DTA measure 1lassu Date: 2026317:1624 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.18 s Mass = 100.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2205 -1.8061 210.0552 211.8613 247.8642 2.0280 -1.8076 210.2242 212.0318 247.8230 2.8150 -1.8075 210.3627 212.1702 247.7935 3.6430 -1.8050 210.5168 212.3218 247.7853 4.4300 -1.8018 210.6752 212.4770 247.7474 5.2273 -1.8055 210.8204 212.6259 247.7032 6.0253 -1.8028 210.9453 212.7481 247.6279 6.8535 -1.8008 211.0593 212.8601 247.5765 7.6200 -1.8018 211.1470 212.9488 247.5478 8.4685 -1.8002 211.2658 213.0660 247.4850 9.2453 -1.7989 211.4082 213.2071 247.4407 10.0630 -1.7965 211.5578 213.3543 247.4025 10.8603 -1.7938 211.6851 213.4789 247.3969 11.6575 -1.7927 211.8099 213.6025 247.3566 12.4855 -1.7902 211.9602 213.7504 247.3366 13.2520 -1.7887 212.1105 213.8992 247.3385 14.1108 -1.7847 212.2988 214.0836 247.3219 14.8670 -1.7836 212.4340 214.2176 247.3212 15.6950 -1.7798 212.5366 214.3164 247.2875 16.4615 -1.7751 212.6425 214.4176 247.2367 17.3203 -1.7744 212.8044 214.5787 247.1872 18.0868 -1.7720 212.9150 214.6870 247.1636 18.9045 -1.7710 213.0762 214.8472 247.1765 19.7128 -1.7691 213.2007 214.9698 247.1628 20.5000 -1.7696 213.3314 215.1010 247.1623 21.3178 -1.7687 213.4624 215.2311 247.1369 22.0843 -1.7717 213.5540 215.3257 247.1469 22.9328 -1.7672 213.6841 215.4512 247.1453 23.6993 -1.7647 213.7836 215.5483 247.1232 24.5170 -1.7607 213.8948 215.6555 247.1308 25.2835 -1.7543 214.0184 215.7727 247.1331 26.1320 -1.7497 214.1712 215.9210 247.1649 26.8985 -1.7451 214.3228 216.0679 247.2050 27.7265 -1.7424 214.4708 216.2132 247.2342 28.5135 -1.7420 214.6162 216.3582 247.2774 29.3010 -1.7406 214.7706 216.5112 247.2837 30.1090 -1.7347 214.9149 216.6496 247.3069 30.8960 -1.7303 215.0422 216.7725 247.3452 31.7138 -1.7260 215.1697 216.8957 247.4191 32.4905 -1.7219 215.2830 217.0049 247.5033 33.3390 -1.7249 215.4226 217.1475 247.5888 34.1055 -1.7216 215.5502 217.2718 247.6736 34.9438 -1.7128 215.6697 217.3825 247.7343 35.6898 -1.7026 215.7466 217.4492 247.7955 36.5485 -1.6971 215.8965 217.5936 247.8922 37.3048 -1.6927 216.0202 217.7128 247.9252 38.1330 -1.6887 216.1607 217.8494 248.0085 38.9310 -1.6823 216.2880 217.9703 248.1308 39.7283 -1.6743 216.4067 218.0810 248.2317 40.5563 -1.6690 216.5695 218.2385 248.3291 41.3125 -1.6678 216.6893 218.3571 248.4161 42.1405 -1.6643 216.8296 218.4939 248.5155 42.9070 -1.6601 216.9456 218.6057 248.5950 43.7555 -1.6587 217.0751 218.7338 248.6884 44.5323 -1.6633 217.2011 218.8644 248.7761 45.3603 -1.6544 217.3592 219.0136 248.8962 46.1473 -1.6523 217.4802 219.1325 249.0132 46.9650 -1.6518 217.5999 219.2517 249.1456 47.7315 -1.6505 217.6900 219.3405 249.2705 48.5595 -1.6475 217.8017 219.4492 249.4207 49.3568 -1.6458 217.9483 219.5941 249.5167 50.1540 -1.6409 218.1113 219.7523 249.6278 50.9718 -1.6368 218.2563 219.8931 249.7864 51.7485 -1.6299 218.3866 220.0165 249.9200 52.5973 -1.6271 218.4949 220.1220 250.0071 53.3645 -1.6252 218.5698 220.1950 250.1210 54.1925 -1.6220 218.6999 220.3219 250.2897 54.9898 -1.6156 218.8473 220.4629 250.4536 55.8075 -1.6140 218.9648 220.5788 250.5954 56.5740 -1.6158 219.0613 220.6771 250.7483 57.4020 -1.6113 219.1535 220.7648 250.9243 58.1890 -1.6078 219.2567 220.8645 251.0503 58.9965 -1.6048 219.4071 221.0119 251.1705 59.8143 -1.6084 219.5454 221.1537 251.3260 60.5808 -1.6055 219.6826 221.2880 251.4657 61.4395 -1.6045 219.8393 221.4437 251.6023 62.2060 -1.6040 219.9337 221.5377 251.7520 63.0340 -1.6059 220.0612 221.6670 251.8876 63.8215 -1.6048 220.2059 221.8107 252.0531 64.6295 -1.6028 220.3285 221.9312 252.1991 65.4473 -1.5988 220.4652 222.0639 252.3779 66.2445 -1.5984 220.5931 222.1915 252.5299 67.0315 -1.5982 220.7316 222.3298 252.6891 67.8288 -1.5940 220.8673 222.4613 252.8321 68.6568 -1.5924 220.9757 222.5681 252.9669 69.4233 -1.5900 221.0787 222.6687 253.0924 70.2820 -1.5840 221.2400 222.8240 253.2508 71.0388 -1.5822 221.3666 222.9488 253.3515 71.8775 -1.5808 221.5032 223.0840 253.5181 72.6645 -1.5822 221.6066 223.1888 253.6590 73.4618 -1.5832 221.6884 223.2716 253.7883 74.2898 -1.5820 221.8104 223.3925 253.9278 75.0563 -1.5858 221.9443 223.5301 254.0700 75.8945 -1.5879 222.0836 223.6714 254.1836 76.6815 -1.5843 222.2154 223.7998 254.3105 77.4993 -1.5838 222.3319 223.9156 254.4362 78.2658 -1.5799 222.4597 224.0397 254.5722 79.1245 -1.5753 222.5855 224.1608 254.7431 79.8910 -1.5722 222.7277 224.2999 254.8791 80.7190 -1.5693 222.8383 224.4076 254.9916 81.5068 -1.5677 222.9662 224.5339 255.1230 82.3145 -1.5659 223.0761 224.6420 255.2384 83.1323 -1.5615 223.1683 224.7298 255.3843 83.8988 -1.5596 223.2835 224.8431 255.5080 84.7268 -1.5604 223.4164 224.9768 255.6446 85.4830 -1.5602 223.5289 225.0891 255.7818 86.4443 -1.5564 223.6766 225.2329 255.9383 87.3338 -1.5574 223.8347 225.3921 256.0681 88.1003 -1.5574 223.9467 225.5041 256.1893 88.9283 -1.5570 224.0920 225.6489 256.3247 89.7160 -1.5595 224.2060 225.7655 256.4588 90.5135 -1.5590 224.3317 225.8907 256.5736 91.3313 -1.5569 224.4875 226.0444 256.7271 92.0875 -1.5513 224.6172 226.1685 256.8598 92.9258 -1.5511 224.7474 226.2985 256.9424 93.6820 -1.5497 224.7898 226.3395 257.0432 94.5408 -1.5526 224.9380 226.4906 257.1530 95.3073 -1.5527 225.0951 226.6478 257.2990 96.1250 -1.5534 225.2511 226.8045 257.3973 96.9228 -1.5543 225.4053 226.9596 257.4975 97.7205 -1.5576 225.5280 227.0856 257.6227 98.5485 -1.5598 225.6516 227.2113 257.7260 99.3048 -1.5561 225.7935 227.3496 257.7883 100.1635 -1.5550 225.9404 227.4954 257.8885 100.9300 -1.5548 226.0590 227.6138 257.9625 101.7580 -1.5536 226.1692 227.7227 258.0639 102.5450 -1.5529 226.2863 227.8392 258.1936 103.3423 -1.5535 226.4075 227.9610 258.3171 104.1703 -1.5561 226.5170 228.0731 258.4316 104.9275 -1.5563 226.6214 228.1777 258.5143 105.7658 -1.5543 226.7743 228.3285 258.6270 106.5220 -1.5541 226.8815 228.4355 258.6792 107.3705 -1.5481 226.9962 228.5444 258.7734 108.1473 -1.5439 227.1038 228.6477 258.8368 108.9650 -1.5404 227.2353 228.7757 258.9362 109.7623 -1.5456 227.3843 228.9299 259.0447 110.5595 -1.5475 227.5018 229.0493 259.1178 111.3875 -1.5445 227.6494 229.1939 259.2277 112.1540 -1.5433 227.7413 229.2846 259.3016 113.0025 -1.5421 227.8389 229.3810 259.4186 113.7793 -1.5373 227.9716 229.5090 259.5088 114.5970 -1.5372 228.1000 229.6372 259.6047 115.3840 -1.5359 228.2090 229.7449 259.6955 116.1915 -1.5355 228.3485 229.8841 259.7872 116.9898 -1.5382 228.4701 230.0083 259.8463 117.8075 -1.5371 228.5679 230.1050 259.9064 118.6253 -1.5375 228.6546 230.1921 259.9996 119.3918 -1.5379 228.7601 230.2980 260.1168 120.2505 -1.5378 228.9006 230.4384 260.2035 121.0170 -1.5348 228.9953 230.5301 260.2897 121.8450 -1.5336 229.1356 230.6692 260.3456 122.6320 -1.5338 229.2842 230.8180 260.4358 123.4395 -1.5319 229.4043 230.9362 260.5663 124.2583 -1.5309 229.5270 231.0579 260.6898 125.0248 -1.5300 229.6754 231.2054 260.7561 125.8835 -1.5265 229.7970 231.3235 260.8504 126.6500 -1.5283 229.9333 231.4616 260.9465 127.6523 -1.5285 230.1041 231.6326 261.0864 128.4700 -1.5287 230.2699 231.7986 261.1564 129.2673 -1.5299 230.3863 231.9162 261.2303 130.0645 -1.5244 230.4857 232.0101 261.3024 130.8925 -1.5233 230.5727 232.0960 261.3785 131.6598 -1.5236 230.6836 232.2072 261.4451 132.5085 -1.5261 230.8075 232.3336 261.5304 133.2853 -1.5220 230.9468 232.4687 261.6383 134.1030 -1.5195 231.0625 232.5820 261.7585 134.9003 -1.5217 231.1916 232.7134 261.8541 135.6975 -1.5203 231.2921 232.8124 261.9651 136.5255 -1.5203 231.4145 232.9348 262.0749 137.2920 -1.5162 231.5388 233.0550 262.1702 138.1405 -1.5145 231.6511 233.1656 262.2767 138.9173 -1.5157 231.7483 233.2640 262.3795 139.7350 -1.5148 231.8806 233.3954 262.4742 140.5323 -1.5105 231.9853 233.4958 262.5662 141.3305 -1.5124 232.1201 233.6325 262.6657 142.1585 -1.5133 232.2954 233.8087 262.7670 142.9250 -1.5107 232.4185 233.9293 262.8897 143.7428 -1.5111 232.5469 234.0580 263.0311 144.5503 -1.5137 232.6721 234.1859 263.0770 145.3680 -1.5137 232.7550 234.2687 263.1872 146.1345 -1.5109 232.8675 234.3784 263.2743 146.9625 -1.5047 233.0032 234.5078 263.3666 147.7700 -1.5021 233.1347 234.6368 263.4666 148.5673 -1.5013 233.2482 234.7495 263.5489 149.3750 -1.5018 233.3911 234.8929 263.6628 150.1423 -1.5020 233.5122 235.0142 263.7682 150.9908 -1.5010 233.6535 235.1545 263.8796 151.7573 -1.4986 233.7315 235.2301 263.9915 152.5750 -1.5000 233.8392 235.3392 264.0715 153.3723 -1.4993 233.9598 235.4591 264.1703 154.1695 -1.5046 234.0845 235.5891 264.2872 154.9873 -1.5019 234.1994 235.7013 264.3877 155.7435 -1.4967 234.3018 235.7984 264.4708 156.6023 -1.4928 234.4022 235.8951 264.5932 157.3593 -1.4907 234.5309 236.0215 264.6872 158.3618 -1.4969 234.7221 236.2190 264.7950 159.1795 -1.4973 234.8336 236.3310 264.9059 159.9870 -1.4976 234.9364 236.4341 264.9587 160.7740 -1.4959 235.0391 236.5350 265.0533 161.5918 -1.4993 235.1502 236.6495 265.1509 162.3685 -1.4969 235.2404 236.7373 265.2039 163.2170 -1.4949 235.3486 236.8436 265.3352 163.9835 -1.4960 235.4682 236.9642 265.4358 164.8118 -1.4975 235.5907 237.0882 265.5531 165.5995 -1.4965 235.7185 237.2150 265.6562 166.3968 -1.4965 235.8354 237.3319 265.7501 167.2248 -1.4960 235.9490 237.4450 265.8582 167.9810 -1.5007 236.0846 237.5853 265.9565 168.8398 -1.5029 236.2059 237.7088 266.0622 169.6063 -1.5004 236.3187 237.8190 266.1415 170.4343 -1.4963 236.4063 237.9026 266.2377 171.2315 -1.4993 236.5187 238.0180 266.3494 172.0185 -1.5007 236.6107 238.1113 266.4358 172.8465 -1.4991 236.7527 238.2518 266.5484 173.6130 -1.4938 236.8994 238.3932 266.6747 174.4615 -1.4919 236.9998 238.4917 266.8097 175.2383 -1.4947 237.1143 238.6091 266.9375 176.0560 -1.4931 237.2477 238.7409 267.0609 176.8533 -1.4927 237.3899 238.8826 267.1461 177.6510 -1.4934 237.4948 238.9882 267.2677 178.4795 -1.4941 237.5944 239.0885 267.3573 179.2460 -1.4934 237.6929 239.1863 267.4470 180.0638 -1.4899 237.7887 239.2786 267.5644 180.8405 -1.4898 237.8752 239.3651 267.6916 181.6890 -1.4935 237.9846 239.4781 267.7858 182.4555 -1.4925 238.1151 239.6077 267.8766 183.2835 -1.4923 238.2002 239.6925 268.0250 184.0808 -1.4930 238.3263 239.8193 268.1534 184.8780 -1.4908 238.4799 239.9707 268.2579 185.6958 -1.4864 238.6336 240.1201 268.3470 186.4725 -1.4828 238.7766 240.2594 268.4944 187.3220 -1.4845 238.8858 240.3703 268.6305 188.0885 -1.4845 238.9928 240.4773 268.7496 188.9370 -1.4856 239.0904 240.5759 268.9064 189.6933 -1.4857 239.2095 240.6952 269.0429 190.5315 -1.4809 239.3295 240.8104 269.1706 191.3185 -1.4806 239.4354 240.9160 269.2845 192.1158 -1.4837 239.5667 241.0504 269.3729 192.9438 -1.4837 239.7029 241.1866 269.5243 193.7103 -1.4830 239.8184 241.3014 269.6439 194.5690 -1.4841 239.9672 241.4513 269.7744 195.3253 -1.4781 240.0837 241.5618 269.9130 196.1645 -1.4760 240.2269 241.7029 270.0565 196.9515 -1.4727 240.3221 241.7948 270.1871 197.7488 -1.4752 240.4474 241.9226 270.3187 198.5870 -1.4789 240.5622 242.0411 270.3994 199.3638 -1.4783 240.6475 242.1257 270.5075 200.1918 -1.4786 240.7398 242.2184 270.6126 200.9583 -1.4785 240.8353 242.3138 270.7135 201.8170 -1.4779 240.9715 242.4495 270.8727 202.5733 -1.4766 241.0875 242.5642 270.9525 203.4115 -1.4751 241.2168 242.6919 271.0838 204.1988 -1.4794 241.3426 242.8220 271.2090 204.9968 -1.4826 241.4698 242.9523 271.3067 205.8248 -1.4841 241.5640 243.0480 271.4263 206.5913 -1.4806 241.6496 243.1302 271.5439 207.4500 -1.4822 241.8050 243.2872 271.6685 208.2063 -1.4786 241.9282 243.4068 271.7835 209.0548 -1.4761 242.0538 243.5298 271.9320 209.7905 -1.4750 242.1412 243.6161 271.9846 210.6595 -1.4728 242.2275 243.7003 272.0901 211.4160 -1.4754 242.3112 243.7866 272.2088 212.2448 -1.4768 242.4304 243.9072 272.3501 213.0420 -1.4793 242.5625 244.0418 272.4532 213.8290 -1.4790 242.7124 244.1913 272.5267 214.6570 -1.4771 242.8557 244.3328 272.6149 215.4235 -1.4763 242.9501 244.4264 272.6829 216.2720 -1.4803 243.1181 244.5984 272.7917 217.0283 -1.4847 243.2115 244.6962 272.8973 217.8665 -1.4873 243.3240 244.8113 273.0201 218.6535 -1.4832 243.4326 244.9158 273.1235 219.4610 -1.4793 243.5245 245.0038 273.2370 220.2275 -1.4750 243.6464 245.1213 273.3288 221.0555 -1.4743 243.7343 245.2086 273.4278 221.8533 -1.4719 243.8578 245.3298 273.5240 222.6408 -1.4730 243.9740 245.4471 273.5965 223.4688 -1.4767 244.0916 245.5683 273.6639 224.2250 -1.4801 244.1984 245.6785 273.7450 225.0838 -1.4777 244.3050 245.7827 273.8495 225.8503 -1.4781 244.4168 245.8949 273.9581 226.6783 -1.4754 244.5568 246.0323 274.0632 227.4755 -1.4710 244.6765 246.1475 274.1451 228.2625 -1.4702 244.8174 246.2876 274.2479 229.0905 -1.4716 244.9492 246.4208 274.3169 229.8775 -1.4719 245.0578 246.5297 274.4190 230.6953 -1.4751 245.1845 246.6596 274.5260 231.4618 -1.4735 245.2913 246.7648 274.6547 232.3205 -1.4680 245.4140 246.8819 274.7582 233.0773 -1.4649 245.5318 246.9966 274.8464 233.9058 -1.4651 245.6524 247.1175 274.9291 234.7030 -1.4686 245.7621 247.2306 275.0316 235.4900 -1.4713 245.8926 247.3639 275.1467 236.3180 -1.4699 245.9989 247.4688 275.2251 237.0845 -1.4676 246.0603 247.5279 275.3027 237.9433 -1.4653 246.1798 247.6451 275.3916 238.7098 -1.4657 246.2837 247.7494 275.4736 239.5378 -1.4660 246.3816 247.8476 275.5651 240.2940 -1.4660 246.5011 247.9671 275.6398 241.1425 -1.4632 246.6358 248.0991 275.7230 241.9203 -1.4658 246.7458 248.2116 275.8024 242.7380 -1.4672 246.8328 248.3000 275.9122 243.5353 -1.4654 246.9487 248.4142 276.0097 244.3325 -1.4669 247.0603 248.5272 276.1035 245.1605 -1.4693 247.1940 248.6633 276.1951 245.9270 -1.4711 247.3309 248.8020 276.2802 246.7755 -1.4699 247.4454 248.9153 276.3816 247.5523 -1.4727 247.5416 249.0143 276.4705 248.3700 -1.4744 247.6563 249.1306 276.5595 249.1673 -1.4766 247.7960 249.2725 276.6706 249.9748 -1.4762 247.9416 249.4178 276.7716 250.7618 -1.4753 248.0480 249.5233 276.8868 251.5795 -1.4766 248.1826 249.6592 276.9418 252.3870 -1.4762 248.2984 249.7747 277.0000 253.1740 -1.4762 248.4127 249.8888 277.0830 254.0020 -1.4759 248.5225 249.9984 277.2178 254.7685 -1.4749 248.6016 250.0765 277.2993 255.6273 -1.4760 248.7127 250.1886 277.4546 256.3938 -1.4742 248.8248 250.2990 277.5388 257.2120 -1.4708 248.9221 250.3929 277.6333 258.0200 -1.4694 249.0238 250.4933 277.7402 258.8070 -1.4664 249.1189 250.5853 277.8396 259.6350 -1.4673 249.2517 250.7190 277.9624 260.4220 -1.4707 249.4068 250.8775 278.0493 261.2603 -1.4707 249.5576 251.0283 278.1488 262.0165 -1.4689 249.6245 251.0935 278.2290 262.8855 -1.4654 249.7593 251.2248 278.3618 263.6418 -1.4648 249.8549 251.3197 278.4757 264.4698 -1.4671 249.9504 251.4176 278.5817 265.2680 -1.4683 250.0745 251.5428 278.6814 266.0653 -1.4646 250.1949 251.6595 278.7666 266.8933 -1.4627 250.3507 251.8133 278.8829 267.6495 -1.4652 250.4637 251.9290 278.9866 268.5185 -1.4668 250.5792 252.0460 279.1348 269.2748 -1.4657 250.7061 252.1718 279.2589 270.1028 -1.4664 250.8240 252.2904 279.3529 270.8590 -1.4689 250.9269 252.3957 279.4374 271.7178 -1.4740 251.0417 252.5157 279.5431 272.4843 -1.4762 251.1438 252.6199 279.6421 273.3125 -1.4787 251.2242 252.7029 279.7447 274.1105 -1.4787 251.2981 252.7768 279.8311 274.8975 -1.4774 251.3872 252.8645 279.9390 275.7358 -1.4794 251.5128 252.9922 280.0302 276.4920 -1.4813 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