DTA measure 1pb_updown3 Date: 2025319:99 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.11 s Mass = 937.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2930 0.1218 203.3802 203.2584 260.6135 2.0810 0.1417 203.6277 203.4860 260.6145 2.8690 0.1490 203.8804 203.7314 260.6025 3.6878 0.1565 204.1427 203.9862 260.6248 4.4470 0.1600 204.3678 204.2078 260.6406 5.2965 0.1645 204.6457 204.4812 260.6423 6.0850 0.1667 204.8940 204.7273 260.6734 6.8740 0.1670 205.1171 204.9501 260.6870 7.6925 0.1668 205.3603 205.1935 260.7359 8.4520 0.1688 205.6067 205.4378 260.7927 9.3015 0.1739 205.8803 205.7063 260.8234 10.0905 0.1771 206.1167 205.9396 260.8625 10.8808 0.1791 206.3456 206.1665 260.9439 11.6993 0.1799 206.5740 206.3941 261.0162 12.4590 0.1801 206.8118 206.6316 261.0857 13.3105 0.1910 207.0778 206.8869 261.1714 14.1008 0.1927 207.3017 207.1090 261.2635 14.8923 0.1941 207.5495 207.3554 261.3667 15.7135 0.1924 207.8109 207.6185 261.4466 16.4750 0.1975 208.0530 207.8555 261.5568 17.3265 0.1945 208.2969 208.1024 261.6709 18.0885 0.1963 208.5206 208.3242 261.7906 18.9110 0.2007 208.7595 208.5587 261.9244 19.7335 0.2035 209.0030 208.7995 262.0485 20.4955 0.2037 209.2165 209.0128 262.1677 21.3475 0.2050 209.4825 209.2775 262.3211 22.1095 0.2038 209.7327 209.5289 262.4859 22.9315 0.2058 209.9633 209.7575 262.6463 23.7235 0.2039 210.1742 209.9703 262.8032 24.5155 0.2044 210.3967 210.1924 262.9509 25.3675 0.2059 210.6451 210.4392 263.1127 26.1295 0.2069 210.8711 210.6642 263.2846 26.9515 0.2087 211.1235 210.9147 263.4628 27.7435 0.2067 211.3506 211.1439 263.6332 28.5353 0.2085 211.5731 211.3646 263.8027 29.3873 0.2122 211.8169 211.6047 263.9831 30.1493 0.2111 212.0428 211.8316 264.1572 30.9708 0.2102 212.2955 212.0853 264.3743 31.7635 0.2123 212.5019 212.2897 264.5417 32.5545 0.2096 212.7363 212.5267 264.7302 33.4073 0.2104 212.9885 212.7781 264.9200 34.1688 0.2117 213.1985 212.9868 265.0946 34.9908 0.2105 213.4343 213.2238 265.3039 35.7830 0.2134 213.6627 213.4493 265.4881 36.5745 0.2150 213.8947 213.6798 265.6729 37.4270 0.2088 214.1334 213.9245 265.8677 38.1888 0.2048 214.3318 214.1270 266.0400 39.0108 0.1980 214.5651 214.3671 266.2333 39.8030 0.1966 214.8012 214.6045 266.4476 40.5945 0.1966 215.0273 214.8307 266.6042 41.4468 0.1992 215.2730 215.0738 266.7930 42.2088 0.1902 215.4755 215.2852 266.9652 43.0308 0.1871 215.7058 215.5188 267.1584 43.8530 0.1912 215.9548 215.7636 267.3372 44.6223 0.1962 216.1764 215.9802 267.5050 45.4458 0.2076 216.4100 216.2024 267.6709 46.2375 0.2106 216.6009 216.3903 267.8423 47.0605 0.2145 216.8412 216.6267 268.0071 47.8528 0.2109 217.0542 216.8433 268.1688 48.6445 0.2082 217.2770 217.0688 268.3169 49.4965 0.2022 217.5090 217.3068 268.4870 50.2585 0.1990 217.7258 217.5267 268.6187 51.0805 0.1934 217.9702 217.7768 268.7833 51.8725 0.1904 218.1752 217.9849 268.9403 52.6645 0.1915 218.4101 218.2186 269.0875 53.5165 0.1865 218.6393 218.4527 269.2437 54.2785 0.1831 218.8434 218.6602 269.3667 55.1005 0.1817 219.0624 218.8807 269.5328 55.9225 0.1778 219.2810 219.1032 269.6892 56.6845 0.1743 219.4965 219.3222 269.8073 57.5365 0.1693 219.7396 219.5702 269.9362 58.3285 0.1688 219.9497 219.7809 270.0435 59.1215 0.1658 220.1593 219.9935 270.1581 59.9435 0.1692 220.3713 220.2021 270.3119 60.7050 0.1652 220.5710 220.4058 270.4176 61.5535 0.1646 220.8042 220.6396 270.5558 62.3113 0.1636 221.0053 220.8417 270.6429 63.1298 0.1638 221.2213 221.0575 270.7623 63.9460 0.1625 221.4476 221.2851 270.8811 64.7050 0.1622 221.6759 221.5137 270.9966 65.5538 0.1627 221.9179 221.7552 271.1171 66.3415 0.1594 222.1060 221.9466 271.2168 67.1293 0.1605 222.3340 222.1735 271.3294 67.9475 0.1495 222.5476 222.3981 271.4278 68.7058 0.1448 222.7346 222.5898 271.5371 69.5535 0.1417 222.9792 222.8375 271.6261 70.3415 0.1394 223.1795 223.0401 271.7523 71.1305 0.1390 223.3824 223.2434 271.8635 71.9493 0.1410 223.6121 223.4711 271.9893 72.7378 0.1557 223.8307 223.6749 272.0745 73.5560 0.1636 224.0420 223.8785 272.1939 74.3450 0.1624 224.2321 224.0697 272.3023 75.1420 0.1603 224.4371 224.2767 272.4097 75.9708 0.1613 224.6435 224.4823 272.5182 76.7300 0.1577 224.8597 224.7020 272.6201 77.5808 0.1558 225.0952 224.9393 272.7454 78.3700 0.1520 225.3037 225.1517 272.8678 79.1608 0.1525 225.5027 225.3502 272.9440 79.9823 0.1518 225.7182 225.5664 273.0792 80.7435 0.1512 225.8949 225.7436 273.1739 81.5960 0.1493 226.1159 225.9666 273.2900 82.3578 0.1475 226.3345 226.1870 273.4033 83.1798 0.1467 226.5378 226.3911 273.5419 84.0020 0.1459 226.7514 226.6055 273.6430 84.7635 0.1446 226.9353 226.7908 273.7683 85.6160 0.1440 227.1487 227.0048 273.8976 86.3778 0.1437 227.3501 227.2064 274.0296 87.1998 0.1395 227.5705 227.4310 274.1654 87.9918 0.1329 227.7763 227.6434 274.2832 88.7835 0.1334 227.9673 227.8339 274.4063 89.6360 0.1355 228.2306 228.0951 274.5509 90.3975 0.1365 228.3806 228.2441 274.6710 91.2198 0.1332 228.5952 228.4621 274.8085 92.0118 0.1325 228.8046 228.6721 274.9370 92.8035 0.1364 228.9875 228.8511 275.0816 93.6258 0.1271 229.2065 229.0794 275.2307 94.4175 0.1278 229.3989 229.2711 275.3699 95.2398 0.1309 229.6038 229.4729 275.5032 96.0368 0.1275 229.8060 229.6785 275.6531 96.8285 0.1241 230.0044 229.8803 275.7832 97.6505 0.1283 230.2054 230.0772 275.9238 98.4125 0.1263 230.4010 230.2747 276.0625 99.2645 0.1229 230.6115 230.4886 276.2040 100.0265 0.1230 230.7993 230.6764 276.3302 100.8485 0.1184 230.9978 230.8794 276.4770 101.6705 0.1138 231.1971 231.0833 276.6120 102.4325 0.1127 231.3846 231.2719 276.7394 103.2845 0.1159 231.6086 231.4927 276.8983 104.0465 0.1097 231.8006 231.6909 277.0421 104.8685 0.1089 231.9989 231.8899 277.1961 105.6908 0.1071 232.2227 232.1156 277.3488 106.4535 0.1089 232.4121 232.3032 277.4718 107.3055 0.1126 232.6031 232.4905 277.6465 108.0675 0.1119 232.7784 232.6664 277.7754 108.8895 0.0933 232.9819 232.8886 277.9167 109.6815 0.0846 233.2023 233.1177 278.0611 110.4733 0.0847 233.3929 233.3082 278.2336 111.3250 0.0882 233.5898 233.5017 278.3724 112.0868 0.0903 233.7641 233.6738 278.5136 112.9088 0.0972 233.9566 233.8595 278.6679 113.7010 0.0931 234.1595 234.0664 278.7978 114.4935 0.0871 234.3753 234.2882 278.9370 115.3160 0.0833 234.5707 234.4874 279.1133 116.1080 0.0762 234.7526 234.6764 279.2432 116.9298 0.0724 234.9545 234.8821 279.3916 117.7220 0.0696 235.1268 235.0572 279.5432 118.5135 0.0695 235.3003 235.2308 279.6835 119.3360 0.0691 235.5313 235.4623 279.8007 120.1278 0.0641 235.7157 235.6516 279.9265 120.9498 0.0597 235.9141 235.8544 280.0924 121.7418 0.0584 236.1065 236.0481 280.2265 122.5345 0.0567 236.2892 236.2325 280.3793 123.3568 0.0528 236.4852 236.4324 280.5118 124.1485 0.0529 236.6743 236.6214 280.6483 124.9693 0.0527 236.8827 236.8301 280.7703 125.7570 0.0506 237.0580 237.0074 280.9006 126.5450 0.0463 237.2538 237.2076 281.0502 127.3618 0.0436 237.4454 237.4018 281.1872 128.1210 0.0385 237.6076 237.5691 281.3030 128.9700 0.0379 237.8422 237.8043 281.4529 129.7580 0.0350 238.0150 237.9801 281.5559 130.5460 0.0310 238.2024 238.1714 281.6694 131.3648 0.0277 238.4002 238.3726 281.8030 132.1530 0.0223 238.5727 238.5505 281.9226 132.9718 0.0195 238.7695 238.7500 282.0326 133.7600 0.0171 238.9694 238.9524 282.1659 134.5490 0.0129 239.1466 239.1338 282.3156 135.3978 0.0148 239.3533 239.3384 282.4505 136.1570 0.0249 239.5062 239.4813 282.5829 136.9758 0.0241 239.6984 239.6743 282.6612 137.7645 0.0256 239.8850 239.8593 282.7908 138.5548 0.0176 240.0743 240.0567 282.9148 139.4038 0.0093 240.2695 240.2602 283.0400 140.1633 0.0070 240.4447 240.4377 283.1477 140.9838 0.0050 240.6359 240.6309 283.2897 141.7728 -0.0001 240.8257 240.8258 283.4129 142.5635 -0.0089 241.0338 241.0428 283.5172 143.4145 -0.0055 241.2170 241.2225 283.6462 144.1765 0.0104 241.3836 241.3732 283.7673 144.9985 0.0092 241.5743 241.5650 283.8864 145.7905 0.0087 241.7663 241.7576 283.9920 146.5825 0.0272 241.9577 241.9305 284.1228 147.4045 0.0308 242.1552 242.1243 284.2480 148.1965 0.0300 242.3416 242.3116 284.3634 149.0185 0.0276 242.5034 242.4758 284.5202 149.8105 0.0221 242.6838 242.6617 284.6356 150.6025 0.0203 242.8821 242.8619 284.7689 151.4245 0.0130 243.0616 243.0486 284.8947 152.2165 0.0133 243.2313 243.2180 285.0187 153.0385 0.0073 243.4256 243.4183 285.1704 153.8305 0.0017 243.6153 243.6137 285.2996 154.6225 -0.0035 243.7967 243.8002 285.4422 155.4445 -0.0051 243.9875 243.9925 285.5799 156.2365 -0.0096 244.1709 244.1804 285.6963 157.0585 -0.0083 244.3271 244.3354 285.8301 157.8505 -0.0112 244.5170 244.5282 285.9930 158.6423 -0.0240 244.6868 244.7108 286.1243 159.4643 -0.0311 244.8767 244.9078 286.2757 160.2560 -0.0168 245.0602 245.0771 286.4100 161.0780 -0.0163 245.2391 245.2555 286.5679 161.8703 -0.0156 245.4124 245.4280 286.6800 162.6618 -0.0165 245.5965 245.6130 286.8166 163.5140 -0.0188 245.8090 245.8278 286.9774 164.2760 -0.0218 245.9683 245.9902 287.1014 165.0978 -0.0209 246.1594 246.1803 287.2677 165.8900 -0.0254 246.3147 246.3400 287.3985 166.6815 -0.0286 246.5038 246.5323 287.5455 167.5340 -0.0355 246.7020 246.7375 287.6768 168.2958 -0.0539 246.8616 246.9156 287.8203 169.1178 -0.0446 247.0396 247.0842 287.9621 169.9400 -0.0409 247.2337 247.2746 288.1232 170.7015 -0.0397 247.3875 247.4272 288.2511 171.5540 -0.0410 247.5776 247.6187 288.4182 172.3458 -0.0447 247.7648 247.8095 288.5471 173.1375 -0.0457 247.9360 247.9817 288.7112 173.9598 -0.0483 248.1210 248.1693 288.8543 174.7215 -0.0510 248.2879 248.3389 288.9987 175.5743 -0.0534 248.4937 248.5471 289.1383 176.3665 -0.0599 248.6679 248.7278 289.2697 177.1585 -0.0636 248.8276 248.8911 289.4190 177.9488 -0.0633 249.0033 249.0665 289.5764 178.7795 -0.0680 249.1862 249.2542 289.7068 179.6015 -0.0646 249.3848 249.4494 289.8484 180.3635 -0.0680 249.5679 249.6359 289.9777 181.2160 -0.0714 249.7375 249.8089 290.1199 181.9785 -0.0727 249.8882 249.9610 290.2465 182.8013 -0.0764 250.0825 250.1589 290.4103 183.6235 -0.0781 250.2537 250.3318 290.4952 184.3855 -0.0800 250.4133 250.4933 290.6398 185.2380 -0.0842 250.6295 250.7137 290.7727 186.0305 -0.0847 250.7929 250.8776 290.9097 186.8225 -0.0833 250.9845 251.0679 291.0311 187.6445 -0.0873 251.1368 251.2241 291.1516 188.4365 -0.0873 251.3095 251.3968 291.2730 189.2578 -0.0960 251.4828 251.5787 291.3892 190.0485 -0.1003 251.6633 251.7636 291.5116 190.8360 -0.1014 251.8461 251.9475 291.6335 191.6548 -0.0998 251.9966 252.0964 291.7707 192.4120 -0.1027 252.1586 252.2613 291.8677 193.2605 -0.1041 252.3406 252.4447 291.9823 194.0485 -0.1098 252.5333 252.6431 292.1113 194.8375 -0.1132 252.7173 252.8305 292.2318 195.6560 -0.1125 252.8914 253.0040 292.3461 196.4140 -0.1130 253.0591 253.1721 292.4510 197.2625 -0.1155 253.2473 253.3628 292.5865 198.0505 -0.1142 253.4062 253.5204 292.6928 198.8398 -0.1168 253.5656 253.6825 292.8148 199.6583 -0.1190 253.7479 253.8668 292.9383 200.4160 -0.1253 253.9044 254.0296 293.0559 201.2650 -0.1285 254.0993 254.2278 293.1784 202.0535 -0.1302 254.2717 254.4019 293.3110 202.8420 -0.1308 254.4259 254.5567 293.4299 203.6608 -0.1318 254.5962 254.7280 293.5484 204.4193 -0.1353 254.7567 254.8919 293.6651 205.2703 -0.1392 254.9421 255.0813 293.7928 206.0598 -0.1410 255.1177 255.2587 293.9257 206.8490 -0.1434 255.2833 255.4267 294.0569 207.6690 -0.1468 255.4681 255.6149 294.1899 208.4293 -0.1465 255.6148 255.7613 294.3369 209.2810 -0.1520 255.8102 255.9622 294.4657 210.0730 -0.1512 255.9768 256.1280 294.5909 210.8645 -0.1494 256.1307 256.2801 294.7407 211.6870 -0.1541 256.3024 256.4565 294.8577 212.4485 -0.1547 256.4533 256.6080 294.9868 213.3010 -0.1567 256.6327 256.7894 295.1227 214.0628 -0.1591 256.8044 256.9635 295.2505 214.8848 -0.1576 256.9922 257.1499 295.3857 215.6770 -0.1644 257.1716 257.3360 295.5215 216.4685 -0.1687 257.3434 257.5121 295.6594 217.2910 -0.1709 257.4958 257.6667 295.7986 218.0525 -0.1735 257.6398 257.8133 295.8923 218.9050 -0.1756 257.8481 258.0237 296.0363 219.6968 -0.1801 258.0023 258.1823 296.1752 220.4885 -0.1824 258.1656 258.3480 296.3124 221.3110 -0.1838 258.3392 258.5230 296.4250 222.0725 -0.1876 258.5126 258.7002 296.5610 222.9250 -0.1883 258.6816 258.8699 296.7127 223.6868 -0.1875 258.8359 259.0234 296.8532 224.5088 -0.1910 259.0052 259.1962 296.9676 225.3308 -0.1924 259.1787 259.3711 297.1341 226.0925 -0.1950 259.3187 259.5138 297.2541 226.9448 -0.1953 259.4978 259.6931 297.3945 227.7065 -0.1980 259.6671 259.8651 297.5062 228.5285 -0.1985 259.8583 260.0568 297.6481 229.3205 -0.2020 260.0057 260.2077 297.7915 230.1125 -0.2035 260.1762 260.3797 297.9128 230.9645 -0.2040 260.3478 260.5518 298.0496 231.7265 -0.2083 260.5093 260.7176 298.1868 232.5485 -0.2118 260.6797 260.8915 298.3145 233.3405 -0.2152 260.8320 261.0472 298.4595 234.1325 -0.2237 260.9995 261.2232 298.6161 234.9845 -0.2362 261.1843 261.4205 298.7507 235.7465 -0.2392 261.3462 261.5854 298.8625 236.5683 -0.2338 261.5013 261.7351 298.9929 237.3605 -0.2313 261.6512 261.8825 299.1559 238.1520 -0.2303 261.8383 262.0687 299.2460 239.0128 -0.2309 262.0274 262.2583 299.4039 239.7540 -0.2325 262.1536 262.3862 299.5485 240.6065 -0.2374 262.3297 262.5671 299.6912 241.3688 -0.2431 262.4856 262.7287 299.8289 242.1908 -0.2456 262.6595 262.9051 299.9694 243.0133 -0.2467 262.8413 263.0880 300.1228 243.7755 -0.2525 262.9876 263.2400 300.2377 244.6280 -0.2520 263.1634 263.4153 300.3590 245.3898 -0.2516 263.3149 263.5665 300.4783 246.2118 -0.2542 263.4643 263.7185 300.6309 247.0340 -0.2570 263.6593 263.9163 300.7499 247.7955 -0.2573 263.8047 264.0620 300.8645 248.6480 -0.2596 263.9966 264.2562 301.0437 249.4175 -0.2610 264.1565 264.4175 301.1777 250.2485 -0.2612 264.3330 264.5942 301.3213 251.0408 -0.2662 264.4842 264.7504 301.4246 251.8325 -0.2682 264.6454 264.9136 301.5650 252.6548 -0.2686 264.8164 265.0850 301.7036 253.4465 -0.2696 264.9716 265.2412 301.8366 254.2660 -0.2787 265.1420 265.4207 301.9663 255.0540 -0.2932 265.2627 265.5558 302.1124 255.8420 -0.3029 265.4667 265.7696 302.2432 256.6600 -0.3078 265.6475 265.9552 302.3809 257.4180 -0.3095 265.8025 266.1120 302.5096 258.2648 -0.2980 265.9568 266.2548 302.6707 259.0540 -0.2907 266.1057 266.3964 302.7921 259.8420 -0.2890 266.2521 266.5411 302.9078 260.6590 -0.2920 266.4238 266.7158 303.0307 261.4480 -0.2942 266.5819 266.8761 303.1566 262.2668 -0.2986 266.7502 267.0488 303.3140 263.0550 -0.2994 266.9117 267.2110 303.4236 263.8433 -0.3002 267.0766 267.3769 303.5831 264.6925 -0.3046 267.2459 267.5505 303.7307 265.4510 -0.3066 267.4050 267.7116 303.8620 266.2698 -0.3100 267.5493 267.8593 303.9910 267.0883 -0.3135 267.7211 268.0346 304.1227 267.8470 -0.3169 267.8816 268.1985 304.2231 268.6973 -0.3204 268.0644 268.3848 304.3643 269.4860 -0.3211 268.2166 268.5377 304.5001 270.2760 -0.3256 268.3484 268.6740 304.6302 271.0970 -0.3271 268.5165 268.8436 304.7775 271.8570 -0.3295 268.6592 268.9887 304.8942 272.7088 -0.3372 268.8538 269.1910 305.0314 273.5008 -0.3363 269.0187 269.3549 305.1680 274.2925 -0.3384 269.1611 269.4995 305.3017 275.1145 -0.3431 269.3235 269.6666 305.4471 275.8765 -0.3445 269.4922 269.8367 305.5554 276.7285 -0.3427 269.6474 269.9901 305.6940 277.5205 -0.3501 269.8030 270.1531 305.8213 278.3125 -0.3501 269.9774 270.3275 305.9611 279.1345 -0.3555 270.1363 270.4917 306.0672 279.9073 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