DTA measure 1gyors Date: 2026317:1052 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.29 s Mass = 1166.200 mg data_number = 1342 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2400 1.0142 236.8217 235.8074 274.1213 2.0260 1.0124 237.0882 236.0758 273.9471 2.8330 1.0137 237.3431 236.3294 273.7622 3.6503 1.0105 237.6062 236.5957 273.5841 4.4160 1.0114 237.8196 236.8082 273.3911 5.2745 1.0176 238.1159 237.0983 273.1838 6.0195 1.0178 238.3823 237.3644 273.0371 6.8675 1.0182 238.6813 237.6631 272.8941 7.6335 1.0146 238.9400 237.9254 272.7961 8.4608 1.0131 239.2236 238.2104 272.7266 9.2575 1.0131 239.4778 238.4647 272.6497 10.0540 1.0127 239.7424 238.7296 272.6249 10.8713 1.0104 240.0270 239.0166 272.6413 11.6475 1.0106 240.2789 239.2683 272.7186 12.4950 1.0123 240.5675 239.5552 272.8278 13.2510 1.0080 240.8060 239.7980 272.9680 14.0885 1.0095 241.0572 240.0478 273.1529 14.8748 1.0107 241.3044 240.2937 273.3825 15.6613 1.0088 241.5614 240.5527 273.6609 16.4988 1.0094 241.8288 240.8194 273.9751 17.2545 1.0110 242.0676 241.0566 274.2995 18.0820 1.0102 242.3171 241.3069 274.6738 18.8475 1.0089 242.5477 241.5389 275.0544 19.7058 1.0063 242.7991 241.7928 275.4769 20.4718 1.0033 243.0370 242.0337 275.8773 21.2888 1.0021 243.2961 242.2940 276.3198 22.0958 0.9968 243.5719 242.5751 276.7737 22.8820 0.9987 243.8352 242.8365 277.2111 23.7093 0.9971 244.0904 243.0932 277.6284 24.4755 0.9948 244.3605 243.3657 278.0023 25.3333 0.9913 244.6630 243.6717 278.4172 26.0995 0.9891 244.9041 243.9149 278.7437 26.9165 0.9845 245.1309 244.1465 279.0598 27.7233 0.9790 245.3616 244.3825 279.3334 28.5200 0.9763 245.6002 244.6239 279.6210 29.3473 0.9685 245.8661 244.8976 279.9037 30.1030 0.9626 246.0786 245.1160 280.1081 30.9715 0.9622 246.3393 245.3771 280.3053 31.7065 0.9611 246.5711 245.6100 280.4456 32.5648 0.9739 246.8463 245.8724 280.5480 33.3305 1.0004 247.0763 246.0760 280.6242 34.1578 0.9946 247.3273 246.3327 280.6728 34.9545 0.9861 247.5680 246.5818 280.7131 35.7510 0.9749 247.7843 246.8094 280.7434 36.5683 0.9672 248.0439 247.0767 280.7478 37.3445 0.9613 248.3049 247.3436 280.6926 38.2023 0.9542 248.5646 247.6104 280.6332 38.9685 0.9480 248.7818 247.8338 280.5657 39.7855 0.9402 249.0066 248.0663 280.5090 40.5923 0.9410 249.2216 248.2806 280.4274 41.3788 0.9393 249.4648 248.5255 280.3048 42.2060 0.9360 249.7234 248.7874 280.2025 42.9718 0.9357 249.9782 249.0424 280.0938 43.8198 0.9369 250.2607 249.3238 279.9908 44.5855 0.9300 250.4969 249.5669 279.9071 45.4128 0.9234 250.7277 249.8043 279.8450 46.2095 0.9123 250.9541 250.0418 279.7619 47.0060 0.9071 251.1874 250.2804 279.7052 47.8230 0.8976 251.4447 250.5470 279.6558 48.5890 0.8939 251.6517 250.7578 279.6348 49.4470 0.8854 251.9021 251.0167 279.6472 50.2025 0.8811 252.1157 251.2346 279.6732 51.0403 0.8757 252.3590 251.4833 279.7470 51.8265 0.8714 252.5998 251.7283 279.8527 52.6230 0.8700 252.8254 251.9554 279.9826 53.4505 0.8641 253.0634 252.1993 280.1870 54.2265 0.8553 253.2786 252.4233 280.3677 55.0743 0.8515 253.4979 252.6463 280.6129 55.8403 0.8459 253.6848 252.8389 280.8632 56.6675 0.8374 253.9026 253.0651 281.1312 57.4640 0.8346 254.1682 253.3336 281.4303 58.2608 0.8329 254.4100 253.5771 281.7652 59.0778 0.8265 254.6065 253.7801 282.1445 59.8538 0.8197 254.8097 253.9900 282.4660 60.7018 0.8143 255.0468 254.2325 282.8590 61.4675 0.8076 255.2724 254.4648 283.1943 62.2948 0.8018 255.5179 254.7161 283.5764 63.0915 0.7933 255.7459 254.9526 283.9289 63.8880 0.7871 255.9771 255.1900 284.2650 64.7153 0.7791 256.2044 255.4253 284.5892 65.4815 0.7714 256.4213 255.6499 284.8933 66.3393 0.7661 256.6912 255.9251 285.1953 67.1053 0.7597 256.9102 256.1505 285.4665 67.9225 0.7529 257.1161 256.3632 285.7423 68.7293 0.7466 257.3438 256.5972 285.9662 69.5260 0.7369 257.5357 256.7988 286.1802 70.3533 0.7266 257.7334 257.0067 286.3581 71.1088 0.7169 257.9290 257.2120 286.4917 71.9775 0.7090 258.1569 257.4479 286.6188 72.7430 0.7040 258.3411 257.6371 286.7104 73.5705 0.6975 258.5811 257.8836 286.7829 74.3570 0.6922 258.8184 258.1262 286.8118 75.1533 0.6888 259.0483 258.3595 286.8325 75.9708 0.6845 259.2641 258.5796 286.8423 76.7365 0.6817 259.4867 258.8050 286.8198 77.5948 0.6773 259.7174 259.0401 286.7953 78.3300 0.6716 259.9304 259.2589 286.7376 79.1775 0.6699 260.1494 259.4795 286.6907 79.9538 0.6644 260.3807 259.7164 286.6485 80.7710 0.6564 260.6033 259.9468 286.5981 81.5675 0.6514 260.8410 260.1895 286.5754 82.3645 0.6427 261.0596 260.4168 286.5370 83.1915 0.6380 261.2812 260.6432 286.4548 83.9575 0.6313 261.4903 260.8590 286.4020 84.8055 0.6255 261.7191 261.0936 286.3641 85.5505 0.6226 261.9087 261.2861 286.3274 86.3985 0.6156 262.1374 261.5218 286.2853 87.1645 0.6093 262.3286 261.7194 286.2525 87.9915 0.6030 262.5171 261.9142 286.2722 88.7883 0.5972 262.7065 262.1093 286.3325 89.5850 0.5952 262.9244 262.3292 286.3998 90.4018 0.5896 263.1365 262.5469 286.5236 91.1783 0.5827 263.3205 262.7378 286.6405 92.0363 0.5835 263.5667 262.9831 286.8013 92.8020 0.5819 263.7636 263.1817 286.9728 93.6193 0.5734 264.0128 263.4394 287.1452 94.4260 0.5652 264.2221 263.6569 287.3692 95.2123 0.5575 264.4217 263.8642 287.5969 96.0090 0.5497 264.5867 264.0371 287.8655 96.8055 0.5432 264.7993 264.2561 288.1437 97.6433 0.5363 265.0161 264.4798 288.4487 98.3990 0.5296 265.1946 264.6650 288.7359 99.2568 0.5267 265.4134 264.8867 289.0815 100.0228 0.5265 265.6222 265.0958 289.4095 100.8503 0.5207 265.8479 265.3272 289.7408 101.6468 0.5144 266.0359 265.5216 290.0673 102.4335 0.5073 266.2565 265.7492 290.4049 103.2708 0.4988 266.4727 265.9739 290.7443 104.0268 0.4919 266.6788 266.1869 291.0517 104.8848 0.4853 266.9185 266.4333 291.3682 105.6508 0.4802 267.0976 266.6174 291.6349 106.4783 0.4723 267.2979 266.8256 291.8889 107.2643 0.4638 267.5064 267.0426 292.0883 108.0613 0.4503 267.6989 267.2487 292.2786 108.8885 0.4391 267.9194 267.4803 292.4536 109.6440 0.4325 268.1197 267.6872 292.5989 110.5023 0.4250 268.3466 267.9217 292.7392 111.2373 0.4202 268.5402 268.1199 292.8471 112.0953 0.4178 268.7721 268.3543 292.9310 112.8513 0.4122 268.9595 268.5473 293.0120 113.6885 0.4051 269.1642 268.7591 293.0859 114.4750 0.3946 269.3648 268.9702 293.1200 115.2718 0.3866 269.5677 269.1811 293.1434 116.0990 0.3822 269.8077 269.4255 293.1780 116.8650 0.3794 269.9801 269.6008 293.1551 117.7230 0.3772 270.1758 269.7987 293.1351 118.4785 0.3723 270.3519 269.9796 293.1343 119.3163 0.3666 270.5834 270.2168 293.1095 120.1025 0.3619 270.7638 270.4019 293.0631 120.8993 0.3535 270.9249 270.5714 293.0193 121.7268 0.3475 271.1178 270.7703 292.9582 122.5028 0.3420 271.3128 270.9708 292.9335 123.3510 0.3360 271.5253 271.1893 292.9003 124.0858 0.3302 271.6975 271.3673 292.8769 124.9440 0.3194 271.9048 271.5854 292.8850 125.7100 0.3094 272.0844 271.7750 292.8785 126.5370 0.3046 272.2945 271.9899 292.9141 127.3340 0.2994 272.4962 272.1968 292.9773 128.1305 0.2956 272.6996 272.4040 293.0541 128.9578 0.2965 272.8975 272.6011 293.1347 129.7238 0.2938 273.0917 272.7979 293.2347 130.5715 0.2870 273.2889 273.0019 293.3288 131.3478 0.2820 273.4662 273.1842 293.4925 132.1750 0.2748 273.6478 273.3730 293.6756 132.9715 0.2707 273.8411 273.5704 293.8787 133.7580 0.2627 274.0238 273.7611 294.0830 134.5958 0.2570 274.2453 273.9883 294.3432 135.3510 0.2476 274.4194 274.1718 294.5838 136.2195 0.2380 274.6283 274.3903 294.8612 136.9753 0.2285 274.8118 274.5833 295.1078 137.8128 0.2136 275.0302 274.8166 295.4246 138.5993 0.2071 275.2312 275.0242 295.7315 139.3958 0.2057 275.4149 275.2092 296.0356 140.2233 0.2027 275.6009 275.3982 296.3598 140.9790 0.2004 275.7922 275.5918 296.6520 141.8265 0.1916 276.0019 275.8103 296.9677 142.6028 0.1849 276.2146 276.0297 297.2575 143.4198 0.1782 276.4023 276.2241 297.5399 144.2163 0.1718 276.5843 276.4125 297.8120 145.0130 0.1674 276.7700 276.6026 298.0565 145.8405 0.1635 276.9583 276.7948 298.3007 146.6063 0.1561 277.1523 276.9962 298.5257 147.4543 0.1465 277.3507 277.2042 298.7492 148.2200 0.1380 277.5207 277.3826 298.9079 149.0475 0.1333 277.7129 277.5797 299.0318 149.8340 0.1267 277.9282 277.8015 299.1307 150.6405 0.1210 278.1430 278.0220 299.2292 151.4578 0.1125 278.3161 278.2036 299.3253 152.2238 0.1221 278.4691 278.3470 299.3832 153.0818 0.2382 278.6722 278.4339 299.4339 153.8480 0.2263 278.8488 278.6225 299.4399 154.6750 0.2012 279.0718 278.8706 299.4747 155.4618 0.1793 279.2597 279.0804 299.4957 156.2685 0.1587 279.4474 279.2887 299.4600 157.0855 0.1422 279.6439 279.5017 299.4672 157.8518 0.1310 279.8029 279.6718 299.4632 158.7095 0.1193 280.0013 279.8819 299.4270 159.4755 0.1128 280.1550 280.0423 299.4198 160.3030 0.1075 280.3518 280.2443 299.3909 161.0890 0.1016 280.5198 280.4182 299.3934 161.8963 0.0902 280.7025 280.6122 299.4141 162.7133 0.0838 280.8927 280.8089 299.4135 163.4790 0.0764 281.0568 280.9804 299.3970 164.3373 0.0684 281.2453 281.1769 299.4148 165.1133 0.0633 281.4180 281.3547 299.4523 165.9405 0.0565 281.6267 281.5702 299.5028 166.7373 0.0422 281.8041 281.7619 299.5626 167.5235 0.0280 281.9889 281.9609 299.6353 168.3613 0.0200 282.1960 282.1760 299.7310 169.1170 0.0157 282.3572 282.3415 299.8394 169.9750 0.0069 282.5918 282.5849 300.0009 170.7410 -0.0023 282.7867 282.7890 300.1568 171.5683 -0.0095 282.9709 282.9804 300.3727 172.3548 -0.0150 283.1501 283.1651 300.6075 173.1515 -0.0223 283.3153 283.3375 300.8326 173.9785 -0.0290 283.4999 283.5289 301.0699 174.7345 -0.0352 283.6542 283.6895 301.2816 175.5925 -0.0486 283.8322 283.8808 301.5498 176.3583 -0.0552 284.0418 284.0970 301.7887 177.1758 -0.0617 284.2417 284.3034 302.0763 177.9413 -0.0669 284.4092 284.4761 302.3314 178.7688 -0.0750 284.5832 284.6583 302.6166 179.5655 -0.0827 284.7449 284.8275 302.8842 180.3515 -0.0901 284.9109 285.0010 303.1899 181.1893 -0.0993 285.1122 285.2115 303.4982 181.9450 -0.1066 285.3096 285.4161 303.7458 182.8030 -0.1133 285.4799 285.5932 304.0137 183.5690 -0.1161 285.6496 285.7656 304.2467 184.3963 -0.0948 285.8532 285.9480 304.4799 185.1930 -0.0689 286.0401 286.1090 304.6613 185.9795 -0.0739 286.2196 286.2935 304.8144 186.8168 -0.0857 286.4111 286.4968 304.9756 187.5725 -0.0977 286.5618 286.6596 305.1068 188.4103 -0.1051 286.7370 286.8422 305.2770 189.1655 -0.1114 286.9101 287.0215 305.3737 190.0343 -0.1214 287.0939 287.2153 305.4950 190.7898 -0.1319 287.2535 287.3854 305.5717 191.6170 -0.1365 287.4303 287.5668 305.6316 192.4140 -0.1429 287.6114 287.7543 305.6854 193.2205 -0.1496 287.8008 287.9504 305.7331 194.0378 -0.1518 287.9832 288.1350 305.7621 194.8038 -0.1593 288.1556 288.3149 305.8035 195.6615 -0.1687 288.3235 288.4922 305.8439 196.4073 -0.1762 288.5213 288.6974 305.8630 197.2550 -0.1865 288.7286 288.9151 305.8612 198.0208 -0.1943 288.8970 289.0913 305.8569 198.8483 -0.1979 289.1101 289.3080 305.8604 199.6448 -0.2017 289.2646 289.4662 305.8950 200.4415 -0.2102 289.4343 289.6445 305.9000 201.2588 -0.2178 289.5852 289.8030 305.9203 202.0348 -0.2213 289.7573 289.9786 305.9433 202.8930 -0.2228 289.9566 290.1794 305.9791 203.6485 -0.2245 290.1242 290.3487 306.0272 204.4758 -0.2266 290.2902 290.5168 306.0731 205.2725 -0.2339 290.4610 290.6949 306.1595 206.0588 -0.2375 290.6390 290.8765 306.2512 206.8860 -0.2416 290.8343 291.0759 306.3642 207.6520 -0.2506 291.0027 291.2533 306.4790 208.4998 -0.2537 291.1955 291.4491 306.6339 209.2658 -0.2565 291.3548 291.6114 306.7636 210.0933 -0.2629 291.5385 291.8014 306.9285 210.8588 -0.2665 291.7116 291.9782 307.1087 211.6760 -0.2646 291.8705 292.1351 307.3040 212.4830 -0.2704 292.0484 292.3188 307.5106 213.2690 -0.2706 292.2218 292.4924 307.7019 214.0965 -0.2726 292.4008 292.6734 307.9221 214.8625 -0.2799 292.5684 292.8483 308.1781 215.7205 -0.2863 292.7592 293.0455 308.4485 216.4865 -0.2934 292.9167 293.2101 308.6859 217.3035 -0.2987 293.0937 293.3924 308.9219 218.1103 -0.3056 293.2915 293.5971 309.1951 218.8968 -0.3098 293.4786 293.7884 309.4725 219.7240 -0.3104 293.6748 293.9852 309.7418 220.4900 -0.3155 293.8339 294.1494 309.9638 221.3483 -0.3200 294.0295 294.3495 310.2259 222.2060 -0.3230 294.2149 294.5379 310.4795 222.9620 -0.3241 294.3785 294.7026 310.6918 223.7995 -0.3306 294.5638 294.8944 310.9241 224.5858 -0.3387 294.7236 295.0623 311.0949 225.3825 -0.3474 294.9060 295.2533 311.2530 226.2098 -0.3575 295.1056 295.4631 311.3976 226.9860 -0.3655 295.2734 295.6389 311.5392 227.8340 -0.3749 295.4546 295.8295 311.6695 228.6610 -0.3813 295.6073 295.9887 311.7838 229.6733 -0.3852 295.8310 296.2163 311.9338 230.4698 -0.3893 295.9727 296.3620 312.0294 231.2663 -0.3919 296.1413 296.5332 312.1018 232.0838 -0.3961 296.3196 296.7157 312.1542 232.8595 -0.4000 296.4743 296.8743 312.1686 233.7178 -0.4039 296.6723 297.0763 312.1949 234.4838 -0.4083 296.8433 297.2516 312.2123 235.3005 -0.4182 297.0037 297.4219 312.2324 236.0665 -0.4224 297.1588 297.5812 312.2401 236.8940 -0.4301 297.3148 297.7449 312.2493 237.6803 -0.4360 297.4898 297.9258 312.2806 238.4770 -0.4384 297.6749 298.1133 312.3184 239.2940 -0.4388 297.8838 298.3226 312.3396 240.0598 -0.4411 298.0611 298.5022 312.3488 240.9180 -0.4420 298.2393 298.6813 312.4017 241.6838 -0.4476 298.4036 298.8511 312.4462 242.5008 -0.4555 298.5651 299.0206 312.5141 243.3080 -0.4604 298.7404 299.2008 312.5639 244.0940 -0.4707 298.9268 299.3975 312.6186 244.9215 -0.4759 299.1035 299.5794 312.6728 245.6875 -0.4870 299.2356 299.7225 312.7760 246.5453 -0.4974 299.3984 299.8958 312.9147 247.3113 -0.5078 299.5573 300.0652 313.0364 248.1285 -0.5173 299.7322 300.2495 313.1900 248.9353 -0.5252 299.9019 300.4271 313.3671 249.7220 -0.5336 300.0607 300.5943 313.5416 250.5490 -0.5389 300.2416 300.7804 313.7606 251.3150 -0.5453 300.4120 300.9573 313.9712 252.1733 -0.5489 300.6059 301.1548 314.2306 252.9390 -0.5552 300.7483 301.3035 314.4500 253.7563 -0.5651 300.9084 301.4735 314.6980 254.5630 -0.5752 301.0747 301.6500 314.9375 255.3598 -0.5833 301.2521 301.8355 315.1794 256.1873 -0.5892 301.4329 302.0221 315.4268 256.9528 -0.5945 301.5717 302.1661 315.6627 257.7803 -0.5972 301.7386 302.3358 315.9237 258.5565 -0.6035 301.8911 302.4946 316.1482 259.4043 -0.6141 302.0660 302.6801 316.3884 260.1703 -0.6202 302.2206 302.8408 316.6038 260.9975 -0.6223 302.4122 303.0346 316.8393 261.7940 -0.6253 302.5840 303.2093 317.0463 262.5910 -0.6309 302.7340 303.3648 317.2252 263.4180 -0.6377 302.9096 303.5472 317.4006 264.1840 -0.6441 303.0641 303.7081 317.5531 265.0423 -0.6491 303.2461 303.8952 317.7095 265.8078 -0.6559 303.3726 304.0284 317.8515 266.6355 -0.6621 303.5612 304.2233 317.9695 267.4320 -0.6655 303.7544 304.4199 318.0623 268.2285 -0.6740 303.9340 304.6080 318.1501 269.0458 -0.6784 304.1185 304.7969 318.2685 269.8115 -0.6818 304.2831 304.9649 318.3543 270.6390 -0.6853 304.4847 305.1700 318.3990 271.3948 -0.6902 304.6369 305.3271 318.4049 272.2525 -0.6964 304.7841 305.4805 318.4581 273.0188 -0.6982 304.9612 305.6594 318.4828 273.8460 -0.7028 305.1592 305.8620 318.5105 274.6323 -0.7072 305.3290 306.0362 318.5620 275.4395 -0.7121 305.4708 306.1829 318.6122 276.2255 -0.7150 305.6393 306.3542 318.6296 277.0223 -0.7218 305.7962 306.5180 318.6728 277.8498 -0.7303 305.9327 306.6630 318.7521 278.6155 -0.7395 306.0916 306.8311 318.7677 279.4738 -0.7372 306.3058 307.0430 318.8039 280.2293 -0.7379 306.4657 307.2036 318.8417 281.0670 -0.7389 306.6208 307.3597 318.9112 281.8535 -0.7435 306.7770 307.5205 318.9926 282.6498 -0.7467 306.9368 307.6835 319.0710 283.4773 -0.7483 307.0718 307.8201 319.1780 284.2433 -0.7542 307.2172 307.9714 319.2705 285.1013 -0.7572 307.4378 308.1950 319.3924 285.8570 -0.7633 307.6063 308.3695 319.5281 286.6945 -0.7698 307.8005 308.5703 319.6904 287.4810 -0.7723 307.9539 308.7262 319.8402 288.2778 -0.7757 308.0993 308.8750 319.9997 289.1050 -0.7796 308.2856 309.0652 320.1974 289.8713 -0.7835 308.4617 309.2452 320.4010 290.7290 -0.7877 308.6056 309.3932 320.6451 291.4850 -0.7888 308.7520 309.5409 320.8622 292.3225 -0.7981 308.9163 309.7144 321.0946 293.1088 -0.8072 309.0730 309.8802 321.3461 293.9058 -0.8128 309.2497 310.0625 321.5961 294.7023 -0.8159 309.4185 310.2344 321.8441 295.5093 -0.8197 309.6215 310.4412 322.0919 296.3263 -0.8252 309.7946 310.6198 322.3474 297.0923 -0.8302 309.9619 310.7921 322.5532 297.9505 -0.8366 310.1288 310.9655 322.7687 298.7160 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