DTA measure 3gyors Date: 2024115:1525 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1305.41 s Mass = 959.1 mg data_number = 1625 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1980 -4.4758 436.7244 441.2001 424.3380 2.0218 -4.4786 436.7893 441.2679 424.3571 2.8135 -4.4820 436.8115 441.2935 424.3732 3.6055 -4.4871 436.8512 441.3384 424.3745 4.4575 -4.4909 436.9048 441.3958 424.3740 5.2195 -4.4936 436.9648 441.4584 424.3831 6.0425 -4.5002 437.0153 441.5156 424.3694 6.8345 -4.5041 437.0457 441.5498 424.3623 7.6265 -4.5088 437.0866 441.5955 424.3375 8.4785 -4.5132 437.1428 441.6560 424.3211 9.2405 -4.5158 437.1932 441.7090 424.2863 10.0750 -4.5207 437.2350 441.7557 424.2443 10.8485 -4.5257 437.2582 441.7838 424.1996 11.6678 -4.5317 437.3022 441.8339 424.1483 12.4558 -4.5331 437.3553 441.8884 424.0936 13.2450 -4.5340 437.3879 441.9219 424.0321 14.0630 -4.5384 437.4271 441.9655 423.9428 14.8508 -4.5421 437.4661 442.0081 423.8656 15.6698 -4.5470 437.5066 442.0537 423.7696 16.4578 -4.5492 437.5474 442.0965 423.6883 17.2453 -4.5527 437.5788 442.1315 423.5785 18.0635 -4.5537 437.6303 442.1841 423.4899 18.8520 -4.5556 437.6740 442.2296 423.3869 19.6698 -4.5558 437.6984 442.2542 423.2759 20.4333 -4.5609 437.7479 442.3088 423.1803 21.2580 -4.5642 437.7835 442.3477 423.0602 22.0768 -4.5654 437.8082 442.3737 422.9502 22.8355 -4.5695 437.8280 442.3975 422.8361 23.6843 -4.5738 437.8660 442.4398 422.7105 24.4443 -4.5780 437.8877 442.4657 422.5992 25.2643 -4.5795 437.9224 442.5019 422.5039 26.0825 -4.5814 437.9725 442.5539 422.3792 26.8410 -4.5846 437.9956 442.5802 422.2885 27.6908 -4.5865 438.0255 442.6120 422.1638 28.4793 -4.5882 438.0591 442.6473 422.0562 29.2680 -4.5890 438.0726 442.6616 421.9385 30.0870 -4.5937 438.1008 442.6945 421.8306 30.8658 -4.5958 438.1293 442.7251 421.7111 31.6913 -4.5970 438.1602 442.7572 421.5983 32.4810 -4.5971 438.1899 442.7871 421.4974 33.3018 -4.6007 438.2097 442.8104 421.3741 34.0930 -4.6066 438.2187 442.8253 421.2810 34.8843 -4.6088 438.2543 442.8631 421.1812 35.7058 -4.6144 438.2896 442.9040 421.0522 36.4675 -4.6225 438.3056 442.9281 420.9458 37.3208 -4.6193 438.3260 442.9454 420.8276 38.1125 -4.6118 438.3440 442.9558 420.7478 38.9045 -4.6108 438.3607 442.9714 420.6451 39.7275 -4.6136 438.3698 442.9834 420.5141 40.4895 -4.6162 438.3893 443.0055 420.4122 41.3328 -4.6207 438.4166 443.0373 420.3033 42.0955 -4.6243 438.4334 443.0577 420.2001 42.9475 -4.6252 438.4465 443.0718 420.0805 43.7395 -4.6270 438.4550 443.0820 419.9950 44.5315 -4.6287 438.4734 443.1021 419.8984 45.3540 -4.6292 438.4986 443.1278 419.7929 46.1165 -4.6315 438.5177 443.1492 419.6781 46.9685 -4.6353 438.5132 443.1485 419.5830 47.7605 -4.6353 438.5288 443.1641 419.4922 48.5520 -4.6361 438.5334 443.1694 419.3867 49.3750 -4.6384 438.5439 443.1823 419.2879 50.1375 -4.6390 438.5495 443.1885 419.1936 50.9980 -4.6411 438.5552 443.1963 419.0903 51.7685 -4.6410 438.5678 443.2088 418.9932 52.5908 -4.6424 438.5735 443.2159 418.8979 53.3833 -4.6441 438.5745 443.2187 418.7999 54.1765 -4.6445 438.5801 443.2246 418.7098 54.9988 -4.6489 438.5826 443.2315 418.6146 55.7905 -4.6525 438.5980 443.2506 418.5213 56.6130 -4.6495 438.6051 443.2546 418.4340 57.4065 -4.6436 438.6066 443.2502 418.3437 58.2005 -4.6407 438.6153 443.2561 418.2421 59.0228 -4.6410 438.6159 443.2569 418.1511 59.7845 -4.6544 438.6138 443.2682 418.0743 60.6365 -4.6558 438.6054 443.2612 417.9880 61.4058 -4.6606 438.6044 443.2650 417.8885 62.2355 -4.6628 438.6032 443.2659 417.7959 63.0275 -4.6655 438.6161 443.2817 417.7064 63.8195 -4.6686 438.6056 443.2742 417.6048 64.6715 -4.6708 438.5961 443.2670 417.5216 65.4335 -4.6753 438.5999 443.2753 417.4322 66.2555 -4.6759 438.5900 443.2659 417.3380 67.0480 -4.6751 438.5821 443.2572 417.2351 67.8405 -4.6777 438.5915 443.2692 417.1238 68.6925 -4.6809 438.5952 443.2761 417.0107 69.4545 -4.6829 438.5903 443.2732 416.9115 70.2760 -4.6785 438.5717 443.2501 416.7985 71.0995 -4.6799 438.5592 443.2391 416.7063 71.8840 -4.6859 438.5460 443.2319 416.6011 72.7063 -4.6883 438.5349 443.2232 416.4979 73.4685 -4.6912 438.5228 443.2140 416.4166 74.3213 -4.6928 438.5173 443.2101 416.2920 75.0828 -4.6964 438.4940 443.1904 416.2062 75.8988 -4.6963 438.4827 443.1791 416.0989 76.7160 -4.7051 438.4751 443.1802 415.9982 77.4733 -4.7185 438.4700 443.1885 415.9049 78.3228 -4.7264 438.4559 443.1823 415.8070 79.0810 -4.7273 438.4557 443.1831 415.7173 79.8993 -4.7253 438.4321 443.1574 415.6074 80.6873 -4.7228 438.4147 443.1374 415.5139 81.4763 -4.7167 438.4157 443.1324 415.4318 82.3070 -4.7135 438.3811 443.0946 415.3170 83.0660 -4.7071 438.3623 443.0694 415.2375 83.9140 -4.7035 438.3527 443.0562 415.1310 84.7023 -4.7094 438.3379 443.0472 415.0392 85.4910 -4.7186 438.3196 443.0382 414.9418 86.3090 -4.7234 438.2947 443.0182 414.8513 87.0970 -4.7244 438.2848 443.0091 414.7560 87.9160 -4.7249 438.2615 442.9864 414.6534 88.7040 -4.7265 438.2419 442.9683 414.5609 89.4938 -4.7281 438.2240 442.9521 414.4364 90.3428 -4.7274 438.1888 442.9162 414.3347 91.1010 -4.7280 438.1748 442.9027 414.2356 91.9323 -4.7313 438.1395 442.8708 414.1244 92.7030 -4.7333 438.1265 442.8598 414.0280 93.5223 -4.7324 438.1042 442.8366 413.9219 94.3423 -4.7333 438.0789 442.8123 413.8285 95.1020 -4.7319 438.0418 442.7736 413.7164 95.9523 -4.7290 438.0216 442.7506 413.5983 96.7428 -4.7261 438.0048 442.7309 413.5064 97.5328 -4.7266 437.9824 442.7090 413.4151 98.3525 -4.7309 437.9489 442.6798 413.3230 99.1130 -4.7325 437.9184 442.6509 413.2273 99.9665 -4.7349 437.8835 442.6184 413.1210 100.7288 -4.7348 437.8474 442.5822 413.0248 101.5520 -4.7332 437.8211 442.5542 412.9150 102.3743 -4.7365 437.8107 442.5472 412.8329 103.1343 -4.7375 437.7756 442.5131 412.7373 103.9855 -4.7352 437.7335 442.4686 412.6282 104.7470 -4.7323 437.7210 442.4533 412.5357 105.5683 -4.7366 437.6956 442.4323 412.4205 106.3905 -4.7403 437.6531 442.3934 412.3409 107.1818 -4.7400 437.6245 442.3645 412.2516 108.0038 -4.7370 437.5829 442.3199 412.1320 108.7975 -4.7357 437.5329 442.2686 412.0393 109.5895 -4.7375 437.5147 442.2522 411.9450 110.4128 -4.7373 437.4813 442.2187 411.8585 111.2045 -4.7380 437.4401 442.1781 411.7497 112.0268 -4.7381 437.4125 442.1505 411.6581 112.8185 -4.7398 437.3685 442.1083 411.5660 113.6105 -4.7454 437.3216 442.0669 411.4778 114.4328 -4.7481 437.3052 442.0532 411.3758 115.2245 -4.7519 437.2672 442.0191 411.2616 116.0468 -4.7516 437.2315 441.9832 411.1583 116.8408 -4.7486 437.1910 441.9395 411.0578 117.6335 -4.7505 437.1365 441.8870 410.9606 118.4555 -4.7473 437.1124 441.8598 410.8534 119.2475 -4.7495 437.0752 441.8247 410.7372 120.0695 -4.7539 437.0382 441.7921 410.6266 120.8615 -4.7591 436.9954 441.7545 410.5275 121.6535 -4.7616 436.9499 441.7115 410.4089 122.4768 -4.7601 436.8973 441.6573 410.3040 123.2445 -4.7606 436.8540 441.6146 410.1996 124.0965 -4.7602 436.8079 441.5682 410.0926 124.8885 -4.7640 436.7784 441.5424 409.9908 125.6805 -4.7645 436.7282 441.4927 409.8968 126.5025 -4.7648 436.6927 441.4575 409.7757 127.2640 -4.7636 436.6596 441.4232 409.6792 128.1178 -4.7570 436.6007 441.3576 409.5603 128.9100 -4.7550 436.5585 441.3136 409.4498 129.7015 -4.7562 436.5215 441.2777 409.3590 130.5283 -4.7526 436.4741 441.2266 409.2469 131.2895 -4.7548 436.4243 441.1791 409.1546 132.1418 -4.7611 436.3653 441.1264 409.0352 132.9343 -4.7633 436.3345 441.0977 408.9403 133.7255 -4.7627 436.2836 441.0463 408.8316 134.5493 -4.7640 436.2416 441.0056 408.7261 135.3115 -4.7619 436.2016 440.9635 408.6285 136.1650 -4.7585 436.1461 440.9046 408.5242 136.9340 -4.7555 436.0922 440.8477 408.4196 137.7558 -4.7607 436.0274 440.7881 408.3191 138.5513 -4.7610 435.9813 440.7423 408.1960 139.3400 -4.7606 435.9343 440.6949 408.1180 140.1853 -4.7565 435.8757 440.6322 408.0018 140.9435 -4.7538 435.8478 440.6016 407.9056 141.7608 -4.7569 435.7952 440.5521 407.8014 142.5478 -4.7607 435.7419 440.5026 407.7193 143.3353 -4.7617 435.6876 440.4494 407.6135 144.1548 -4.7618 435.6181 440.3799 407.5197 144.9430 -4.7636 435.5781 440.3417 407.4159 145.7610 -4.7656 435.5160 440.2816 407.3288 146.5490 -4.7649 435.4608 440.2257 407.2416 147.3370 -4.7641 435.4193 440.1834 407.1363 148.1855 -4.7654 435.3640 440.1294 407.0387 148.9443 -4.7658 435.3178 440.0835 406.9469 149.7640 -4.7655 435.2776 440.0430 406.8403 150.5520 -4.7608 435.1977 439.9585 406.7416 151.3400 -4.7535 435.1490 439.9025 406.6547 152.1880 -4.7550 435.0935 439.8485 406.5413 152.9460 -4.7562 435.0372 439.7934 406.4647 153.7640 -4.7558 434.9823 439.7382 406.3684 154.5820 -4.7564 434.9170 439.6734 406.2677 155.3400 -4.7579 434.8735 439.6314 406.1824 156.1893 -4.7598 434.8220 439.5817 406.0765 156.9780 -4.7595 434.7551 439.5147 405.9925 157.7675 -4.7600 434.6957 439.4557 405.9034 158.5878 -4.7601 434.6347 439.3949 405.7898 159.3495 -4.7608 434.5891 439.3499 405.6915 160.1993 -4.7582 434.5249 439.2831 405.5849 160.9883 -4.7625 434.4640 439.2265 405.4722 161.7793 -4.7651 434.4099 439.1750 405.3605 162.6020 -4.7610 434.3516 439.1127 405.2676 163.3635 -4.7614 434.2825 439.0439 405.1745 164.2088 -4.7617 434.2188 438.9805 405.0552 164.9695 -4.7618 434.1716 438.9334 404.9495 165.8220 -4.7586 434.1036 438.8622 404.8438 166.5838 -4.7578 434.0421 438.7998 404.7414 167.4058 -4.7580 433.9814 438.7394 404.6420 168.1998 -4.7563 433.9180 438.6742 404.5288 168.9925 -4.7563 433.8622 438.6186 404.4283 169.8450 -4.7549 433.7929 438.5478 404.3199 170.6068 -4.7544 433.7281 438.4825 404.2261 171.4288 -4.7536 433.6682 438.4218 404.1287 172.2208 -4.7524 433.6049 438.3572 404.0343 173.0125 -4.7525 433.5455 438.2980 403.9223 173.8408 -4.7531 433.4804 438.2335 403.8228 174.6075 -4.7520 433.4088 438.1608 403.7375 175.4598 -4.7522 433.3465 438.0987 403.6202 176.2218 -4.7526 433.2735 438.0262 403.5046 177.0448 -4.7522 433.2163 437.9685 403.4028 177.8665 -4.7523 433.1499 437.9022 403.3179 178.6285 -4.7509 433.1000 437.8509 403.2115 179.4825 -4.7489 433.0322 437.7811 403.0998 180.2458 -4.7468 432.9730 437.7197 403.0045 181.0695 -4.7457 432.8952 437.6409 402.9224 181.8615 -4.7460 432.8293 437.5753 402.8146 182.6535 -4.7452 432.7635 437.5087 402.7111 183.4770 -4.7426 432.6962 437.4388 402.6026 184.2445 -4.7410 432.6321 437.3731 402.5157 185.1025 -4.7420 432.5705 437.3124 402.4139 185.8940 -4.7427 432.5091 437.2518 402.3284 186.6855 -4.7409 432.4244 437.1653 402.2262 187.5080 -4.7396 432.3435 437.0831 402.1398 188.2695 -4.7396 432.2891 437.0287 402.0556 189.1218 -4.7393 432.2165 436.9558 401.9339 189.9138 -4.7366 432.1409 436.8775 401.8249 190.7055 -4.7359 432.0817 436.8176 401.7415 191.5285 -4.7357 432.0141 436.7498 401.6370 192.2905 -4.7350 431.9424 436.6774 401.5311 193.1428 -4.7326 431.8667 436.5993 401.4242 193.9348 -4.7307 431.7978 436.5286 401.3112 194.7515 -4.7281 431.7270 436.4551 401.1887 195.5140 -4.7306 431.6621 436.3926 401.0768 196.3375 -4.7285 431.5872 436.3157 400.9833 197.1598 -4.7258 431.5079 436.2338 400.8754 197.9215 -4.7272 431.4548 436.1820 400.7723 198.7735 -4.7233 431.3719 436.0952 400.6733 199.5358 -4.7242 431.3126 436.0368 400.5759 200.3585 -4.7246 431.2396 435.9642 400.4695 201.1805 -4.7239 431.1585 435.8824 400.3385 201.9425 -4.7219 431.0806 435.8025 400.2351 202.7945 -4.7189 430.9991 435.7180 400.1413 203.5865 -4.7158 430.9399 435.6557 400.0388 204.3758 -4.7131 430.8748 435.5879 399.9339 205.1830 -4.7145 430.7777 435.4922 399.8238 205.9715 -4.7137 430.7186 435.4323 399.7224 206.7900 -4.7130 430.6606 435.3736 399.6135 207.5480 -4.7177 430.5783 435.2960 399.5116 208.3980 -4.7149 430.4913 435.2062 399.3922 209.1858 -4.7127 430.4150 435.1278 399.2878 209.9735 -4.7112 430.3635 435.0747 399.1865 210.7923 -4.7070 430.2822 434.9892 399.0719 211.5810 -4.7071 430.2137 434.9208 398.9898 212.3995 -4.7000 430.1306 434.8305 398.8824 213.1878 -4.6996 430.0502 434.7497 398.7715 213.9770 -4.6990 429.9644 434.6634 398.6608 214.8023 -4.6950 429.8828 434.5778 398.5576 215.5678 -4.6960 429.8228 434.5188 398.4514 216.4163 -4.6968 429.7398 434.4366 398.3343 217.2045 -4.6945 429.6532 434.3477 398.2416 217.9930 -4.6941 429.5795 434.2736 398.1604 218.8118 -4.6936 429.5059 434.1995 398.0497 219.6015 -4.6911 429.4287 434.1198 397.9546 220.4200 -4.6906 429.3561 434.0467 397.8532 221.2090 -4.6891 429.2787 433.9679 397.7466 221.9998 -4.6905 429.1945 433.8850 397.6555 222.8215 -4.6882 429.1261 433.8143 397.5524 223.6118 -4.6876 429.0597 433.7473 397.4487 224.4310 -4.6847 428.9694 433.6541 397.3460 225.2025 -4.6831 428.8911 433.5742 397.2509 226.0378 -4.6796 428.8204 433.4999 397.1437 226.8280 -4.6789 428.7501 433.4290 397.0540 227.6183 -4.6781 428.6681 433.3462 396.9571 228.4695 -4.6771 428.5743 433.2513 396.8527 229.2318 -4.6756 428.4995 433.1751 396.7610 230.0548 -4.6752 428.4310 433.1062 396.6767 230.8468 -4.6737 428.3400 433.0137 396.5740 231.6385 -4.6730 428.2580 432.9310 396.4727 232.4620 -4.6724 428.1719 432.8442 396.3716 233.2545 -4.6696 428.0983 432.7679 396.2909 234.0768 -4.6698 428.0188 432.6886 396.1919 234.8690 -4.6668 427.9435 432.6103 396.0793 235.6775 -4.6672 427.8550 432.5222 395.9791 236.4695 -4.6636 427.7785 432.4421 395.8721 237.2615 -4.6608 427.7092 432.3700 395.7718 238.1135 -4.6569 427.6290 432.2859 395.6699 238.8755 -4.6556 427.5554 432.2110 395.5870 239.6988 -4.6547 427.4647 432.1194 395.4706 240.4905 -4.6560 427.3775 432.0335 395.3682 241.2825 -4.6560 427.3026 431.9586 395.2631 242.1345 -4.6531 427.2132 431.8662 395.1604 242.8963 -4.6550 427.1414 431.7964 395.0627 243.7188 -4.6571 427.0663 431.7234 394.9503 244.5110 -4.6507 426.9809 431.6316 394.8372 245.3025 -4.6484 426.8972 431.5456 394.7335 246.1398 -4.6463 426.8020 431.4483 394.6224 246.9015 -4.6415 426.7319 431.3734 394.5412 247.7553 -4.6445 426.6557 431.3002 394.4198 248.5175 -4.6438 426.5711 431.2149 394.3102 249.3398 -4.6431 426.4819 431.1250 394.2023 250.1618 -4.6422 426.3994 431.0416 394.1033 250.9235 -4.6388 426.3072 430.9460 394.0052 251.7758 -4.6368 426.2174 430.8542 393.8892 252.5378 -4.6338 426.1410 430.7748 393.7910 253.3608 -4.6311 426.0553 430.6863 393.6799 254.1828 -4.6275 425.9797 430.6072 393.5643 254.9445 -4.6277 425.8917 430.5194 393.4719 255.8070 -4.6249 425.8143 430.4393 393.3696 256.5505 -4.6225 425.7388 430.3613 393.2617 257.4025 -4.6224 425.6314 430.2538 393.1487 258.1945 -4.6220 425.5616 430.1836 393.0596 258.9865 -4.6187 425.4775 430.0963 392.9456 259.8085 -4.6198 425.3922 430.0119 392.8268 260.6005 -4.6196 425.2988 429.9184 392.7358 261.4225 -4.6153 425.2130 429.8283 392.6491 262.2148 -4.6148 425.1302 429.7450 392.5287 263.0075 -4.6140 425.0551 429.6691 392.4301 263.8293 -4.6124 424.9641 429.5765 392.3268 264.6208 -4.6118 424.8798 429.4916 392.2228 265.4428 -4.6100 424.7833 429.3933 392.1139 266.2163 -4.6086 424.7107 429.3193 392.0180 267.0528 -4.6062 424.6204 429.2266 391.9171 267.8445 -4.6050 424.5310 429.1359 391.8211 268.6333 -4.6055 424.4465 429.0519 391.7117 269.4530 -4.6025 424.3543 428.9569 391.6038 270.2410 -4.6005 424.2723 428.8728 391.4958 271.0595 -4.5992 424.1880 428.7872 391.4112 271.8475 -4.5951 424.0972 428.6923 391.3164 272.6370 -4.5898 424.0187 428.6085 391.2018 273.4560 -4.5727 423.9282 428.5009 391.0943 274.2440 -4.5810 423.8454 428.4264 390.9820 275.0620 -4.5838 423.7497 428.3335 390.8873 275.8508 -4.5767 423.6751 428.2518 390.8001 276.6508 -4.5701 423.5844 428.1545 390.6939 277.4703 -4.5620 423.4952 428.0572 390.5973 278.2290 -4.5688 423.4140 427.9828 390.4920 279.0770 -4.5732 423.3234 427.8966 390.3910 279.8653 -4.5733 423.2252 427.7984 390.3004 280.6540 -4.5717 423.1470 427.7186 390.1958 281.4725 -4.5734 423.0501 427.6235 390.0789 282.2610 -4.5696 422.9681 427.5377 389.9859 283.0803 -4.5646 422.8643 427.4289 389.8907 283.8695 -4.5619 422.7845 427.3463 389.7926 284.6590 -4.5610 422.6925 427.2535 389.6918 285.5075 -4.5598 422.6131 427.1729 389.5746 286.2670 -4.5596 422.5337 427.0933 389.4821 287.0863 -4.5567 422.4312 426.9880 389.3703 287.9053 -4.5539 422.3396 426.8934 389.2834 288.6648 -4.5524 422.2653 426.8176 389.1734 289.5163 -4.5500 422.1782 426.7283 389.0545 290.2775 -4.5497 422.0827 426.6324 388.9503 291.0985 -4.5473 421.9959 426.5431 388.8331 291.9200 -4.5456 421.9082 426.4539 388.7348 292.6813 -4.5413 421.8248 426.3661 388.6379 293.5328 -4.5408 421.7339 426.2747 388.5259 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