DTA measure 1gyors2 Date: 2026317:1515 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.37 s Mass = 100.000 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1993 1.7011 308.1117 306.4107 280.9825 2.0475 1.7129 307.9509 306.2380 280.7963 2.8140 1.7190 307.8582 306.1392 280.6596 3.6413 1.7283 307.7598 306.0315 280.4981 4.4280 1.7354 307.6335 305.8981 280.3815 5.2253 1.7421 307.5239 305.7818 280.2464 6.0420 1.7536 307.4301 305.6765 280.0858 6.8290 1.7621 307.3263 305.5641 279.9079 7.6263 1.7701 307.1784 305.4083 279.7579 8.4228 1.7715 307.0327 305.2611 279.5753 9.2505 1.7773 306.9170 305.1397 279.4288 10.0170 1.7788 306.8256 305.0468 279.2982 10.8650 1.7828 306.7650 304.9822 279.1349 11.6310 1.7913 306.6770 304.8857 279.0081 12.4590 1.7972 306.5479 304.7506 278.8653 13.2450 1.8025 306.4763 304.6738 278.7244 14.0525 1.8083 306.3704 304.5621 278.5934 14.8395 1.8133 306.2563 304.4430 278.4300 15.6360 1.8213 306.1664 304.3452 278.2903 16.4638 1.8277 306.0400 304.2123 278.1593 17.2508 1.8303 305.9368 304.1065 278.0212 18.0780 1.8341 305.8169 303.9828 277.8911 18.8443 1.8384 305.6677 303.8293 277.7590 19.7030 1.8505 305.5461 303.6956 277.5933 20.4583 1.8575 305.4601 303.6026 277.4347 21.2863 1.8625 305.3718 303.5093 277.3197 22.0835 1.8708 305.2613 303.3904 277.1521 22.8698 1.8798 305.1479 303.2681 276.9817 23.6770 1.8872 305.0239 303.1367 276.8089 24.4640 1.8946 304.9180 303.0234 276.6894 25.2910 1.9012 304.7648 302.8637 276.5369 26.0575 1.9068 304.6250 302.7182 276.3999 26.9163 1.9087 304.5614 302.6527 276.2497 27.6718 1.9153 304.5167 302.6013 276.0986 28.5303 1.9264 304.3918 302.4654 275.9386 29.2968 1.9320 304.2651 302.3331 275.8216 30.1138 1.9377 304.1516 302.2139 275.6448 30.9210 1.9441 304.0197 302.0756 275.5191 31.7080 1.9476 303.9502 302.0025 275.4064 32.5353 1.9546 303.8072 301.8526 275.2628 33.3015 1.9618 303.6847 301.7229 275.1367 34.1398 1.9685 303.5851 301.6166 274.9812 34.8953 1.9734 303.4795 301.5060 274.8459 35.7538 1.9812 303.3564 301.3752 274.6998 36.5203 1.9869 303.2401 301.2533 274.5773 37.3473 1.9935 303.1263 301.1328 274.4285 38.1445 1.9962 303.0416 301.0454 274.2806 38.9418 1.9982 302.9005 300.9024 274.1590 39.7688 1.9990 302.7828 300.7838 274.0422 40.5353 2.0025 302.6250 300.6226 273.9384 41.3940 2.0077 302.5208 300.5131 273.7625 42.1493 2.0150 302.4299 300.4150 273.5978 42.9875 2.0213 302.3344 300.3132 273.4430 43.7745 2.0234 302.2229 300.1995 273.3153 44.5710 2.0246 302.0814 300.0568 273.1881 45.3680 2.0303 301.9213 299.8911 273.0550 46.1755 2.0353 301.7798 299.7445 272.9390 46.9925 2.0440 301.6596 299.6156 272.8318 47.7588 2.0481 301.5524 299.5043 272.7061 48.6175 2.0462 301.4417 299.3955 272.5735 49.3833 2.0521 301.3527 299.3006 272.4249 50.2110 2.0573 301.2098 299.1525 272.3018 51.0083 2.0673 301.1049 299.0376 272.1691 51.8053 2.0746 301.0006 298.9260 272.0259 52.6325 2.0813 300.8287 298.7474 271.9210 53.3990 2.0854 300.6736 298.5882 271.7924 54.2475 2.0874 300.5319 298.4445 271.6207 55.0233 2.0909 300.3925 298.3016 271.4834 55.8410 2.0946 300.2858 298.1912 271.3886 56.6485 2.0900 300.1936 298.1036 271.2607 57.4345 2.0930 300.1061 298.0131 271.1363 58.2420 2.1004 299.9792 297.8788 271.0006 59.0288 2.1047 299.8455 297.7409 270.8521 59.8458 2.1096 299.7002 297.5905 270.6976 60.6225 2.1133 299.6022 297.4888 270.5375 61.4708 2.1154 299.4953 297.3799 270.4205 62.2263 2.1184 299.3728 297.2544 270.3109 63.0645 2.1204 299.1878 297.0674 270.1894 63.8513 2.1262 299.0746 296.9484 270.0848 64.6375 2.1313 298.9611 296.8298 269.9740 65.4655 2.1397 298.8290 296.6893 269.8524 66.2318 2.1439 298.6736 296.5297 269.7534 67.0488 2.1489 298.5473 296.3985 269.6359 67.8255 2.1554 298.4872 296.3318 269.5148 68.6738 2.1584 298.3690 296.2106 269.3621 69.4395 2.1617 298.2395 296.0779 269.2221 70.2675 2.1672 298.1129 295.9458 269.0742 71.0645 2.1695 298.0060 295.8365 268.9840 71.8508 2.1675 297.8808 295.7133 268.8916 72.6788 2.1687 297.7396 295.5709 268.7768 73.4450 2.1686 297.6301 295.4615 268.7197 74.2723 2.1676 297.4700 295.3023 268.6567 75.0285 2.1753 297.3372 295.1619 268.5674 75.8973 2.1792 297.2029 295.0238 268.4898 76.6528 2.1806 297.1340 294.9534 268.4224 77.4705 2.1859 297.0238 294.8379 268.3126 78.2778 2.1881 296.9125 294.7243 268.2046 79.0640 2.1870 296.7785 294.5915 268.1394 79.8920 2.1902 296.6399 294.4497 268.0664 80.6583 2.1893 296.5163 294.3270 267.9955 81.5163 2.1928 296.4019 294.2092 267.8720 82.2828 2.1968 296.2513 294.0545 267.7790 83.1003 2.1988 296.1033 293.9046 267.7176 83.9070 2.1994 296.0116 293.8122 267.6159 84.6940 2.2030 295.8841 293.6810 267.5166 85.5218 2.2012 295.7714 293.5702 267.4329 86.2875 2.1976 295.6600 293.4625 267.3517 87.1463 2.1974 295.5268 293.3294 267.2910 87.8818 2.1998 295.4360 293.2362 267.2451 88.7500 2.1999 295.3287 293.1288 267.1749 89.4960 2.2021 295.1910 292.9889 267.1288 90.3445 2.2054 295.0425 292.8370 267.0933 91.1203 2.2074 294.9000 292.6926 267.0544 91.9380 2.2059 294.7701 292.5642 267.0251 92.7353 2.2083 294.6753 292.4670 266.9767 93.5315 2.2069 294.5424 292.3355 266.9260 94.3595 2.2119 294.4194 292.2075 266.8991 95.1258 2.2151 294.3169 292.1018 266.8866 95.9735 2.2176 294.1785 291.9609 266.8926 96.7503 2.2164 294.0768 291.8604 266.8734 97.5680 2.2146 293.9588 291.7442 266.8709 98.3643 2.2137 293.8823 291.6686 266.8672 99.1820 2.2138 293.7583 291.5445 266.8679 99.9485 2.2161 293.6387 291.4226 266.8166 100.7758 2.2190 293.4834 291.2644 266.8009 101.5728 2.2190 293.3201 291.1010 266.8152 102.3700 2.2157 293.1894 290.9737 266.8169 103.1875 2.2104 293.0727 290.8622 266.8325 103.9635 2.2076 292.9783 290.7707 266.8566 104.8120 2.2045 292.8840 290.6795 266.8770 105.5780 2.2010 292.7771 290.5761 266.8785 106.4055 2.1973 292.6803 290.4830 266.9109 107.2028 2.1853 292.5475 290.3622 266.9383 107.9998 2.1797 292.3775 290.1978 266.9495 108.8270 2.1750 292.2486 290.0736 266.9657 109.5935 2.1733 292.1579 289.9846 267.0036 110.4523 2.1757 292.0708 289.8952 267.0545 111.2178 2.1760 291.9839 289.8079 267.0750 112.0355 2.1724 291.8306 289.6583 267.1308 112.8430 2.1710 291.7035 289.5325 267.1609 113.6290 2.1639 291.5612 289.3973 267.2018 114.4570 2.1639 291.4843 289.3205 267.2796 115.2235 2.1650 291.3609 289.1958 267.3263 116.0818 2.1661 291.2290 289.0629 267.3898 116.8478 2.1641 291.1305 288.9664 267.4741 117.6655 2.1637 290.9978 288.8340 267.5304 118.4723 2.1591 290.8931 288.7340 267.5956 119.2590 2.1575 290.7853 288.6278 267.6385 120.0870 2.1516 290.6654 288.5138 267.7259 120.8530 2.1475 290.5675 288.4200 267.7993 121.7113 2.1384 290.4875 288.3491 267.9051 122.4470 2.1352 290.3819 288.2467 267.9912 123.2953 2.1352 290.2601 288.1250 268.0604 124.0610 2.1313 290.1403 288.0089 268.1669 124.8788 2.1249 289.9970 287.8721 268.2492 125.6758 2.1203 289.9000 287.7797 268.3058 126.4723 2.1162 289.7701 287.6539 268.3742 127.2900 2.1102 289.6582 287.5481 268.4612 128.0560 2.1032 289.5655 287.4622 268.5527 128.9040 2.0995 289.4564 287.3569 268.6820 129.6603 2.0916 289.3587 287.2671 268.7672 130.4883 2.0870 289.2329 287.1458 268.8629 131.2743 2.0762 289.1084 287.0322 268.9783 132.0715 2.0713 289.0410 286.9697 269.1006 132.8993 2.0649 288.9649 286.9000 269.2031 133.6650 2.0586 288.8382 286.7796 269.2927 134.4828 2.0484 288.7230 286.6745 269.4179 135.2593 2.0374 288.6475 286.6101 269.5453 136.1070 2.0327 288.5561 286.5235 269.6781 136.8735 2.0232 288.4789 286.4558 269.7659 137.7013 2.0151 288.3949 286.3798 269.8399 138.4670 2.0085 288.2987 286.2902 269.9335 139.2950 1.9992 288.1938 286.1946 270.0398 140.1125 1.9934 288.0818 286.0884 270.1519 140.8885 1.9822 287.9729 285.9907 270.2728 141.7370 1.9743 287.8459 285.8716 270.3895 142.4933 1.9666 287.7440 285.7774 270.5249 143.3305 1.9503 287.6125 285.6622 270.6830 144.0868 1.9443 287.5189 285.5746 270.7612 144.9148 1.9333 287.4293 285.4959 270.9220 145.7110 1.9219 287.3245 285.4026 271.0383 146.5083 1.9127 287.1879 285.2752 271.1620 147.3358 1.9039 287.1162 285.2124 271.2939 148.0915 1.8951 287.0269 285.1318 271.3946 148.9605 1.8870 286.9338 285.0468 271.5450 149.6855 1.8812 286.8611 284.9799 271.6812 150.5643 1.8690 286.7635 284.8944 271.8489 151.3308 1.8576 286.6787 284.8212 271.9934 152.1583 1.8475 286.6011 284.7536 272.1246 152.9550 1.8356 286.5099 284.6742 272.2650 153.7420 1.8251 286.4123 284.5872 272.4311 154.5698 1.8131 286.3289 284.5158 272.5780 155.3355 1.8055 286.2243 284.4188 272.6854 156.1943 1.7944 286.1108 284.3164 272.8150 156.9605 1.7807 286.0160 284.2353 272.9493 157.7775 1.7626 285.9078 284.1453 273.1023 158.5850 1.7522 285.8442 284.0920 273.2615 159.3715 1.7454 285.7587 284.0133 273.3820 160.1888 1.7327 285.6510 283.9183 273.5158 160.9963 1.7189 285.5778 283.8589 273.6552 161.7933 1.7047 285.5348 283.8300 273.7871 162.5795 1.6987 285.4637 283.7650 273.9137 163.4178 1.6865 285.3829 283.6964 274.0744 164.1738 1.6749 285.3134 283.6385 274.1678 165.0318 1.6616 285.2208 283.5593 274.2958 165.7983 1.6541 285.1450 283.4909 274.4255 166.6258 1.6455 285.0549 283.4094 274.5953 167.4225 1.6396 284.9615 283.3218 274.7131 168.2095 1.6288 284.8670 283.2382 274.8344 169.0473 1.6151 284.7770 283.1619 274.9798 169.8030 1.6009 284.7079 283.1070 275.1035 170.6720 1.5840 284.6421 283.0581 275.2687 171.4173 1.5717 284.5500 282.9783 275.3684 172.2655 1.5588 284.4520 282.8933 275.5070 173.0423 1.5481 284.3864 282.8383 275.6318 173.8595 1.5379 284.3177 282.7798 275.7461 174.6563 1.5255 284.2449 282.7194 275.8767 175.4535 1.5137 284.2173 282.7036 276.0305 176.2810 1.5006 284.1949 282.6943 276.1429 177.0470 1.4887 284.1203 282.6316 276.2462 177.8955 1.4771 284.0172 282.5401 276.3634 178.6715 1.4660 283.9306 282.4646 276.4835 179.4890 1.4552 283.8684 282.4132 276.5824 180.2863 1.4396 283.7991 282.3595 276.6797 181.0830 1.4287 283.7027 282.2740 276.7785 181.9105 1.4154 283.6372 282.2218 276.9474 182.6770 1.3996 283.5774 282.1778 277.0466 183.5255 1.3870 283.4782 282.0912 277.1422 184.3013 1.3783 283.3953 282.0170 277.2514 185.1190 1.3660 283.3502 281.9842 277.3630 185.9163 1.3542 283.3032 281.9490 277.4654 186.7125 1.3449 283.2476 281.9027 277.6175 187.5405 1.3303 283.1912 281.8609 277.7711 188.2965 1.3190 283.1125 281.7935 277.8950 189.1545 1.3033 283.0508 281.7476 277.9892 189.9108 1.2928 283.0261 281.7333 278.0639 190.7280 1.2813 282.9782 281.6970 278.1792 191.5248 1.2694 282.9138 281.6443 278.2951 192.3220 1.2585 282.8621 281.6036 278.4266 193.1190 1.2469 282.8166 281.5697 278.5088 193.9155 1.2328 282.7780 281.5452 278.6236 194.7333 1.2207 282.7352 281.5145 278.7155 195.4895 1.2131 282.6654 281.4524 278.8036 196.3575 1.2041 282.6311 281.4270 278.9420 197.1138 1.1926 282.6029 281.4103 279.0669 197.9315 1.1754 282.5566 281.3812 279.1971 198.7380 1.1634 282.5133 281.3499 279.3398 199.5250 1.1509 282.4634 281.3125 279.4496 200.3428 1.1400 282.4252 281.2853 279.5489 201.1188 1.1245 282.3896 281.2652 279.6079 201.9670 1.1058 282.3408 281.2350 279.7188 202.7335 1.0939 282.2818 281.1878 279.8058 203.5608 1.0819 282.2138 281.1320 279.8820 204.3578 1.0706 282.1715 281.1009 279.9517 205.1550 1.0571 282.1539 281.0968 280.0257 205.9410 1.0418 282.1117 281.0698 280.1158 206.7485 1.0293 282.0435 281.0142 280.2038 207.5663 1.0181 281.9997 280.9816 280.3078 208.3215 1.0109 281.9290 280.9182 280.3978 209.1905 1.0003 281.9204 280.9201 280.5140 209.9468 0.9891 281.9383 280.9492 280.6438 210.7740 0.9724 281.9310 280.9586 280.8052 211.5710 0.9611 281.9128 280.9517 280.9000 212.3785 0.9491 281.8490 280.8998 281.0055 213.1958 0.9370 281.7991 280.8621 281.1238 213.9618 0.9282 281.7334 280.8053 281.2223 214.8205 0.9186 281.6878 280.7692 281.3148 215.5863 0.9046 281.6264 280.7218 281.4244 216.4140 0.8905 281.5703 280.6798 281.5734 217.2010 0.8805 281.5244 280.6440 281.6310 218.0080 0.8704 281.4901 280.6198 281.7140 218.8253 0.8596 281.4413 280.5817 281.8499 219.5918 0.8477 281.4341 280.5864 281.9439 220.4500 0.8329 281.4615 280.6287 282.0635 221.2160 0.8245 281.4229 280.5984 282.1603 222.2183 0.8114 281.3698 280.5584 282.3263 223.0458 0.7990 281.3266 280.5276 282.4217 223.8425 0.7845 281.2960 280.5114 282.5419 224.6295 0.7745 281.2632 280.4887 282.6404 225.4365 0.7614 281.1978 280.4364 282.7442 226.2333 0.7533 281.1776 280.4243 282.8420 227.0613 0.7410 281.1573 280.4162 282.9475 227.8170 0.7336 281.1477 280.4141 283.0531 228.6855 0.7233 281.1291 280.4059 283.1611 229.4418 0.7124 281.1195 280.4071 283.2621 230.2695 0.6969 281.1058 280.4089 283.3842 231.0660 0.6886 281.0917 280.4030 283.5096 231.8633 0.6744 281.0644 280.3900 283.6168 232.6908 0.6644 281.0194 280.3550 283.7340 233.4465 0.6528 280.9546 280.3019 283.8485 234.3155 0.6413 280.9341 280.2927 283.9476 235.0713 0.6341 280.9369 280.3029 284.0573 235.9090 0.6234 280.9075 280.2841 284.1616 236.6960 0.6096 280.8731 280.2635 284.2928 237.5033 0.5959 280.8373 280.2414 284.4158 238.3203 0.5866 280.8452 280.2586 284.4935 239.0868 0.5770 280.8355 280.2585 284.6036 239.9453 0.5667 280.8424 280.2757 284.7103 240.7110 0.5563 280.8314 280.2750 284.7967 241.5390 0.5487 280.7972 280.2485 284.8745 242.3360 0.5372 280.7964 280.2592 284.9750 243.1325 0.5287 280.7760 280.2472 285.1070 243.9605 0.5167 280.7725 280.2557 285.2397 244.7265 0.5084 280.6976 280.1892 285.3447 245.5745 0.4986 280.6528 280.1541 285.4709 246.3513 0.4831 280.6146 280.1315 285.5976 247.1685 0.4725 280.6142 280.1417 285.7459 247.9653 0.4652 280.6289 280.1637 285.8512 248.7625 0.4566 280.6347 280.1780 285.9706 249.5900 0.4515 280.6342 280.1827 286.1050 250.3560 0.4377 280.6149 280.1772 286.2392 251.2045 0.4240 280.5938 280.1697 286.3771 251.9808 0.4110 280.6018 280.1907 286.5180 252.8185 0.4020 280.6189 280.2170 286.6451 253.5543 0.3940 280.6192 280.2252 286.7571 254.4025 0.3836 280.6060 280.2224 286.8777 255.1683 0.3715 280.6126 280.2411 286.9649 255.9860 0.3616 280.6111 280.2495 287.0872 256.7833 0.3510 280.6200 280.2690 287.2107 257.5798 0.3421 280.6391 280.2970 287.3084 258.4075 0.3294 280.6347 280.3053 287.4556 259.1635 0.3187 280.6385 280.3198 287.5819 260.0215 0.3071 280.6046 280.2974 287.7093 260.7778 0.2991 280.6155 280.3164 287.7934 261.5955 0.2877 280.6209 280.3332 287.9137 262.4228 0.2763 280.6330 280.3568 288.0167 263.3940 0.2616 280.6344 280.3728 288.1280 264.1810 0.2499 280.6208 280.3709 288.2354 265.0085 0.2362 280.6194 280.3832 288.3745 265.7745 0.2267 280.5969 280.3702 288.5367 266.6333 0.2180 280.6181 280.4000 288.6808 267.3990 0.2098 280.6120 280.4022 288.7817 268.2165 0.1980 280.6279 280.4299 288.8870 269.0138 0.1869 280.6483 280.4614 289.0000 269.8105 0.1773 280.6417 280.4645 289.1156 270.6278 0.1708 280.6418 280.4709 289.2240 271.4045 0.1632 280.6331 280.4699 289.3287 272.2525 0.1525 280.6220 280.4695 289.4586 273.0185 0.1452 280.6524 280.5072 289.5542 273.8465 0.1377 280.6887 280.5510 289.6981 274.6433 0.1306 280.6840 280.5534 289.8408 275.4298 0.1192 280.6744 280.5552 289.9448 276.2578 0.1075 280.6711 280.5636 290.0728 277.0238 0.0974 280.6869 280.5896 290.2250 277.8820 0.0838 280.6682 280.5844 290.3589 278.6383 0.0762 280.6809 280.6047 290.4820 279.4658 0.0683 280.6946 280.6262 290.6077 280.2625 0.0532 280.6915 280.6383 290.7477 281.0495 0.0438 280.7165 280.6727 290.8959 281.8870 0.0357 280.7553 280.7195 291.0188 282.6430 0.0269 280.7751 280.7482 291.1208 283.5120 0.0168 280.7813 280.7645 291.2624 284.2470 0.0095 280.7508 280.7413 291.3750 285.1055 -0.0032 280.7411 280.7443 291.5175 285.8720 -0.0110 280.7569 280.7679 291.6456 286.6998 -0.0245 280.7469 280.7714 291.7861 287.4860 -0.0331 280.7395 280.7726 291.9330 288.2935 -0.0414 280.7442 280.7856 292.0617 289.1110 -0.0557 280.7692 280.8249 292.1943 289.8768 -0.0670 280.7963 280.8633 292.3213 290.7355 -0.0777 280.8639 280.9416 292.4319 291.5020 -0.0839 280.9128 280.9967 292.5746 292.3290 -0.0936 280.9409 281.0345 292.7160 293.1365 -0.1046 280.9464 281.0510 292.8657 293.9440 -0.1112 280.9369 281.0481 293.0161 294.7300 -0.1224 280.9525 281.0749 293.1236 295.5375 -0.1347 280.9748 281.1095 293.1891 296.3553 -0.1430 281.0222 281.1652 293.2683 297.1210 -0.1525 281.0487 281.2012 293.3583 297.9795 -0.1626 281.0495 281.2120 293.4901 298.7460 -0.1702 281.0937 281.2640 293.6327 299.5735 -0.1813 281.1050 281.2863 293.7447 300.3600 -0.1879 281.1122 281.3001 293.8582 301.1675 -0.1922 281.1287 281.3209 294.0085 301.9848 -0.2007 281.1217 281.3224 294.1302 302.7508 -0.2122 281.1281 281.3402 294.2444 303.6198 -0.2303 281.1641 281.3944 294.3709 304.3758 -0.2418 281.2089 281.4507 294.5053 305.1928 -0.2526 281.2513 281.5039 294.6213 305.9695 -0.2597 281.2617 281.5213 294.7458 306.8175 -0.2682 281.2999 281.5680 294.8867 307.5835 -0.2785 281.3502 281.6287 294.9993 308.4115 -0.2886 281.4097 281.6983 295.1319 309.2083 -0.2957 281.4526 281.7483 295.2532 310.0050 -0.3045 281.4587 281.7632 295.3567 310.8330 -0.3163 281.4958 281.8120 295.4879 311.5993 -0.3243 281.5131 281.8374 295.6087 312.4573 -0.3302 281.5621 281.8922 295.7289 313.2238 -0.3342 281.5712 281.9054 295.8385 314.0720 -0.3431 281.5994 281.9425 295.9822 314.8070 -0.3542 281.6268 281.9809 296.0769 315.6658 -0.3657 281.6377 282.0034 296.1852 316.4320 -0.3762 281.6764 282.0526 296.2990 317.2490 -0.3828 281.6977 282.0806 296.3923 318.0463 -0.3894 281.7380 282.1274 296.4959 318.8433 -0.3954 281.7774 282.1729 296.6275 319.6603 -0.4017 281.8136 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