DTA measure 1pbupdown3 Date: 20241113:1016 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 13.24 s Mass = 106.000 mg data_number = 65 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.4430 -4.0687 256.9140 260.9828 416.3968 0.6270 -4.0704 257.0459 261.1164 416.5880 0.8090 -4.0727 257.1763 261.2491 416.7810 0.9920 -4.0753 257.3317 261.4070 416.9784 1.1750 -4.0785 257.4729 261.5513 417.1569 1.3580 -4.0805 257.6224 261.7029 417.3494 1.6610 -4.0820 257.8672 261.9492 417.6597 1.8440 -4.0824 258.0207 262.1031 417.8485 2.0270 -4.0858 258.1989 262.2847 418.0368 2.2100 -4.0894 258.3514 262.4407 418.2319 2.3930 -4.0894 258.5043 262.5937 418.4264 2.5760 -4.0924 258.6404 262.7328 418.6246 2.7590 -4.0945 258.7885 262.8830 418.8224 3.0620 -4.0954 259.0244 263.1198 419.1342 3.2450 -4.0991 259.1636 263.2626 419.3242 3.4280 -4.1021 259.3179 263.4200 419.5045 3.6110 -4.1050 259.4669 263.5719 419.6861 3.7940 -4.1074 259.6305 263.7379 419.8792 3.9770 -4.1089 259.7648 263.8737 420.0675 4.1600 -4.1100 259.9198 264.0298 420.2665 4.4630 -4.1097 260.1988 264.3085 420.5697 4.6460 -4.1108 260.3442 264.4550 420.7533 4.8290 -4.1142 260.5020 264.6162 420.9424 5.0120 -4.1179 260.6420 264.7599 421.1286 5.1950 -4.1183 260.7853 264.9037 421.3154 5.3780 -4.1203 260.9437 265.0639 421.4898 5.6810 -4.1233 261.1876 265.3108 421.8084 5.8640 -4.1265 261.3442 265.4707 421.9900 6.0470 -4.1299 261.4942 265.6241 422.1782 6.2300 -4.1319 261.6492 265.7811 422.3717 6.4130 -4.1356 261.8000 265.9356 422.5512 6.5960 -4.1358 261.9495 266.0853 422.7380 6.7790 -4.1372 262.1113 266.2485 422.9293 7.0820 -4.1393 262.3752 266.5145 423.2452 7.2650 -4.1417 262.5169 266.6586 423.4458 7.4480 -4.1435 262.6647 266.8082 423.6335 7.6310 -4.1446 262.8269 266.9715 423.8136 7.8140 -4.1454 262.9889 267.1343 423.9874 7.9970 -4.1474 263.1408 267.2882 424.1670 8.1810 -4.1493 263.2993 267.4486 424.3500 8.4840 -4.1529 263.5625 267.7154 424.6700 8.6670 -4.1540 263.7242 267.8782 424.8652 8.8500 -4.1542 263.8779 268.0321 425.0519 9.0330 -4.1569 264.0222 268.1791 425.2513 9.2150 -4.1594 264.1736 268.3331 425.4344 9.3990 -4.1609 264.3249 268.4858 425.6002 9.7010 -4.1635 264.5959 268.7595 425.9050 9.8850 -4.1614 264.7591 268.9205 426.0938 10.0670 -4.1649 264.9314 269.0963 426.2921 10.2500 -4.1668 265.0789 269.2457 426.4686 10.4330 -4.1675 265.2398 269.4073 426.6653 10.6160 -4.1675 265.3942 269.5617 426.8540 10.7990 -4.1692 265.5454 269.7146 427.0377 11.1030 -4.1706 265.8131 269.9837 427.3415 11.2860 -4.1717 265.9769 270.1486 427.5313 11.4680 -4.1735 266.1402 270.3137 427.7280 11.6510 -4.1755 266.3099 270.4854 427.9102 11.8340 -4.1781 266.4724 270.6505 428.0900 12.0170 -4.1805 266.6331 270.8136 428.2663 12.2000 -4.1829 266.7850 270.9679 428.4426 12.5030 -4.1880 267.0477 271.2357 428.7473 12.6870 -4.1890 267.2086 271.3976 428.9426 12.8690 -4.1894 267.3713 271.5607 429.1443 13.0520 -4.1917 267.5335 271.7253 429.3230 13.2350 -4.1935 267.6780 271.8714 429.5203