DTA measure 1pb_updown4 Date: 2025319:1014 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.75 s Mass = 937.000 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4545 0.9125 213.8504 212.9379 206.6902 4.0520 0.9016 213.7855 212.8838 206.7025 5.6655 0.8792 213.7273 212.8481 206.7051 7.2645 0.8542 213.6603 212.8060 206.7117 8.8785 0.8702 213.5926 212.7223 206.7111 10.4775 0.9172 213.5310 212.6138 206.7415 12.0915 0.9970 213.4837 212.4867 206.7585 13.6905 0.9412 213.4183 212.4771 206.7827 15.2895 0.9109 213.3693 212.4584 206.8237 16.9185 0.9150 213.2994 212.3843 206.8466 18.5175 0.9286 213.2400 212.3114 206.8951 20.1310 0.9709 213.1818 212.2108 206.9478 21.7299 0.9051 213.1413 212.2362 207.0303 23.3289 0.8961 213.0749 212.1788 207.1118 24.9579 0.8984 213.0210 212.1226 207.1883 26.5719 0.9265 212.9572 212.0307 207.3082 28.1708 0.9300 212.9048 211.9748 207.4236 29.7698 0.9267 212.8610 211.9343 207.5606 31.3836 0.9111 212.8009 211.8898 207.6756 32.9976 0.8884 212.7529 211.8645 207.8124 34.6119 0.8661 212.7077 211.8416 207.9842 36.2103 0.8562 212.6629 211.8068 208.1605 37.8246 0.8448 212.6035 211.7588 208.3154 39.4235 0.8398 212.5708 211.7310 208.5083 41.0525 0.8386 212.5191 211.6805 208.7170 42.6515 0.8418 212.4724 211.6306 208.9183 44.2655 0.9391 212.4404 211.5013 209.1137 45.8645 0.9561 212.4046 211.4485 209.3319 47.4790 0.9498 212.3521 211.4023 209.5573 49.0908 1.0164 212.3080 211.2916 209.7873 50.6965 1.1812 212.2767 211.0955 210.0335 52.2875 0.9340 212.2505 211.3165 210.2495 53.8790 0.7564 212.2085 211.4521 210.4821 55.5008 0.8614 212.1739 211.3125 210.7420 57.0918 0.7496 212.1522 211.4026 210.9933 58.6986 0.7146 212.0965 211.3820 211.2364 60.2899 0.7119 212.0709 211.3589 211.4716 61.8979 0.7098 212.0468 211.3370 211.7244 63.5211 0.7386 212.0236 211.2850 211.9653 65.1151 0.6871 211.9916 211.3045 212.2043 66.7124 0.6871 211.9804 211.2933 212.4416 68.3249 0.7133 211.9572 211.2438 212.6535 69.9239 0.7227 211.9259 211.2032 212.8716 71.5379 0.7049 211.9312 211.2264 213.0998 73.1369 0.7074 211.9087 211.2013 213.3295 74.7508 0.7693 211.8983 211.1291 213.5402 76.3498 0.8880 211.8755 210.9875 213.7644 77.9488 0.8296 211.8725 211.0428 213.9701 79.5651 0.8046 211.8666 211.0620 214.1911 81.1798 0.8383 211.8460 211.0077 214.3799 82.7788 0.8295 211.8551 211.0256 214.5783 84.3776 0.8120 211.8557 211.0437 214.7819 85.9916 0.8110 211.8360 211.0250 214.9914 87.5905 0.8464 211.8246 210.9782 215.1879 89.2195 0.8058 211.8367 211.0309 215.3773 90.8185 0.8123 211.8332 211.0210 215.5591 92.4175 0.8735 211.8223 210.9489 215.7417 94.0165 0.9299 211.8261 210.8962 215.9289 95.6305 0.8884 211.8392 210.9508 216.1216 97.2445 0.8726 211.8513 210.9788 216.3020 98.8584 0.8449 211.8478 211.0029 216.4678 100.4571 0.8304 211.8701 211.0396 216.6527 102.0558 0.8495 211.8710 211.0215 216.8242 103.6698 0.8773 211.8763 210.9990 217.0024 105.2839 0.9011 211.9034 211.0023 217.1846 106.8829 0.8417 211.9218 211.0801 217.3573 108.4978 0.8276 211.9177 211.0901 217.5416 110.0966 0.8194 211.9292 211.1098 217.7240 111.6958 0.8318 211.9519 211.1201 217.9164 113.3244 0.8231 211.9828 211.1598 218.0866 114.9165 0.8151 211.9996 211.1845 218.2716 116.5230 0.8275 212.0161 211.1885 218.4905 118.1140 0.8049 212.0469 211.2420 218.6635 119.7058 0.8107 212.0761 211.2653 218.8507 121.3271 0.8015 212.1014 211.2999 219.0409 122.9350 0.8070 212.1107 211.3038 219.2152 124.5270 0.7951 212.1422 211.3471 219.4158 126.1335 0.7907 212.1746 211.3839 219.6146 127.7269 0.7866 212.2066 211.4201 219.8161 129.3511 0.7851 212.2370 211.4519 220.0271 130.9465 0.7826 212.2830 211.5004 220.2155 132.5445 0.7821 212.3078 211.5257 220.4132 134.1435 0.7784 212.3562 211.5777 220.6172 135.7575 0.7745 212.3634 211.5888 220.8264 137.3715 0.7765 212.4295 211.6530 221.0303 138.9855 0.7704 212.4727 211.7023 221.2483 140.5856 0.7719 212.5147 211.7427 221.4633 142.1865 0.7653 212.5442 211.7789 221.6553 143.7854 0.7608 212.5953 211.8345 221.8628 145.4145 0.7654 212.6336 211.8682 222.0656 147.0135 0.7596 212.6915 211.9319 222.2684 148.6269 0.7562 212.7411 211.9849 222.4678 150.2258 0.7629 212.7667 212.0038 222.6879 151.8248 0.7534 212.8298 212.0764 222.9031 153.4539 0.7480 212.8696 212.1216 223.0975 155.0529 0.7451 212.9350 212.1898 223.2974 156.6666 0.7441 212.9885 212.2444 223.5026 158.2656 0.7440 213.0533 212.3093 223.7040 159.8798 0.7417 213.1065 212.3647 223.9263 161.4936 0.7371 213.1687 212.4315 224.0937 163.1086 0.7353 213.2123 212.4769 224.3017 164.7075 0.7347 213.2716 212.5368 224.4839 166.3065 0.7326 213.3481 212.6155 224.6954 167.9205 0.7226 213.4064 212.6838 224.8728 169.5503 0.7228 213.4727 212.7500 225.0893 171.1495 0.7278 213.5404 212.8126 225.2864 172.7485 0.7222 213.6137 212.8915 225.5063 174.3624 0.7251 213.6596 212.9345 225.7008 175.9613 0.7154 213.7285 213.0131 225.9226 177.5893 0.7101 213.7984 213.0884 226.1110 179.1814 0.6979 213.8758 213.1780 226.3344 180.7728 0.7003 213.9534 213.2531 226.5566 182.3696 0.7005 214.0283 213.3279 226.7660 183.9618 0.7001 214.1081 213.4080 226.9942 185.5835 0.6988 214.1853 213.4865 227.2084 187.1758 0.6973 214.2507 213.5534 227.4325 188.7840 0.6935 214.3392 213.6457 227.6497 190.3778 0.6761 214.4159 213.7398 227.8659 191.9724 0.6837 214.5009 213.8173 228.0623 193.5959 0.7899 214.5755 213.7856 228.2852 195.1936 0.7951 214.6481 213.8530 228.5058 196.7905 0.6987 214.7407 214.0421 228.7148 198.4030 0.6875 214.8130 214.1255 228.9261 200.0018 0.6940 214.9218 214.2278 229.1428 201.6008 0.6887 214.9915 214.3028 229.3398 203.2300 0.6864 215.0930 214.4066 229.5669 204.8288 0.6812 215.1730 214.4918 229.7692 206.4278 0.6843 215.2678 214.5835 229.9768 208.0268 0.6792 215.3606 214.6814 230.1830 209.6408 0.6743 215.4526 214.7783 230.3792 211.2546 0.6761 215.5560 214.8799 230.5920 212.8536 0.6717 215.6344 214.9627 230.7859 214.4675 0.6746 215.7338 215.0592 230.9958 216.0665 0.6763 215.8450 215.1687 231.1829 217.6655 0.6676 215.9398 215.2722 231.3954 219.2945 0.6655 216.0335 215.3679 231.5871 220.8935 0.6632 216.1528 215.4896 231.7814 222.5075 0.6614 216.2441 215.5827 231.9774 224.1064 0.6733 216.3597 215.6864 232.1709 225.7054 0.6661 216.4309 215.7647 232.3651 227.3341 0.6558 216.5705 215.9147 232.5487 228.9329 0.6543 216.6627 216.0084 232.7434 230.5468 0.6534 216.7607 216.1074 232.9422 232.1458 0.6502 216.8699 216.2197 233.1272 233.7449 0.6486 216.9813 216.3328 233.3284 235.3739 0.6481 217.0985 216.4504 233.4942 236.9736 0.6444 217.1926 216.5482 233.6953 238.5876 0.6444 217.3031 216.6587 233.8848 240.1866 0.6442 217.4215 216.7774 234.0869 241.7843 0.6426 217.5341 216.8915 234.2956 243.4060 0.6392 217.6498 217.0106 234.4984 244.9970 0.6434 217.7683 217.1249 234.7042 246.6033 0.6361 217.8897 217.2536 234.9062 248.1954 0.6371 217.9804 217.3433 235.1073 249.8020 0.6305 218.0888 217.4582 235.3283 251.4230 0.6260 218.2125 217.5866 235.4978 253.0145 0.6247 218.3303 217.7056 235.7377 254.6225 0.6261 218.4594 217.8333 235.9476 256.2163 0.6237 218.5868 217.9632 236.1563 257.8393 0.6212 218.7077 218.0865 236.3906 259.4505 0.6197 218.8357 218.2160 236.5925 261.0495 0.6165 218.9408 218.3242 236.7964 262.6486 0.6115 219.0677 218.4562 237.0060 264.2475 0.6097 219.1946 218.5850 237.2161 265.8756 0.6094 219.3145 218.7052 237.4238 267.4745 0.6060 219.4510 218.8450 237.6482 269.0885 0.6059 219.5772 218.9713 237.8535 270.6875 0.6053 219.7072 219.1019 238.0527 272.2865 0.6020 219.8383 219.2363 238.2670 273.9153 0.6007 219.9622 219.3615 238.4761 275.5293 0.5988 220.1042 219.5055 238.6743 277.1280 0.5980 220.2193 219.6213 238.8893 278.7268 0.5981 220.3438 219.7457 239.0776 280.3415 0.5938 220.4719 219.8781 239.2924 281.9559 0.5919 220.6118 220.0199 239.5048 283.5714 0.5872 220.7407 220.1535 239.7153 285.1756 0.5844 220.8866 220.3022 239.9175 286.7748 0.5881 221.0143 220.4262 240.1119 288.3886 0.5839 221.1566 220.5727 240.3065 290.0026 0.5788 221.2890 220.7102 240.5020 291.6168 0.5728 221.4366 220.8637 240.7073 293.2155 0.5725 221.5630 220.9905 240.8965 294.8145 0.5712 221.7096 221.1384 241.0659 296.4291 0.5679 221.8495 221.2816 241.2918 298.0435 0.5645 221.9908 221.4263 241.4911 299.6436 0.5632 222.1246 221.5614 241.6849 301.2465 0.5628 222.2648 221.7020 241.9054 302.8604 0.5605 222.4116 221.8511 242.1071 304.4603 0.5573 222.5620 222.0047 242.3096 306.0578 0.5551 222.7098 222.1548 242.5327 307.6790 0.5503 222.8562 222.3058 242.7465 309.2704 0.5508 222.9809 222.4301 242.9573 310.8614 0.5482 223.1335 222.5853 243.1942 312.4680 0.5460 223.2711 222.7251 243.3940 314.0606 0.5436 223.4135 222.8699 243.6089 315.6835 0.5420 223.5737 223.0317 243.8426 317.2758 0.5418 223.7096 223.1678 244.0679 318.8710 0.5357 223.8626 223.3269 244.2920 320.4819 0.5334 224.0071 223.4737 244.4988 322.0776 0.5296 224.1655 223.6358 244.7153 323.7043 0.5284 224.3076 223.7791 244.9320 325.3009 0.5257 224.4790 223.9533 245.1398 326.8984 0.5221 224.6246 224.1025 245.3636 328.4978 0.5214 224.7666 224.2452 245.5733 330.1118 0.5165 224.9101 224.3935 245.7941 331.7258 0.5137 225.0846 224.5709 246.0012 333.3398 0.5102 225.2288 224.7186 246.2272 334.9386 0.5092 225.3900 224.8809 246.4357 336.5378 0.5084 225.5418 225.0334 246.6448 338.1365 0.5009 225.6936 225.1927 246.8542 339.7656 0.4992 225.8464 225.3473 247.0657 341.3645 0.5007 225.9952 225.4945 247.2750 342.9785 0.4974 226.1763 225.6790 247.4910 344.5775 0.4913 226.3153 225.8241 247.6795 346.1765 0.4872 226.4824 225.9952 247.8979 347.8055 0.4941 226.6430 226.1488 248.1174 349.4045 0.4782 226.8000 226.3218 248.2987 351.0185 0.4756 226.9606 226.4850 248.5144 352.6624 0.4841 227.1409 226.6567 248.7308 354.3960 0.4760 227.3002 226.8242 248.9390 356.0098 0.4768 227.4814 227.0046 249.1212 357.6088 0.4765 227.6308 227.1543 249.3067 359.2078 0.4762 227.7957 227.3195 249.5233 360.8376 0.4697 227.9705 227.5009 249.7292 362.4369 0.4692 228.1317 227.6625 249.9266 364.0506 0.4665 228.2977 227.8312 250.1071 365.6496 0.4686 228.4499 227.9813 250.3135 367.2486 0.4673 228.6385 228.1712 250.4974 368.8784 0.4607 228.7881 228.3274 250.6959 370.4776 0.4595 228.9725 228.5131 250.9028 372.0840 0.4582 229.1479 228.6897 251.0813 373.6750 0.4563 229.3007 228.8444 251.2792 375.2660 0.4537 229.4666 229.0129 251.4845 376.8871 0.4548 229.6394 229.1846 251.6744 378.4951 0.4534 229.8073 229.3538 251.8804 380.0875 0.4557 229.9801 229.5244 252.0429 381.6945 0.4583 230.1443 229.6860 252.2421 383.3016 0.4553 230.3129 229.8575 252.4474 384.9093 0.4496 230.4765 230.0269 252.6430 386.5070 0.4460 230.6532 230.2073 252.8498 388.1201 0.4409 230.8263 230.3855 253.0564 389.7168 0.4497 230.9975 230.5478 253.2887 391.3145 0.4559 231.1617 230.7058 253.4943 392.9435 0.4547 231.3398 230.8851 253.7355 394.5425 0.4528 231.5061 231.0533 253.9664 396.1415 0.4362 231.6666 231.2305 254.1944 397.7555 0.4270 231.8396 231.4125 254.4129 399.3544 0.4277 232.0191 231.5914 254.6391 400.9834 0.4276 232.1934 231.7658 254.8717 402.5821 0.4478 232.3770 231.9292 255.0971 404.1808 0.4447 232.5654 232.1207 255.3307 405.7948 0.4416 232.7530 232.3114 255.5513 407.3938 0.4359 232.9156 232.4797 255.7959 409.0230 0.4353 233.0870 232.6517 256.0193 410.6218 0.4353 233.2730 232.8377 256.2370 412.2208 0.4408 233.4516 233.0109 256.4745 413.8348 0.4415 233.6207 233.1792 256.6872 415.4336 0.4155 233.7928 233.3773 256.9149 417.0633 0.4082 233.9853 233.5771 257.1518 418.6638 0.4095 234.1574 233.7480 257.3655 420.2635 0.4032 234.3329 233.9297 257.5750 421.8775 0.3968 234.5213 234.1245 257.8021 423.4915 0.3910 234.6940 234.3031 258.0072 425.1055 0.3927 234.8859 234.4932 258.1977 426.7046 0.3900 235.0550 234.6650 258.3976 428.3198 0.3843 235.2567 234.8725 258.5998 429.9193 0.3863 235.4328 235.0466 258.7804 431.5330 0.3769 235.6275 235.2506 258.9615 433.1478 0.3739 235.7978 235.4239 259.1309 434.7465 0.3716 235.9848 235.6133 259.3217 436.3525 0.3716 236.1669 235.7953 259.4942 437.9443 0.3704 236.3545 235.9841 259.6794 439.5511 0.3753 236.5402 236.1648 259.8774 441.1579 0.3807 236.7037 236.3230 260.0569 442.7494 0.3763 236.9039 236.5276 260.2485 444.3571 0.3760 237.0730 236.6970 260.4587 445.9499 0.3643 237.2709 236.9067 260.6461 447.5728 0.3628 237.4395 237.0767 260.8456 449.1668 0.3570 237.6277 237.2707 261.0266 450.7764 0.3549 237.8254 237.4705 261.2438 452.3724 0.3528 238.0104 237.6576 261.4289 453.9698 0.3474 238.1992 237.8518 261.6254 455.5989 0.3456 238.3858 238.0402 261.8374 457.1979 0.3400 238.5665 238.2264 262.0424 458.8118 0.3370 238.7542 238.4171 262.2510 460.4106 0.3338 238.9374 238.6036 262.4401 462.0096 0.3303 239.1376 238.8074 262.6554 463.6238 0.3310 239.3277 238.9967 262.8639 465.2381 0.3311 239.5009 239.1698 263.0654 466.8376 0.3250 239.6842 239.3592 263.2987 468.4515 0.3246 239.9002 239.5756 263.5088 470.0505 0.3201 240.0753 239.7553 263.7187 471.6645 0.3158 240.2661 239.9503 263.9437 473.2785 0.3103 240.4642 240.1538 264.1755 474.8783 0.3122 240.6470 240.3348 264.3978 476.4795 0.3185 240.8216 240.5031 264.6213 478.0935 0.3208 241.0367 240.7160 264.8589 479.7071 0.3049 241.2051 240.9001 265.1050 481.3213 0.3016 241.3928 241.0912 265.3500 482.9198 0.2990 241.5892 241.2901 265.5664 484.5338 0.2964 241.7868 241.4903 265.7952 486.1328 0.2960 241.9846 241.6885 266.0300 487.7619 0.2887 242.1928 241.9041 266.2556 489.3618 0.2885 242.3732 242.0847 266.4754 490.9756 0.2825 242.5600 242.2775 266.7024 492.5750 0.2777 242.7469 242.4692 266.9246 494.1896 0.2767 242.9313 242.6546 267.1113 495.8035 0.2700 243.1365 242.8664 267.3232 497.4186 0.2682 243.3437 243.0755 267.5251 499.0165 0.2670 243.5262 243.2591 267.7362 500.6080 0.2627 243.7539 243.4911 267.9235 502.2148 0.2577 243.9323 243.6746 268.1388 503.8219 0.2573 244.1161 243.8588 268.3125 505.4291 0.2544 244.3119 244.0574 268.5030 507.0215 0.2502 244.5104 244.2602 268.6886 508.6289 0.2473 244.6997 244.4524 268.8757 510.2368 0.2488 244.8806 244.6318 269.0609 511.8465 0.2460 245.0764 244.8304 269.2614 513.4415 0.2464 245.2909 245.0445 269.4361 515.0508 0.2432 245.4900 245.2467 269.6521 516.6485 0.2395 245.6812 245.4417 269.8486 518.2623 0.2377 245.8776 245.6399 270.0420 519.8755 0.2400 246.0804 245.8404 270.2576 521.4745 0.2440 246.2612 246.0171 270.4738 523.0884 0.2710 246.4740 246.2030 270.6562 524.6874 0.2775 246.6655 246.3879 270.8749 526.3014 0.2333 246.8614 246.6281 271.0983 527.9154 0.2311 247.0723 246.8412 271.3276 529.5290 0.2217 247.2658 247.0441 271.5279 531.1278 0.2162 247.4593 247.2431 271.7197 532.7270 0.2297 247.6790 247.4493 271.9462 534.3565 0.2175 247.8697 247.6522 272.1769 535.9609 0.2108 248.0668 247.8560 272.3969 537.5748 0.2236 248.2532 248.0296 272.6023 539.1738 0.2241 248.4652 248.2412 272.8151 540.7821 0.2072 248.6611 248.4539 273.0210 542.3976 0.2276 248.8738 248.6462 273.2639 544.0118 0.2281 249.0652 248.8371 273.4714 545.6116 0.2086 249.2434 249.0348 273.6807 547.2260 0.2029 249.4485 249.2456 273.9011 548.8255 0.2009 249.6631 249.4622 274.1120 550.4545 0.1886 249.8704 249.6818 274.3331 552.0544 0.1875 250.0548 249.8673 274.5546 553.6685 0.1905 250.2637 250.0732 274.7696 555.2675 0.1934 250.4621 250.2687 274.9706 556.8819 0.2048 250.6647 250.4599 275.1721 558.4961 0.2023 250.8753 250.6730 275.3912 560.1099 0.1978 251.0621 250.8643 275.6108 561.7090 0.1973 251.2782 251.0810 275.8269 563.3206 0.1824 251.4746 251.2922 276.0275 564.9123 0.1760 251.6817 251.5056 276.2291 566.5194 0.1711 251.8760 251.7050 276.4424 568.1266 0.1651 252.0691 251.9040 276.6453 569.7228 0.1643 252.2895 252.1252 276.8550 571.3186 0.1568 252.4915 252.3346 277.0550 572.9108 0.1535 252.6891 252.5356 277.2768 574.5348 0.1518 252.8928 252.7410 277.4825 576.1438 0.1560 253.1003 252.9443 277.6760 577.7396 0.1721 253.3062 253.1341 277.8952 579.3504 0.1594 253.5048 253.3454 278.1151 580.9476 0.1512 253.7072 253.5560 278.3073 582.5760 0.1436 253.9081 253.7645 278.5054 584.1736 0.1350 254.1038 253.9687 278.7198 585.7718 0.1283 254.3066 254.1783 278.9231 587.3708 0.1241 254.5100 254.3859 279.1274 588.9846 0.1250 254.7123 254.5873 279.3296 590.5989 0.1204 254.9253 254.8049 279.5165 592.2128 0.1180 255.1264 255.0084 279.7489 593.8116 0.1177 255.3219 255.2042 279.9569 595.4105 0.1351 255.5434 255.4083 280.1582 597.0245 0.1059 255.7512 255.6452 280.3537 598.6385 0.0959 255.9764 255.8806 280.5655 600.2533 0.0915 256.1781 256.0866 280.7612 601.8525 0.0893 256.3750 256.2857 280.9325 603.4515 0.0853 256.5777 256.4924 281.1432 605.0655 0.0871 256.7882 256.7011 281.3457 606.6793 0.0886 256.9995 256.9109 281.5524 608.2931 0.0809 257.1916 257.1107 281.7746 609.8919 0.0763 257.3965 257.3202 281.9974 611.5058 0.0750 257.5923 257.5173 282.2174 613.1199 0.0719 257.7986 257.7267 282.4161 614.7339 0.0668 258.0166 257.9498 282.6430 616.3328 0.0617 258.2259 258.1642 282.8898 617.9471 0.0561 258.4225 258.3664 283.1175 619.5471 0.0356 258.6371 258.6015 283.3345 621.1616 -0.0544 258.8204 258.8748 283.5933 622.7766 -0.0095 259.0527 259.0622 283.8169 624.3765 -0.0179 259.2545 259.2724 284.0310 625.9909 -0.0103 259.4698 259.4802 284.2755 627.5898 -0.0129 259.6719 259.6848 284.5021 629.1963 -0.0141 259.8676 259.8817 284.7124 630.8030 -0.0145 260.0938 260.1083 284.9263 632.3949 -0.0103 260.2921 260.3023 285.1408 634.0010 -0.0082 260.5126 260.5208 285.3363 635.5929 -0.0112 260.7236 260.7348 285.5491 637.2015 -0.0192 260.9161 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