4090 241.3038 206.5188 -0.4607 244.0259 244.4866 241.4968 208.1389 -0.4528 244.1204 244.5732 241.6841 209.7433 -0.4523 244.1861 244.6383 241.8846 211.3525 -0.4525 244.2400 244.6925 242.0465 212.9573 -0.4549 244.2810 244.7359 242.2443 214.5671 -0.4515 244.3318 244.7833 242.3753 216.1716 -0.4460 244.4147 244.8607 242.5169 217.7808 -0.4414 244.5122 244.9536 242.6725 219.4009 -0.4411 244.6056 245.0467 242.8466 221.0108 -0.4391 244.6975 245.1366 243.0257 222.6199 -0.4339 244.7686 245.2025 243.1838 224.2244 -0.4339 244.8248 245.2587 243.3712 225.8189 -0.4335 244.9130 245.3464 243.5584 227.4286 -0.4337 244.9873 245.4209 243.7703 229.0376 -0.4301 245.0803 245.5103 244.0475 230.6424 -0.4291 245.1449 245.5740 244.3122 232.2676 -0.4288 245.2406 245.6694 244.5392 233.8775 -0.4306 245.3204 245.7509 244.7648 235.4864 -0.4253 245.4016 245.8269 244.9920 237.0911 -0.4197 245.4918 245.9115 245.2606 238.6856 -0.4195 245.5887 246.0082 245.5154 240.2899 -0.4175 245.7066 246.1240 245.7838 241.8941 -0.4159 245.8255 246.2415 246.0162 243.4938 -0.4147 245.9393 246.3539 246.2675 245.1036 -0.4142 246.0348 246.4490 246.5318 246.7076 -0.4111 246.1234 246.5344 246.7966 248.3070 -0.4038 246.2027 246.6065 247.0349 249.9118 -0.3980 246.3052 246.7032 247.2370 251.5165 -0.3926 246.4157 246.8083 247.4248 253.1256 -0.3922 246.4936 246.8858 247.5957 254.7301 -0.3937 246.5926 246.9863 247.8049 256.3503 -0.3921 246.7190 247.1111 247.9675 257.9601 -0.3877 246.8158 247.2035 248.1025 259.5644 -0.3808 246.9021 247.2829 248.2704 261.1738 -0.3729 246.9707 247.3437 248.4026 262.7785 -0.3687 247.1328 247.5015 248.5373 264.3884 -0.3673 247.2473 247.6146 248.7230 265.9931 -0.3627 247.3847 247.7474 248.8827 267.5919 -0.3648 247.5138 247.8786 249.0487 269.2119 -0.3675 247.5926 247.9602 249.2880 270.8269 -0.3668 247.6891 248.0559 249.5097 272.4306 -0.3653 247.8215 248.1868 249.7249 274.0200 -0.3575 247.9268 248.2843 249.9347 275.6299 -0.3596 248.0592 248.4188 250.1526 277.2398 -0.3630 248.2063 248.5693 250.3851 278.8486 -0.3613 248.3204 248.6817 250.6309 280.4534 -0.3523 248.4645 248.8168 250.8858 282.0786 -0.3444 248.6044 248.9489 251.1459 283.6834 -0.3421 248.7311 249.0732 251.3868 285.2771 -0.3387 248.8963 249.2350 251.6564 286.8816 -0.3342 249.0133 249.3475 251.9234 288.4915 -0.3353 249.1269 249.4622 252.1851 290.1014 -0.3372 249.2678 249.6050 252.4216 291.7051 -0.3341 249.4231 249.7572 252.6281 293.3150 -0.3305 249.5408 249.8712 252.8662 294.9351 -0.3316 249.6779 250.0095 253.0277 296.5450 -0.3295 249.8179 250.1474 253.2511 298.1495 -0.3252 249.9418 250.2670 253.4585 299.7433 -0.3270 250.0731 250.4000 253.6537 301.3429 -0.3279 250.2004 250.5283 253.8336 302.9425 -0.3243 250.3053 250.6296 253.9914 304.5464 -0.3179 250.4383 250.7562 254.1514 306.1510 -0.3095 250.5987 250.9082 254.3251 307.7660 -0.3106 250.6987 251.0093 254.5303 309.3503 -0.3104 250.8190 251.1294 254.7245 310.9593 -0.3022 250.9781 251.2803 254.8870 312.5588 -0.2997 251.1512 251.4509 255.0784 314.1635 -0.2991 251.2879 251.5870 255.3223 315.7680 -0.3002 251.5046 251.8049 255.5043 317.3720 -0.2950 251.6815 251.9765 255.6856 318.9819 -0.2902 251.8301 252.1203 255.8752 320.5969 -0.2857 251.9880 252.2737 256.0727 322.2009 -0.2806 252.1541 252.4347 256.2886 323.7951 -0.2804 252.2984 252.5788 256.5362 325.3999 -0.2760 252.4217 252.6977 256.7492 327.0098 -0.2732 252.5744 252.8476 256.9985 328.6190 -0.2699 252.7198 252.9897 257.2727 330.2285 -0.2725 252.9213 253.1937 257.5265 331.8384 -0.2708 253.0515 253.3223 257.7641 333.4431 -0.2656 253.1999 253.4655 258.0097 335.0633 -0.2639 253.3618 253.6257 258.2779 336.6725 -0.2626 253.5103 253.7729 258.5088 338.2718 -0.2559 253.6801 253.9360 258.7191 339.8816 -0.2510 253.8600 254.1110 258.9840 341.4864 -0.2521 254.0022 254.2543 259.2209 343.0963 -0.2531 254.1835 254.4366 259.4309 344.7001 -0.2499 254.3396 254.5895 259.6465 346.3099 -0.2486 254.4943 254.7429 259.8295 347.9300 -0.2449 254.6614 254.9062 260.0380 349.5399 -0.2460 254.8717 255.1177 260.2312 351.1438 -0.2448 255.0568 255.3016 260.3893 352.7484 -0.2406 255.2297 255.4703 260.5288 354.3634 -0.2407 255.4109 255.6517 260.6924 355.9676 -0.2361 255.5400 255.7761 260.8779 357.5770 -0.2367 255.7170 255.9537 260.9955 359.1920 -0.2436 255.9290 256.1726 261.1655 360.8019 -0.2408 256.1337 256.3745 261.3882 362.4165 -0.2372 256.2558 256.4930 261.5825 364.0206 -0.2329 256.3906 256.6236 261.7812 365.6203 -0.2230 256.5300 256.7530 261.9705 367.2301 -0.2215 256.6900 256.9115 262.1847 368.8090 -0.2183 256.8674 257.0857 262.4189 370.4079 -0.2213 257.0956 257.3170 262.6627 372.0178 -0.2223 257.2861 257.5084 262.9131 373.6328 -0.2257 257.4401 257.6658 263.1687 375.2318 -0.2260 257.6405 257.8664 263.4290 376.8361 -0.2244 257.8303 258.0547 263.6538 378.4255 -0.2207 258.0142 258.2349 263.8874 380.0303 -0.2176 258.1638 258.3814 264.1391 381.6393 -0.2179 258.3496 258.5674 264.3632 383.2439 -0.2169 258.4858 258.7028 264.6235 384.8538 -0.2192 258.6659 258.8851 264.8681 386.4429 -0.2219 258.8732 259.0951 265.1149 388.0623 -0.2211 259.0647 259.2858 265.3312 389.6721 -0.2145 259.2576 259.4721 265.5414 391.2769 -0.2123 259.4400 259.6524 265.7146 392.8813 -0.2157 259.6263 259.8421 265.9017 394.4854 -0.2147 259.7875 260.0021 266.0837 396.0748 -0.2110 259.9574 260.1684 266.2436 397.6846 -0.2083 260.1452 260.3534 266.4138 399.2888 -0.2072 260.3435 260.5507 266.5902 400.9136 -0.2077 260.5358 260.7435 266.7985 402.5184 -0.2089 260.7500 260.9589 266.9499 404.1283 -0.2145 260.9656 261.1801 267.0847 405.7320 -0.2146 261.1414 261.3560 267.2609 407.3368 -0.2077 261.3134 261.5211 267.4236 408.9466 -0.2041 261.4973 261.7014 267.6321 410.5506 -0.2050 261.6893 261.8942 267.8807 412.1756 -0.2056 261.8875 262.0931 268.1336 413.7804 -0.2060 262.0982 262.3043 268.3885 415.3903 -0.2106 262.2794 262.4900 268.6559 416.9941 -0.2085 262.4772 262.6857 268.9384 418.5988 -0.2024 262.6501 262.8525 269.1812 420.2086 -0.1989 262.8462 263.0450 269.4358 421.8134 -0.2008 263.0655 263.2663 269.6836 423.4378 -0.2060 263.2891 263.4951 269.9633 425.0424 -0.2084 263.4649 263.6733 270.2215 426.6523 -0.2070 263.6596 263.8666 270.4947 428.2570 -0.2078 263.8654 264.0732 270.7550 429.8660 -0.2082 264.0751 264.2833 270.9731 431.4655 -0.2136 264.2584 264.4719 271.1199 433.0703 -0.2187 264.4656 264.6843 271.3242 434.6850 -0.2195 264.6455 264.8650 271.4915 436.2736 -0.2153 264.8309 265.0462 271.6413 437.8886 -0.2129 265.0692 265.2821 271.7801 439.4780 -0.2114 265.2570 265.4684 271.9055 441.0875 -0.2098 265.4242 265.6340 272.0591 442.7019 -0.2118 265.6645 265.8763 272.1907 444.2913 -0.2122 265.8964 266.1086 272.3422 445.9010 -0.2114 266.1142 266.3256 272.5244 447.5049 -0.2067 266.2909 266.4977 272.6556 449.1096 -0.2096 266.4770 266.6866 272.8614 450.7298 -0.2136 266.6601 266.8737 273.0862 452.3345 -0.2122 266.8806 267.0928 273.2971 453.9435 -0.2134 267.0697 267.2831 273.5038 455.5481 -0.2117 267.3018 267.5135 273.7520 457.1580 -0.2100 267.4774 267.6874 274.0287 458.7625 -0.2107 267.6817 267.8923 274.3069 460.3665 -0.2115 267.8799 268.0913 274.6245 461.9918 -0.2093 268.0981 268.3074 274.9104 463.5965 -0.2052 268.2961 268.5013 275.2241 465.2055 -0.2116 268.4979 268.7095 275.4917 466.8101 -0.2144 268.6956 268.9100 275.7561 468.4200 -0.2148 268.8975 269.1124 275.9831 470.0248 -0.2136 269.1451 269.3587 276.2366 471.6389 -0.2161 269.3724 269.5885 276.4550 473.2589 -0.2212 269.5504 269.7717 276.6711 474.8636 -0.2294 269.7510 269.9804 276.8498 476.4735 -0.2303 269.9601 270.1903 277.0125 478.0825 -0.2327 270.1721 270.4048 277.1822 479.6923 -0.2366 270.3857 270.6223 277.3655 481.2970 -0.2349 270.5939 270.8289 277.5179 482.9063 -0.2363 270.8132 271.0496 277.6540 484.5260 -0.2408 271.0295 271.2703 277.7854 486.1359 -0.2379 271.2571 271.4950 277.9344 487.7405 -0.2382 271.4685 271.7067 278.1238 489.3495 -0.2374 271.6855 271.9230 278.2773 490.9594 -0.2419 271.9105 272.1525 278.4470 492.5641 -0.2425 272.1379 272.3804 278.6580 494.1738 -0.2409 272.3594 272.6003 278.8787 495.7880 -0.2465 272.5595 272.8060 279.1249 497.3876 -0.2429 272.7318 272.9747 279.3897 498.9821 -0.2437 272.9281 273.1718 279.6137 500.5814 -0.2483 273.1371 273.3854 279.8460 502.1855 -0.2500 273.3432 273.5932 280.1165 503.7851 -0.2506 273.5638 273.8145 280.3822 505.3899 -0.2518 273.7775 274.0293 280.6316 506.9946 -0.2539 274.0058 274.2597 280.9219 508.6141 -0.2556 274.2554 274.5111 281.1953 510.2185 -0.2573 274.4751 274.7324 281.4258 511.8284 -0.2621 274.7165 274.9786 281.6438 513.4330 -0.2644 274.9506 275.2150 281.8877 515.0318 -0.2697 275.1610 275.4307 282.1069 516.6416 -0.2744 275.3284 275.6028 282.3329 518.2464 -0.2787 275.5516 275.8303 282.5441 519.8710 -0.2824 275.7842 276.0666 282.7258 521.4754 -0.2823 275.9908 276.2731 282.8935 523.0853 -0.2851 276.2274 276.5125 283.0393 524.6900 -0.2872 276.4174 276.7045 283.1941 526.2939 -0.2835 276.6549 276.9383 283.3581 527.9036 -0.2895 276.8843 277.1738 283.5289 529.4930 -0.2887 277.0913 277.3800 283.6839 531.1020 -0.2853 277.3247 277.6100 283.8830 532.7220 -0.2845 277.5097 277.7942 284.0812 534.3319 -0.2858 277.6656 277.9514 284.2730 535.9360 -0.2831 277.8982 278.1813 284.4381 537.5404 -0.2882 278.1208 278.4090 284.6027 539.1503 -0.2957 278.3474 278.6431 284.7838 540.7550 -0.3004 278.5619 278.8623 285.0463 542.3694 -0.2990 278.8066 279.1055 285.3109 543.9891 -0.2998 279.0208 279.3206 285.5847 545.5990 -0.3027 279.2483 279.5510 285.8412 547.2089 -0.3029 279.4834 279.7863 286.1439 548.8179 -0.3010 279.7212 280.0222 286.4424 550.4071 -0.3026 279.9366 280.2392 286.7236 552.0170 -0.3125 280.1241 280.4366 286.9494 553.6215 -0.3174 280.3371 280.6546 287.1871 555.2358 -0.3211 280.5451 280.8662 287.4290 556.8559 -0.3246 280.7635 281.0882 287.6819 558.4553 -0.3271 280.9970 281.3241 287.8946 560.0541 -0.3303 281.2624 281.5927 288.0958 561.6538 -0.3319 281.5078 281.8397 288.2800 563.2585 -0.3330 281.7580 282.0910 288.4373 564.8528 -0.3355 281.9601 282.2956 288.6040 566.4619 -0.3412 282.1911 282.5322 288.7478 568.0769 -0.3446 282.3758 282.7204 288.8572 569.6816 -0.3492 282.5816 282.9308 289.0188 571.2754 -0.3561 282.8072 283.1633 289.1988 572.8748 -0.3608 283.0449 283.4057 289.3420 574.4846 -0.3581 283.2335 283.5916 289.5272 576.0894 -0.3633 283.4461 283.8094 289.7472 577.6935 -0.3663 283.6926 284.0589 289.9695 579.3030 -0.3690 283.9134 284.2825 290.2052 580.8924 -0.3739 284.1517 284.5256 290.4104 582.5176 -0.3787 284.3717 284.7505 290.6053 584.1220 -0.3882 284.6089 284.9970 290.8477 585.7313 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