DTA measure 2elso_pbud3 Date: 2026422:915 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.39 s Mass = 960.700 mg data_number = 1343 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1375 1.4711 198.8765 197.4053 248.0604 1.9655 1.4718 199.1566 197.6848 248.0655 2.7628 1.4713 199.4419 197.9706 248.0694 3.5598 1.4712 199.7245 198.2533 248.0712 4.3768 1.4721 200.0157 198.5437 248.0707 5.1535 1.4737 200.2737 198.8000 248.0763 5.9713 1.4733 200.5440 199.0707 248.0855 6.7480 1.4736 200.8055 199.3319 248.1002 7.5963 1.4726 201.0997 199.6272 248.1120 8.3723 1.4726 201.3591 199.8865 248.1313 9.1900 1.4745 201.6395 200.1651 248.1581 9.9873 1.4744 201.9129 200.4385 248.1921 10.7845 1.4742 202.1788 200.7045 248.2251 11.6120 1.4729 202.4432 200.9703 248.2705 12.3780 1.4727 202.6929 201.2202 248.3302 13.2265 1.4702 202.9652 201.4950 248.3750 14.0033 1.4695 203.2464 201.7769 248.4194 14.8210 1.4688 203.5191 202.0503 248.4858 15.6173 1.4676 203.7787 202.3111 248.5409 16.4145 1.4668 204.0421 202.5753 248.5952 17.2528 1.4653 204.3131 202.8478 248.6647 18.0090 1.4654 204.5542 203.0887 248.7344 18.8675 1.4659 204.8188 203.3529 248.8090 19.6333 1.4660 205.0671 203.6010 248.8815 20.4613 1.4649 205.3356 203.8708 248.9695 21.2585 1.4635 205.5784 204.1149 249.0646 22.0453 1.4626 205.8254 204.3628 249.1646 22.8828 1.4606 206.0900 204.6294 249.2689 23.6493 1.4591 206.3409 204.8818 249.3772 24.4875 1.4595 206.6016 205.1420 249.4853 25.2643 1.4581 206.8444 205.3862 249.6013 26.0813 1.4551 207.1085 205.6534 249.7239 26.8680 1.4525 207.3524 205.8999 249.8425 27.6653 1.4511 207.6094 206.1583 249.9578 28.4933 1.4492 207.8837 206.4345 250.0846 29.2488 1.4481 208.1187 206.6706 250.1974 30.1073 1.4455 208.3895 206.9440 250.3359 30.8738 1.4430 208.6241 207.1811 250.4609 31.6915 1.4401 208.8845 207.4445 250.6012 32.4988 1.4383 209.1335 207.6953 250.7292 33.2850 1.4358 209.3807 207.9448 250.8645 34.1130 1.4316 209.6262 208.1946 251.0139 34.8795 1.4294 209.8516 208.4222 251.1589 35.7280 1.4269 210.1071 208.6801 251.3220 36.4938 1.4249 210.3452 208.9203 251.4550 37.3215 1.4215 210.6028 209.1814 251.6172 38.1188 1.4179 210.8384 209.4205 251.7628 38.9160 1.4133 211.0782 209.6649 251.9098 39.7335 1.4089 211.3186 209.9096 252.0713 40.5095 1.4056 211.5440 210.1383 252.2301 41.3580 1.4019 211.8022 210.4003 252.3924 42.1245 1.3976 212.0402 210.6426 252.5425 42.9525 1.3931 212.2957 210.9026 252.7266 43.7490 1.3890 212.5286 211.1396 252.8827 44.5460 1.3852 212.7507 211.3655 253.0333 45.3638 1.3810 212.9936 211.6126 253.1951 46.1405 1.3779 213.2286 211.8508 253.3447 46.9988 1.3741 213.4910 212.1169 253.5246 47.7648 1.3699 213.7145 212.3446 253.6832 48.5825 1.3665 213.9517 212.5852 253.8473 49.3900 1.3629 214.1908 212.8279 254.0151 50.1770 1.3596 214.4220 213.0625 254.1728 51.0040 1.3547 214.6561 213.3014 254.3304 51.7705 1.3507 214.8773 213.5266 254.4735 52.6395 1.3463 215.1271 213.7808 254.6380 53.3958 1.3418 215.3411 213.9992 254.7924 54.2228 1.3377 215.5782 214.2405 254.9402 55.0200 1.3323 215.8081 214.4758 255.0795 55.8173 1.3280 216.0351 214.7071 255.2120 56.6035 1.3228 216.2641 214.9414 255.3439 57.4005 1.3167 216.4986 215.1819 255.4833 58.2285 1.3120 216.7491 215.4371 255.6252 58.9848 1.3077 216.9623 215.6545 255.7539 59.8433 1.3021 217.2037 215.9016 255.9128 60.5988 1.2975 217.4178 216.1204 256.0428 61.4268 1.2926 217.6523 216.3597 256.1873 62.2240 1.2876 217.8774 216.5898 256.3288 63.0213 1.2825 218.1075 216.8250 256.4624 63.8483 1.2761 218.3471 217.0710 256.5996 64.6045 1.2704 218.5611 217.2906 256.7238 65.4428 1.2643 218.8080 217.5437 256.8573 66.1990 1.2586 219.0312 217.7726 256.9896 67.0573 1.2529 219.2670 218.0141 257.1403 67.8233 1.2473 219.4690 218.2216 257.2648 68.6615 1.2425 219.7036 218.4611 257.4139 69.4485 1.2375 219.9191 218.6816 257.5555 70.2450 1.2319 220.1450 218.9132 257.6871 71.0420 1.2260 220.3669 219.1409 257.8166 71.8393 1.2201 220.5850 219.3649 257.9475 72.6673 1.2152 220.8150 219.5998 258.0864 73.4233 1.2096 221.0268 219.8172 258.2054 74.2915 1.2048 221.2765 220.0717 258.3517 75.0478 1.1996 221.4867 220.2871 258.4716 75.8758 1.1935 221.7120 220.5185 258.6120 76.6730 1.1885 221.9540 220.7655 258.7540 77.4695 1.1833 222.1724 220.9891 258.8821 78.2973 1.1773 222.3955 221.2182 259.0172 79.0535 1.1729 222.5947 221.4218 259.1401 79.9225 1.1679 222.8197 221.6519 259.2743 80.6473 1.1642 223.0213 221.8571 259.3878 81.5160 1.1566 223.2574 222.1007 259.5308 82.2723 1.1500 223.4586 222.3085 259.6504 83.1105 1.1438 223.6860 222.5422 259.7918 83.9078 1.1388 223.9008 222.7619 259.9222 84.7040 1.1322 224.1129 222.9807 260.0507 85.5218 1.1260 224.3356 223.2096 260.1812 86.2985 1.1199 224.5463 223.4264 260.3200 87.1470 1.1150 224.7783 223.6634 260.4573 87.8925 1.1109 224.9832 223.8723 260.5806 88.7405 1.1061 225.2211 224.1150 260.7182 89.5070 1.1010 225.4290 224.3280 260.8422 90.3248 1.0957 225.6454 224.5498 260.9710 91.1213 1.0896 225.8506 224.7611 261.1072 91.9183 1.0823 226.0515 224.9692 261.2481 92.7360 1.0764 226.2637 225.1873 261.3883 93.5025 1.0708 226.4691 225.3984 261.5233 94.3605 1.0651 226.7059 225.6408 261.6586 95.0960 1.0599 226.9028 225.8429 261.7817 95.9445 1.0539 227.1164 226.0625 261.9237 96.7213 1.0476 227.3221 226.2744 262.0495 97.5388 1.0425 227.5389 226.4965 262.1892 98.3353 1.0355 227.7519 226.7164 262.3234 99.1325 1.0296 227.9640 226.9344 262.4520 99.9605 1.0239 228.1839 227.1600 262.5939 100.7270 1.0189 228.3808 227.3619 262.7144 101.5748 1.0116 228.6042 227.5925 262.8414 102.3205 1.0062 228.8072 227.8010 262.9590 103.1690 0.9991 229.0287 228.0297 263.0979 103.9350 0.9920 229.2291 228.2371 263.2164 104.7625 0.9843 229.4458 228.4615 263.3457 105.5598 0.9789 229.6529 228.6740 263.4765 106.3570 0.9720 229.8531 228.8811 263.6050 107.1745 0.9645 230.0608 229.0963 263.7277 107.9505 0.9576 230.2572 229.2996 263.8560 108.7990 0.9508 230.4716 229.5208 263.9852 109.5655 0.9460 230.6667 229.7208 264.1085 110.3935 0.9381 230.8825 229.9444 264.2366 111.2000 0.9305 231.1043 230.1738 264.3566 111.9870 0.9253 231.3072 230.3820 264.4751 112.8150 0.9199 231.5178 230.5978 264.6102 113.5815 0.9136 231.7172 230.8036 264.7275 114.4398 0.9066 231.9290 231.0224 264.8645 115.2058 0.9013 232.1100 231.2087 264.9834 116.0235 0.8957 232.3166 231.4209 265.1109 116.8310 0.8897 232.5212 231.6315 265.2453 117.6178 0.8829 232.7098 231.8269 265.3688 118.4450 0.8770 232.9195 232.0425 265.4973 119.2115 0.8710 233.1206 232.2496 265.6215 120.0703 0.8640 233.3495 232.4855 265.7558 120.8265 0.8599 233.5361 232.6762 265.8771 121.6535 0.8529 233.7466 232.8937 266.0170 122.4508 0.8462 233.9493 233.1031 266.1444 123.2378 0.8420 234.1420 233.3000 266.2700 124.0655 0.8396 234.3438 233.5042 266.4067 124.8313 0.8344 234.5387 233.7042 266.5282 125.6593 0.8284 234.7425 233.9141 266.6649 126.4155 0.8219 234.9238 234.1019 266.7837 127.2845 0.8159 235.1331 234.3172 266.9193 128.0403 0.8085 235.3311 234.5226 267.0402 128.8678 0.7995 235.5404 234.7409 267.1707 129.6650 0.7920 235.7326 234.9405 267.2982 130.4520 0.7853 235.9184 235.1330 267.4317 131.2800 0.7786 236.1218 235.3432 267.5617 132.0458 0.7727 236.3167 235.5440 267.6949 132.9043 0.7665 236.5251 235.7586 267.8295 133.6708 0.7596 236.7160 235.9563 267.9587 134.4885 0.7515 236.9127 236.1612 268.0945 135.2955 0.7435 237.1119 236.3684 268.2242 136.0820 0.7370 237.3079 236.5709 268.3437 136.9100 0.7319 237.5059 236.7740 268.4793 137.6765 0.7269 237.6875 236.9606 268.6039 138.5350 0.7222 237.8940 237.1718 268.7457 139.3008 0.7155 238.0771 237.3616 268.8687 140.1185 0.7108 238.2837 237.5729 269.0153 140.9260 0.7050 238.4903 237.7853 269.1424 141.7130 0.6997 238.6805 237.9808 269.2660 142.5400 0.6937 238.8762 238.1825 269.4022 143.3065 0.6885 239.0480 238.3595 269.5244 144.1653 0.6819 239.2516 238.5698 269.6651 144.9318 0.6754 239.4467 238.7713 269.7860 145.7488 0.6694 239.6411 238.9717 269.9262 146.5560 0.6645 239.8348 239.1703 270.0661 147.3430 0.6596 240.0181 239.3585 270.1940 148.1710 0.6528 240.2240 239.5712 270.3202 148.9373 0.6471 240.4203 239.7732 270.4321 149.8055 0.6398 240.6274 239.9876 270.5696 150.5618 0.6328 240.8122 240.1794 270.6932 151.3898 0.6267 240.9993 240.3727 270.8335 152.1868 0.6198 241.1836 240.5638 270.9580 152.9833 0.6125 241.3676 240.7551 271.0849 153.8010 0.6061 241.5684 240.9623 271.2144 154.5675 0.6003 241.7576 241.1573 271.3372 155.4158 0.5943 241.9534 241.3591 271.4701 156.1815 0.5895 242.1357 241.5462 271.5949 157.0095 0.5837 242.3344 241.7507 271.7270 157.8068 0.5787 242.5260 241.9473 271.8635 158.5935 0.5724 242.7162 242.1438 271.9855 159.4208 0.5655 242.9160 242.3505 272.1235 160.1873 0.5603 243.0906 242.5303 272.2621 161.0358 0.5539 243.2838 242.7299 272.4013 161.8023 0.5466 243.4619 242.9154 272.5235 162.6295 0.5407 243.6659 243.1252 272.6575 163.4265 0.5359 243.8522 243.3163 272.7913 164.2135 0.5298 244.0324 243.5026 272.9215 165.0515 0.5251 244.2226 243.6975 273.0516 165.8070 0.5195 244.3981 243.8786 273.1657 166.6658 0.5142 244.5992 244.0849 273.2941 167.4323 0.5095 244.7775 244.2680 273.4153 168.2598 0.5022 244.9760 244.4739 273.5425 169.0565 0.4963 245.1614 244.6651 273.6680 169.8435 0.4899 245.3288 244.8389 273.8075 170.6818 0.4856 245.5126 245.0270 273.9398 171.4378 0.4806 245.6825 245.2020 274.0526 172.3060 0.4736 245.8945 245.4209 274.1905 173.0623 0.4663 246.0747 245.6083 274.3000 173.9005 0.4596 246.2623 245.8027 274.4409 174.6560 0.4540 246.4282 245.9741 274.5624 175.4838 0.4491 246.6132 246.1641 274.7015 176.2810 0.4441 246.7999 246.3558 274.8323 177.0783 0.4399 246.9824 246.5425 274.9520 177.9370 0.4330 247.1825 246.7495 275.0846 178.6720 0.4284 247.3552 246.9268 275.2078 179.5305 0.4229 247.5515 247.1285 275.3399 180.2970 0.4192 247.7255 247.3063 275.4588 181.1250 0.4150 247.9120 247.4970 275.5936 181.9110 0.4095 248.0901 247.6806 275.7278 182.7185 0.4045 248.2688 247.8642 275.8512 183.5465 0.4006 248.4564 248.0558 275.9826 184.3028 0.3946 248.6275 248.2329 276.1058 185.1608 0.3879 248.8226 248.4347 276.2383 185.8860 0.3811 248.9869 248.6058 276.3529 186.7345 0.3743 249.1874 248.8131 276.4792 187.5113 0.3679 249.3652 248.9973 276.5957 188.3290 0.3616 249.5478 249.1861 276.7140 189.1150 0.3564 249.7232 249.3668 276.8349 189.9225 0.3500 249.8971 249.5471 276.9638 190.7403 0.3452 250.0839 249.7387 277.1047 191.5068 0.3416 250.2691 249.9275 277.2222 192.3650 0.3356 250.4632 250.1276 277.3591 193.1208 0.3292 250.6340 250.3048 277.4904 193.9488 0.3224 250.8290 250.5066 277.6387 194.7460 0.3163 251.0019 250.6856 277.7796 195.5428 0.3108 251.1718 250.8610 277.9142 196.3395 0.3045 251.3444 251.0399 278.0619 197.1265 0.2992 251.5167 251.2175 278.1946 197.9648 0.2939 251.7012 251.4073 278.3477 198.7208 0.2892 251.8665 251.5773 278.4885 199.5788 0.2839 252.0624 251.7785 278.6504 200.3453 0.2784 252.2269 251.9485 278.7825 201.1733 0.2728 252.4092 252.1363 278.9272 201.9705 0.2673 252.5903 252.3230 279.0680 202.7565 0.2607 252.7695 252.5087 279.2206 203.5948 0.2551 252.9541 252.6989 279.3808 204.3510 0.2496 253.1336 252.8839 279.5191 205.2098 0.2442 253.3375 253.0933 279.6747 205.9758 0.2386 253.5005 253.2620 279.8145 206.8033 0.2343 253.6721 253.4378 279.9756 207.5698 0.2285 253.8361 253.6076 280.1218 208.3978 0.2226 254.0259 253.8033 280.2727 209.1950 0.2176 254.1949 253.9773 280.4301 209.9913 0.2136 254.3714 254.1578 280.5804 210.8193 0.2097 254.5516 254.3419 280.7414 211.5858 0.2036 254.7090 254.5054 280.8814 212.4445 0.1983 254.8868 254.6885 281.0408 213.2110 0.1939 255.0513 254.8574 281.1762 214.0380 0.1875 255.2405 255.0530 281.3282 214.8250 0.1812 255.4099 255.2287 281.4706 215.6325 0.1753 255.5780 255.4028 281.6069 216.4605 0.1699 255.7635 255.5936 281.7462 217.2158 0.1643 255.9276 255.7633 281.8718 218.0745 0.1587 256.1142 255.9555 282.0146 218.8308 0.1557 256.2769 256.1212 282.1449 219.6485 0.1523 256.4531 256.3008 282.2814 220.4558 0.1461 256.6194 256.4733 282.4170 221.2420 0.1423 256.7837 256.6413 282.5399 222.0598 0.1369 256.9592 256.8224 282.6619 222.8365 0.1326 257.1231 256.9905 282.7842 223.6540 0.1270 257.3033 257.1762 282.9231 224.4198 0.1202 257.4711 257.3509 283.0385 225.2785 0.1142 257.6608 257.5465 283.1657 226.0348 0.1094 257.8313 257.7219 283.2864 226.8628 0.1037 258.0174 257.9137 283.4064 227.6593 0.0991 258.2010 258.1018 283.5211 228.4563 0.0949 258.3719 258.2770 283.6359 229.2843 0.0897 258.5414 258.4517 283.7543 230.0405 0.0847 258.7023 258.6176 283.8687 230.9093 0.0791 258.8791 258.8001 283.9977 231.6648 0.0736 259.0433 258.9697 284.1091 232.4928 0.0689 259.2298 259.1609 284.2318 233.2900 0.0642 259.4020 259.3378 284.3449 234.0873 0.0594 259.5715 259.5121 284.4568 234.9143 0.0532 259.7414 259.6882 284.5675 235.6705 0.0486 259.9025 259.8539 284.6688 236.5395 0.0432 260.0887 260.0455 284.7874 237.2958 0.0387 260.2530 260.2143 284.8970 238.1233 0.0335 260.4343 260.4008 285.0183 238.9200 0.0287 260.6065 260.5778 285.1315 239.7173 0.0236 260.7748 260.7512 285.2412 240.5453 0.0175 260.9478 260.9303 285.3581 241.3010 0.0136 261.1136 261.1000 285.4695 242.1695 0.0078 261.3044 261.2966 285.6151 242.9258 0.0049 261.4666 261.4617 285.7270 243.7538 0.0009 261.6412 261.6402 285.8711 244.5510 -0.0034 261.8070 261.8104 285.9981 245.3473 -0.0091 261.9786 261.9877 286.1323 246.1753 -0.0144 262.1513 262.1657 286.2665 246.9315 -0.0173 262.3037 262.3210 286.3910 247.8005 -0.0216 262.4818 262.5034 286.5408 248.5663 -0.0262 262.6497 262.6760 286.6744 249.3838 -0.0319 262.8247 262.8566 286.8144 250.1810 -0.0376 263.0029 263.0404 286.9401 250.9783 -0.0440 263.1715 263.2155 287.0656 251.8058 -0.0487 263.3471 263.3959 287.2053 252.5615 -0.0526 263.5088 263.5614 287.3353 253.4203 -0.0548 263.6907 263.7455 287.4799 254.1868 -0.0585 263.8436 263.9021 287.6237 255.0038 -0.0638 264.0190 264.0828 287.7783 255.8008 -0.0675 264.1795 264.2470 287.9282 256.5980 -0.0724 264.3500 264.4224 288.0709 257.4158 -0.0790 264.5124 264.5915 288.2076 258.1925 -0.0846 264.6781 264.7627 288.3356 259.0400 -0.0901 264.8569 264.9471 288.4834 259.8065 -0.0959 265.0126 265.1086 288.6180 260.6345 -0.1011 265.1749 265.2760 288.7679 261.4318 -0.1054 265.3416 265.4470 288.9001 262.2280 -0.1100 265.5060 265.6160 289.0450 263.0458 -0.1135 265.6693 265.7828 289.1911 263.8225 -0.1170 265.8364 265.9533 289.3339 264.6710 -0.1208 266.0112 266.1320 289.4775 265.4365 -0.1251 266.1651 266.2902 289.6034 266.2645 -0.1298 266.3425 266.4723 289.7398 267.0618 -0.1367 266.5121 266.6488 289.8810 267.8590 -0.1416 266.6777 266.8193 290.0212 268.6558 -0.1461 266.8400 266.9860 290.1606 269.4525 -0.1498 267.0053 267.1550 290.3144 270.2805 -0.1531 267.1942 267.3473 290.4637 271.0470 -0.1579 267.3560 267.5139 290.6054 271.8955 -0.1619 267.5260 267.6879 290.7683 272.6713 -0.1664 267.6807 267.8471 290.9051 273.4890 -0.1710 267.8425 268.0135 291.0457 274.2863 -0.1765 268.0038 268.1803 291.1829 275.0835 -0.1807 268.1702 268.3510 291.3153 275.9113 -0.1857 268.3389 268.5246 291.4657 276.6770 -0.1906 268.4968 268.6874 291.5986 277.5255 -0.1968 268.6843 268.8811 291.7320 278.3023 -0.2011 268.8514 269.0525 291.8594 279.1198 -0.2061 269.0209 269.2270 292.0035 279.9163 -0.2119 269.1805 269.3923 292.1411 280.7135 -0.2172 269.3493 269.5664 292.2895 281.5415 -0.2223 269.5143 269.7366 292.4400 282.3078 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295.5332 300.7720 -0.3265 273.3995 273.7260 295.6511 301.5693 -0.3306 273.5686 273.8991 295.7669 302.3665 -0.3351 273.7331 274.0682 295.8858 303.1935 -0.3398 273.9077 274.2476 296.0089 303.9600 -0.3455 274.0631 274.4086 296.1073 304.8085 -0.3501 274.2308 274.5809 296.2209 305.5853 -0.3544 274.3820 274.7365 296.3285 306.4023 -0.3586 274.5515 274.9101 296.4480 307.1993 -0.3632 274.7091 275.0723 296.5557 307.9965 -0.3682 274.8706 275.2388 296.6653 308.8348 -0.3721 275.0471 275.4191 296.7794 309.5905 -0.3745 275.2083 275.5827 296.8829 310.4488 -0.3767 275.3980 275.7748 296.9885 311.1845 -0.3809 275.5484 275.9293 297.0868 312.0433 -0.3853 275.7123 276.0976 297.2027 312.8098 -0.3891 275.8600 276.2491 297.3033 313.6265 -0.3943 276.0193 276.4136 297.4138 314.4238 -0.3991 276.1745 276.5736 297.5257 315.2210 -0.4023 276.3354 276.7377 297.6403 316.0388 -0.4052 276.4934 276.8986 297.7598 316.8048 -0.4076 276.6443 277.0519 297.8789 317.6630 -0.4113 276.8179 277.2292 298.0110 318.4193 -0.4143 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