DTA measure 1lassu Date: 2024115:1550 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1393.91 s Mass = 959.1 mg data_number = 1734 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2318 -1.4262 282.8472 284.2734 253.1594 2.0240 -1.4250 282.7620 284.1869 253.1460 2.8165 -1.4260 282.6606 284.0865 253.1253 3.6385 -1.4280 282.5691 283.9971 253.1245 4.4305 -1.4271 282.4829 283.9100 253.1402 5.2525 -1.4269 282.3913 283.8182 253.1156 6.0303 -1.4262 282.3184 283.7446 253.1200 6.8525 -1.4258 282.2338 283.6596 253.1214 7.6450 -1.4249 282.1342 283.5590 253.1269 8.4375 -1.4276 282.0436 283.4712 253.1359 9.2895 -1.4242 281.9510 283.3753 253.1630 10.0515 -1.4245 281.8705 283.2950 253.1779 10.8735 -1.4246 281.7806 283.2052 253.2029 11.6655 -1.4244 281.7070 283.1314 253.2259 12.4570 -1.4275 281.6346 283.0621 253.2608 13.3090 -1.4266 281.5460 282.9726 253.2853 14.0708 -1.4294 281.4580 282.8873 253.3370 14.8948 -1.4292 281.3739 282.8031 253.3887 15.6973 -1.4283 281.2828 282.7111 253.4257 16.5035 -1.4296 281.1903 282.6199 253.4788 17.2983 -1.4302 281.1101 282.5403 253.5484 18.0935 -1.4293 281.0257 282.4549 253.6102 18.9158 -1.4303 280.9430 282.3733 253.6842 19.7075 -1.4296 280.8840 282.3136 253.7395 20.5298 -1.4310 280.7887 282.2197 253.8311 21.3223 -1.4349 280.7151 282.1500 253.9047 22.1155 -1.4331 280.6334 282.0665 253.9708 22.9378 -1.4309 280.5476 281.9785 254.0670 23.7295 -1.4299 280.4633 281.8932 254.1483 24.5515 -1.4327 280.3794 281.8120 254.2162 25.3443 -1.4338 280.3136 281.7473 254.3306 26.1428 -1.4313 280.2257 281.6570 254.4231 26.9688 -1.4336 280.1472 281.5808 254.5479 27.7270 -1.4361 280.0766 281.5127 254.6271 28.5750 -1.4382 279.9927 281.4309 254.7483 29.3330 -1.4351 279.9258 281.3609 254.8372 30.1510 -1.4350 279.8485 281.2835 254.9410 30.9690 -1.4355 279.7813 281.2168 255.0512 31.7270 -1.4376 279.7017 281.1393 255.1565 32.5750 -1.4374 279.6213 281.0587 255.2687 33.3630 -1.4391 279.5498 280.9890 255.3676 34.1520 -1.4414 279.4616 280.9029 255.4775 34.9705 -1.4424 279.3864 280.8288 255.5945 35.7290 -1.4449 279.3351 280.7800 255.6956 36.5935 -1.4465 279.2703 280.7168 255.8190 37.3520 -1.4468 279.1860 280.6328 255.9024 38.1708 -1.4475 279.1249 280.5724 256.0197 38.9593 -1.4505 279.0399 280.4904 256.1162 39.7480 -1.4534 278.9953 280.4486 256.2139 40.5973 -1.4569 278.9064 280.3633 256.3244 41.3560 -1.4621 278.8400 280.3020 256.4303 42.1748 -1.4586 278.7876 280.2462 256.5429 42.9933 -1.4651 278.7275 280.1926 256.6434 43.7520 -1.4672 278.6628 280.1299 256.7210 44.6015 -1.4719 278.5669 280.0388 256.8372 45.3910 -1.4739 278.5056 279.9795 256.9387 46.1810 -1.4754 278.4427 279.9181 257.0391 46.9950 -1.4732 278.3835 279.8567 257.1409 47.7850 -1.4763 278.3253 279.8017 257.2384 48.6053 -1.4759 278.2550 279.7308 257.3467 49.3963 -1.4764 278.1885 279.6649 257.4270 50.2165 -1.4773 278.1368 279.6141 257.5378 51.0073 -1.4778 278.0901 279.5678 257.6371 51.7985 -1.4802 278.0132 279.4934 257.7350 52.6210 -1.4810 277.9625 279.4435 257.8287 53.4125 -1.4832 277.9113 279.3944 257.9128 54.2348 -1.4821 277.8478 279.3300 258.0310 55.0258 -1.4820 277.7930 279.2750 258.1207 55.8175 -1.4838 277.7406 279.2244 258.2072 56.6530 -1.4949 277.6822 279.1771 258.2999 57.4285 -1.4913 277.6316 279.1229 258.3917 58.2508 -1.4889 277.5593 279.0482 258.5013 59.0125 -1.4928 277.5116 279.0043 258.5866 59.8655 -1.5004 277.4632 278.9637 258.6915 60.6575 -1.4891 277.4134 278.9025 258.7866 61.4495 -1.4811 277.3633 278.8444 258.8818 62.2730 -1.4876 277.3105 278.7981 258.9963 63.0365 -1.4926 277.2527 278.7453 259.0860 63.8885 -1.4935 277.1848 278.6784 259.2159 64.6505 -1.4946 277.1523 278.6469 259.2851 65.4725 -1.4964 277.0977 278.5941 259.3758 66.2945 -1.4952 277.0466 278.5418 259.5040 67.0620 -1.4931 277.0038 278.4969 259.6087 67.8913 -1.4945 276.9502 278.4447 259.6965 68.6835 -1.4949 276.8980 278.3929 259.7881 69.5050 -1.4927 276.8602 278.3529 259.8922 70.2970 -1.4931 276.8173 278.3104 259.9839 71.0885 -1.4955 276.7725 278.2681 260.0923 71.9410 -1.4945 276.7328 278.2273 260.1948 72.7030 -1.4952 276.6814 278.1766 260.2771 73.5258 -1.4967 276.6389 278.1356 260.3658 74.3180 -1.4970 276.5980 278.0950 260.4882 75.1095 -1.4985 276.5644 278.0629 260.5815 75.9333 -1.4986 276.5156 278.0141 260.6540 76.7255 -1.4990 276.4627 277.9617 260.7511 77.5685 -1.4999 276.4265 277.9264 260.8713 78.3305 -1.5002 276.3815 277.8816 260.9517 79.1548 -1.4999 276.3558 277.8557 261.0571 79.9468 -1.5018 276.3109 277.8127 261.1526 80.7385 -1.5006 276.2695 277.7701 261.2386 81.5908 -1.5029 276.2325 277.7354 261.3382 82.3525 -1.5029 276.2010 277.7039 261.4178 83.1745 -1.5015 276.1753 277.6767 261.5283 83.9965 -1.5004 276.1267 277.6271 261.6385 84.7585 -1.4977 276.0862 277.5839 261.7296 85.6105 -1.5003 276.0596 277.5599 261.8315 86.3728 -1.5038 276.0329 277.5368 261.9261 87.1955 -1.5063 275.9960 277.5023 262.0461 88.0075 -1.5073 275.9701 277.4774 262.1384 88.7995 -1.5068 275.9455 277.4522 262.2466 89.6215 -1.5071 275.9028 277.4099 262.3304 90.4135 -1.5056 275.8602 277.3658 262.4503 91.2348 -1.5068 275.8372 277.3439 262.5755 92.0268 -1.5054 275.8186 277.3239 262.6751 92.8155 -1.5056 275.7771 277.2826 262.7740 93.6338 -1.5076 275.7457 277.2533 262.8915 94.3913 -1.5043 275.7270 277.2313 262.9727 95.2405 -1.5067 275.7029 277.2097 263.0858 96.0288 -1.5076 275.6787 277.1862 263.1870 96.8178 -1.5063 275.6384 277.1447 263.2901 97.6415 -1.5071 275.6105 277.1176 263.3921 98.4073 -1.5084 275.5941 277.1025 263.4630 99.2265 -1.5094 275.5788 277.0882 263.5630 100.0143 -1.5078 275.5597 277.0675 263.6723 100.8333 -1.5065 275.5321 277.0386 263.7725 101.6223 -1.5065 275.5349 277.0414 263.8704 102.4133 -1.5067 275.4979 277.0046 263.9660 103.2320 -1.5079 275.4759 276.9838 264.0657 104.0200 -1.5070 275.4397 276.9467 264.1542 104.8390 -1.5060 275.4393 276.9453 264.2536 105.6278 -1.5052 275.4287 276.9339 264.3463 106.4170 -1.5045 275.4136 276.9180 264.4467 107.2658 -1.5044 275.3810 276.8854 264.5496 108.0048 -1.5040 275.3597 276.8637 264.6283 108.8658 -1.5048 275.3366 276.8414 264.7140 109.6253 -1.5049 275.3094 276.8142 264.8090 110.4448 -1.5039 275.3054 276.8093 264.9172 111.2635 -1.5040 275.2929 276.7969 265.0398 112.0238 -1.5039 275.2741 276.7780 265.1244 112.8750 -1.5050 275.2490 276.7540 265.2275 113.6363 -1.5025 275.2514 276.7539 265.3128 114.4573 -1.5028 275.2404 276.7432 265.4199 115.2780 -1.5025 275.2348 276.7373 265.5303 116.0390 -1.5022 275.2143 276.7165 265.6402 116.8910 -1.5016 275.2095 276.7111 265.7437 117.6523 -1.4998 275.2024 276.7022 265.8487 118.4895 -1.5021 275.1960 276.6981 265.9641 119.2815 -1.5018 275.1949 276.6967 266.0733 120.0735 -1.5019 275.1891 276.6910 266.1782 120.8950 -1.4985 275.1758 276.6744 266.2830 121.6565 -1.4985 275.1712 276.6697 266.3757 122.5085 -1.4974 275.1465 276.6439 266.4948 123.2708 -1.4986 275.1349 276.6334 266.5957 124.0935 -1.4988 275.1327 276.6315 266.7067 124.9155 -1.4944 275.1306 276.6250 266.8057 125.6775 -1.4975 275.1113 276.6087 266.8990 126.5310 -1.4970 275.1258 276.6228 267.0225 127.2943 -1.4958 275.1294 276.6252 267.1021 128.1163 -1.4955 275.1200 276.6155 267.2209 128.9283 -1.4969 275.1247 276.6216 267.3228 129.7195 -1.4960 275.1134 276.6094 267.4240 130.5420 -1.4957 275.1043 276.6000 267.5225 131.3035 -1.4936 275.1152 276.6087 267.6035 132.1558 -1.4922 275.1213 276.6136 267.7195 132.9478 -1.4942 275.1098 276.6040 267.8132 133.7395 -1.4933 275.1025 276.5958 267.9136 134.5620 -1.4907 275.1108 276.6014 268.0158 135.3235 -1.4914 275.1018 276.5932 268.1107 136.1758 -1.4887 275.1104 276.5991 268.2020 136.9700 -1.4875 275.1154 276.6029 268.3167 137.7645 -1.4906 275.1185 276.6091 268.3977 138.5968 -1.4905 275.1160 276.6065 268.4862 139.3675 -1.4880 275.1139 276.6019 268.5861 140.1905 -1.4874 275.1250 276.6124 268.6974 140.9535 -1.4882 275.1301 276.6183 268.7832 141.8055 -1.4838 275.1445 276.6283 268.8660 142.5975 -1.4832 275.1507 276.6338 268.9666 143.3895 -1.4838 275.1633 276.6472 269.0590 144.2123 -1.4827 275.1665 276.6492 269.1640 144.9745 -1.4826 275.1706 276.6532 269.2404 145.8265 -1.4809 275.1734 276.6543 269.3634 146.6185 -1.4806 275.1834 276.6640 269.4516 147.4105 -1.4780 275.1974 276.6755 269.5579 148.2323 -1.4788 275.2061 276.6849 269.6750 149.0038 -1.4779 275.2122 276.6901 269.7697 149.8383 -1.4765 275.2184 276.6950 269.8765 150.6298 -1.4758 275.2416 276.7174 269.9738 151.4518 -1.4746 275.2615 276.7361 270.0846 152.2438 -1.4755 275.2618 276.7373 270.1928 153.0355 -1.4736 275.2908 276.7644 270.2907 153.8620 -1.4719 275.2884 276.7603 270.3922 154.6545 -1.4720 275.2999 276.7719 270.4945 155.4768 -1.4714 275.3231 276.7945 270.6111 156.2670 -1.4721 275.3402 276.8123 270.7209 157.0550 -1.4708 275.3581 276.8290 270.8351 157.8740 -1.4677 275.3673 276.8349 270.9342 158.6330 -1.4678 275.3896 276.8574 271.0458 159.4910 -1.4673 275.4054 276.8727 271.1499 160.2498 -1.4648 275.4083 276.8732 271.2435 161.0690 -1.4655 275.4290 276.8946 271.3531 161.8573 -1.4655 275.4423 276.9078 271.4434 162.6450 -1.4633 275.4786 276.9418 271.5429 163.4938 -1.4623 275.4979 276.9602 271.6704 164.2523 -1.4610 275.5098 276.9708 271.7771 165.0725 -1.4632 275.5194 276.9826 271.8940 165.8618 -1.4632 275.5354 276.9986 271.9834 166.6510 -1.4621 275.5612 277.0233 272.0858 167.4990 -1.4615 275.5938 277.0553 272.1894 168.2573 -1.4612 275.6124 277.0736 272.2828 169.0768 -1.4586 275.6336 277.0923 272.3920 169.8815 -1.4575 275.6619 277.1194 272.4873 170.6710 -1.4611 275.6836 277.1447 272.5825 171.4898 -1.4601 275.6938 277.1539 272.7016 172.2800 -1.4586 275.7186 277.1772 272.7894 173.0995 -1.4572 275.7562 277.2134 272.8842 173.8898 -1.4564 275.7815 277.2379 272.9869 174.6800 -1.4580 275.8045 277.2625 273.0829 175.5288 -1.4591 275.8366 277.2957 273.2011 176.2883 -1.4568 275.8608 277.3176 273.2977 177.1118 -1.4571 275.8820 277.3391 273.3937 177.9025 -1.4558 275.9184 277.3742 273.5026 178.6945 -1.4542 275.9388 277.3930 273.5858 179.5295 -1.4488 275.9709 277.4197 273.6839 180.3025 -1.4469 275.9875 277.4344 273.7908 181.1245 -1.4453 276.0062 277.4515 273.8773 181.9158 -1.4479 276.0320 277.4799 273.9817 182.7375 -1.4461 276.0711 277.5172 274.0812 183.5303 -1.4455 276.1012 277.5467 274.1724 184.3225 -1.4430 276.1423 277.5852 274.2678 185.1435 -1.4410 276.1750 277.6160 274.3711 185.9048 -1.4452 276.2103 277.6555 274.4602 186.7580 -1.4432 276.2527 277.6960 274.5715 187.5500 -1.4422 276.2735 277.7156 274.6658 188.3415 -1.4407 276.3066 277.7473 274.7641 189.1650 -1.4407 276.3349 277.7756 274.8673 189.9328 -1.4392 276.3656 277.8048 274.9802 190.7898 -1.4368 276.4114 277.8482 275.0879 191.5515 -1.4367 276.4383 277.8750 275.1874 192.3738 -1.4371 276.4807 277.9179 275.2871 193.1660 -1.4369 276.5078 277.9447 275.3962 193.9575 -1.4382 276.5473 277.9855 275.4961 194.8098 -1.4360 276.5715 278.0075 275.6268 195.5715 -1.4336 276.6178 278.0515 275.7246 196.3958 -1.4323 276.6526 278.0848 275.8272 197.1875 -1.4331 276.6850 278.1181 275.9372 197.9795 -1.4332 276.7307 278.1639 276.0488 198.8318 -1.4355 276.7727 278.2082 276.1671 199.5935 -1.4339 276.8049 278.2388 276.2535 200.4363 -1.4321 276.8431 278.2751 276.3627 201.1985 -1.4307 276.8841 278.3148 276.4729 202.0205 -1.4267 276.9090 278.3357 276.5773 202.8425 -1.4250 276.9612 278.3861 276.6848 203.6045 -1.4264 277.0091 278.4355 276.7770 204.4565 -1.4267 277.0441 278.4707 276.8860 205.2185 -1.4254 277.0818 278.5072 276.9933 206.0405 -1.4229 277.1426 278.5655 277.1133 206.8623 -1.4236 277.1729 278.5965 277.2180 207.6238 -1.4214 277.2073 278.6288 277.3114 208.4775 -1.4220 277.2316 278.6537 277.4264 209.2395 -1.4222 277.2987 278.7208 277.5108 210.0618 -1.4205 277.3435 278.7640 277.6288 210.8733 -1.4184 277.3939 278.8122 277.7465 211.6645 -1.4194 277.4343 278.8537 277.8406 212.4885 -1.4166 277.4721 278.8886 277.9434 213.2515 -1.4150 277.5089 278.9239 278.0438 214.1038 -1.4146 277.5514 278.9660 278.1505 214.8958 -1.4143 277.5889 279.0031 278.2668 215.6875 -1.4142 277.6323 279.0465 278.3617 216.5105 -1.4134 277.6919 279.1053 278.4670 217.2735 -1.4133 277.7375 279.1507 278.5516 218.1255 -1.4149 277.7949 279.2098 278.6728 218.9175 -1.4119 277.8413 279.2532 278.7673 219.7093 -1.4096 277.8794 279.2890 278.8763 220.5375 -1.4093 277.9363 279.3456 278.9906 221.3060 -1.4090 277.9729 279.3819 279.0832 222.1243 -1.4061 278.0308 279.4370 279.1828 222.9120 -1.4070 278.0846 279.4916 279.2719 223.7300 -1.4086 278.1368 279.5454 279.3874 224.5185 -1.4065 278.1886 279.5951 279.4813 225.3070 -1.4070 278.2314 279.6385 279.5831 226.1255 -1.4078 278.2862 279.6940 279.6854 226.9140 -1.4048 278.3337 279.7385 279.7821 227.7320 -1.4040 278.3867 279.7907 279.8867 228.5203 -1.4058 278.4488 279.8546 279.9775 229.3090 -1.4041 278.4927 279.8968 280.0691 230.1273 -1.4037 278.5413 279.9449 280.1570 230.8920 -1.4034 278.5977 280.0011 280.2374 231.7480 -1.4023 278.6524 280.0547 280.3422 232.5360 -1.3993 278.7057 280.1050 280.4483 233.3250 -1.3996 278.7497 280.1493 280.5453 234.1438 -1.3999 278.8013 280.2012 280.6269 234.9030 -1.4003 278.8545 280.2548 280.7254 235.7525 -1.3985 278.9194 280.3179 280.8244 236.5430 -1.3983 278.9637 280.3620 280.9362 237.3348 -1.3991 279.0215 280.4207 281.0234 238.1535 -1.3971 279.0694 280.4666 281.1244 238.9430 -1.3959 279.1231 280.5189 281.2318 239.7625 -1.3959 279.1859 280.5818 281.3430 240.5520 -1.3954 279.2456 280.6409 281.4509 241.3410 -1.3934 279.3108 280.7042 281.5496 242.1900 -1.3982 279.3596 280.7578 281.6744 242.9498 -1.3926 279.4070 280.7996 281.7762 243.7728 -1.3898 279.4847 280.8745 281.8835 244.5643 -1.3872 279.5421 280.9293 281.9847 245.3558 -1.3847 279.5951 280.9799 282.0922 246.2078 -1.3862 279.6464 281.0326 282.2197 246.9698 -1.3859 279.7144 281.1003 282.3152 247.7918 -1.3832 279.7755 281.1587 282.4184 248.5838 -1.3830 279.8251 281.2081 282.5395 249.3755 -1.3835 279.8751 281.2586 282.6577 250.1988 -1.3837 279.9507 281.3344 282.7685 250.9905 -1.3826 280.0075 281.3901 282.8757 251.8128 -1.3813 280.0698 281.4511 282.9842 252.6048 -1.3806 280.1227 281.5033 283.0910 253.3965 -1.3805 280.1935 281.5740 283.1995 254.2195 -1.3815 280.2575 281.6390 283.3030 254.9825 -1.3811 280.3127 281.6938 283.4127 255.8345 -1.3784 280.3707 281.7491 283.5255 256.5965 -1.3798 280.4362 281.8159 283.6341 257.4185 -1.3799 280.5092 281.8891 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