DTA measure 1gyors.dat Date: 2025930:1125 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.54 s Mass = 967.800 mg data_number = 1261 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1683 -37.1234 288.7911 325.9145 288.3649 1.9543 -37.1232 288.5848 325.7080 288.2387 2.7510 -37.1116 288.3795 325.4912 288.1112 3.5785 -37.0843 288.1938 325.2780 287.9913 4.3440 -37.0454 288.0032 325.0486 287.8850 5.1920 -36.9888 287.8573 324.8461 287.7690 5.9580 -36.9305 287.7360 324.6666 287.6368 6.7853 -36.8543 287.6424 324.4967 287.4833 7.5718 -36.7730 287.5301 324.3031 287.3559 8.3785 -36.6776 287.4252 324.1027 287.2047 9.1650 -36.5739 287.3543 323.9282 287.0387 9.9615 -36.4615 287.3176 323.7791 286.8956 10.7888 -36.3347 287.2788 323.6135 286.7421 11.5548 -36.2117 287.2243 323.4360 286.5926 12.4130 -36.0663 287.1726 323.2389 286.4321 13.1683 -35.9283 287.1585 323.0868 286.2530 14.0060 -35.7682 287.1460 322.9141 286.0970 14.7925 -35.6140 287.1287 322.7426 285.9957 15.5888 -35.4460 287.0777 322.5237 285.8635 16.4165 -35.2679 287.0821 322.3500 285.7385 17.1823 -35.0982 287.0825 322.1807 285.6120 18.0400 -34.9008 287.0746 321.9754 285.4645 18.7958 -34.7247 287.0848 321.8095 285.3631 19.6335 -34.5193 287.0718 321.5911 285.2222 20.4198 -34.3198 287.0950 321.4148 285.0721 21.2165 -34.1170 287.1544 321.2714 284.9232 22.0438 -33.9019 287.2157 321.1176 284.7503 22.8198 -33.6980 287.2872 320.9852 284.6074 23.6678 -33.4693 287.3328 320.8021 284.4625 24.4335 -33.2560 287.4188 320.6748 284.3301 25.2608 -33.0257 287.4761 320.5018 284.1898 26.0575 -32.7994 287.5112 320.3105 284.0686 26.8540 -32.5714 287.5713 320.1427 283.9258 27.6710 -32.3385 287.6337 319.9723 283.7701 28.4473 -32.1139 287.6938 319.8076 283.6454 29.3053 -31.8604 287.7872 319.6476 283.5037 30.0710 -31.6317 287.8814 319.5131 283.3634 30.8883 -31.3837 287.9873 319.3710 283.1914 31.6950 -31.1349 288.0503 319.1851 283.0270 32.4813 -30.8938 288.1450 319.0388 282.8922 33.3088 -30.6451 288.2768 318.9219 282.7390 34.0745 -30.4096 288.3497 318.7592 282.6473 34.9223 -30.1473 288.4607 318.6081 282.5011 35.6780 -29.9139 288.5533 318.4672 282.3685 36.5155 -29.6499 288.6942 318.3441 282.2368 37.3018 -29.3980 288.8027 318.2007 282.1360 38.0883 -29.1463 288.8746 318.0210 281.9860 38.8950 -28.8908 288.9938 317.8846 281.8381 39.6813 -28.6442 289.1368 317.7810 281.6903 40.5088 -28.3871 289.2610 317.6482 281.5934 41.2745 -28.1437 289.3682 317.5119 281.5185 42.1325 -27.8680 289.5026 317.3707 281.3835 42.8985 -27.6269 289.6328 317.2597 281.2990 43.7155 -27.3695 289.7580 317.1275 281.2562 44.5223 -27.1106 289.8780 316.9886 281.1900 45.3088 -26.8614 289.9740 316.8354 281.1255 46.1360 -26.6001 290.1105 316.7106 281.0867 46.9018 -26.3589 290.2300 316.5889 281.0498 47.7703 -26.0872 290.3626 316.4498 281.0469 48.5258 -25.8546 290.4942 316.3488 281.0442 49.3528 -25.5969 290.6092 316.2061 281.0723 50.1293 -25.3555 290.6849 316.0404 281.1374 50.9565 -25.1010 290.7767 315.8778 281.2533 51.7325 -24.8648 290.8969 315.7618 281.3879 52.5500 -24.6223 291.0188 315.6411 281.5496 53.3770 -24.3708 291.1538 315.5246 281.7266 54.1430 -24.1374 291.3006 315.4380 281.9306 55.0010 -23.8780 291.4297 315.3077 282.1922 55.7668 -23.6470 291.5418 315.1888 282.4452 56.5940 -23.4010 291.6795 315.0804 282.7624 57.3908 -23.1602 291.7832 314.9434 283.0435 58.1975 -22.9198 291.8731 314.7929 283.3492 58.9838 -22.6904 291.9624 314.6528 283.6672 59.7805 -22.4565 292.0585 314.5150 284.0000 60.6078 -22.2211 292.1537 314.3748 284.3706 61.3840 -21.9997 292.2645 314.2642 284.6844 62.2318 -21.7579 292.4315 314.1893 285.0072 62.9975 -21.5435 292.5340 314.0774 285.2846 63.8248 -21.3093 292.6883 313.9976 285.6135 64.6215 -21.0888 292.8276 313.9164 285.9220 65.4180 -20.8673 292.9356 313.8029 286.2195 66.2350 -20.6408 293.0736 313.7144 286.5256 67.0013 -20.4356 293.1576 313.5931 286.7679 67.8283 -20.2151 293.2809 313.4960 287.0162 68.5838 -20.0119 293.4042 313.4161 287.2237 69.4523 -19.7796 293.4929 313.2725 287.4143 70.2078 -19.5802 293.5677 313.1479 287.5504 71.0248 -19.3712 293.6781 313.0493 287.7164 71.8318 -19.1653 293.8221 312.9874 287.8548 72.6180 -18.9603 293.9248 312.8851 287.9815 73.4453 -18.7498 294.0176 312.7674 288.0619 74.2113 -18.5583 294.0959 312.6543 288.1594 75.0693 -18.3405 294.2124 312.5529 288.2486 75.8043 -18.1590 294.3291 312.4882 288.3050 76.6523 -17.9508 294.4654 312.4162 288.4029 77.4283 -17.7604 294.5682 312.3286 288.4396 78.2453 -17.5619 294.6885 312.2503 288.4572 79.0420 -17.3685 294.7939 312.1624 288.4532 79.8385 -17.1777 294.8886 312.0664 288.4503 80.6760 -16.9796 294.9879 311.9675 288.4189 81.4318 -16.8056 295.1028 311.9084 288.3704 82.2898 -16.6080 295.2502 311.8582 288.3639 83.0248 -16.4423 295.3137 311.7559 288.3281 83.8933 -16.2450 295.4000 311.6450 288.3370 84.6488 -16.0756 295.4622 311.5378 288.2949 85.4760 -15.8910 295.5509 311.4419 288.2693 86.2728 -15.7196 295.6558 311.3754 288.2668 87.0795 -15.5482 295.7813 311.3296 288.3026 87.8965 -15.3754 295.9086 311.2841 288.2880 88.6625 -15.2153 296.0026 311.2179 288.2846 89.5205 -15.0336 296.0789 311.1124 288.2766 90.2658 -14.8748 296.1777 311.0526 288.3219 91.1138 -14.6965 296.2851 310.9817 288.3706 91.8795 -14.5438 296.4093 310.9530 288.4119 92.7068 -14.3774 296.5253 310.9028 288.4416 93.5138 -14.2213 296.6156 310.8370 288.5100 94.3000 -14.0692 296.7260 310.7952 288.6241 95.1273 -13.9058 296.8243 310.7301 288.7394 95.8933 -13.7555 296.9047 310.6601 288.8677 96.7615 -13.5908 296.9846 310.5754 289.0824 97.5170 -13.4486 297.0500 310.4986 289.2719 98.3343 -13.2962 297.1538 310.4500 289.5248 99.1308 -13.1499 297.2572 310.4070 289.7516 99.9275 -13.0067 297.3573 310.3640 290.0218 100.7140 -12.8664 297.4715 310.3380 290.2811 101.5205 -12.7248 297.5621 310.2868 290.5413 102.3378 -12.5806 297.6575 310.2381 290.7971 103.1038 -12.4478 297.7467 310.1945 291.0466 103.9615 -12.3027 297.8502 310.1529 291.3538 104.7175 -12.1776 297.9093 310.0869 291.6251 105.5448 -12.0384 297.9623 310.0007 291.9010 106.3413 -11.9089 298.0573 309.9662 292.1492 107.1380 -11.7801 298.1544 309.9345 292.4168 107.9653 -11.6517 298.1950 309.8467 292.6867 108.7208 -11.5272 298.2874 309.8146 292.9336 109.5893 -11.3915 298.3724 309.7639 293.2359 110.3140 -11.2820 298.4380 309.7200 293.4474 111.1720 -11.1523 298.5143 309.6666 293.6746 111.9380 -11.0365 298.5680 309.6045 293.8598 112.7653 -10.9128 298.6406 309.5534 294.0403 113.5620 -10.7944 298.7424 309.5368 294.2041 114.3485 -10.6800 298.8040 309.4840 294.3585 115.1858 -10.5631 298.8297 309.3928 294.4859 115.9518 -10.4586 298.8787 309.3374 294.5613 116.8100 -10.3361 298.9706 309.3067 294.6446 117.5653 -10.2289 298.9944 309.2233 294.7094 118.4030 -10.1098 299.0419 309.1516 294.7521 119.1998 -10.0033 299.1338 309.1371 294.8093 119.9963 -9.8906 299.2219 309.1125 294.8415 120.8135 -9.7838 299.3262 309.1100 294.8725 121.5895 -9.6823 299.3872 309.0695 294.9065 122.4375 -9.5721 299.4839 309.0561 294.9240 123.2035 -9.4724 299.5778 309.0502 294.9610 124.0305 -9.3692 299.6649 309.0341 294.9870 124.8378 -9.2662 299.7526 309.0188 295.0092 125.6240 -9.1733 299.8337 309.0070 295.0033 126.4513 -9.0709 299.8914 308.9622 294.9791 127.2175 -8.9760 299.9303 308.9064 294.9749 128.0753 -8.8740 299.9956 308.8696 294.9995 128.8415 -8.7840 300.0498 308.8338 294.9900 129.6688 -8.6913 300.0805 308.7718 294.9938 130.4345 -8.6014 300.1704 308.7718 295.0231 131.2618 -8.5089 300.2555 308.7644 295.0524 132.0483 -8.4174 300.3523 308.7697 295.0862 132.8448 -8.3290 300.4388 308.7677 295.1374 133.6723 -8.2368 300.5244 308.7612 295.1982 134.4380 -8.1549 300.5615 308.7164 295.2559 135.2858 -8.0671 300.5832 308.6504 295.3890 136.0620 -7.9837 300.6729 308.6566 295.5088 136.8790 -7.8961 300.7467 308.6429 295.6661 137.6755 -7.8189 300.7976 308.6165 295.8260 138.4723 -7.7348 300.8533 308.5882 296.0023 139.2688 -7.6485 300.9238 308.5722 296.2230 140.0653 -7.5699 300.9945 308.5645 296.4322 140.8825 -7.4927 301.0736 308.5663 296.6773 141.6585 -7.4151 301.1535 308.5686 296.8914 142.5063 -7.3326 301.2297 308.5623 297.1511 143.2723 -7.2579 301.3206 308.5785 297.4044 144.0995 -7.1800 301.3987 308.5787 297.6813 144.8960 -7.1073 301.4396 308.5469 297.9269 145.6928 -7.0375 301.4901 308.5276 298.2216 146.5098 -6.9644 301.5669 308.5313 298.5097 147.2858 -6.8924 301.6057 308.4980 298.7965 148.1338 -6.8234 301.7007 308.5240 299.0716 148.9098 -6.7581 301.7779 308.5360 299.3278 149.7268 -6.6883 301.8434 308.5317 299.6020 150.5338 -6.6204 301.9016 308.5219 299.8086 151.3200 -6.5581 301.9302 308.4882 300.0198 152.1473 -6.4907 301.9925 308.4831 300.2357 152.9133 -6.4307 302.0354 308.4660 300.4411 153.7713 -6.3626 302.0745 308.4371 300.5933 154.5370 -6.3041 302.1350 308.4390 300.7328 155.3543 -6.2383 302.2195 308.4577 300.8415 156.1610 -6.1712 302.3019 308.4731 300.9356 156.9473 -6.1116 302.3788 308.4904 301.0237 157.7850 -6.0557 302.4932 308.5489 301.1096 158.5405 -6.0061 302.5317 308.5378 301.2001 159.4088 -5.9428 302.5877 308.5305 301.2501 160.1648 -5.8898 302.6419 308.5317 301.3033 161.0020 -5.8336 302.6672 308.5008 301.3382 161.7885 -5.7767 302.7076 308.4842 301.3515 162.5853 -5.7232 302.7581 308.4813 301.3954 163.4123 -5.6651 302.8034 308.4685 301.4538 164.1680 -5.6153 302.8678 308.4831 301.4789 165.0365 -5.5570 302.9363 308.4933 301.4699 165.7918 -5.5080 303.0063 308.5143 301.4565 166.6090 -5.4575 303.0659 308.5234 301.4516 167.3853 -5.4083 303.1203 308.5286 301.4394 168.2020 -5.3525 303.2044 308.5569 301.4398 168.9988 -5.3019 303.2731 308.5751 301.4552 169.7955 -5.2541 303.3650 308.6192 301.4848 170.6225 -5.2041 303.4111 308.6153 301.4847 171.3885 -5.1597 303.4482 308.6079 301.4862 172.2365 -5.1103 303.5426 308.6528 301.5466 172.9815 -5.0608 303.6229 308.6837 301.6031 173.8500 -5.0118 303.7002 308.7120 301.7103 174.6058 -4.9686 303.7572 308.7258 301.7944 175.4328 -4.9232 303.8140 308.7372 301.9052 176.2295 -4.8794 303.8592 308.7385 302.0597 177.0365 -4.8300 303.9115 308.7415 302.2241 177.8533 -4.7815 303.9903 308.7717 302.4199 178.6193 -4.7399 304.0734 308.8133 302.6139 179.4775 -4.6972 304.1615 308.8587 302.8402 180.2533 -4.6572 304.1979 308.8551 303.0737 181.0705 -4.6181 304.2520 308.8702 303.3002 181.8673 -4.5755 304.2829 308.8585 303.5640 182.6635 -4.5377 304.3225 308.8602 303.8285 183.4603 -4.4953 304.3755 308.8708 304.1207 184.2570 -4.4572 304.4152 308.8724 304.3799 185.0840 -4.4132 304.4551 308.8683 304.6277 185.8500 -4.3749 304.4968 308.8717 304.8761 186.7083 -4.3370 304.5688 308.9058 305.1850 187.4738 -4.3028 304.6708 308.9736 305.4230 188.2910 -4.2629 304.7282 308.9911 305.6794 189.0980 -4.2243 304.7925 309.0168 305.9074 189.8840 -4.1897 304.8375 309.0272 306.1038 190.7113 -4.1528 304.8852 309.0380 306.3593 191.4775 -4.1171 304.9484 309.0656 306.5287 192.3455 -4.0802 305.0353 309.1155 306.7125 193.0705 -4.0511 305.1441 309.1952 306.8646 193.9288 -4.0129 305.2434 309.2563 307.0405 194.6943 -3.9815 305.3188 309.3003 307.2146 195.5115 -3.9466 305.3839 309.3305 307.3604 196.3083 -3.9163 305.4438 309.3601 307.4723 197.1045 -3.8865 305.5045 309.3910 307.5823 197.9218 -3.8543 305.5466 309.4008 307.6759 198.6878 -3.8234 305.6349 309.4583 307.7354 199.5455 -3.7924 305.7292 309.5216 307.7912 200.3013 -3.7612 305.7998 309.5611 307.8286 201.1288 -3.7325 305.8345 309.5670 307.8648 201.8943 -3.7032 305.9023 309.6054 307.8713 202.7218 -3.6716 305.9761 309.6477 307.8777 203.5185 -3.6422 306.0401 309.6823 307.9003 204.3045 -3.6139 306.1151 309.7290 307.9095 205.1423 -3.5853 306.1890 309.7743 307.8805 205.8978 -3.5607 306.2786 309.8393 307.8509 206.7558 -3.5309 306.3728 309.9037 307.8505 207.5215 -3.5010 306.4588 309.9598 307.8705 208.3493 -3.4730 306.5303 310.0033 307.8752 209.1455 -3.4462 306.6034 310.0496 307.8870 209.9320 -3.4202 306.6608 310.0811 307.9089 210.7698 -3.3892 306.7350 310.1242 307.9229 211.5250 -3.3593 306.8254 310.1847 307.9587 212.3833 -3.3310 306.9059 310.2369 308.0469 213.1185 -3.3074 306.9772 310.2846 308.1497 213.9868 -3.2754 307.0166 310.2920 308.2817 214.7425 -3.2508 307.0787 310.3295 308.4017 215.5698 -3.2224 307.1508 310.3732 308.4937 216.3663 -3.1992 307.2244 310.4236 308.6420 217.1630 -3.1781 307.2934 310.4716 308.8312 217.9903 -3.1547 307.3652 310.5199 309.0321 218.7458 -3.1338 307.4519 310.5856 309.2343 219.6143 -3.1067 307.5397 310.6464 309.5256 220.3698 -3.0854 307.5757 310.6611 309.7666 221.1970 -3.0623 307.6554 310.7176 309.9889 221.9938 -3.0379 307.7543 310.7922 310.2071 222.8005 -3.0151 307.8218 310.8369 310.4941 223.6178 -2.9900 307.9618 310.9518 310.7798 224.3838 -2.9674 308.0420 311.0094 311.0351 225.2415 -2.9433 308.0951 311.0384 311.3375 226.0178 -2.9219 308.1621 311.0839 311.6026 226.8348 -2.9002 308.2407 311.1409 311.8936 227.6210 -2.8794 308.2975 311.1769 312.1745 228.4178 -2.8608 308.3692 311.2299 312.4258 229.2350 -2.8398 308.4382 311.2779 312.6184 230.0008 -2.8244 308.5306 311.3550 312.8146 230.8590 -2.8017 308.5908 311.3926 313.0410 231.6145 -2.7836 308.6663 311.4500 313.2360 232.4420 -2.7616 308.7550 311.5167 313.4349 233.2388 -2.7437 308.8400 311.5837 313.5890 234.0350 -2.7271 308.9034 311.6305 313.7330 234.8318 -2.7086 308.9787 311.6873 313.8541 235.6285 -2.6888 309.0352 311.7240 313.9773 236.4555 -2.6689 309.1386 311.8075 314.0719 237.2218 -2.6521 309.2459 311.8980 314.1379 238.0695 -2.6396 309.3336 311.9731 314.2000 238.8458 -2.6205 309.3827 312.0032 314.2594 239.6630 -2.6021 309.4674 312.0695 314.3074 240.4593 -2.5843 309.5513 312.1356 314.3304 241.2560 -2.5639 309.6216 312.1856 314.3273 242.0835 -2.5482 309.7153 312.2635 314.2836 242.8490 -2.5355 309.8029 312.3384 314.2568 243.6970 -2.5133 309.9005 312.4138 314.2637 244.4733 -2.4964 309.9756 312.4719 314.2542 245.2900 -2.4785 310.0261 312.5046 314.2564 246.0970 -2.4597 310.1084 312.5681 314.2248 246.8835 -2.4460 310.1991 312.6451 314.2373 247.6900 -2.4301 310.2935 312.7236 314.2435 248.4765 -2.4123 310.3655 312.7778 314.2445 249.3040 -2.3967 310.4542 312.8509 314.2590 250.0695 -2.3810 310.4985 312.8795 314.3071 250.9380 -2.3656 310.6159 312.9815 314.3935 251.7860 -2.3475 310.7141 313.0617 314.4468 252.6438 -2.3313 310.8323 313.1637 314.5434 253.5020 -2.3135 310.9423 313.2558 314.6746 254.2680 -2.2998 311.0428 313.3427 314.7929 255.0950 -2.2844 311.1318 313.4163 314.9272 255.8918 -2.2719 311.2208 313.4927 315.0936 256.6885 -2.2563 311.2895 313.5457 315.2891 257.5158 -2.2401 311.4126 313.6527 315.5275 258.2818 -2.2253 311.4904 313.7157 315.7283 259.1295 -2.2132 311.5821 313.7953 315.9334 259.9055 -2.1974 311.6498 313.8473 316.1688 260.7743 -2.1813 311.6984 313.8797 316.5051 261.5705 -2.1711 311.7833 313.9543 316.7902 262.3983 -2.1615 311.8400 314.0015 317.0745 263.1538 -2.1497 311.9033 314.0530 317.3331 264.0118 -2.1353 312.0070 314.1423 317.6803 264.7470 -2.1290 312.0784 314.2075 317.9460 265.5948 -2.1160 312.1957 314.3118 318.2520 266.3913 -2.0997 312.2964 314.3962 318.5101 267.1880 -2.0922 312.3962 314.4884 318.7561 268.0153 -2.0778 312.4975 314.5752 319.0033 268.7708 -2.0653 312.5547 314.6200 319.2186 269.6393 -2.0548 312.6220 314.6768 319.4868 270.4255 -2.0428 312.7122 314.7549 319.6974 271.3758 -2.0290 312.8227 314.8518 319.8969 272.2033 -2.0189 312.9480 314.9669 320.0880 272.9998 -2.0065 313.0691 315.0756 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