DTA measure 3Pb_updown Date: 2026225:937 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.77 s Mass = 1163.600 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5429 -4.6973 459.1521 463.8494 434.3383 4.1255 -4.7113 459.1827 463.8940 434.5885 5.7239 -4.7255 459.2339 463.9594 434.6939 7.3274 -4.7403 459.3279 464.0683 434.6889 8.9305 -4.7539 459.3967 464.1506 434.5637 10.5289 -4.7679 459.3808 464.1487 434.2941 12.1525 -4.7823 459.3985 464.1808 433.8509 13.7406 -4.7860 459.4525 464.2385 433.4204 15.3491 -4.7943 459.5071 464.3015 432.9405 16.9524 -4.8032 459.5775 464.3807 432.4083 18.5609 -4.8120 459.6061 464.4181 431.8484 20.1641 -4.8125 459.6033 464.4158 431.2731 21.7676 -4.8138 459.6285 464.4423 430.7147 23.3763 -4.8188 459.6933 464.5120 430.1704 24.9948 -4.8215 459.7347 464.5562 429.6345 26.6034 -4.8233 459.7493 464.5725 429.1760 28.2068 -4.8262 459.7521 464.5783 428.8146 29.8151 -4.8295 459.7374 464.5669 428.5302 31.4186 -4.8339 459.7247 464.5586 428.2986 33.0219 -4.8428 459.7097 464.5525 428.1214 34.6613 -4.8468 459.7358 464.5826 428.0059 36.2698 -4.8494 459.7145 464.5639 427.9648 37.8781 -4.8587 459.7002 464.5589 427.9794 39.4816 -4.8648 459.6531 464.5178 428.0355 41.0953 -4.8712 459.6243 464.4955 428.0894 42.6985 -4.8753 459.5869 464.4622 428.1438 44.3019 -4.8820 459.5710 464.4530 428.1976 45.9154 -4.8888 459.5281 464.4169 428.2045 47.5343 -4.8976 459.4900 464.3876 428.1284 49.1376 -4.9022 459.4565 464.3587 428.0417 50.7511 -4.9126 459.4718 464.3844 427.8978 52.3546 -4.9229 459.4409 464.3638 427.6763 53.9680 -4.9311 459.3683 464.2994 427.4074 55.5613 -4.9387 459.3155 464.2542 427.0794 57.1696 -4.9445 459.2348 464.1793 426.7428 58.7783 -4.9501 459.1991 464.1491 426.3591 60.4021 -4.9557 459.1645 464.1201 425.9762 62.0054 -4.9593 459.1723 464.1317 425.5979 63.6141 -4.9615 459.1276 464.0891 425.2126 65.2175 -4.9639 459.0587 464.0226 424.8592 66.8258 -4.9684 458.9919 463.9602 424.5395 68.4089 -4.9740 458.9404 463.9144 424.2341 70.0073 -4.9769 458.8558 463.8327 423.9727 71.6105 -4.9740 458.7764 463.7504 423.7173 73.2294 -4.9722 458.7443 463.7165 423.4931 74.8276 -4.9754 458.7020 463.6774 423.3452 76.4360 -4.9745 458.6065 463.5810 423.2238 78.0241 -4.9796 458.5427 463.5222 423.0765 79.6225 -4.9837 458.4693 463.4530 422.9258 81.2309 -4.9896 458.3432 463.3328 422.8062 82.8293 -4.9962 458.2758 463.2720 422.6699 84.4378 -4.9984 458.1694 463.1678 422.5856 86.0565 -4.9978 458.0848 463.0827 422.4824 87.6600 -4.9984 457.9462 462.9446 422.3624 89.2686 -4.9986 457.8611 462.8597 422.2366 90.8719 -4.9977 457.7908 462.7885 422.1153 92.4806 -5.0020 457.6787 462.6808 421.9360 94.0841 -5.0052 457.5961 462.6012 421.7416 95.6924 -5.0178 457.4925 462.5104 421.4905 97.3113 -5.0237 457.4146 462.4383 421.2526 98.9199 -5.0253 457.3269 462.3522 421.0584 100.5283 -5.0287 457.2235 462.2521 420.8048 102.1319 -5.0298 457.1283 462.1581 420.5157 103.7405 -5.0241 457.0325 462.0565 420.1757 105.3436 -5.0226 456.9160 461.9386 419.8936 106.9523 -5.0268 456.8002 461.8271 419.6307 108.5760 -5.0311 456.7335 461.7645 419.3381 110.1895 -5.0353 456.6465 461.6818 419.0965 111.7929 -5.0311 456.5010 461.5321 418.8269 113.4013 -5.0286 456.3941 461.4227 418.6033 115.0048 -5.0300 456.2811 461.3111 418.4086 116.6181 -5.0300 456.1619 461.1919 418.1815 118.2216 -5.0294 456.0545 461.0839 418.0087 119.8455 -5.0258 455.9395 460.9653 417.8122 121.4488 -5.0291 455.8016 460.8307 417.6483 123.0471 -5.0343 455.6570 460.6913 417.4705 124.6555 -5.0371 455.5440 460.5811 417.2870 126.2641 -5.0383 455.3861 460.4244 417.1037 127.8728 -5.0390 455.2694 460.3084 416.9700 129.4811 -5.0427 455.0864 460.1290 416.8290 131.0794 -5.0417 454.9542 459.9958 416.6456 132.6981 -5.0463 454.8329 459.8792 416.4668 134.3014 -5.0445 454.7490 459.7935 416.2746 135.8844 -5.0475 454.5971 459.6447 416.0634 137.4876 -5.0446 454.4236 459.4682 415.8930 139.0963 -5.0491 454.3008 459.3499 415.6753 140.6944 -5.0504 454.1734 459.2238 415.4506 142.2976 -5.0457 454.0670 459.1127 415.2250 143.8909 -5.0446 453.9098 458.9545 414.9947 145.4940 -5.0439 453.7492 458.7931 414.7593 147.1179 -5.0448 453.5659 458.6107 414.5048 148.7211 -5.0439 453.4620 458.5059 414.2600 150.3298 -5.0423 453.3344 458.3766 414.0147 151.9176 -5.0386 453.1905 458.2292 413.7425 153.5210 -5.0361 453.0356 458.0717 413.5019 155.1348 -5.0325 452.8995 457.9320 413.2582 156.7381 -5.0328 452.7442 457.7770 413.0305 158.3518 -5.0288 452.6105 457.6393 412.8243 159.9399 -5.0381 452.4449 457.4830 412.6634 161.5638 -5.0356 452.2804 457.3160 412.4685 163.1671 -5.0311 452.1173 457.1484 412.2762 164.7809 -5.0319 451.9321 456.9640 412.1201 166.3843 -5.0284 451.7810 456.8094 411.9095 167.9928 -5.0221 451.6257 456.6477 411.7050 169.5808 -5.0175 451.5052 456.5227 411.5331 171.1891 -5.0210 451.3684 456.3894 411.3226 172.7978 -5.0124 451.2053 456.2177 411.1341 174.4215 -5.0124 451.0407 456.0531 410.9350 176.0249 -5.0118 450.9065 455.9184 410.7302 177.6283 -5.0100 450.7705 455.7805 410.5300 179.2366 -5.0024 450.6216 455.6240 410.3321 180.8401 -4.9969 450.4285 455.4254 410.1188 182.4536 -4.9931 450.2400 455.2331 409.8753 184.0570 -4.9892 450.0772 455.0664 409.6500 185.6810 -4.9849 449.8915 454.8764 409.4012 187.2893 -4.9827 449.7454 454.7281 409.1757 188.8979 -4.9806 449.5705 454.5511 408.9629 190.5065 -4.9820 449.4062 454.3882 408.7158 192.1149 -4.9794 449.2433 454.2227 408.5181 193.7184 -4.9724 449.0861 454.0585 408.3171 195.3219 -4.9690 448.9308 453.8998 408.1171 196.9250 -4.9679 448.7349 453.7028 407.9531 198.5234 -4.9626 448.5467 453.5093 407.7472 200.1266 -4.9611 448.3332 453.2943 407.5168 201.7301 -4.9565 448.1558 453.1123 407.3128 203.3336 -4.9614 448.0075 452.9689 407.0899 204.9421 -4.9623 447.8510 452.8133 406.8771 206.5455 -4.9535 447.7103 452.6638 406.6812 208.1438 -4.9461 447.5278 452.4739 406.4894 209.7675 -4.9404 447.3643 452.3047 406.2392 211.3710 -4.9406 447.1971 452.1377 406.0149 212.9796 -4.9389 447.0331 451.9720 405.8094 214.5829 -4.9374 446.8372 451.7745 405.6185 216.1914 -4.9355 446.6498 451.5853 405.4408 217.7950 -4.9330 446.4666 451.3996 405.2590 219.3983 -4.9231 446.3127 451.2358 405.0336 221.0223 -4.9178 446.1499 451.0676 404.8180 222.6258 -4.9199 445.9407 450.8606 404.5945 224.2341 -4.9166 445.7500 450.6666 404.4013 225.8376 -4.9077 445.5772 450.4850 404.1832 227.4514 -4.9002 445.3720 450.2722 403.9562 229.0546 -4.8935 445.2164 450.1100 403.7393 230.6633 -4.8924 445.0216 449.9141 403.5002 232.2821 -4.8904 444.8388 449.7292 403.3142 233.8955 -4.8884 444.6590 449.5474 403.1566 235.4990 -4.8802 444.4691 449.3494 402.9372 237.0969 -4.8764 444.2709 449.1473 402.7321 238.7005 -4.8708 444.1144 448.9852 402.5225 240.3193 -4.8679 443.9041 448.7719 402.2944 241.9276 -4.8618 443.7100 448.5718 402.0648 243.5363 -4.8591 443.5190 448.3780 401.8481 245.1448 -4.8582 443.3742 448.2324 401.6363 246.7533 -4.8552 443.1963 448.0515 401.4085 248.3618 -4.8539 443.0149 447.8688 401.2029 249.9651 -4.8486 442.8268 447.6754 400.9673 251.5738 -4.8433 442.6469 447.4902 400.7528 253.1824 -4.8358 442.4859 447.3217 400.5108 254.7755 -4.8311 442.2988 447.1299 400.3089 256.3840 -4.8297 442.1399 446.9696 400.1100 258.0081 -4.8269 441.9247 446.7516 399.9264 259.6115 -4.8207 441.7406 446.5613 399.7018 261.2045 -4.8158 441.5244 446.3402 399.4656 262.8133 -4.8101 441.3191 446.1293 399.2542 264.3909 -4.8073 441.1071 445.9144 399.0470 265.9943 -4.8019 440.9155 445.7174 398.8509 267.5976 -4.7933 440.7297 445.5230 398.6253 269.2009 -4.7901 440.5428 445.3329 398.4057 270.8196 -4.7812 440.3644 445.1455 398.2313 272.4128 -4.7763 440.1561 444.9325 398.0659 274.0160 -4.7671 439.9686 444.7357 397.9120 275.6248 -4.7632 439.7609 444.5241 397.7518 277.2280 -4.7612 439.5926 444.3538 397.5701 278.8366 -4.7591 439.3995 444.1586 397.4070 280.4400 -4.7577 439.2276 443.9853 397.1831 282.0433 -4.7557 438.9951 443.7508 396.9792 283.6673 -4.7456 438.8410 443.5866 396.7435 285.2706 -4.7448 438.6359 443.3807 396.5252 286.8841 -4.7361 438.4245 443.1606 396.2608 288.4875 -4.7268 438.2049 442.9317 396.0039 290.0959 -4.7201 438.0109 442.7310 395.7669 291.6890 -4.7136 437.8082 442.5218 395.5019 293.3026 -4.7111 437.5589 442.2700 395.2887 294.9059 -4.7142 437.3616 442.0759 395.1204 296.5299 -4.7071 437.2003 441.9073 394.8709 298.1331 -4.7011 437.0031 441.7042 394.6547 299.7418 -4.7000 436.7816 441.4817 394.4419 301.3503 -4.6924 436.5685 441.2609 394.2221 302.9586 -4.6889 436.3930 441.0819 394.0280 304.5673 -4.6887 436.2286 440.9173 393.8184 306.1604 -4.6853 436.0611 440.7464 393.6026 307.7689 -4.6762 435.8718 440.5481 393.4050 309.3979 -4.6702 435.6170 440.2872 393.2318 311.0011 -4.6599 435.4228 440.0827 393.0297 312.6098 -4.6509 435.2249 439.8758 392.8528 314.2184 -4.6503 434.9925 439.6429 392.6330 315.8320 -4.6462 434.8430 439.4892 392.4357 317.4354 -4.6421 434.6477 439.2898 392.2189 319.0440 -4.6439 434.4641 439.1079 392.0081 320.6678 -4.6453 434.2784 438.9237 391.8252 322.2763 -4.6365 434.0675 438.7040 391.6244 323.8746 -4.6292 433.8527 438.4819 391.4303 325.4780 -4.6217 433.6368 438.2585 391.2047 327.0815 -4.6154 433.4474 438.0629 391.0011 328.6645 -4.6121 433.2778 437.8899 390.7884 330.2676 -4.6056 433.0786 437.6842 390.5685 331.8763 -4.5962 432.8493 437.4454 390.3622 333.4899 -4.5853 432.6384 437.2237 390.1527 335.0933 -4.5807 432.4013 436.9820 389.9153 336.7019 -4.5733 432.1829 436.7562 389.6583 338.3051 -4.5623 431.9752 436.5376 389.4017 339.8983 -4.5656 431.7873 436.3529 389.2069 341.5015 -4.5617 431.5771 436.1388 388.9735 343.1100 -4.5556 431.3802 435.9357 388.7370 344.7134 -4.5486 431.1850 435.7337 388.5178 346.3165 -4.5455 430.9830 435.5285 388.3317 347.9251 -4.5407 430.7408 435.2815 388.1210 349.5285 -4.5351 430.5192 435.0543 387.9141 351.1370 -4.5275 430.3231 434.8506 387.7149 352.7405 -4.5217 430.1269 434.6485 387.4929 354.3490 -4.5142 429.9572 434.4713 387.2945 355.9575 -4.5095 429.8196 434.3291 387.1094 357.5661 -4.5077 429.6419 434.1496 386.9329 359.1849 -4.4988 429.4101 433.9088 386.7472 360.7729 -4.4998 429.1699 433.6697 386.5827 362.3866 -4.4957 429.0021 433.4978 386.3757 363.9900 -4.4934 428.8022 433.2956 386.1567 365.6036 -4.4923 428.5787 433.0710 385.8879 367.2071 -4.4836 428.3816 432.8653 385.6850 368.8206 -4.4770 428.1706 432.6476 385.4758 370.4086 -4.4747 427.9580 432.4328 385.2459 372.0224 -4.4670 427.7783 432.2453 385.0535 373.6409 -4.4540 427.5631 432.0171 384.8634 375.2495 -4.4468 427.3686 431.8154 384.6615 376.8529 -4.4408 427.1471 431.5879 384.4380 378.4665 -4.4383 426.9433 431.3816 384.2259 380.0700 -4.4397 426.6972 431.1369 384.0039 381.6783 -4.4334 426.4760 430.9094 383.7495 383.2869 -4.4243 426.2854 430.7097 383.5574 384.9106 -4.4228 426.0717 430.4945 383.3521 386.5140 -4.4148 425.8603 430.2751 383.1290 388.1124 -4.4015 425.6612 430.0627 382.9068 389.7156 -4.3928 425.4346 429.8275 382.7005 391.3036 -4.3901 425.2091 429.5992 382.5271 392.9174 -4.3855 425.0003 429.3858 382.3341 394.5104 -4.3721 424.8085 429.1806 382.1284 396.1086 -4.3660 424.6286 428.9946 381.9066 397.7325 -4.3612 424.4148 428.7760 381.6761 399.3358 -4.3567 424.1909 428.5476 381.4766 400.9393 -4.3506 423.9613 428.3119 381.2525 402.5321 -4.3461 423.7538 428.0999 381.0350 404.1356 -4.3456 423.5787 427.9243 380.8023 405.7441 -4.3413 423.3617 427.7029 380.5719 407.3475 -4.3374 423.1404 427.4777 380.3693 408.9561 -4.3358 422.9542 427.2900 380.1752 410.5749 -4.3259 422.7250 427.0510 379.9768 412.1783 -4.3169 422.4896 426.8065 379.7631 413.7870 -4.3096 422.2556 426.5652 379.4959 415.3904 -4.3054 422.0730 426.3785 379.2883 416.9989 -4.3044 421.8743 426.1787 379.0557 418.6024 -4.2966 421.6837 425.9803 378.8554 420.2161 -4.2805 421.4884 425.7689 378.6303 421.8348 -4.2711 421.2773 425.5484 378.4215 423.4434 -4.2658 421.0799 425.3457 378.2441 425.0469 -4.2639 420.8732 425.1371 378.0555 426.6604 -4.2583 420.6617 424.9200 377.8609 428.2639 -4.2532 420.4529 424.7061 377.6707 429.8775 -4.2490 420.2296 424.4786 377.4272 431.4808 -4.2434 420.0064 424.2498 377.2256 433.0996 -4.2393 419.7854 424.0247 377.0116 434.7081 -4.2325 419.6004 423.8328 376.8235 436.3166 -4.2225 419.4015 423.6240 376.6244 437.9253 -4.2202 419.1713 423.3915 376.3987 439.5338 -4.2173 418.9562 423.1735 376.1761 441.1423 -4.2108 418.7680 422.9787 376.0097 442.7509 -4.1978 418.5901 422.7879 375.7956 444.3748 -4.1877 418.4015 422.5892 375.6050 445.9833 -4.1811 418.1888 422.3700 375.3946 447.5919 -4.1766 417.9835 422.1601 375.1720 449.1953 -4.1696 417.7758 421.9454 374.9608 450.8089 -4.1614 417.5719 421.7333 374.7486 452.4071 -4.1581 417.3277 421.4858 374.5362 454.0104 -4.1557 417.1264 421.2821 374.3215 455.5933 -4.1557 416.9010 421.0567 374.0953 457.2120 -4.1519 416.6817 420.8336 373.8675 458.8103 -4.1497 416.4725 420.6222 373.6272 460.4188 -4.1404 416.2679 420.4083 373.4161 462.0219 -4.1338 416.0846 420.2185 373.2246 463.6305 -4.1263 415.8756 420.0019 372.9769 465.2289 -4.1129 415.6685 419.7814 372.7616 466.8323 -4.1067 415.4265 419.5332 372.5233 468.4254 -4.1027 415.2129 419.3156 372.3027 470.0443 -4.0939 414.9957 419.0896 372.1015 471.6526 -4.0885 414.7772 418.8657 371.8828 473.2561 -4.0873 414.5739 418.6612 371.6879 474.8698 -4.0829 414.3944 418.4773 371.4981 476.4730 -4.0780 414.1927 418.2706 371.3029 478.0816 -4.0686 413.9508 418.0195 371.0755 479.6849 -4.0613 413.7140 417.7752 370.8913 481.3038 -4.0543 413.5052 417.5594 370.6596 482.9124 -4.0502 413.2925 417.3427 370.4643 484.5208 -4.0455 413.0642 417.1097 370.2786 486.1294 -4.0368 412.8755 416.9123 370.0774 487.7329 -4.0287 412.6705 416.6992 369.8960 489.3415 -4.0284 412.4504 416.4788 369.6691 490.9295 -4.0219 412.2395 416.2614 369.4953 492.5690 -4.0159 412.0473 416.0632 369.2635 494.1723 -4.0135 411.7965 415.8100 369.0505 495.7705 -4.0057 411.5566 415.5622 368.8683 497.3791 -3.9955 411.2951 415.2906 368.6609 498.9876 -3.9932 411.0994 415.0926 368.4479 500.5960 -3.9875 410.9121 414.8996 368.2367 502.2046 -3.9816 410.6890 414.6705 368.0124 503.8080 -3.9754 410.4880 414.4634 367.7641 505.4371 -3.9677 410.3014 414.2690 367.5110 507.0405 -3.9626 410.0998 414.0624 367.2455 508.6439 -3.9608 409.9078 413.8686 367.0059 510.2524 -3.9537 409.6933 413.6470 366.7961 511.8611 -3.9457 409.4630 413.4087 366.5959 513.4696 -3.9431 409.2691 413.2122 366.3809 515.0781 -3.9369 409.0919 413.0288 366.1811 516.6969 -3.9327 408.8719 412.8045 366.0132 518.2848 -3.9283 408.6451 412.5734 365.7988 519.8831 -3.9217 408.4230 412.3446 365.5586 521.4919 -3.9109 408.1902 412.1010 365.3615 523.0951 -3.8994 407.9847 411.8841 365.1781 524.6986 -3.8876 407.7601 411.6478 364.9778 526.3021 -3.8837 407.5296 411.4133 364.7515 527.8899 -3.8851 407.3225 411.2076 364.5508 529.4985 -3.8835 407.0975 410.9810 364.3599 531.1173 -3.8744 406.9035 410.7779 364.1559 532.7256 -3.8679 406.7262 410.5942 363.9789 534.3290 -3.8590 406.5145 410.3735 363.7868 535.9375 -3.8554 406.2993 410.1546 363.5877 537.5409 -3.8495 406.0859 409.9355 363.3938 539.1445 -3.8462 405.8539 409.7001 363.1750 540.7529 -3.8422 405.6238 409.4660 362.9284 542.3715 -3.8399 405.3962 409.2361 362.7254 543.9800 -3.8327 405.1744 409.0071 362.5202 545.5834 -3.8238 404.9550 408.7788 362.3270 547.1971 -3.8176 404.7217 408.5392 362.1266 548.8003 -3.8134 404.5368 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