DTA measure 11_meres Date: 2024116:945 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1503.53 s Mass = 100.000 mg data_number = 1867 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2315 0.2357 150.8864 150.6507 186.7798 1.9933 0.2416 151.0587 150.8171 186.7800 2.8453 0.2469 151.2773 151.0303 186.7851 3.6068 0.2530 151.4493 151.1962 186.7761 4.4288 0.2618 151.6294 151.3677 186.7850 5.2508 0.2675 151.8011 151.5336 186.7866 6.0125 0.2728 151.9616 151.6889 186.7891 6.8648 0.2793 152.1660 151.8867 186.7992 7.6568 0.2861 152.3492 152.0632 186.8175 8.4485 0.2929 152.5282 152.2354 186.8484 9.2713 0.2981 152.7091 152.4110 186.8773 10.0335 0.3024 152.8905 152.5881 186.9146 10.8858 0.3082 153.0757 152.7675 186.9411 11.6778 0.3135 153.2403 152.9268 186.9890 12.4695 0.3217 153.4235 153.1019 187.0535 13.2918 0.3264 153.6029 153.2765 187.1243 14.0835 0.3311 153.7658 153.4347 187.1916 14.9055 0.3370 153.9388 153.6018 187.2743 15.6975 0.3408 154.1126 153.7718 187.3649 16.4905 0.3466 154.2808 153.9342 187.4527 17.3128 0.3495 154.4741 154.1246 187.5584 18.1030 0.3556 154.6660 154.3104 187.6756 18.9210 0.3622 154.8251 154.4629 187.7927 19.7088 0.3651 154.9893 154.6242 187.9452 20.4970 0.3688 155.1590 154.7902 188.0679 21.3153 0.3721 155.3505 154.9783 188.2038 22.1040 0.3758 155.5210 155.1452 188.3383 22.9220 0.3829 155.6924 155.3094 188.4779 23.7100 0.3870 155.8724 155.4854 188.6196 24.4990 0.3912 156.0381 155.6469 188.7852 25.3478 0.3975 156.2100 155.8125 188.9455 26.1070 0.3994 156.3844 155.9850 189.0989 26.9273 0.4012 156.5566 156.1554 189.2595 27.7160 0.4055 156.7201 156.3147 189.4200 28.5050 0.4104 156.8953 156.4849 189.5871 29.3535 0.4142 157.0715 156.6573 189.7512 30.1120 0.4153 157.2321 156.8168 189.9070 30.9310 0.4169 157.4311 157.0142 190.0844 31.7500 0.4159 157.5883 157.1724 190.2702 32.5115 0.4173 157.7348 157.3175 190.4167 33.3635 0.4226 157.9085 157.4859 190.5916 34.1255 0.4259 158.0642 157.6383 190.7464 34.9465 0.4277 158.2431 157.8155 190.9205 35.7383 0.4303 158.4045 157.9742 191.0822 36.5295 0.4340 158.5737 158.1397 191.2236 37.3825 0.4343 158.7469 158.3126 191.3899 38.1435 0.4368 158.9030 158.4662 191.5441 38.9658 0.4391 159.0792 158.6400 191.7057 39.7580 0.4416 159.2577 158.8161 191.8441 40.5495 0.4416 159.4187 158.9771 191.9932 41.3720 0.4397 159.5786 159.1389 192.1459 42.1635 0.4431 159.7686 159.3254 192.2900 42.9858 0.4451 159.9245 159.4794 192.4437 43.7778 0.4440 160.0901 159.6461 192.5628 44.5695 0.4462 160.2657 159.8195 192.7006 45.3918 0.4485 160.4175 159.9691 192.8315 46.1535 0.4473 160.5828 160.1355 192.9529 47.0058 0.4502 160.7600 160.3099 193.0836 47.7978 0.4502 160.9243 160.4741 193.2238 48.5923 0.4537 161.0621 160.6085 193.3499 49.4168 0.4548 161.2542 160.7994 193.4804 50.1785 0.4529 161.4205 160.9677 193.6102 51.0308 0.4573 161.5915 161.1341 193.7398 51.8225 0.4599 161.7241 161.2642 193.8636 52.6145 0.4629 161.8900 161.4271 193.9983 53.4365 0.4618 162.0772 161.6154 194.1296 54.1985 0.4595 162.2411 161.7817 194.2612 55.0505 0.4607 162.4051 161.9443 194.3761 55.8425 0.4621 162.5683 162.1062 194.4859 56.6345 0.4660 162.7231 162.2571 194.6082 57.4565 0.4649 162.8847 162.4198 194.7488 58.2185 0.4636 163.0503 162.5868 194.8612 59.0700 0.4669 163.2112 162.7443 194.9891 59.8323 0.4662 163.3637 162.8975 195.0969 60.6540 0.4656 163.5377 163.0721 195.2182 61.4760 0.4641 163.7293 163.2653 195.3473 62.2375 0.4641 163.8754 163.4113 195.4587 63.0900 0.4639 164.0371 163.5732 195.5870 63.8515 0.4655 164.1832 163.7177 195.6855 64.6738 0.4656 164.3603 163.8947 195.8130 65.4960 0.4668 164.5255 164.0588 195.9264 66.2585 0.4649 164.6671 164.2022 196.0323 67.1108 0.4676 164.8338 164.3662 196.1578 67.8725 0.4694 164.9896 164.5203 196.2905 68.6948 0.4697 165.1728 164.7032 196.4016 69.4918 0.4713 165.3324 164.8611 196.5272 70.2835 0.4688 165.5015 165.0327 196.6610 71.1058 0.4678 165.6616 165.1938 196.7946 71.8975 0.4656 165.8203 165.3547 196.9358 72.7195 0.4662 165.9719 165.5058 197.0730 73.5115 0.4653 166.1371 165.6718 197.1790 74.3035 0.4645 166.2845 165.8200 197.2997 75.1255 0.4650 166.4493 165.9843 197.4593 75.9175 0.4659 166.6109 166.1450 197.5933 76.7395 0.4656 166.7731 166.3074 197.7371 77.5315 0.4626 166.9308 166.4682 197.8754 78.3235 0.4661 167.0955 166.6294 197.9987 79.1455 0.4626 167.2476 166.7850 198.1439 79.9375 0.4605 167.4084 166.9479 198.2630 80.7590 0.4534 167.5748 167.1214 198.4048 81.6413 0.4489 167.7376 167.2887 198.5574 82.4935 0.4475 167.9066 167.4591 198.7028 83.3113 0.4475 168.0633 167.6158 198.8518 84.0980 0.4472 168.2218 167.7746 198.9739 84.8850 0.4472 168.3703 167.9231 199.1072 85.7333 0.4417 168.5411 168.0994 199.2634 86.4913 0.4434 168.6914 168.2480 199.3872 87.3105 0.4431 168.8462 168.4031 199.5392 88.0985 0.4426 169.0149 168.5723 199.6745 88.8870 0.4421 169.1695 168.7274 199.8060 89.7350 0.4480 169.3232 168.8752 199.9417 90.4933 0.4502 169.4853 169.0351 200.0598 91.3130 0.4489 169.6338 169.1849 200.1922 92.1013 0.4468 169.7947 169.3478 200.3440 92.8900 0.4442 169.9541 169.5098 200.5003 93.7390 0.4445 170.1131 169.6686 200.6289 94.4990 0.4443 170.2598 169.8155 200.7597 95.3185 0.4406 170.4150 169.9744 200.9053 96.1073 0.4381 170.5757 170.1375 201.0400 96.8975 0.4404 170.7274 170.2870 201.1921 97.7470 0.4375 170.8914 170.4539 201.3301 98.5073 0.4394 171.0483 170.6088 201.4613 99.3288 0.4365 171.1966 170.7601 201.5984 100.1208 0.4329 171.3660 170.9332 201.7434 100.9125 0.4313 171.5222 171.0909 201.8692 101.7335 0.4308 171.6736 171.2427 202.0025 102.4955 0.4275 171.8182 171.3907 202.1334 103.3478 0.4267 171.9747 171.5480 202.2730 104.1108 0.4255 172.1242 171.6987 202.4174 104.9348 0.4220 172.2974 171.8754 202.5581 105.7568 0.4218 172.4370 172.0152 202.7043 106.5185 0.4203 172.5812 172.1609 202.8120 107.3708 0.4184 172.7544 172.3360 202.9438 108.1325 0.4158 172.9013 172.4855 203.0817 108.9545 0.4149 173.0599 172.6449 203.2455 109.7465 0.4135 173.2268 172.8133 203.3736 110.5685 0.4118 173.3812 172.9695 203.4906 111.5105 0.4075 173.5602 173.1527 203.6393 112.2725 0.4029 173.7009 173.2980 203.7779 113.0945 0.4009 173.8735 173.4726 203.9189 113.9165 0.4002 174.0150 173.6147 204.0600 114.6785 0.3978 174.1611 173.7632 204.1964 115.5305 0.3973 174.3377 173.9404 204.3284 116.2923 0.3962 174.4741 174.0779 204.4575 117.1143 0.3944 174.6437 174.2492 204.5822 117.9063 0.3926 174.8017 174.4091 204.7111 118.6978 0.3899 174.9411 174.5512 204.8270 119.5500 0.3883 175.1061 174.7178 204.9764 120.3118 0.3836 175.2578 174.8742 205.0945 121.1338 0.3803 175.4235 175.0432 205.2361 121.9260 0.3777 175.5807 175.2030 205.3628 122.7175 0.3755 175.7083 175.3328 205.4983 123.5698 0.3751 175.8782 175.5031 205.6189 124.3315 0.3740 176.0340 175.6600 205.7547 125.2140 0.3695 176.1767 175.8072 205.8930 126.0055 0.3678 176.3264 175.9587 206.0254 126.8578 0.3662 176.4980 176.1318 206.1599 127.6195 0.3637 176.6449 176.2812 206.2875 128.4418 0.3624 176.8046 176.4422 206.4291 129.2335 0.3598 176.9714 176.6116 206.5783 130.0555 0.3579 177.1113 176.7534 206.6931 131.0575 0.3581 177.3088 176.9507 206.8300 132.1195 0.3540 177.5259 177.1719 207.0018 132.9715 0.3523 177.6901 177.3378 207.1472 133.7935 0.3503 177.8521 177.5018 207.2742 134.5855 0.3484 177.9846 177.6362 207.3917 135.3775 0.3393 178.1282 177.7889 207.5245 136.2295 0.3327 178.2893 177.9566 207.6602 136.9915 0.3294 178.4447 178.1153 207.7834 137.8135 0.3285 178.6061 178.2776 207.9146 138.6055 0.3258 178.7508 178.4250 208.0263 139.3968 0.3287 178.9044 178.5757 208.1627 140.2495 0.3291 179.0624 178.7333 208.2942 141.0118 0.3287 179.2026 178.8739 208.4004 141.8345 0.3239 179.3621 179.0382 208.5202 142.6268 0.3206 179.5245 179.2039 208.6497 143.4195 0.3209 179.6797 179.3588 208.7827 144.2418 0.3199 179.8326 179.5127 208.9082 145.0335 0.3160 179.9828 179.6668 209.0291 145.8565 0.3134 180.1321 179.8187 209.1660 146.6463 0.3151 180.2811 179.9660 209.2860 147.4350 0.3125 180.4216 180.1092 209.4014 148.2525 0.3101 180.5804 180.2703 209.5356 149.0100 0.3091 180.7097 180.4006 209.6540 149.8575 0.3095 180.8834 180.5739 209.7762 150.7050 0.3048 181.0508 180.7460 209.8944 151.6430 0.3025 181.2245 180.9221 210.0417 152.5210 0.3006 181.3997 181.0991 210.1776 153.3390 0.2977 181.5560 181.2583 210.3127 154.0970 0.2959 181.6927 181.3968 210.4259 154.9450 0.2940 181.8480 181.5540 210.5648 155.7330 0.2911 181.9961 181.7050 210.7073 156.5220 0.2895 182.1524 181.8629 210.8445 157.3400 0.2898 182.3024 182.0126 210.9715 158.0980 0.2901 182.4439 182.1538 211.0960 158.9473 0.2913 182.6162 182.3249 211.2440 159.7360 0.2925 182.7618 182.4693 211.4015 160.5265 0.2895 182.9213 182.6317 211.5300 161.3470 0.2869 183.0938 182.8069 211.6820 162.1060 0.2834 183.2421 182.9587 211.8236 163.0448 0.2811 183.3981 183.1170 211.9828 164.1073 0.2876 183.5946 183.3070 212.1754 164.8988 0.2854 183.7232 183.4378 212.3030 165.7475 0.2810 183.9031 183.6222 212.4716 166.6868 0.2711 184.0847 183.8136 212.6469 167.5385 0.2665 184.2608 183.9943 212.7866 168.3648 0.2640 184.4078 184.1438 212.9331 169.1585 0.2677 184.5415 184.2738 213.0893 169.9805 0.2628 184.6908 184.4280 213.2395 170.7725 0.2597 184.8377 184.5780 213.3908 171.5945 0.2581 184.9955 184.7373 213.5467 172.3865 0.2524 185.1429 184.8906 213.6815 173.1785 0.2452 185.2926 185.0474 213.8100 174.0005 0.2399 185.4523 185.2124 213.9558 174.7923 0.2354 185.5802 185.3448 214.0788 175.6140 0.2367 185.7388 185.5021 214.2087 176.4060 0.2383 185.8944 185.6561 214.3251 177.1975 0.2375 186.0471 185.8096 214.4607 178.0200 0.2360 186.2073 185.9713 214.5908 178.8115 0.2314 186.3443 186.1129 214.7018 179.6338 0.2258 186.5105 186.2847 214.8358 180.5760 0.2207 186.6797 186.4590 214.9904 181.3975 0.2203 186.8353 186.6151 215.0996 182.2195 0.2166 186.9899 186.7732 215.2194 183.0418 0.2101 187.1544 186.9443 215.3511 183.8638 0.2067 187.2925 187.0858 215.4676 184.6858 0.2035 187.4544 187.2509 215.5949 185.5978 0.2078 187.6336 187.4258 215.7265 186.3595 0.2050 187.7672 187.5622 215.8293 187.1818 0.2026 187.9170 187.7143 215.9533 187.9735 0.2000 188.0851 187.8851 216.0477 188.7655 0.1968 188.2298 188.0330 216.1581 189.5875 0.1939 188.3848 188.1909 216.3000 190.3795 0.1931 188.5398 188.3467 216.4103 191.2015 0.1858 188.6912 188.5055 216.5643 191.9935 0.1805 188.8297 188.6492 216.6765 192.8455 0.1802 188.9930 188.8128 216.8188 193.6675 0.1848 189.1334 188.9486 216.9527 194.4895 0.1841 189.3101 189.1260 217.0995 195.3115 0.1821 189.4598 189.2777 217.2353 196.0735 0.1801 189.5964 189.4164 217.3522 196.9260 0.1786 189.7564 189.5778 217.4921 197.6885 0.1773 189.9006 189.7233 217.6147 198.5098 0.1768 190.0644 189.8875 217.7530 199.3323 0.1730 190.2245 190.0515 217.8917 200.0945 0.1719 190.3570 190.1851 218.0242 200.9470 0.1640 190.5136 190.3496 218.1729 201.7085 0.1588 190.6637 190.5049 218.3047 202.5308 0.1544 190.8032 190.6489 218.4437 203.3228 0.1577 190.9528 190.7951 218.5831 204.2348 0.1596 191.1336 190.9740 218.7436 204.9965 0.1520 191.2679 191.1159 218.8657 205.8188 0.1475 191.4271 191.2796 219.0114 206.6108 0.1529 191.5720 191.4191 219.1442 207.4035 0.1530 191.7147 191.5617 219.2699 208.2555 0.1542 191.8754 191.7212 219.4046 209.0175 0.1501 192.0081 191.8580 219.5418 209.8395 0.1413 192.1753 192.0339 219.6912 210.6608 0.1342 192.3262 192.1920 219.8204 211.5390 0.1330 192.4940 192.3610 219.9903 212.2973 0.1335 192.6239 192.4904 220.1135 213.1160 0.1322 192.7779 192.6457 220.2470 213.9045 0.1297 192.9252 192.7956 220.3845 214.6930 0.1270 193.0717 192.9446 220.5195 215.5410 0.1261 193.2364 193.1103 220.6659 216.2990 0.1222 193.3674 193.2452 220.7688 217.1188 0.1205 193.5155 193.3950 220.9200 217.9070 0.1181 193.6835 193.5654 221.0615 218.6950 0.1174 193.8214 193.7040 221.1894 219.5438 0.1147 193.9876 193.8729 221.3262 220.3020 0.1153 194.1305 194.0152 221.4673 221.1208 0.1091 194.2677 194.1586 221.6054 221.9393 0.1057 194.4142 194.3085 221.7338 222.7060 0.1052 194.5569 194.4517 221.8664 223.5328 0.1053 194.7274 194.6221 222.0134 224.3228 0.1048 194.8732 194.7685 222.1389 225.1425 0.1039 195.0310 194.9270 222.2712 225.9335 0.1019 195.1719 195.0699 222.4124 226.7245 0.1005 195.3184 195.2179 222.5683 227.5465 0.0945 195.4697 195.3752 222.6923 228.3080 0.0899 195.6136 195.5237 222.8291 229.1588 0.0877 195.7687 195.6811 222.9713 229.9505 0.0858 195.9089 195.8232 223.1021 230.7423 0.0844 196.0607 195.9763 223.2331 231.5645 0.0801 196.2168 196.1367 223.3775 232.3260 0.0772 196.3434 196.2662 223.4990 233.1780 0.0745 196.4967 196.4222 223.6259 233.9398 0.0732 196.6583 196.5851 223.7624 234.7618 0.0718 196.8034 196.7316 223.9017 235.5838 0.0696 196.9534 196.8839 224.0306 236.3455 0.0736 197.0941 197.0205 224.1739 237.1978 0.0669 197.2720 197.2050 224.3037 237.9595 0.0630 197.4054 197.3424 224.4363 238.7818 0.0627 197.5417 197.4790 224.5733 239.5738 0.0591 197.7051 197.6459 224.7065 240.3655 0.0616 197.8554 197.7938 224.8444 241.2178 0.0536 198.0267 197.9731 224.9557 241.9795 0.0515 198.1525 198.1010 225.0985 242.8018 0.0491 198.3004 198.2513 225.2477 243.5843 0.0482 198.4562 198.4080 225.3707 244.4065 0.0448 198.6062 198.5614 225.4997 245.1985 0.0418 198.7374 198.6956 225.6381 245.9905 0.0412 198.8954 198.8541 225.7756 246.8125 0.0441 199.0557 199.0116 225.9050 247.6045 0.0398 199.2060 199.1662 226.0425 248.4265 0.0358 199.3488 199.3130 226.1741 249.2185 0.0353 199.4902 199.4549 226.2934 250.0105 0.0324 199.6483 199.6159 226.4384 250.8325 0.0278 199.7958 199.7681 226.5719 251.6245 0.0278 199.9369 199.9091 226.6969 252.4465 0.0273 200.0939 200.0666 226.8215 253.2385 0.0215 200.2592 200.2377 226.9455 254.0303 0.0315 200.4092 200.3776 227.0769 254.8523 0.0241 200.5445 200.5204 227.2022 255.6443 0.0304 200.6820 200.6515 227.3243 256.4665 0.0180 200.8254 200.8075 227.4558 257.2590 0.0076 200.9836 200.9760 227.5806 258.0515 0.0037 201.1499 201.1463 227.7120 258.8738 0.0043 201.2948 201.2905 227.8464 259.6355 0.0074 201.4362 201.4288 227.9925 260.4878 0.0166 201.5832 201.5666 228.1229 261.2798 0.0026 201.7374 201.7348 228.2574 262.0725 -0.0043 201.8726 201.8769 228.3739 262.8948 -0.0083 202.0450 202.0533 228.5080 263.6715 -0.0085 202.1712 202.1797 228.6357 264.5088 -0.0037 202.3336 202.3372 228.7692 265.2705 -0.0056 202.4811 202.4867 228.8953 266.1228 -0.0145 202.6410 202.6555 229.0179 266.8845 -0.0010 202.7767 202.7777 229.1248 267.7065 -0.0012 202.9413 202.9425 229.2557 268.5288 -0.0150 203.0889 203.1040 229.3937 269.2915 -0.0181 203.2260 203.2440 229.5248 270.1435 -0.0234 203.3764 203.3998 229.6704 270.9055 -0.0265 203.5161 203.5426 229.7825 271.7275 -0.0257 203.6760 203.7017 229.9076 272.5495 -0.0262 203.8272 203.8534 230.0538 273.3115 -0.0286 203.9734 204.0020 230.1676 274.1638 -0.0309 204.1293 204.1602 230.3020 274.9248 -0.0355 204.2710 204.3065 230.4257 275.7435 -0.0379 204.4204 204.4583 230.5596 276.5620 -0.0377 204.5557 204.5934 230.6773 277.3198 -0.0403 204.7049 204.7452 230.7917 278.1683 -0.0438 204.8551 204.8990 230.9383 278.9270 -0.0460 205.0008 205.0468 231.0340 279.7460 -0.0448 205.1557 205.2005 231.1708 280.5638 -0.0468 205.3097 205.3565 231.2964 281.3218 -0.0487 205.4422 205.4909 231.4195 282.1705 -0.0496 205.6074 205.6570 231.5428 282.9590 -0.0536 205.7519 205.8055 231.6548 283.7475 -0.0563 205.9068 205.9631 231.7926 284.5663 -0.0581 206.0574 206.1154 231.9240 285.3550 -0.0592 206.2025 206.2617 232.0399 286.1733 -0.0608 206.3407 206.4015 232.1774 286.9623 -0.0644 206.5151 206.5796 232.3214 287.7533 -0.0647 206.6596 206.7243 232.4554 288.5728 -0.0667 206.8070 206.8737 232.5760 289.3610 -0.0656 206.9577 207.0233 232.7117 290.1810 -0.0697 207.0910 207.1608 232.8328 290.9708 -0.0716 207.2393 207.3109 232.9759 291.7610 -0.0723 207.3812 207.4535 233.1239 292.6120 -0.0757 207.5424 207.6181 233.2705 293.3728 -0.0769 207.6869 207.7638 233.4137 294.1948 -0.0762 207.8270 207.9032 233.5415 294.9868 -0.0779 207.9814 208.0594 233.6786 295.7780 -0.0812 208.1320 208.2132 233.8249 296.6005 -0.0837 208.2801 208.3638 233.9649 297.3925 -0.0853 208.4313 208.5167 234.1144 298.2148 -0.0876 208.5867 208.6743 234.2710 299.0065 -0.0871 208.7282 208.8152 234.4257 299.7988 -0.0860 208.8671 208.9531 234.5700 300.6205 -0.0885 209.0335 209.1220 234.7037 301.4125 -0.0925 209.1842 209.2767 234.8567 302.2348 -0.0958 209.3282 209.4241 234.9997 303.0265 -0.0983 209.4717 209.5700 235.1510 303.8185 -0.0987 209.6301 209.7287 235.2769 304.6408 -0.0982 209.7638 209.8620 235.4144 305.4325 -0.1001 209.9086 210.0087 235.5361 306.2545 -0.1008 210.0693 210.1701 235.6751 307.0465 -0.1041 210.2130 210.3171 235.8199 307.8385 -0.1066 210.3689 210.4755 235.9408 308.6605 -0.1093 210.5362 210.6456 236.0571 309.4530 -0.1083 210.6678 210.7761 236.1942 310.2765 -0.1112 210.8079 210.9191 236.3112 311.0685 -0.1122 210.9663 211.0786 236.4365 311.8605 -0.1151 211.1136 211.2286 236.5680 312.6823 -0.1160 211.2522 211.3682 236.6990 313.4738 -0.1155 211.3859 211.5014 236.8106 314.2960 -0.1154 211.5425 211.6579 236.9277 315.0883 -0.1173 211.6974 211.8147 237.0389 315.8795 -0.1180 211.8369 211.9548 237.1567 316.7318 -0.1229 212.0065 212.1294 237.2854 317.4935 -0.1267 212.1518 212.2784 237.4049 318.3158 -0.1277 212.3014 212.4291 237.5142 319.1078 -0.1276 212.4451 212.5726 237.6578 319.8995 -0.1297 212.6287 212.7584 237.7799 320.7518 -0.1306 212.7658 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