DTA measure 3elso_pbud3 Date: 2026422:944 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.37 s Mass = 960.700 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5076 -4.2498 425.1525 429.4023 406.1719 4.1124 -4.2575 425.1619 429.4194 406.1787 5.7216 -4.2658 425.1703 429.4360 406.1907 7.3260 -4.2746 425.1713 429.4459 406.2029 8.9303 -4.2839 425.1579 429.4419 406.2018 10.5448 -4.2953 425.1550 429.4503 406.2101 12.1493 -4.3049 425.1445 429.4493 406.2066 13.7738 -4.3148 425.1378 429.4526 406.1931 15.3784 -4.3224 425.1434 429.4658 406.1657 16.9618 -4.3335 425.1261 429.4596 406.1314 18.5665 -4.3415 425.1211 429.4626 406.0819 20.1703 -4.3509 425.1083 429.4592 406.0078 21.7750 -4.3610 425.0956 429.4566 405.9323 23.3736 -4.3682 425.0898 429.4580 405.8430 24.9784 -4.3756 425.0751 429.4507 405.7598 26.5876 -4.3824 425.0517 429.4341 405.6635 28.1920 -4.3895 425.0480 429.4375 405.5431 29.8013 -4.3959 425.0370 429.4330 405.4094 31.4056 -4.4032 425.0326 429.4358 405.2678 33.0098 -4.4099 425.0207 429.4306 405.1220 34.6193 -4.4151 425.0098 429.4249 404.9811 36.2288 -4.4208 424.9860 429.4068 404.8301 37.8380 -4.4268 424.9688 429.3956 404.6747 39.4631 -4.4313 424.9599 429.3912 404.4859 41.0721 -4.4340 424.9449 429.3789 404.3018 42.6615 -4.4390 424.9322 429.3712 404.1340 44.2756 -4.4442 424.9106 429.3548 403.9520 45.8803 -4.4485 424.8846 429.3331 403.7621 47.4893 -4.4526 424.8453 429.2979 403.5734 49.0939 -4.4559 424.8050 429.2608 403.3829 50.6876 -4.4596 424.7785 429.2381 403.1998 52.3126 -4.4623 424.7423 429.2046 403.0081 53.9113 -4.4658 424.7090 429.1748 402.8255 55.5160 -4.4678 424.6793 429.1470 402.6238 57.1200 -4.4702 424.6438 429.1140 402.4241 58.7245 -4.4732 424.6040 429.0772 402.2332 60.3339 -4.4749 424.5784 429.0533 402.0517 61.9381 -4.4789 424.5495 429.0284 401.8611 63.5480 -4.4806 424.5110 428.9916 401.6744 65.1569 -4.4826 424.4799 428.9625 401.4832 66.7616 -4.4860 424.4433 428.9293 401.2983 68.3709 -4.4886 424.3936 428.8822 401.1131 69.9753 -4.4927 424.3344 428.8271 400.9157 71.5846 -4.4953 424.2725 428.7679 400.7221 73.1889 -4.4982 424.2079 428.7061 400.5243 74.7983 -4.4983 424.1602 428.6585 400.3366 76.4230 -4.4994 424.1083 428.6077 400.1381 78.0321 -4.5014 424.0526 428.5540 399.9344 79.6418 -4.5023 423.9933 428.4956 399.7365 81.2304 -4.5048 423.9379 428.4427 399.5415 82.8298 -4.5054 423.8890 428.3943 399.3326 84.4338 -4.5069 423.8219 428.3287 399.1211 86.0434 -4.5082 423.7558 428.2641 398.9159 87.6423 -4.5093 423.6949 428.2042 398.7162 89.2314 -4.5108 423.6255 428.1362 398.5200 90.8564 -4.5119 423.5699 428.0818 398.3177 92.4604 -4.5100 423.4904 428.0004 398.1267 94.0701 -4.5127 423.4214 427.9341 397.9284 95.6740 -4.5148 423.3495 427.8643 397.7395 97.2788 -4.5162 423.2766 427.7927 397.5503 98.8723 -4.5178 423.1920 427.7098 397.3561 100.4770 -4.5191 423.1156 427.6347 397.1684 102.0863 -4.5179 423.0461 427.5640 396.9801 103.7060 -4.5177 422.9658 427.4834 396.7874 105.3153 -4.5175 422.8772 427.3947 396.6000 106.9196 -4.5185 422.7947 427.3132 396.4232 108.5240 -4.5204 422.7172 427.2375 396.2455 110.1384 -4.5209 422.6359 427.1568 396.0691 111.7429 -4.5228 422.5586 427.0813 395.8853 113.3469 -4.5230 422.4727 426.9957 395.7035 114.9615 -4.5225 422.3769 426.8995 395.5132 116.5605 -4.5235 422.2868 426.8103 395.3444 118.1698 -4.5248 422.2011 426.7259 395.1735 119.7741 -4.5234 422.1030 426.6265 394.9944 121.3735 -4.5231 422.0110 426.5341 394.8126 122.9673 -4.5238 421.9025 426.4263 394.6351 124.5719 -4.5231 421.8043 426.3274 394.4451 126.1809 -4.5209 421.7006 426.2215 394.2649 127.8010 -4.5217 421.6011 426.1228 394.0701 129.4099 -4.5234 421.4797 426.0031 393.8773 131.0146 -4.5230 421.3794 425.9023 393.7020 132.6184 -4.5222 421.2785 425.8008 393.5005 134.2283 -4.5198 421.1772 425.6970 393.2948 135.8375 -4.5210 421.0801 425.6011 393.0965 137.4470 -4.5218 420.9697 425.4914 392.9175 139.0718 -4.5216 420.8523 425.3738 392.7311 140.6811 -4.5222 420.7392 425.2614 392.5398 142.2854 -4.5215 420.6270 425.1485 392.3467 143.8948 -4.5194 420.5260 425.0454 392.1645 145.4890 -4.5190 420.4169 424.9359 391.9790 147.0930 -4.5167 420.3034 424.8201 391.7909 148.6976 -4.5163 420.1943 424.7107 391.6087 150.3169 -4.5137 420.0869 424.6006 391.4364 151.9061 -4.5141 419.9765 424.4906 391.2599 153.5151 -4.5128 419.8692 424.3819 391.0724 155.1199 -4.5136 419.7434 424.2570 390.8967 156.7289 -4.5140 419.6180 424.1320 390.7149 158.3335 -4.5138 419.4989 424.0128 390.5191 159.9424 -4.5132 419.3802 423.8934 390.3077 161.5470 -4.5124 419.2681 423.7805 390.1234 163.1663 -4.5116 419.1458 423.6574 389.9347 164.7659 -4.5109 419.0333 423.5442 389.7329 166.3696 -4.5101 418.9076 423.4177 389.5381 167.9795 -4.5067 418.7794 423.2860 389.3290 169.5834 -4.5060 418.6469 423.1529 389.1245 171.1983 -4.5034 418.5152 423.0186 388.9279 172.8025 -4.5005 418.3949 422.8954 388.7443 174.4119 -4.4996 418.2610 422.7606 388.5330 176.0006 -4.4981 418.1274 422.6256 388.3325 177.6204 -4.4966 418.0006 422.4972 388.1498 179.2250 -4.4960 417.8753 422.3712 387.9401 180.8238 -4.4938 417.7368 422.2306 387.7495 182.4336 -4.4911 417.6032 422.0942 387.5654 184.0221 -4.4883 417.4642 421.9525 387.3795 185.6216 -4.4847 417.3301 421.8148 387.1685 187.2308 -4.4838 417.1876 421.6714 386.9667 188.8353 -4.4821 417.0589 421.5410 386.7835 190.4596 -4.4807 416.9197 421.4004 386.5917 192.0489 -4.4805 416.7820 421.2624 386.4115 193.6530 -4.4784 416.6362 421.1146 386.2300 195.2625 -4.4772 416.5152 420.9924 386.0347 196.8668 -4.4763 416.3850 420.8613 385.8316 198.4761 -4.4759 416.2370 420.7130 385.6401 200.0858 -4.4757 416.0831 420.5588 385.4590 201.6949 -4.4742 415.9295 420.4038 385.2786 203.3150 -4.4706 415.7882 420.2589 385.0920 204.9239 -4.4689 415.6470 420.1159 384.9036 206.5133 -4.4657 415.5056 419.9713 384.7137 208.1171 -4.4603 415.3573 419.8176 384.5216 209.7423 -4.4585 415.2100 419.6685 384.3171 211.3258 -4.4583 415.0722 419.5306 384.1248 212.9303 -4.4573 414.9323 419.3897 383.9134 214.5346 -4.4548 414.7875 419.2423 383.7053 216.1490 -4.4525 414.6383 419.0908 383.5057 217.7589 -4.4498 414.4875 418.9373 383.2954 219.3626 -4.4475 414.3422 418.7897 383.0726 220.9623 -4.4447 414.1853 418.6300 382.8687 222.5715 -4.4428 414.0282 418.4710 382.6625 224.1759 -4.4423 413.8790 418.3212 382.4784 225.7854 -4.4390 413.7308 418.1698 382.2736 227.4100 -4.4351 413.5759 418.0110 382.0715 229.0045 -4.4324 413.4261 417.8585 381.8639 230.6083 -4.4291 413.2695 417.6986 381.6581 232.2233 -4.4261 413.1170 417.5431 381.4539 233.8271 -4.4228 412.9665 417.3893 381.2436 235.4318 -4.4223 412.8240 417.2463 381.0565 237.0461 -4.4182 412.6789 417.0970 380.8566 238.6505 -4.4147 412.5236 416.9383 380.6532 240.2755 -4.4112 412.3684 416.7797 380.4449 241.8795 -4.4089 412.2075 416.6164 380.2389 243.4790 -4.4045 412.0392 416.4437 380.0425 245.0829 -4.4035 411.8809 416.2844 379.8522 246.6825 -4.4009 411.7189 416.1198 379.6668 248.2914 -4.3971 411.5597 415.9568 379.4736 249.8961 -4.3946 411.3900 415.7846 379.2782 251.4899 -4.3937 411.2420 415.6357 379.0802 253.1149 -4.3900 411.0769 415.4668 378.8862 254.7190 -4.3871 410.9175 415.3046 378.7027 256.3285 -4.3844 410.7561 415.1406 378.5210 257.9326 -4.3808 410.5919 414.9727 378.3394 259.5421 -4.3781 410.4269 414.8050 378.1437 261.1465 -4.3757 410.2553 414.6310 377.9506 262.7558 -4.3732 410.0832 414.4564 377.7715 264.3756 -4.3708 409.9100 414.2808 377.5879 265.9796 -4.3661 409.7496 414.1157 377.3994 267.5946 -4.3632 409.5947 413.9579 377.2221 269.1990 -4.3597 409.4351 413.7948 377.0405 270.7980 -4.3551 409.2660 413.6211 376.8499 272.4025 -4.3522 409.1053 413.4574 376.6542 274.0065 -4.3491 408.9592 413.3084 376.4508 275.6060 -4.3470 408.7900 413.1369 376.2497 277.1945 -4.3442 408.6159 412.9601 376.0530 278.8146 -4.3399 408.4470 412.7869 375.8519 280.4184 -4.3344 408.2844 412.6188 375.6503 282.0281 -4.3301 408.1127 412.4428 375.4515 283.6320 -4.3276 407.9450 412.2726 375.2485 285.2213 -4.3234 407.7787 412.1020 375.0402 286.8303 -4.3196 407.6125 411.9321 374.8400 288.4348 -4.3148 407.4506 411.7654 374.6349 290.0439 -4.3105 407.2769 411.5874 374.4287 291.6640 -4.3084 407.1040 411.4123 374.2322 293.2730 -4.3069 406.9387 411.2456 374.0450 294.8623 -4.3041 406.7636 411.0677 373.8485 296.4663 -4.3005 406.5860 410.8865 373.6642 298.0759 -4.2958 406.4128 410.7086 373.4713 299.6800 -4.2928 406.2354 410.5282 373.2786 301.2895 -4.2916 406.0704 410.3620 373.0670 302.8990 -4.2865 405.8924 410.1789 372.8576 304.5236 -4.2820 405.7187 410.0007 372.6587 306.1280 -4.2782 405.5447 409.8229 372.4680 307.7219 -4.2753 405.3880 409.6632 372.2750 309.3315 -4.2723 405.2253 409.4976 372.0740 310.9355 -4.2675 405.0604 409.3280 371.8715 312.5196 -4.2651 404.8848 409.1499 371.6898 314.1286 -4.2615 404.6903 408.9518 371.5037 315.7333 -4.2571 404.5206 408.7776 371.3074 317.3576 -4.2526 404.3364 408.5891 371.1273 318.9624 -4.2490 404.1602 408.4091 370.9377 320.5715 -4.2450 403.9751 408.2200 370.7361 322.1760 -4.2426 403.7982 408.0408 370.5484 323.7803 -4.2407 403.6191 407.8598 370.3540 325.3896 -4.2364 403.4513 407.6877 370.1682 326.9941 -4.2289 403.2648 407.4937 369.9622 328.6196 -4.2246 403.0724 407.2970 369.7663 330.2248 -4.2204 402.8987 407.1191 369.5679 331.8353 -4.2174 402.7263 406.9437 369.3511 333.4405 -4.2124 402.5654 406.7778 369.1414 335.0560 -4.2094 402.3919 406.6013 368.9298 336.6454 -4.2033 402.2211 406.4244 368.7097 338.2510 -4.1923 402.0299 406.2222 368.5045 339.8559 -4.1811 401.8560 406.0371 368.2898 341.4718 -4.1741 401.6776 405.8517 368.0668 343.0715 -4.1684 401.5070 405.6754 367.8502 344.6818 -4.1635 401.3115 405.4750 367.6485 346.2820 -4.1589 401.1333 405.2921 367.4515 347.8868 -4.1528 400.9575 405.1102 367.2373 349.5025 -4.1484 400.7823 404.9307 367.0128 351.1075 -4.1445 400.5918 404.7363 366.8075 352.7024 -4.1416 400.4036 404.5451 366.6037 354.3231 -4.1390 400.2223 404.3613 366.4032 355.9331 -4.1343 400.0443 404.1786 366.1880 357.5388 -4.1309 399.8626 403.9935 365.9715 359.1486 -4.1254 399.6873 403.8127 365.7678 360.7541 -4.1223 399.5044 403.6267 365.5704 362.3591 -4.1180 399.3242 403.4422 365.3663 363.9696 -4.1119 399.1408 403.2527 365.1723 365.5901 -4.1075 398.9396 403.0471 364.9593 367.2006 -4.1020 398.7425 402.8445 364.7504 368.7904 -4.0974 398.5623 402.6597 364.5523 370.3951 -4.0933 398.3794 402.4727 364.3533 371.9958 -4.0888 398.2045 402.2933 364.1525 373.6005 -4.0839 398.0256 402.1095 363.9542 375.1959 -4.0797 397.8402 401.9200 363.7513 376.8059 -4.0770 397.6483 401.7253 363.5514 378.3961 -4.0725 397.4636 401.5360 363.3624 380.0164 -4.0662 397.2708 401.3371 363.1598 381.6214 -4.0609 397.0858 401.1467 362.9600 383.2115 -4.0576 396.8990 400.9566 362.7794 384.8214 -4.0548 396.7111 400.7659 362.5858 386.4270 -4.0517 396.5373 400.5890 362.3846 388.0370 -4.0466 396.3635 400.4102 362.2025 389.6423 -4.0436 396.1723 400.2159 362.0268 391.2475 -4.0394 395.9759 400.0153 361.8362 392.8420 -4.0360 395.7893 399.8253 361.6495 394.4631 -4.0335 395.6002 399.6338 361.4760 396.0731 -4.0300 395.4192 399.4491 361.2816 397.6788 -4.0254 395.2241 399.2494 361.0796 399.2886 -4.0215 395.0295 399.0510 360.8852 400.8943 -4.0145 394.8319 398.8464 360.6975 402.4940 -4.0119 394.6377 398.6496 360.4986 404.0893 -4.0082 394.4426 398.4507 360.3113 405.7148 -4.0015 394.2637 398.2652 360.1140 407.3146 -3.9985 394.0756 398.0742 359.9169 408.9253 -3.9951 393.8945 397.8896 359.7109 410.5249 -3.9890 393.7048 397.6938 359.5101 412.1305 -3.9837 393.5301 397.5139 359.3104 413.7405 -3.9793 393.3447 397.3240 359.1004 415.3304 -3.9761 393.1503 397.1265 358.8894 416.9408 -3.9726 392.9589 396.9315 358.6803 418.5611 -3.9691 392.7597 396.7288 358.4677 420.1666 -3.9632 392.5682 396.5314 358.2602 421.7765 -3.9564 392.3702 396.3266 358.0689 423.3820 -3.9529 392.1925 396.1454 357.8532 424.9921 -3.9474 392.0090 395.9563 357.6483 426.5974 -3.9425 391.8164 395.7589 357.4441 428.2078 -3.9401 391.6275 395.5676 357.2333 429.8281 -3.9370 391.4435 395.3805 357.0188 431.4336 -3.9328 391.2592 395.1920 356.8056 433.0436 -3.9283 391.0715 394.9998 356.6070 434.6493 -3.9245 390.8780 394.8025 356.4080 436.2591 -3.9202 390.6884 394.6086 356.2011 437.8598 -3.9150 390.5002 394.4152 356.0009 439.4594 -3.9100 390.3049 394.2149 355.8131 441.0801 -3.9045 390.1142 394.0188 355.6020 442.6853 -3.9018 389.9361 393.8378 355.3971 444.2850 -3.8961 389.7484 393.6445 355.1924 445.8958 -3.8918 389.5475 393.4393 354.9878 447.5005 -3.8877 389.3482 393.2360 354.7990 449.1111 -3.8835 389.1611 393.0446 354.6116 450.7161 -3.8793 388.9880 392.8672 354.4093 452.3364 -3.8739 388.7924 392.6663 354.2141 453.9471 -3.8692 388.5995 392.4688 354.0254 455.5519 -3.8648 388.4109 392.2757 353.8368 457.1624 -3.8621 388.2191 392.0813 353.6352 458.7675 -3.8584 388.0216 391.8800 353.4571 460.3781 -3.8519 387.8242 391.6761 353.2622 461.9831 -3.8487 387.6299 391.4786 353.0705 463.6034 -3.8433 387.4299 391.2733 352.8950 465.2141 -3.8402 387.2439 391.0840 352.7025 466.8189 -3.8354 387.0427 390.8781 352.5084 468.4295 -3.8321 386.8426 390.6747 352.3157 470.0243 -3.8276 386.6511 390.4788 352.1299 471.6241 -3.8226 386.4583 390.2809 351.9427 473.2348 -3.8185 386.2547 390.0732 351.7445 474.8499 -3.8133 386.0628 389.8761 351.5598 476.4555 -3.8103 385.8691 389.6794 351.3665 478.0655 -3.8043 385.6828 389.4871 351.1678 479.6711 -3.7983 385.4852 389.2835 350.9667 481.2708 -3.7919 385.2931 389.0849 350.7623 482.8814 -3.7883 385.1158 388.9040 350.5571 484.4864 -3.7841 384.9150 388.6990 350.3738 486.1118 -3.7795 384.7232 388.5027 350.1791 487.7174 -3.7749 384.5357 388.3105 349.9764 489.3273 -3.7710 384.3443 388.1152 349.7687 490.9328 -3.7654 384.1633 387.9287 349.5596 492.5378 -3.7605 383.9780 387.7385 349.3705 494.1484 -3.7569 383.7783 387.5352 349.1787 495.7534 -3.7530 383.5768 387.3298 348.9796 497.3789 -3.7477 383.3913 387.1390 348.7638 498.9844 -3.7443 383.1966 386.9409 348.5683 500.5741 -3.7393 383.0047 386.7441 348.3829 502.1795 -3.7358 382.8059 386.5417 348.1778 503.7794 -3.7314 382.6066 386.3381 347.9831 505.3849 -3.7258 382.4092 386.1350 347.7767 506.9896 -3.7199 382.2198 385.9397 347.5975 508.5950 -3.7151 382.0267 385.7417 347.4184 510.1848 -3.7112 381.8347 385.5459 347.2098 511.8049 -3.7072 381.6463 385.3536 347.0031 513.4106 -3.7026 381.4541 385.1567 346.8178 515.0206 -3.6972 381.2706 384.9678 346.6250 516.6263 -3.6928 381.0650 384.7579 346.4298 518.2361 -3.6874 380.8765 384.5639 346.2432 519.8414 -3.6833 380.6971 384.3803 346.0553 521.4518 -3.6784 380.5022 384.1805 345.8726 523.0719 -3.6723 380.3076 383.9799 345.6735 524.6775 -3.6689 380.1154 383.7843 345.4773 526.2875 -3.6647 379.9092 383.5740 345.2957 527.8933 -3.6585 379.7018 383.3604 345.1051 529.5031 -3.6553 379.5165 383.1717 344.9095 531.1086 -3.6503 379.3220 382.9723 344.7132 532.7136 -3.6464 379.1289 382.7753 344.5133 534.2983 -3.6411 378.9255 382.5666 344.3039 535.9241 -3.6359 378.7405 382.3764 344.0901 537.5240 -3.6295 378.5486 382.1781 343.8892 539.1295 -3.6261 378.3569 381.9831 343.6840 540.7189 -3.6220 378.1764 381.7983 343.4716 542.3294 -3.6165 377.9689 381.5853 343.2603 543.9345 -3.6102 377.7815 381.3917 343.0453 545.5444 -3.6065 377.5818 381.1883 342.8360 547.1399 -3.6014 377.3857 380.9871 342.6201 548.7498 -3.5968 377.1853 380.7820 342.4106 550.3706 -3.5924 376.9798 380.5722 342.2074 551.9859 -3.5881 376.7897 380.3778 342.0009 553.5910 -3.5834 376.5988 380.1821 341.7937 555.1964 -3.5792 376.4007 379.9799 341.5819 556.8063 -3.5743 376.2090 379.7832 341.3733 558.4118 -3.5689 376.0113 379.5803 341.1599 560.0219 -3.5640 375.8126 379.3766 340.9551 561.6428 -3.5600 375.6105 379.1705 340.7750 563.2580 -3.5562 375.4165 378.9727 340.5700 564.8425 -3.5525 375.2287 378.7812 340.3722 566.4429 -3.5497 375.0405 378.5902 340.1625 568.0528 -3.5443 374.8423 378.3867 339.9667 569.6583 -3.5384 374.6620 378.2004 339.7646 571.2581 -3.5305 374.4578 377.9883 339.5729 572.8630 -3.5261 374.2602 377.7863 339.3607 574.4686 -3.5206 374.0682 377.5888 339.1532 576.0785 -3.5154 373.8807 377.3961 338.9494 577.6835 -3.5114 373.6790 377.1903 338.7528 579.2890 -3.5078 373.4833 376.9911 338.5444 580.8989 -3.5034 373.2943 376.7977 338.3474 582.5045 -3.4969 373.1054 376.6023 338.1621 584.1145 -3.4925 372.9151 376.4076 337.9557 585.7198 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