DTA measure 21_meres Date: 2024116:1015 Lower limit = 30.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.53 s Mass = 100.000 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5421 -4.6107 441.6532 446.2639 424.5540 4.1410 -4.6180 441.6678 446.2858 424.5393 5.7546 -4.6272 441.6955 446.3227 424.5100 7.3536 -4.6333 441.7238 446.3571 424.4548 8.9526 -4.6391 441.7315 446.3706 424.3711 10.5666 -4.6444 441.7677 446.4121 424.2764 12.1808 -4.6504 441.7792 446.4296 424.1457 13.7796 -4.6581 441.7956 446.4537 423.9882 15.3936 -4.6613 441.8136 446.4749 423.8062 16.9925 -4.6670 441.8289 446.4959 423.6253 18.6065 -4.6787 441.8468 446.5255 423.4242 20.2205 -4.6867 441.8365 446.5232 423.2094 21.8195 -4.6876 441.8512 446.5388 422.9810 23.4339 -4.6911 441.8674 446.5585 422.7778 25.0330 -4.6868 441.8783 446.5650 422.5523 26.6475 -4.6901 441.8732 446.5633 422.3230 28.2628 -4.6931 441.8824 446.5755 422.1011 29.8616 -4.6929 441.8811 446.5739 421.8810 31.4760 -4.6953 441.8743 446.5695 421.6573 33.0756 -4.7000 441.8732 446.5732 421.4404 34.6861 -4.7013 441.8530 446.5543 421.2289 36.2921 -4.7012 441.8558 446.5570 421.0075 37.8840 -4.7048 441.8515 446.5562 420.7732 39.4904 -4.7064 441.8418 446.5482 420.5542 41.0833 -4.7083 441.8011 446.5094 420.3465 42.6901 -4.7104 441.7912 446.5016 420.1407 44.2988 -4.7106 441.7837 446.4944 419.9189 45.9064 -4.7118 441.7601 446.4719 419.7178 47.5008 -4.7126 441.7299 446.4425 419.5151 49.0979 -4.7144 441.7047 446.4191 419.3214 50.7259 -4.7155 441.6684 446.3839 419.1228 52.3243 -4.7162 441.6434 446.3596 418.9353 53.9225 -4.7169 441.6000 446.3169 418.7297 55.5365 -4.7176 441.5805 446.2981 418.5237 57.1355 -4.7206 441.5343 446.2549 418.3430 58.7491 -4.7208 441.5005 446.2213 418.1654 60.3631 -4.7232 441.4522 446.1754 417.9745 61.9620 -4.7251 441.4122 446.1373 417.7932 63.5689 -4.7256 441.3621 446.0877 417.6057 65.1706 -4.7262 441.3350 446.0612 417.4200 66.7846 -4.7271 441.2728 446.0000 417.2306 68.4138 -4.7273 441.2167 445.9440 417.0170 70.0126 -4.7280 441.1581 445.8860 416.8009 71.6115 -4.7282 441.1249 445.8531 416.6181 73.2261 -4.7286 441.0618 445.7904 416.4374 74.8255 -4.7277 441.0002 445.7279 416.2261 76.4545 -4.7288 440.9401 445.6689 415.9979 78.0535 -4.7270 440.8833 445.6103 415.8190 79.6525 -4.7290 440.8174 445.5464 415.6395 81.2665 -4.7277 440.7568 445.4845 415.4496 82.8803 -4.7286 440.6704 445.3989 415.2680 84.4946 -4.7270 440.5941 445.3211 415.0731 86.0936 -4.7269 440.5432 445.2701 414.8677 87.6926 -4.7268 440.4657 445.1925 414.6648 89.3066 -4.7248 440.3987 445.1235 414.4522 90.9206 -4.7258 440.3147 445.0405 414.2233 92.5356 -4.7241 440.2302 444.9543 414.0115 94.1355 -4.7232 440.1672 444.8905 413.8017 95.7505 -4.7239 440.0785 444.8024 413.5962 97.3499 -4.7216 439.9936 444.7151 413.3760 98.9449 -4.7203 439.9050 444.6253 413.1500 100.5658 -4.7162 439.8279 444.5441 412.9325 102.1580 -4.7162 439.7361 444.4523 412.7265 103.7490 -4.7172 439.6639 444.3812 412.5159 105.3555 -4.7173 439.5809 444.2982 412.2979 106.9478 -4.7140 439.4841 444.1981 412.0836 108.5571 -4.7124 439.3867 444.0991 411.8805 110.1665 -4.7129 439.2957 444.0086 411.6879 111.7610 -4.7137 439.1829 443.8967 411.4771 113.3564 -4.7118 439.0929 443.8047 411.2747 114.9676 -4.7091 438.9954 443.7045 411.0874 116.5803 -4.7109 438.8977 443.6087 410.8819 118.1805 -4.7091 438.7985 443.5076 410.6917 119.7858 -4.7063 438.6936 443.3998 410.4825 121.3848 -4.7047 438.5934 443.2981 410.3006 122.9838 -4.7063 438.4660 443.1723 410.1000 124.5976 -4.7026 438.3589 443.0615 409.9219 126.2116 -4.7008 438.2527 442.9535 409.7343 127.8108 -4.7023 438.1439 442.8462 409.5474 129.4245 -4.7028 438.0237 442.7265 409.3644 131.0235 -4.7004 437.9093 442.6096 409.1646 132.6225 -4.7004 437.8072 442.5076 408.9592 134.2515 -4.7023 437.6882 442.3905 408.7556 135.8505 -4.6984 437.5585 442.2568 408.5446 137.4645 -4.6976 437.4449 442.1426 408.3376 139.0634 -4.6967 437.3349 442.0317 408.1257 140.6618 -4.6947 437.2210 441.9157 407.9116 142.2908 -4.6912 437.0724 441.7636 407.7184 143.8898 -4.6919 436.9639 441.6557 407.5098 145.5036 -4.6899 436.8390 441.5288 407.3025 147.1026 -4.6889 436.7118 441.4007 407.0980 148.7173 -4.6895 436.5806 441.2701 406.8949 150.3316 -4.6879 436.4489 441.1368 406.6860 151.9458 -4.6863 436.3180 441.0043 406.4886 153.5448 -4.6844 436.1893 440.8738 406.2932 155.1445 -4.6843 436.0581 440.7424 406.0961 156.7591 -4.6814 435.9223 440.6037 405.8955 158.3885 -4.6794 435.7927 440.4721 405.6998 159.9876 -4.6790 435.6657 440.3447 405.4941 161.5870 -4.6761 435.5288 440.2049 405.3047 163.1829 -4.6742 435.3960 440.0702 405.1162 164.7903 -4.6723 435.2590 439.9313 404.9092 166.3973 -4.6688 435.1210 439.7898 404.6999 168.0041 -4.6623 434.9740 439.6363 404.4961 169.5970 -4.6678 434.8374 439.5052 404.2842 171.2051 -4.6638 434.7100 439.3738 404.0658 172.8128 -4.6629 434.5567 439.2197 403.8621 174.4216 -4.6606 434.4125 439.0731 403.6297 176.0173 -4.6574 434.2743 438.9316 403.4232 177.6288 -4.6542 434.1227 438.7769 403.2070 179.2266 -4.6528 433.9799 438.6327 402.9843 180.8396 -4.6476 433.8272 438.4749 402.7761 182.4536 -4.6475 433.6787 438.3262 402.5641 184.0525 -4.6446 433.5387 438.1833 402.3388 185.6516 -4.6386 433.3970 438.0356 402.1242 187.2655 -4.6322 433.2427 437.8749 401.9132 188.8645 -4.6339 433.0903 437.7242 401.7087 190.4935 -4.6337 432.9393 437.5730 401.4947 192.0925 -4.6306 432.7918 437.4225 401.2909 193.6915 -4.6265 432.6285 437.2550 401.0715 195.2905 -4.6253 432.4779 437.1032 400.8570 196.9045 -4.6226 432.3340 436.9566 400.6542 198.5183 -4.6191 432.1749 436.7940 400.4423 200.1320 -4.6181 432.0183 436.6364 400.2459 201.7308 -4.6167 431.8487 436.4654 400.0343 203.3296 -4.6127 431.6973 436.3100 399.8326 204.9436 -4.6078 431.5428 436.1506 399.6307 206.5576 -4.6039 431.3828 435.9867 399.4236 208.1719 -4.6008 431.2295 435.8302 399.2276 209.7715 -4.5976 431.0666 435.6642 399.0423 211.3705 -4.5932 430.8953 435.4885 398.8340 212.9695 -4.5910 430.7389 435.3299 398.6520 214.5985 -4.5909 430.5877 435.1786 398.4469 216.1975 -4.5925 430.4273 435.0198 398.2698 217.8115 -4.5875 430.2563 434.8439 398.0884 219.4101 -4.5823 430.0954 434.6777 397.8813 221.0088 -4.5804 429.9219 434.5023 397.6738 222.6384 -4.5819 429.7518 434.3337 397.4692 224.2379 -4.5786 429.5901 434.1688 397.2611 225.8519 -4.5693 429.4258 433.9951 397.0509 227.4490 -4.5634 429.2605 433.8239 396.8451 229.0400 -4.5602 429.0961 433.6562 396.6358 230.6469 -4.5572 428.9337 433.4909 396.4211 232.2543 -4.5519 428.7651 433.3170 396.2221 233.8465 -4.5509 428.6021 433.1530 396.0094 235.4540 -4.5462 428.4319 432.9781 395.7901 237.0464 -4.5410 428.2652 432.8062 395.5874 238.6701 -4.5384 428.0907 432.6291 395.3689 240.2645 -4.5359 427.9286 432.4645 395.1621 241.8616 -4.5338 427.7503 432.2841 394.9553 243.4748 -4.5290 427.5877 432.1167 394.7464 245.0729 -4.5260 427.4209 431.9469 394.5364 246.6715 -4.5225 427.2446 431.7671 394.3281 248.3005 -4.5180 427.0633 431.5813 394.1281 249.9001 -4.5115 426.8984 431.4099 393.9364 251.4995 -4.5092 426.7298 431.2389 393.7483 253.0985 -4.5063 426.5459 431.0522 393.5306 254.7120 -4.5022 426.3651 430.8673 393.3255 256.3260 -4.4984 426.2041 430.7025 393.1467 257.9399 -4.4935 426.0158 430.5093 392.9214 259.5388 -4.4905 425.8542 430.3447 392.7261 261.1378 -4.4871 425.6610 430.1480 392.5360 262.7516 -4.4826 425.4840 429.9666 392.3440 264.3808 -4.4904 425.3163 429.8067 392.1497 265.9796 -4.4799 425.1547 429.6347 391.9472 267.5785 -4.4690 424.9593 429.4283 391.7350 269.1925 -4.4650 424.7940 429.2590 391.5356 270.7915 -4.4603 424.6124 429.0727 391.3212 272.4246 -4.4548 424.4252 428.8801 391.0892 274.0245 -4.4524 424.2525 428.7049 390.8793 275.6233 -4.4473 424.0693 428.5165 390.6769 277.2376 -4.4473 423.8905 428.3378 390.4612 278.8518 -4.4415 423.7160 428.1575 390.2399 280.4658 -4.4365 423.5266 427.9631 390.0321 282.0656 -4.4330 423.3537 427.7867 389.8122 283.6800 -4.4306 423.1596 427.5902 389.6032 285.2801 -4.4270 422.9823 427.4092 389.3871 286.8946 -4.4212 422.8022 427.2234 389.1675 288.5095 -4.4187 422.6230 427.0417 388.9557 290.1235 -4.4125 422.4423 426.8548 388.7370 291.7189 -4.4083 422.2563 426.6646 388.5309 293.3100 -4.4024 422.0754 426.4778 388.3189 294.9169 -4.3967 421.8840 426.2807 388.1087 296.5231 -4.3921 421.7199 426.1120 387.8939 298.1154 -4.3876 421.5182 425.9057 387.6940 299.7240 -4.3851 421.3434 425.7285 387.4955 301.3179 -4.3804 421.1576 425.5380 387.2885 302.9273 -4.3760 420.9635 425.3395 387.0899 304.5254 -4.3725 420.7827 425.1552 386.8907 306.1404 -4.3664 420.5925 424.9589 386.6878 307.7371 -4.3643 420.4052 424.7696 386.4911 309.3349 -4.3606 420.2312 424.5919 386.2913 310.9473 -4.3544 420.0227 424.3771 386.0686 312.5613 -4.3519 419.8390 424.1909 385.8890 314.1599 -4.3450 419.6533 423.9983 385.6793 315.7588 -4.3378 419.4606 423.7984 385.4699 317.3576 -4.3343 419.2952 423.6295 385.2914 318.9716 -4.3294 419.1048 423.4341 385.0833 320.5706 -4.3251 418.9061 423.2312 384.8783 322.1846 -4.3186 418.7164 423.0350 384.6794 323.7988 -4.3155 418.5318 422.8473 384.4971 325.3975 -4.3122 418.3373 422.6496 384.2804 326.9965 -4.3079 418.1591 422.4671 384.0638 328.6105 -4.3020 417.9632 422.2652 383.8540 330.2245 -4.2982 417.7768 422.0749 383.6333 331.8235 -4.2922 417.5854 421.8777 383.4124 333.4375 -4.2894 417.4035 421.6929 383.1972 335.0365 -4.2830 417.2028 421.4857 382.9795 336.6350 -4.2791 417.0114 421.2905 382.7619 338.2636 -4.2732 416.8208 421.0940 382.5255 339.8628 -4.2694 416.6206 420.8900 382.3059 341.4618 -4.2623 416.4309 420.6933 382.0874 343.0766 -4.2572 416.2435 420.5007 381.8656 344.6756 -4.2534 416.0422 420.2956 381.6411 346.2924 -4.2496 415.8550 420.1046 381.4116 347.9075 -4.2435 415.6638 419.9073 381.1927 349.5065 -4.2376 415.4783 419.7159 380.9841 351.1209 -4.2342 415.2798 419.5140 380.7566 352.7210 -4.2284 415.0793 419.3077 380.5462 354.3355 -4.2228 414.9038 419.1266 380.3336 355.9445 -4.2178 414.7056 418.9234 380.1166 357.5361 -4.2144 414.5031 418.7175 379.8935 359.1428 -4.2083 414.3017 418.5099 379.6805 360.7345 -4.2040 414.1123 418.3163 379.4638 362.3419 -4.1986 413.9212 418.1198 379.2739 363.9504 -4.1922 413.7228 417.9149 379.0557 365.5419 -4.1862 413.5298 417.7160 378.8623 367.1511 -4.1808 413.3375 417.5183 378.6553 368.7446 -4.1781 413.1376 417.3157 378.4582 370.3698 -4.1721 412.9482 417.1203 378.2475 371.9800 -4.1682 412.7452 416.9134 378.0378 373.5776 -4.1654 412.5501 416.7155 377.8457 375.1766 -4.1584 412.3550 416.5134 377.6593 376.7756 -4.1549 412.1706 416.3255 377.4450 378.4046 -4.1493 411.9794 416.1287 377.2457 380.0036 -4.1459 411.7743 415.9202 377.0284 381.6175 -4.1413 411.5706 415.7119 376.8371 383.2166 -4.1368 411.3823 415.5191 376.6442 384.8155 -4.1326 411.1713 415.3038 376.4292 386.4445 -4.1265 410.9677 415.0942 376.2385 388.0585 -4.1234 410.7781 414.9015 376.0377 389.6575 -4.1192 410.5747 414.6939 375.8445 391.2565 -4.1144 410.3911 414.5055 375.6581 392.8703 -4.1093 410.1928 414.3021 375.4602 394.4839 -4.1033 409.9987 414.1020 375.2619 396.0979 -4.1002 409.7870 413.8872 375.0683 397.6968 -4.0948 409.5840 413.6789 374.8759 399.3106 -4.0879 409.3915 413.4794 374.6834 400.9246 -4.0838 409.1776 413.2614 374.4797 402.5388 -4.0806 408.9893 413.0699 374.2831 404.1385 -4.0777 408.7882 412.8659 374.0726 405.7526 -4.0720 408.5947 412.6667 373.8629 407.3521 -4.0701 408.3934 412.4635 373.6561 408.9671 -4.0646 408.1881 412.2527 373.4337 410.5815 -4.0603 407.9873 412.0476 373.2347 412.1815 -4.0553 407.7961 411.8514 373.0311 413.7958 -4.0495 407.5895 411.6390 372.8230 415.3953 -4.0461 407.3986 411.4447 372.6066 417.0246 -4.0410 407.1972 411.2382 372.3914 418.6236 -4.0360 407.0095 411.0456 372.1690 420.2179 -4.0308 406.8129 410.8437 371.9706 421.8250 -4.0251 406.5984 410.6234 371.7655 423.4168 -4.0195 406.4078 410.4273 371.5592 425.0230 -4.0157 406.1998 410.2155 371.3592 426.6318 -4.0093 406.0138 410.0231 371.1509 428.2255 -4.0052 405.8152 409.8204 370.9465 429.8335 -4.0001 405.6173 409.6173 370.7362 431.4283 -3.9951 405.4321 409.4271 370.5491 433.0526 -3.9916 405.2167 409.2082 370.3224 434.6491 -3.9847 405.0149 408.9997 370.1254 436.2476 -3.9799 404.8176 408.7975 369.9387 437.8604 -3.9799 404.6274 408.6073 369.7332 439.4589 -3.9780 404.4374 408.4153 369.5327 441.0575 -3.9690 404.2206 408.1896 369.3209 442.6865 -3.9619 404.0176 407.9795 369.1205 444.2855 -3.9606 403.8401 407.8007 368.9233 445.8845 -3.9523 403.6401 407.5925 368.7242 447.4985 -3.9481 403.4267 407.3748 368.5285 449.0975 -3.9430 403.2336 407.1766 368.3202 450.7264 -3.9391 403.0282 406.9673 368.1035 452.3246 -3.9333 402.8264 406.7597 367.8994 453.9238 -3.9285 402.6221 406.5506 367.6830 455.5376 -3.9222 402.4313 406.3535 367.4554 457.1366 -3.9153 402.2310 406.1463 367.2468 458.7658 -3.9099 402.0273 405.9372 367.0141 460.3646 -3.9052 401.8133 405.7185 366.7894 461.9636 -3.9006 401.6205 405.5211 366.5770 463.5775 -3.8929 401.4143 405.3072 366.3545 465.1915 -3.8892 401.2212 405.1104 366.1315 466.8056 -3.8826 401.0241 404.9066 365.9208 468.4055 -3.8771 400.8160 404.6930 365.7012 470.0199 -3.8742 400.6173 404.4914 365.4811 471.6199 -3.8689 400.4213 404.2902 365.2654 473.2339 -3.8626 400.2211 404.0836 365.0541 474.8486 -3.8566 400.0140 403.8706 364.8337 476.4636 -3.8516 399.8165 403.6680 364.6290 478.0630 -3.8479 399.6144 403.4623 364.4275 479.6631 -3.8404 399.4132 403.2536 364.1919 481.2926 -3.8369 399.1917 403.0286 363.9773 482.8926 -3.8327 398.9993 402.8320 363.7583 484.5054 -3.8285 398.8087 402.6373 363.5544 486.0985 -3.8222 398.6138 402.4360 363.3434 487.6906 -3.8146 398.4035 402.2181 363.1306 489.3129 -3.8097 398.1999 402.0096 362.9213 490.9043 -3.8040 398.0134 401.8174 362.7106 492.5140 -3.8007 397.7831 401.5838 362.5068 494.1070 -3.7932 397.5829 401.3761 362.3176 495.7148 -3.7891 397.3894 401.1785 362.1203 497.3404 -3.7831 397.1819 400.9650 361.9199 498.9361 -3.7782 396.9888 400.7670 361.7101 500.5314 -3.7728 396.7954 400.5682 361.5278 502.1444 -3.7679 396.5901 400.3580 361.3379 503.7416 -3.7614 396.3845 400.1459 361.1405 505.3705 -3.7583 396.1719 399.9302 360.9558 506.9691 -3.7532 395.9778 399.7311 360.7775 508.5828 -3.7495 395.7658 399.5154 360.5798 510.1818 -3.7445 395.5560 399.3005 360.4008 511.7956 -3.7381 395.3577 399.0958 360.1962 513.4098 -3.7337 395.1699 398.9036 360.0107 515.0086 -3.7296 394.9715 398.7011 359.8087 516.6226 -3.7264 394.7641 398.4905 359.6057 518.2216 -3.7207 394.5522 398.2729 359.4154 519.8356 -3.7160 394.3546 398.0706 359.2107 521.4498 -3.7086 394.1455 397.8541 359.0006 523.0495 -3.7051 393.9422 397.6474 358.7912 524.6635 -3.6966 393.7456 397.4421 358.5932 526.2625 -3.6948 393.5474 397.2422 358.3813 527.8915 -3.6900 393.3426 397.0326 358.1704 529.4911 -3.6839 393.1372 396.8211 357.9642 531.1060 -3.6796 392.9306 396.6103 357.7647 532.7046 -3.6744 392.7293 396.4037 357.5560 534.3186 -3.6684 392.5259 396.1943 357.3366 535.9334 -3.6641 392.3192 395.9834 357.1369 537.5479 -3.6588 392.1253 395.7841 356.9204 539.1479 -3.6508 391.9193 395.5701 356.7348 540.7636 -3.6472 391.7134 395.3606 356.5374 542.3643 -3.6436 391.5155 395.1591 356.3257 543.9944 -3.6377 391.2990 394.9366 356.1202 545.5935 -3.6342 391.1179 394.7520 355.9178 547.1925 -3.6275 390.9041 394.5316 355.7274 548.8030 -3.6246 390.7208 394.3455 355.5166 550.3948 -3.6183 390.5156 394.1339 355.3036 552.0169 -3.6165 390.2987 393.9152 355.0829 553.6088 -3.6096 390.0901 393.6997 354.8748 555.2008 -3.6067 389.8893 393.4960 354.6807 556.8099 -3.6015 389.6942 393.2957 354.4556 558.4040 -3.5951 389.5036 393.0987 354.2271 560.0290 -3.5896 389.2889 392.8785 354.0031 561.6248 -3.5843 389.0875 392.6718 353.7874 563.2216 -3.5797 388.8835 392.4633 353.5718 564.8349 -3.5744 388.6795 392.2538 353.3502 566.4326 -3.5674 388.4825 392.0498 353.1410 568.0468 -3.5628 388.2706 391.8334 352.9272 569.6608 -3.5577 388.0692 391.6268 352.7155 571.2596 -3.5549 387.8639 391.4188 352.4860 572.8586 -3.5486 387.6685 391.2171 352.2802 574.4726 -3.5414 387.4695 391.0110 352.0627 576.0866 -3.5341 387.2548 390.7889 351.8560 577.7006 -3.5128 387.0560 390.5687 351.6575 579.2995 -3.4981 386.8486 390.3467 351.4281 580.8985 -3.4899 386.6455 390.1355 351.2197 582.5125 -3.4995 386.4439 389.9434 351.0049 584.1265 -3.4846 386.2421 389.7267 350.7931 585.7304 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