DTA measure 12meresb Date: 2024116:1055 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1531.05 s Mass = 100.000 mg data_number = 1905 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.0563 -0.4878 235.6659 236.1537 233.6894 1.8778 -0.4859 235.7221 236.2080 233.7061 2.6653 -0.4852 235.7639 236.2491 233.7217 3.4533 -0.4864 235.8052 236.2916 233.7323 4.3015 -0.4867 235.8379 236.3246 233.7443 5.0590 -0.4869 235.8902 236.3771 233.7522 5.8783 -0.4864 235.9365 236.4230 233.7557 6.6665 -0.4862 235.9810 236.4672 233.7860 7.4555 -0.4874 236.0191 236.5064 233.8076 8.2775 -0.4849 236.0630 236.5479 233.8207 9.0660 -0.4841 236.1152 236.5994 233.8468 9.8853 -0.4846 236.1642 236.6488 233.8974 10.6738 -0.4829 236.2029 236.6858 233.9349 11.4640 -0.4829 236.2306 236.7135 233.9519 12.2828 -0.4834 236.2881 236.7715 234.0106 13.0710 -0.4817 236.3347 236.8164 234.0647 13.8905 -0.4823 236.3759 236.8581 234.1244 14.6818 -0.4847 236.4142 236.8990 234.1839 15.4710 -0.4847 236.4444 236.9290 234.2442 16.3200 -0.4841 236.5016 236.9857 234.3320 17.0800 -0.4846 236.5284 237.0130 234.4040 17.9018 -0.4863 236.5770 237.0632 234.4802 18.6930 -0.4886 236.6155 237.1040 234.5591 19.4845 -0.4883 236.6518 237.1401 234.6423 20.3073 -0.4882 236.6924 237.1806 234.7237 21.0695 -0.4908 236.7332 237.2240 234.8141 21.9215 -0.4889 236.7877 237.2765 234.9256 22.7138 -0.4908 236.8301 237.3209 235.0113 23.5090 -0.4910 236.8589 237.3499 235.1151 24.3308 -0.4903 236.9095 237.3998 235.2187 25.0925 -0.4930 236.9561 237.4492 235.3163 25.9448 -0.4936 237.0016 237.4952 235.4424 26.7065 -0.4946 237.0491 237.5437 235.5700 27.5288 -0.4950 237.0803 237.5753 235.6763 28.3205 -0.4956 237.1080 237.6036 235.7982 29.1125 -0.4967 237.1533 237.6500 235.9064 29.9645 -0.5002 237.2155 237.7158 236.0385 30.7265 -0.5005 237.2362 237.7368 236.1540 31.5485 -0.4993 237.2774 237.7767 236.2883 32.3405 -0.5013 237.3207 237.8220 236.3873 33.1325 -0.5036 237.3753 237.8788 236.5333 33.9553 -0.5047 237.4155 237.9202 236.6518 34.7485 -0.5052 237.4597 237.9650 236.7770 35.5705 -0.5064 237.4962 238.0026 236.9050 36.3620 -0.5081 237.5342 238.0422 237.0258 37.1543 -0.5066 237.5691 238.0756 237.1446 37.9760 -0.5095 237.6267 238.1362 237.2638 38.7375 -0.5110 237.6675 238.1785 237.3716 39.5898 -0.5138 237.7147 238.2285 237.4698 40.3818 -0.5165 237.7555 238.2720 237.5818 41.1735 -0.5189 237.7884 238.3073 237.6956 41.9958 -0.5219 237.8414 238.3634 237.8089 42.7575 -0.5234 237.8888 238.4122 237.9153 43.6150 -0.5245 237.9314 238.4559 238.0330 44.3825 -0.5269 237.9655 238.4924 238.1283 45.2048 -0.5296 238.0365 238.5661 238.2337 45.9968 -0.5303 238.0616 238.5919 238.3243 46.7885 -0.5316 238.0902 238.6218 238.4190 47.6408 -0.5330 238.1343 238.6673 238.5334 48.4025 -0.5338 238.1969 238.7306 238.6293 49.2248 -0.5369 238.2369 238.7738 238.7248 50.0168 -0.5393 238.2730 238.8123 238.8168 50.8095 -0.5416 238.3244 238.8660 238.9226 51.6315 -0.5425 238.3671 238.9097 239.0218 52.4235 -0.5440 238.4124 238.9563 239.1031 53.2463 -0.5504 238.4700 239.0204 239.2029 54.0385 -0.5503 238.5050 239.0553 239.2970 54.8305 -0.5520 238.5432 239.0952 239.4089 55.6525 -0.5530 238.5872 239.1402 239.5045 56.4143 -0.5537 238.6260 239.1796 239.5719 57.2665 -0.5576 238.6616 239.2192 239.6702 58.0585 -0.5604 238.7209 239.2813 239.7539 58.8498 -0.5612 238.7617 239.3228 239.8582 59.6720 -0.5651 238.8079 239.3730 239.9599 60.4335 -0.5673 238.8472 239.4145 240.0355 61.2860 -0.5665 238.9015 239.4680 240.1453 62.0778 -0.5715 238.9581 239.5296 240.2377 62.8705 -0.5746 239.0068 239.5814 240.3199 63.6928 -0.5752 239.0414 239.6166 240.4292 64.4545 -0.5777 239.0835 239.6613 240.5242 65.3065 -0.5788 239.1427 239.7215 240.6262 66.0950 -0.5790 239.1799 239.7589 240.7234 66.8830 -0.5805 239.2154 239.7959 240.8217 67.7010 -0.5851 239.2697 239.8548 240.9335 68.4590 -0.5870 239.3106 239.8976 241.0292 69.3080 -0.5902 239.3788 239.9690 241.1509 70.0960 -0.5790 239.4211 240.0001 241.2671 70.8840 -0.5682 239.4749 240.0431 241.3570 71.7020 -0.5562 239.5200 240.0762 241.4714 72.4600 -0.5516 239.5675 240.1191 241.5689 73.3080 -0.5533 239.6151 240.1684 241.6861 74.0960 -0.5612 239.6693 240.2305 241.7896 74.8840 -0.5641 239.7241 240.2882 241.9046 75.7028 -0.5657 239.7536 240.3193 242.0140 76.4920 -0.5703 239.8176 240.3879 242.1067 77.3100 -0.5745 239.8599 240.4345 242.2169 78.0980 -0.5776 239.9197 240.4973 242.3245 78.8870 -0.5816 239.9541 240.5357 242.4327 79.7065 -0.5813 240.0081 240.5894 242.5338 80.4973 -0.5794 240.0512 240.6306 242.6368 81.3168 -0.5791 240.0991 240.6782 242.7545 82.1053 -0.5795 240.1425 240.7219 242.8621 82.8958 -0.5858 240.2042 240.7900 242.9477 83.7470 -0.5833 240.2600 240.8433 243.0518 84.5075 -0.5891 240.3168 240.9058 243.1536 85.3295 -0.5929 240.3698 240.9627 243.2738 86.1515 -0.5928 240.4318 241.0246 243.3697 86.9125 -0.5933 240.4666 241.0598 243.4710 87.7645 -0.5925 240.5205 241.1130 243.5766 88.5258 -0.5927 240.5722 241.1648 243.6721 89.3475 -0.5956 240.6268 241.2224 243.7873 90.1695 -0.6005 240.6779 241.2784 243.8777 90.9313 -0.6028 240.7213 241.3240 243.9820 91.7835 -0.6039 240.7812 241.3851 244.0933 92.5453 -0.6069 240.8392 241.4462 244.1922 93.3673 -0.6113 240.9003 241.5116 244.2859 94.1895 -0.6139 240.9445 241.5584 244.4083 94.9513 -0.6142 241.0015 241.6157 244.5048 95.8033 -0.6156 241.0443 241.6599 244.5917 96.5650 -0.6178 241.0966 241.7144 244.6933 97.3868 -0.6244 241.1595 241.7839 244.7972 98.2088 -0.6245 241.2120 241.8365 244.8910 98.9705 -0.6263 241.2607 241.8870 244.9918 99.8228 -0.6263 241.3206 241.9469 245.0982 100.5848 -0.6230 241.3800 242.0030 245.1796 101.4068 -0.6252 241.4274 242.0526 245.2784 102.2288 -0.6279 241.5092 242.1371 245.3803 102.9905 -0.6310 241.5615 242.1925 245.4711 103.8428 -0.6340 241.6082 242.2422 245.5923 104.6045 -0.6366 241.6520 242.2886 245.6878 105.4268 -0.6363 241.7187 242.3549 245.7969 106.2488 -0.6402 241.7811 242.4213 245.8979 107.0105 -0.6408 241.8280 242.4687 245.9997 107.8625 -0.6416 241.9001 242.5417 246.0893 108.6245 -0.6435 241.9376 242.5811 246.1981 109.4465 -0.6464 242.0010 242.6474 246.3129 110.2685 -0.6457 242.0584 242.7042 246.4153 111.0305 -0.6479 242.1162 242.7641 246.5368 111.8825 -0.6509 242.1880 242.8390 246.6518 112.6445 -0.6486 242.2305 242.8791 246.7665 113.4665 -0.6517 242.2873 242.9390 246.8677 114.2885 -0.6544 242.3370 242.9914 246.9865 115.0503 -0.6563 242.4050 243.0613 247.0972 115.9023 -0.6574 242.4773 243.1347 247.2199 116.6643 -0.6614 242.5443 243.2057 247.3236 117.4858 -0.6660 242.5778 243.2438 247.4291 118.3093 -0.6674 242.6385 243.3059 247.5410 119.0705 -0.6647 242.6961 243.3608 247.6407 119.9228 -0.6669 242.7628 243.4296 247.7447 120.7148 -0.6765 242.8307 243.5072 247.8756 121.5075 -0.6885 242.8905 243.5789 247.9817 122.3298 -0.6926 242.9495 243.6421 248.1008 123.0915 -0.6939 243.0111 243.7050 248.2063 123.9438 -0.6948 243.0616 243.7564 248.3460 124.7055 -0.6955 243.1348 243.8304 248.4160 125.5278 -0.6956 243.1913 243.8868 248.5223 126.3500 -0.6930 243.2657 243.9587 248.6642 127.1125 -0.6966 243.3109 244.0075 248.7849 127.9645 -0.7012 243.3708 244.0719 248.9119 128.7265 -0.7034 243.4238 244.1272 249.0031 129.5478 -0.7027 243.5074 244.2102 249.0991 130.3663 -0.7013 243.5561 244.2574 249.2200 131.1245 -0.6932 243.6409 244.3341 249.3128 131.9720 -0.6925 243.7018 244.3944 249.4459 132.7303 -0.6960 243.7534 244.4494 249.5431 133.5485 -0.6941 243.8084 244.5025 249.6367 134.3370 -0.6966 243.8735 244.5701 249.7370 135.1250 -0.6958 243.9258 244.6217 249.8270 135.9435 -0.6977 244.0040 244.7017 249.9419 136.7620 -0.6998 244.0888 244.7886 250.0203 137.5500 -0.7013 244.1467 244.8480 250.1054 138.3683 -0.7080 244.2006 244.9085 250.2011 139.1270 -0.7084 244.2573 244.9657 250.2743 139.9750 -0.7084 244.3274 245.0358 250.3666 140.7635 -0.7057 244.3924 245.0981 250.4685 141.5530 -0.7063 244.4586 245.1649 250.5627 142.3718 -0.7080 244.5320 245.2401 250.6560 143.1318 -0.7113 244.5991 245.3103 250.7364 143.9805 -0.7126 244.6632 245.3759 250.8451 144.7713 -0.7113 244.7198 245.4311 250.9443 145.5608 -0.7140 244.7904 245.5044 251.0388 146.3800 -0.7151 244.8525 245.5676 251.1437 147.1415 -0.7159 244.9273 245.6433 251.2561 147.9935 -0.7158 244.9989 245.7147 251.3483 148.7855 -0.7170 245.0700 245.7870 251.4459 149.5753 -0.7200 245.1209 245.8409 251.5471 150.3975 -0.7189 245.1871 245.9060 251.6457 151.1590 -0.7199 245.2658 245.9857 251.7440 152.0155 -0.7204 245.3425 246.0629 251.8489 152.7768 -0.7248 245.4118 246.1366 251.9287 153.5988 -0.7230 245.4747 246.1977 252.0240 154.3910 -0.7259 245.5457 246.2716 252.1339 155.1825 -0.7218 245.6117 246.3335 252.2383 156.0048 -0.7223 245.6781 246.4004 252.3400 156.7965 -0.7239 245.7377 246.4616 252.4502 157.6188 -0.7252 245.8245 246.5497 252.5439 158.4108 -0.7229 245.8974 246.6203 252.6366 159.2025 -0.7269 245.9579 246.6847 252.7317 160.0248 -0.7278 246.0294 246.7572 252.8287 160.7865 -0.7316 246.1112 246.8429 252.9221 161.6408 -0.7323 246.1733 246.9056 253.0446 162.4325 -0.7337 246.2435 246.9772 253.1538 163.2245 -0.7348 246.3031 247.0380 253.2450 164.0465 -0.7366 246.3825 247.1192 253.3651 164.8085 -0.7382 246.4497 247.1879 253.4719 165.6605 -0.7402 246.5252 247.2654 253.5969 166.4525 -0.7388 246.5927 247.3314 253.6876 167.2445 -0.7409 246.6615 247.4024 253.8183 168.0665 -0.7404 246.7422 247.4825 253.9339 168.8285 -0.7416 246.8168 247.5584 254.0231 169.6805 -0.7408 246.8791 247.6199 254.1410 170.4725 -0.7416 246.9499 247.6915 254.2573 171.2645 -0.7449 247.0299 247.7748 254.3869 172.0865 -0.7440 247.0933 247.8373 254.5027 172.8485 -0.7441 247.1722 247.9163 254.5989 173.7003 -0.7468 247.2568 248.0037 254.7300 174.4925 -0.7468 247.3072 248.0540 254.8527 175.2840 -0.7482 247.3739 248.1221 254.9506 176.1063 -0.7534 247.4598 248.2133 255.0757 176.8675 -0.7736 247.5309 248.3045 255.1861 177.7203 -0.7799 247.6235 248.4034 255.3194 178.5118 -0.7839 247.6899 248.4738 255.4432 179.3035 -0.7871 247.7606 248.5477 255.5472 180.1258 -0.7876 247.8288 248.6165 255.6574 180.8875 -0.7869 247.8960 248.6829 255.7483 181.7398 -0.7870 247.9950 248.7821 255.8607 182.5318 -0.7884 248.0697 248.8581 255.9615 183.3235 -0.7892 248.1546 248.9439 256.0582 184.1458 -0.7892 248.2223 249.0115 256.1709 184.9375 -0.7912 248.2967 249.0879 256.2672 185.7605 -0.7945 248.3712 249.1657 256.3692 186.5535 -0.7954 248.4496 249.2450 256.4664 187.3455 -0.7910 248.5292 249.3203 256.5535 188.1675 -0.7947 248.6119 249.4066 256.6488 188.9595 -0.7954 248.6952 249.4907 256.7360 189.7823 -0.7976 248.7549 249.5525 256.8278 190.5745 -0.7998 248.8364 249.6361 256.9149 191.3665 -0.7996 248.9120 249.7116 257.0151 192.1885 -0.7983 248.9856 249.7839 257.1141 192.9805 -0.7990 249.0698 249.8688 257.2002 193.8010 -0.8006 249.1588 249.9593 257.2892 194.5888 -0.8026 249.2306 250.0332 257.3854 195.3780 -0.8041 249.3082 250.1123 257.4782 196.1960 -0.8036 249.3885 250.1922 257.5878 196.9838 -0.8043 249.4585 250.2628 257.6879 197.8015 -0.8037 249.5373 250.3410 257.7894 198.5900 -0.8042 249.6062 250.4104 257.9063 199.3788 -0.8044 249.6863 250.4907 258.0036 200.1968 -0.8055 249.7721 250.5776 258.0996 200.9855 -0.8045 249.8521 250.6566 258.2020 201.8043 -0.8010 249.9184 250.7194 258.2986 202.5923 -0.8026 250.0108 250.8134 258.4071 203.3803 -0.8038 250.0962 250.9000 258.5234 204.1980 -0.7992 250.1759 250.9750 258.6075 204.9865 -0.8016 250.2539 251.0556 258.7042 205.8050 -0.8031 250.3427 251.1458 258.8260 206.5930 -0.8012 250.4057 251.2069 258.9392 207.3810 -0.7989 250.4898 251.2887 259.0360 208.2300 -0.8025 250.5933 251.3958 259.1395 208.9905 -0.8058 250.6553 251.4611 259.2513 209.8118 -0.8055 250.7292 251.5347 259.3605 210.6028 -0.8073 250.8150 251.6224 259.4750 211.3930 -0.8018 250.9055 251.7073 259.5731 212.2428 -0.8111 250.9831 251.7942 259.6770 213.0045 -0.8131 251.0574 251.8705 259.7821 213.8268 -0.8121 251.1412 251.9533 259.8879 214.6188 -0.8148 251.2304 252.0453 259.9785 215.4105 -0.8167 251.3067 252.1234 260.0852 216.2628 -0.8291 251.3987 252.2279 260.1875 217.0245 -0.8370 251.4778 252.3148 260.2917 217.8468 -0.8415 251.5668 252.4083 260.4263 218.6388 -0.8406 251.6474 252.4880 260.5078 219.4305 -0.8410 251.7367 252.5777 260.6059 220.2825 -0.8426 251.8104 252.6530 260.7271 221.0445 -0.8492 251.8782 252.7274 260.8188 221.8665 -0.8521 251.9609 252.8130 260.9354 222.6585 -0.8534 252.0498 252.9032 261.0290 223.4505 -0.8550 252.1354 252.9905 261.1297 224.3025 -0.8526 252.2405 253.0931 261.2315 225.0645 -0.8537 252.3167 253.1704 261.3360 225.8865 -0.8532 252.3956 253.2488 261.4551 226.6785 -0.8407 252.4897 253.3305 261.5406 227.4705 -0.8266 252.5665 253.3931 261.6393 228.3225 -0.8237 252.6623 253.4860 261.7383 229.0845 -0.8225 252.7536 253.5761 261.8490 229.9065 -0.8248 252.8413 253.6660 261.9440 230.7285 -0.8241 252.9071 253.7312 262.0607 231.4905 -0.8271 252.9764 253.8035 262.1618 232.3423 -0.8281 253.0773 253.9054 262.2684 233.1043 -0.8298 253.1614 253.9911 262.3566 233.9258 -0.8293 253.2518 254.0811 262.4537 234.7478 -0.8309 253.3494 254.1803 262.5460 235.5095 -0.8308 253.4240 254.2549 262.6554 236.3620 -0.8320 253.5088 254.3408 262.7550 237.1235 -0.8327 253.5871 254.4198 262.8508 237.9458 -0.8331 253.6736 254.5066 262.9627 238.7678 -0.8329 253.7662 254.5991 263.0695 239.5295 -0.8357 253.8508 254.6864 263.1646 240.3818 -0.8329 253.9405 254.7734 263.2691 241.1440 -0.8335 254.0254 254.8589 263.3728 241.9668 -0.8325 254.1241 254.9567 263.4848 242.7888 -0.8340 254.2119 255.0459 263.5882 243.5505 -0.8350 254.2898 255.1247 263.6924 244.4028 -0.8339 254.3926 255.2266 263.8277 245.1645 -0.8340 254.4682 255.3023 263.9201 245.9865 -0.8331 254.5533 255.3864 264.0359 246.8085 -0.8347 254.6492 255.4839 264.1638 247.5705 -0.8331 254.7354 255.5685 264.2617 248.4225 -0.8303 254.8349 255.6652 264.3907 249.1845 -0.8306 254.9141 255.7448 264.5034 250.0065 -0.8313 255.0153 255.8465 264.6250 250.7985 -0.8296 255.0902 255.9198 264.7487 251.5905 -0.8336 255.1690 256.0027 264.8545 252.4430 -0.8327 255.2575 256.0902 264.9845 253.2055 -0.8347 255.3367 256.1714 265.0963 254.0268 -0.8346 255.4442 256.2789 265.2091 254.8225 -0.8347 255.5305 256.3652 265.3216 255.6155 -0.8350 255.6110 256.4460 265.4359 256.4413 -0.8369 255.7136 256.5505 265.5565 257.2335 -0.8370 255.7992 256.6361 265.6645 258.0558 -0.8378 255.8899 256.7277 265.7764 258.8453 -0.8394 255.9732 256.8126 265.8754 259.6330 -0.8445 256.0669 256.9114 265.9625 260.4510 -0.8432 256.1713 257.0145 266.0729 261.2093 -0.8376 256.2609 257.0986 266.1702 262.0570 -0.8378 256.3535 257.1913 266.2633 262.8455 -0.8446 256.4401 257.2847 266.3535 263.6340 -0.8408 256.5292 257.3700 266.4643 264.4520 -0.8390 256.6190 257.4581 266.5551 265.2400 -0.8406 256.7221 257.5627 266.6460 266.0580 -0.8409 256.7925 257.6334 266.7620 266.8460 -0.8426 256.8785 257.7211 266.8368 267.6340 -0.8403 256.9769 257.8172 266.9388 268.4523 -0.8432 257.0670 257.9102 267.0394 269.2430 -0.8440 257.1674 258.0114 267.1467 270.0630 -0.8443 257.2627 258.1070 267.2337 270.8518 -0.8483 257.3382 258.1865 267.3124 271.6415 -0.8547 257.4297 258.2844 267.4000 272.4608 -0.8553 257.5378 258.3932 267.4969 273.2503 -0.8509 257.6361 258.4870 267.5938 274.0708 -0.8487 257.7317 258.5804 267.7015 274.8595 -0.8491 257.8151 258.6642 267.7903 275.6498 -0.8552 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