DTA measure 1gyors2 Date: 2026317:1127 Lower limit = 220.0 C Upper limit = 440.0 C Rate = 8.00 C/min Mtime = 1648.81 s Mass = 1166.200 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4508 -5.8590 468.8958 474.7548 431.1962 4.0594 -5.8522 468.7888 474.6410 430.8396 5.6626 -5.8353 468.6751 474.5105 430.6174 7.2661 -5.8303 468.5448 474.3751 430.5254 8.8591 -5.8238 468.4061 474.2299 430.5650 10.4574 -5.8168 468.3000 474.1168 430.7659 12.0660 -5.8140 468.2343 474.0484 431.0829 13.6694 -5.8127 468.0731 473.8858 431.3883 15.2933 -5.8119 467.9726 473.7845 431.7325 16.8968 -5.8085 467.8646 473.6732 432.0492 18.5050 -5.8036 467.7389 473.5426 432.2971 20.1085 -5.8016 467.6066 473.4082 432.4370 21.7171 -5.7966 467.5005 473.2971 432.5030 23.3101 -5.7885 467.4221 473.2106 432.4803 24.9136 -5.7831 467.3095 473.0926 432.3284 26.5223 -5.7834 467.1668 472.9502 432.0659 28.1408 -5.7806 467.0823 472.8628 431.7391 29.7545 -5.7734 466.9622 472.7356 431.3457 31.3578 -5.7638 466.8551 472.6189 430.9045 32.9663 -5.7569 466.7657 472.5226 430.4016 34.5695 -5.7485 466.6685 472.4170 429.8893 36.1831 -5.7410 466.5277 472.2686 429.3630 37.7814 -5.7274 466.4133 472.1407 428.8446 39.3949 -5.7110 466.2858 471.9969 428.3197 41.0035 -5.7021 466.1910 471.8931 427.8488 42.6016 -5.6974 466.1223 471.8197 427.4250 44.2050 -5.6904 466.0135 471.7039 427.0402 45.8136 -5.6816 465.9184 471.6000 426.7276 47.4170 -5.6726 465.7600 471.4327 426.5017 49.0256 -5.6595 465.6511 471.3107 426.3101 50.6445 -5.6501 465.5330 471.1831 426.1730 52.2530 -5.6382 465.3954 471.0336 426.1003 53.8564 -5.6295 465.2663 470.8957 426.0820 55.4649 -5.6216 465.1512 470.7728 426.0617 57.0631 -5.6182 465.0562 470.6744 426.0659 58.6768 -5.6122 464.9200 470.5322 426.0736 60.2803 -5.6076 464.7672 470.3748 426.0617 61.8939 -5.6101 464.6337 470.2438 425.9970 63.5126 -5.6077 464.5102 470.1179 425.9353 65.1263 -5.6014 464.3850 469.9863 425.8451 66.7295 -5.5976 464.2322 469.8298 425.7035 68.3433 -5.5890 464.1109 469.6999 425.5070 69.9464 -5.5814 463.9366 469.5180 425.2739 71.5241 -5.5750 463.8002 469.3752 425.0004 73.1328 -5.5551 463.6678 469.2229 424.6465 74.7359 -5.5498 463.5299 469.0797 424.3525 76.3548 -5.5450 463.3896 468.9346 424.0044 77.9579 -5.5366 463.2490 468.7856 423.6861 79.5614 -5.5296 463.1397 468.6693 423.3286 81.1700 -5.5227 462.9982 468.5209 422.9580 82.7733 -5.5173 462.8376 468.3549 422.6406 84.3716 -5.5085 462.7076 468.2161 422.3455 85.9751 -5.5004 462.5671 468.0675 422.0573 87.5835 -5.4966 462.4415 467.9381 421.8111 89.2024 -5.4944 462.2816 467.7760 421.5712 90.8160 -5.4872 462.1569 467.6441 421.3667 92.4193 -5.4864 462.0217 467.5081 421.2440 94.0074 -5.4840 461.8712 467.3552 421.1099 95.6314 -5.4821 461.6998 467.1819 420.9928 97.2193 -5.4801 461.5185 466.9986 420.8674 98.8484 -5.4795 461.3637 466.8431 420.7349 100.4364 -5.4746 461.2094 466.6839 420.5944 102.0500 -5.4683 461.0635 466.5318 420.4563 103.6535 -5.4680 460.9034 466.3714 420.3554 105.2569 -5.4638 460.7826 466.2464 420.2143 106.8500 -5.4524 460.6391 466.0914 420.0377 108.4534 -5.4471 460.4244 465.8716 419.8439 110.0618 -5.4437 460.2321 465.6759 419.6229 111.6653 -5.4389 460.0825 465.5214 419.3929 113.2685 -5.4371 459.9029 465.3400 419.1695 114.8924 -5.4312 459.7275 465.1587 418.9312 116.4959 -5.4283 459.5425 464.9708 418.6844 118.1044 -5.4215 459.3836 464.8051 418.4336 119.7129 -5.4146 459.2377 464.6523 418.1619 121.3061 -5.4120 459.1103 464.5223 417.9109 122.9146 -5.4084 458.9631 464.3715 417.6445 124.5230 -5.4042 458.7810 464.1852 417.3809 126.1264 -5.4013 458.6118 464.0131 417.1292 127.7553 -5.3940 458.4490 463.8431 416.8587 129.3588 -5.3925 458.3019 463.6944 416.6060 130.9673 -5.3825 458.1265 463.5091 416.4005 132.5705 -5.3785 457.9997 463.3782 416.1983 134.1689 -5.3707 457.8265 463.1972 415.9973 135.7771 -5.3625 457.6426 463.0052 415.8036 137.3755 -5.3568 457.4465 462.8033 415.6219 138.9943 -5.3540 457.2434 462.5974 415.4208 140.6028 -5.3483 457.0676 462.4159 415.2632 142.2061 -5.3387 456.9255 462.2642 415.0886 143.8144 -5.3344 456.7574 462.0918 414.9035 145.4180 -5.3328 456.5519 461.8847 414.7453 147.0264 -5.3333 456.3534 461.6867 414.5864 148.6299 -5.3324 456.1803 461.5127 414.4220 150.2333 -5.3279 455.9786 461.3065 414.2487 151.8520 -5.3227 455.7711 461.0938 414.0370 153.4655 -5.3175 455.5831 460.9006 413.8492 155.0690 -5.3159 455.3994 460.7153 413.6227 156.6826 -5.3075 455.2341 460.5416 413.4078 158.2860 -5.2995 455.0979 460.3974 413.1761 159.8946 -5.2934 454.9054 460.1988 412.9254 161.5030 -5.2853 454.7016 459.9869 412.6928 163.1270 -5.2766 454.5443 459.8209 412.4552 164.7354 -5.2727 454.4051 459.6778 412.2104 166.3386 -5.2783 454.1939 459.4723 412.0118 167.9370 -5.2709 453.9989 459.2698 411.7860 169.5299 -5.2710 453.8423 459.1133 411.5548 171.1231 -5.2695 453.6854 458.9548 411.3374 172.7318 -5.2624 453.5044 458.7668 411.1246 174.3351 -5.2526 453.3598 458.6125 410.9087 175.9385 -5.2461 453.1888 458.4349 410.6807 177.5470 -5.2411 452.9898 458.2309 410.4678 179.1555 -5.2334 452.8206 458.0540 410.2557 180.7641 -5.2248 452.6183 457.8432 410.0234 182.3726 -5.2230 452.4354 457.6584 409.8013 183.9810 -5.2167 452.2361 457.4528 409.5906 185.5693 -5.2081 452.0183 457.2265 409.3933 187.1776 -5.2073 451.7648 456.9721 409.2040 188.7861 -5.2026 451.5738 456.7764 409.0130 190.3948 -5.1985 451.3917 456.5902 408.8169 192.0031 -5.1950 451.2233 456.4182 408.6439 193.6271 -5.1864 451.0485 456.2349 408.4456 195.2204 -5.1797 450.8780 456.0577 408.2454 196.8288 -5.1742 450.7194 455.8936 408.0855 198.4321 -5.1689 450.5101 455.6790 407.9140 200.0355 -5.1673 450.2970 455.4642 407.6985 201.6286 -5.1606 450.1003 455.2609 407.4852 203.2270 -5.1531 449.9107 455.0638 407.2807 204.8355 -5.1495 449.7230 454.8725 407.0491 206.4389 -5.1444 449.5477 454.6921 406.8159 208.0629 -5.1417 449.3310 454.4726 406.5732 209.6661 -5.1339 449.1578 454.2917 406.3516 211.2593 -5.1307 448.9905 454.1212 406.1505 212.8678 -5.1244 448.7707 453.8951 405.9071 214.4710 -5.1148 448.5572 453.6720 405.6523 216.0796 -5.1072 448.3753 453.4825 405.4147 217.6879 -5.1052 448.1889 453.2941 405.2038 219.2965 -5.0975 447.9933 453.0908 404.9679 220.9154 -5.0912 447.7754 452.8667 404.7383 222.5238 -5.0834 447.5576 452.6410 404.5201 224.1324 -5.0763 447.3632 452.4395 404.3035 225.7408 -5.0644 447.1803 452.2447 404.0852 227.3441 -5.0599 446.9937 452.0536 403.9010 228.9579 -5.0563 446.8075 451.8638 403.6912 230.5561 -5.0528 446.6207 451.6736 403.4935 232.1698 -5.0491 446.4172 451.4663 403.2670 233.7784 -5.0447 446.2318 451.2765 403.0635 235.3764 -5.0385 446.0393 451.0778 402.8882 236.9800 -5.0327 445.8363 450.8690 402.6919 238.5731 -5.0269 445.6477 450.6746 402.5153 240.1764 -5.0255 445.4305 450.4561 402.3204 241.7849 -5.0196 445.2574 450.2770 402.0982 243.3936 -5.0151 445.0583 450.0734 401.8900 244.9968 -5.0080 444.8187 449.8268 401.6533 246.6208 -5.0000 444.5972 449.5972 401.4602 248.2295 -4.9954 444.4398 449.4352 401.2432 249.8378 -4.9862 444.2249 449.2110 401.0592 251.4464 -4.9788 444.0117 448.9904 400.8547 253.0500 -4.9731 443.7958 448.7689 400.6235 254.6584 -4.9694 443.5901 448.5595 400.3735 256.2670 -4.9697 443.3686 448.3383 400.1684 257.8910 -4.9600 443.1634 448.1234 399.9571 259.4943 -4.9550 442.9741 447.9291 399.7190 261.1080 -4.9503 442.7578 447.7081 399.4873 262.7064 -4.9442 442.5509 447.4951 399.2868 264.3045 -4.9381 442.3558 447.2939 399.0460 265.8926 -4.9329 442.1239 447.0569 398.8150 267.4959 -4.9240 441.9245 446.8485 398.6508 269.1044 -4.9157 441.7324 446.6480 398.4555 270.7233 -4.9122 441.5354 446.4476 398.2765 272.3266 -4.9003 441.3379 446.2382 398.0531 273.9351 -4.8931 441.1264 446.0195 397.8346 275.5233 -4.8895 440.9740 445.8635 397.6183 277.1316 -4.8874 440.7732 445.6606 397.4325 278.7351 -4.8824 440.5485 445.4309 397.2081 280.3438 -4.8747 440.3489 445.2237 397.0043 281.9469 -4.8654 440.1414 445.0068 396.8182 283.5760 -4.8550 439.9364 444.7914 396.5830 285.1795 -4.8472 439.7043 444.5515 396.4054 286.7929 -4.8447 439.5249 444.3696 396.1946 288.3964 -4.8425 439.3068 444.1493 395.9802 289.9946 -4.8413 439.0918 443.9331 395.7870 291.5980 -4.8397 438.9042 443.7439 395.5820 293.2065 -4.8399 438.7160 443.5559 395.3665 294.8098 -4.8361 438.4935 443.3296 395.1650 296.4234 -4.8273 438.2919 443.1192 394.9628 298.0266 -4.8187 438.0878 442.9065 394.7542 299.6148 -4.8158 437.8665 442.6823 394.5483 301.2181 -4.8067 437.6464 442.4531 394.3146 302.8265 -4.7951 437.4725 442.2676 394.0862 304.4299 -4.7888 437.2703 442.0591 393.8675 306.0385 -4.7818 437.0921 441.8738 393.6236 307.6418 -4.7707 436.8712 441.6419 393.3972 309.2401 -4.7632 436.6411 441.4044 393.1901 310.8589 -4.7633 436.4088 441.1720 392.9833 312.4623 -4.7570 436.1848 440.9418 392.7747 314.0709 -4.7560 435.9918 440.7478 392.5645 315.6794 -4.7525 435.8002 440.5527 392.3354 317.2878 -4.7434 435.6070 440.3503 392.1064 318.8964 -4.7319 435.4054 440.1374 391.8842 320.5050 -4.7294 435.1798 439.9092 391.6746 322.1135 -4.7281 434.9919 439.7200 391.4693 323.7271 -4.7229 434.7692 439.4921 391.2638 325.3303 -4.7147 434.5637 439.2784 391.0124 326.9390 -4.7087 434.3778 439.0865 390.8097 328.5374 -4.7032 434.1831 438.8862 390.6309 330.1355 -4.6951 433.9713 438.6664 390.4299 331.7390 -4.6927 433.7160 438.4087 390.2676 333.3475 -4.6863 433.4916 438.1779 390.0828 334.9458 -4.6824 433.2658 437.9482 389.9110 336.5646 -4.6757 433.0416 437.7173 389.7257 338.1730 -4.6641 432.8384 437.5025 389.5148 339.7764 -4.6521 432.6474 437.2995 389.3216 341.3850 -4.6426 432.4708 437.1134 389.1190 342.9883 -4.6390 432.2724 436.9115 388.9113 344.6019 -4.6362 432.0951 436.7313 388.7167 346.2051 -4.6323 431.8878 436.5201 388.5002 347.8290 -4.6278 431.6233 436.2512 388.2690 349.4376 -4.6189 431.4214 436.0403 388.0268 351.0460 -4.6120 431.2327 435.8447 387.7895 352.6545 -4.6094 431.0454 435.6548 387.5617 354.2631 -4.6031 430.8139 435.4169 387.3378 355.8715 -4.5933 430.5850 435.1783 387.1445 357.4853 -4.5884 430.3502 434.9386 386.8848 359.0886 -4.5874 430.0945 434.6819 386.6385 360.6868 -4.5761 429.8858 434.4619 386.4226 362.2955 -4.5723 429.6970 434.2693 386.1707 363.8834 -4.5695 429.5149 434.0844 385.9726 365.4919 -4.5610 429.3209 433.8819 385.7474 367.0953 -4.5522 429.1351 433.6873 385.5408 368.6985 -4.5449 428.9175 433.4624 385.3471 370.3071 -4.5381 428.7152 433.2532 385.1546 371.9158 -4.5320 428.4952 433.0271 384.9388 373.5395 -4.5256 428.2595 432.7851 384.7217 375.1431 -4.5193 428.0314 432.5507 384.4916 376.7518 -4.5161 427.7770 432.2930 384.3215 378.3551 -4.5068 427.5595 432.0663 384.1226 379.9636 -4.4978 427.3930 431.8908 383.9094 381.5569 -4.4938 427.1798 431.6736 383.7531 383.1654 -4.4884 426.9751 431.4636 383.5971 384.7688 -4.4784 426.7380 431.2164 383.3926 386.3979 -4.4719 426.5556 431.0275 383.1688 388.0011 -4.4642 426.3648 430.8290 382.9793 389.6148 -4.4656 426.1459 430.6115 382.7800 391.1975 -4.4591 425.9619 430.4210 382.5653 392.8009 -4.4556 425.7488 430.2045 382.3579 394.4094 -4.4489 425.5586 430.0075 382.1509 396.0126 -4.4385 425.3186 429.7572 381.9138 397.6058 -4.4322 425.1011 429.5334 381.7108 399.2091 -4.4240 424.8623 429.2863 381.4761 400.8278 -4.4186 424.6643 429.0830 381.2131 402.4259 -4.4113 424.4651 428.8764 380.9855 404.0293 -4.4083 424.2476 428.6559 380.7387 405.6481 -4.4042 424.0486 428.4528 380.5022 407.2566 -4.3986 423.7969 428.1955 380.2385 408.8600 -4.3887 423.5372 427.9259 380.0111 410.4686 -4.3832 423.3301 427.7134 379.7782 412.0771 -4.3788 423.1408 427.5196 379.5839 413.6651 -4.3708 422.9262 427.2970 379.3905 415.2943 -4.3638 422.7101 427.0739 379.1462 416.9028 -4.3605 422.5138 426.8743 378.9562 418.5164 -4.3556 422.3425 426.6981 378.7575 420.1250 -4.3457 422.1351 426.4808 378.6053 421.7333 -4.3400 421.8930 426.2330 378.4092 423.3316 -4.3372 421.6927 426.0298 378.2304 424.9299 -4.3232 421.4945 425.8177 378.0674 426.5229 -4.3130 421.2820 425.5950 377.8736 428.1263 -4.3067 421.0828 425.3896 377.7103 429.7396 -4.3010 420.8938 425.1947 377.5539 431.3483 -4.2908 420.6832 424.9740 377.3527 432.9516 -4.2917 420.4820 424.7737 377.1286 434.5550 -4.2837 420.2732 424.5569 376.9139 436.1635 -4.2781 420.0542 424.3323 376.7038 437.7668 -4.2773 419.7760 424.0533 376.4903 439.3804 -4.2677 419.5146 423.7822 376.2823 440.9684 -4.2617 419.3350 423.5966 376.0171 442.5973 -4.2529 419.1335 423.3864 375.7324 444.2008 -4.2444 418.9275 423.1719 375.4979 445.8040 -4.2369 418.6913 422.9281 375.2507 447.4176 -4.2333 418.4582 422.6915 375.0290 449.0210 -4.2286 418.2610 422.4896 374.7945 450.6244 -4.2219 418.0506 422.2725 374.5385 452.2381 -4.2231 417.8452 422.0683 374.2922 453.8415 -4.2140 417.6428 421.8568 374.0945 455.4653 -4.2032 417.4229 421.6261 373.8555 457.0636 -4.1975 417.2144 421.4119 373.6704 458.6668 -4.1884 416.9971 421.1855 373.4600 460.2703 -4.1815 416.8001 420.9816 373.2432 461.8685 -4.1787 416.6129 420.7916 373.0449 463.5230 -4.1769 416.3753 420.5522 372.8444 465.1469 -4.1656 416.1602 420.3259 372.6769 466.7399 -4.1579 415.9229 420.0808 372.4586 468.3485 -4.1518 415.7011 419.8529 372.2634 469.9570 -4.1475 415.5132 419.6608 372.1106 471.5604 -4.1400 415.3090 419.4489 371.9367 473.1844 -4.1387 415.0718 419.2105 371.7449 474.7929 -4.1319 414.8653 418.9972 371.5501 476.3963 -4.1228 414.6403 418.7631 371.3386 478.0049 -4.1130 414.4076 418.5206 371.1343 479.6085 -4.1019 414.1590 418.2608 370.9012 481.2219 -4.0916 413.9744 418.0659 370.6893 482.8305 -4.0881 413.7993 417.8874 370.5016 484.4444 -4.0784 413.5839 417.6623 370.2928 486.0630 -4.0767 413.3593 417.4360 370.0537 487.6716 -4.0722 413.1457 417.2179 369.8406 489.2700 -4.0659 412.9664 417.0322 369.6325 490.8731 -4.0584 412.7382 416.7966 369.4095 492.4766 -4.0483 412.5148 416.5631 369.1718 494.0800 -4.0409 412.2919 416.3328 368.9266 495.6884 -4.0318 412.0744 416.1062 368.6733 497.2919 -4.0321 411.8695 415.9016 368.4188 498.9156 -4.0277 411.6670 415.6947 368.2017 500.5191 -4.0283 411.4531 415.4814 367.9953 502.1225 -4.0219 411.2132 415.2350 367.7746 503.7310 -4.0103 411.0043 415.0147 367.5885 505.3396 -4.0024 410.8018 414.8042 367.3528 506.9483 -3.9894 410.6298 414.6192 367.1784 508.5720 -3.9794 410.4273 414.4067 366.9524 510.1806 -3.9761 410.1771 414.1532 366.7011 511.7839 -3.9674 409.9733 413.9407 366.4892 513.3975 -3.9598 409.7483 413.7081 366.3055 515.0010 -3.9528 409.5187 413.4715 366.1440 516.6145 -3.9484 409.3025 413.2509 365.9540 518.2179 -3.9470 409.1071 413.0541 365.7340 519.8314 -3.9430 408.9130 412.8560 365.5540 521.4296 -3.9370 408.6932 412.6301 365.3755 523.0331 -3.9319 408.4282 412.3601 365.1676 524.6364 -3.9268 408.2025 412.1293 364.9740 526.2398 -3.9224 407.9782 411.9007 364.7621 527.8484 -3.9156 407.7766 411.6922 364.5638 529.4516 -3.9074 407.5838 411.4912 364.3369 531.0500 -3.9020 407.3880 411.2900 364.1178 532.6740 -3.8934 407.1562 411.0496 363.8988 534.2773 -3.8881 406.9209 410.8090 363.6780 535.8859 -3.8761 406.7061 410.5821 363.4471 537.4894 -3.8676 406.5020 410.3695 363.2764 539.0978 -3.8609 406.2973 410.1582 363.0679 540.7064 -3.8612 406.0451 409.9064 362.8631 542.3148 -3.8529 405.8140 409.6669 362.6692 543.9335 -3.8451 405.6093 409.4544 362.4608 545.5473 -3.8428 405.4120 409.2548 362.2482 547.1504 -3.8404 405.2363 409.0767 362.0450 548.7643 -3.8326 405.0593 408.8919 361.8337 550.3676 -3.8260 404.8544 408.6804 361.6150 551.9709 -3.8199 404.6370 408.4569 361.3921 553.5796 -3.8169 404.4052 408.2220 361.1754 555.1780 -3.8142 404.1767 407.9909 360.9758 556.7864 -3.8025 403.9794 407.7819 360.7618 558.3898 -3.7920 403.7782 407.5703 360.5466 559.9933 -3.7814 403.5596 407.3410 360.3090 561.6019 -3.7792 403.3106 407.0898 360.0626 563.2053 -3.7727 403.0976 406.8702 359.8223 564.8139 -3.7657 402.8643 406.6300 359.5637 566.4174 -3.7608 402.6348 406.3956 359.3193 568.0413 -3.7546 402.4214 406.1761 359.1117 569.6448 -3.7461 402.2028 405.9490 358.8810 571.2534 -3.7397 401.9777 405.7174 358.6581 572.8618 -3.7307 401.7439 405.4746 358.4699 574.4499 -3.7232 401.5274 405.2506 358.2907 576.0739 -3.7163 401.3208 405.0372 358.0826 577.6770 -3.7112 401.1201 404.8313 357.8793 579.3061 -3.7061 400.8873 404.5934 357.7071 580.8941 -3.6993 400.6716 404.3709 357.4938 582.5078 -3.6922 400.4747 404.1669 357.3111 584.1111 -3.6910 400.2690 403.9601 357.1186 585.7196 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