DTA measure 1lassu Date: 2024101:1618 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.26 s Mass = 958.900 mg data_number = 1586 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1740 -0.7135 273.6272 274.3406 267.7432 1.9355 -0.7253 273.6342 274.3595 267.5682 2.7578 -0.7216 273.6684 274.3900 267.6509 3.5500 -0.7132 273.5798 274.2930 267.6736 4.3415 -0.7465 273.6042 274.3507 267.5459 5.1640 -0.7023 273.7516 274.4539 267.6318 5.9555 -0.6946 273.8975 274.5921 267.7257 6.7778 -0.7004 273.7923 274.4928 267.7470 7.5698 -0.6892 273.9482 274.6374 267.8836 8.3615 -0.7057 274.0721 274.7778 267.7038 9.1838 -0.6879 273.9531 274.6410 267.8395 9.9455 -0.6896 273.9168 274.6064 267.8928 10.7978 -0.7064 274.0402 274.7467 267.7997 11.5898 -0.6816 274.0180 274.6996 267.7494 12.3815 -0.6983 274.1563 274.8546 267.8261 13.2035 -0.7091 274.0824 274.7914 267.9825 13.9655 -0.7438 274.1717 274.9156 268.0985 14.8175 -0.7471 274.3823 275.1294 268.1506 15.5745 -0.7753 274.3835 275.1588 268.2508 16.4273 -0.7836 274.2448 275.0283 268.2251 17.1895 -0.7898 274.3907 275.1805 268.4154 18.0115 -0.7799 274.3605 275.1404 268.4589 18.8335 -0.7666 274.3067 275.0733 268.5976 19.5955 -0.7774 274.1894 274.9668 268.5646 20.4480 -0.7697 274.4362 275.2058 268.7997 21.2105 -0.7824 274.4477 275.2302 268.9185 22.0323 -0.7623 274.3516 275.1139 269.0270 22.8245 -0.8026 274.3979 275.2004 269.0083 23.6165 -0.7880 274.5153 275.3033 269.1294 24.4680 -0.7812 274.5979 275.3792 269.1716 25.2313 -0.7659 274.6470 275.4130 269.2263 26.0605 -0.7610 274.7229 275.4839 269.2800 26.8530 -0.7954 274.6341 275.4295 269.3415 27.6455 -0.7993 274.6848 275.4841 269.4786 28.4678 -0.7852 274.6961 275.4813 269.7882 29.2595 -0.7764 274.8770 275.6534 269.8261 30.0818 -0.7790 274.7334 275.5124 269.9194 30.8738 -0.7517 274.9637 275.7154 270.0560 31.6655 -0.7500 274.8782 275.6281 270.1242 32.5183 -0.7464 274.7912 275.5377 270.1725 33.2805 -0.7898 275.0185 275.8083 270.2786 34.1035 -0.8018 275.0756 275.8774 270.4073 34.8958 -0.7783 275.0518 275.8301 270.4231 35.6875 -0.7676 274.8554 275.6230 270.6954 36.5395 -0.7639 274.9852 275.7491 270.8470 37.3015 -0.7929 275.0343 275.8272 270.9508 38.1243 -0.7991 275.1180 275.9172 270.8472 38.9165 -0.7905 275.1097 275.9002 270.9794 39.7095 -0.7896 275.1366 275.9261 271.1799 40.5620 -0.7792 275.1585 275.9376 271.2970 41.3245 -0.7666 275.0512 275.8179 271.5065 42.1473 -0.7859 275.0866 275.8725 271.8031 42.9395 -0.7869 275.2739 276.0608 271.9466 43.7315 -0.7892 275.4482 276.2374 272.0654 44.5833 -0.7853 275.4450 276.2302 272.0361 45.3448 -0.7594 275.4034 276.1628 272.0234 46.1675 -0.7654 275.4125 276.1779 272.0313 46.9598 -0.7944 275.5909 276.3853 272.1628 47.7493 -0.8051 275.5815 276.3866 272.3350 48.5680 -0.8067 275.6398 276.4465 272.3160 49.3563 -0.7955 275.4701 276.2656 272.6079 50.1743 -0.8241 275.6079 276.4320 272.7229 50.9625 -0.8270 275.6582 276.4852 272.8302 51.7513 -0.8166 275.7514 276.5680 272.9168 52.5705 -0.8172 275.6369 276.4541 273.0058 53.3595 -0.8317 275.7858 276.6175 273.1582 54.1790 -0.8289 275.8835 276.7124 273.1449 54.9678 -0.8444 275.9349 276.7794 273.3589 55.7570 -0.8556 275.7987 276.6543 273.5143 56.5763 -0.8473 275.7537 276.6009 273.5341 57.3650 -0.8482 275.8929 276.7412 273.6379 58.1840 -0.8731 275.9625 276.8356 273.7069 58.9730 -0.8726 276.1041 276.9767 273.7416 59.7620 -0.8235 276.1297 276.9531 273.9710 60.6110 -0.8516 276.2372 277.0889 274.1058 61.3715 -0.8542 276.2521 277.1063 274.1444 62.1928 -0.8394 276.2271 277.0665 274.1901 62.9825 -0.8475 276.2117 277.0592 274.2343 63.7735 -0.8666 276.1941 277.0608 274.3326 64.5958 -0.8649 276.3050 277.1699 274.5786 65.3875 -0.9086 276.3304 277.2390 274.5906 66.2088 -0.8960 276.4078 277.3038 274.7680 67.0005 -0.8826 276.5125 277.3950 274.8216 67.7925 -0.8654 276.5295 277.3949 274.8923 68.6148 -0.8865 276.5043 277.3908 275.0013 69.3765 -0.8674 276.3871 277.2545 275.0422 70.2285 -0.8978 276.4100 277.3078 275.0675 71.0208 -0.8794 276.5983 277.4778 275.2836 71.8125 -0.8825 276.6822 277.5647 275.3927 72.6345 -0.8793 276.6610 277.5403 275.4810 73.3965 -0.8890 276.5940 277.4830 275.6187 74.2485 -0.9265 276.7503 277.6768 275.6680 75.0405 -0.9262 276.7839 277.7101 275.7556 75.8325 -0.9351 276.7806 277.7157 275.9965 76.6545 -0.9245 276.9975 277.9221 276.1403 77.4165 -0.8952 276.9290 277.8242 276.2211 78.2685 -0.9045 277.0594 277.9639 276.3994 79.0605 -0.9117 277.0221 277.9337 276.4465 79.8523 -0.9487 277.0261 277.9748 276.3444 80.6743 -0.9380 277.2056 278.1436 276.4998 81.4360 -0.9409 277.1772 278.1181 276.6539 82.2883 -0.9394 277.1577 278.0971 276.6649 83.0800 -0.9342 277.1865 278.1207 276.7062 83.8715 -0.9458 277.3182 278.2640 277.0320 84.6940 -0.9378 277.3154 278.2532 277.0555 85.4855 -0.9465 277.3502 278.2967 277.1649 86.3078 -0.9437 277.4315 278.3752 277.3584 87.0998 -0.9602 277.4485 278.4087 277.3159 87.8915 -0.9476 277.3960 278.3436 277.3886 88.7165 -0.9612 277.5029 278.4641 277.4195 89.5085 -0.9791 277.6567 278.6359 277.5458 90.3308 -0.9674 277.7319 278.6993 277.7855 91.1228 -0.9688 277.8806 278.8494 277.7848 91.9145 -0.9747 277.9630 278.9376 277.9172 92.7368 -0.9740 277.9230 278.8969 278.0731 93.5285 -0.9578 277.8771 278.8349 278.0447 94.3508 -0.9540 277.8800 278.8340 278.2324 95.1428 -0.9732 277.9689 278.9421 278.3934 95.9355 -0.9805 277.9985 278.9789 278.5076 96.7575 -0.9925 277.9665 278.9590 278.5116 97.5495 -0.9542 278.0825 279.0368 278.6712 98.3715 -0.9690 278.1390 279.1080 278.6812 99.1635 -0.9707 278.1578 279.1285 278.9211 99.9565 -0.9868 278.2168 279.2036 279.2268 100.7785 -0.9785 278.2736 279.2521 279.2971 101.5405 -0.9923 278.3624 279.3547 279.2408 102.3925 -0.9823 278.3967 279.3790 279.3973 103.1845 -0.9786 278.4503 279.4289 279.4136 103.9765 -0.9985 278.4843 279.4828 279.7030 104.7990 -0.9990 278.6617 279.6606 279.9399 105.5605 -1.0079 278.5620 279.5698 279.9546 106.4128 -0.9959 278.6765 279.6723 279.9170 107.2048 -1.0298 278.6788 279.7087 279.9561 107.9975 -1.0296 278.7881 279.8176 280.0766 108.8198 -1.0369 278.8571 279.8940 280.1265 109.5815 -1.0243 278.9535 279.9778 280.1669 110.4338 -1.0106 278.7948 279.8055 280.1832 111.2250 -1.0239 278.9353 279.9592 280.2672 112.0130 -1.0339 278.9645 279.9984 280.4924 112.8318 -1.0345 279.0307 280.0653 280.7027 113.5900 -1.0429 279.1611 280.2040 280.5892 114.4380 -1.0202 279.2500 280.2701 280.7038 115.2263 -1.0281 279.2262 280.2543 280.9115 116.0150 -1.0227 279.2498 280.2725 281.0516 116.8330 -1.0250 279.3176 280.3426 281.1479 117.6070 -1.0170 279.2460 280.2630 281.2603 118.4130 -1.0268 279.4029 280.4297 281.3183 119.2020 -1.0357 279.5937 280.6294 281.3888 120.0510 -1.0343 279.5557 280.5900 281.3717 120.8090 -1.0417 279.5931 280.6347 281.5866 121.6278 -1.0396 279.7395 280.7791 281.6237 122.4463 -1.0198 279.6701 280.6899 281.9019 123.2068 -1.0141 279.7745 280.7886 282.0077 124.0555 -1.0228 279.7725 280.7953 282.1265 124.8153 -1.0005 279.9550 280.9555 282.4004 125.6360 -0.9959 280.1133 281.1092 282.5129 126.4553 -0.9716 279.9890 280.9606 282.5031 127.2165 -0.9549 280.1105 281.0655 282.5663 128.0685 -0.9748 280.0193 280.9941 282.7037 128.8305 -0.9722 280.1995 281.1717 282.9198 129.6525 -0.9786 280.2185 281.1971 282.9835 130.4745 -0.9819 280.4397 281.4216 283.0888 131.2365 -0.9431 280.5155 281.4585 283.2658 132.0885 -0.9473 280.4874 281.4348 283.3076 132.8505 -0.9437 280.3716 281.3152 283.4631 133.6725 -0.9847 280.7753 281.7599 283.5174 134.4645 -0.9738 280.8185 281.7922 283.6132 135.2565 -0.9949 280.7461 281.7411 283.6495 136.1085 -1.0233 280.7556 281.7789 283.6871 136.8705 -0.9883 280.8391 281.8274 283.8556 137.6923 -1.0065 280.9638 281.9703 283.8442 138.4843 -1.0170 280.9660 281.9831 283.8180 139.2758 -1.0089 281.0075 282.0165 283.9483 140.1280 -0.9921 281.0400 282.0321 284.0589 140.8900 -1.1013 281.1275 282.2288 284.1897 141.7118 -1.1690 281.1265 282.2955 284.2191 142.5038 -1.2166 281.3289 282.5454 284.3305 143.2955 -1.2084 281.2369 282.4453 284.4142 144.1480 -1.2014 281.2992 282.5005 284.3434 144.9095 -1.1427 281.4095 282.5522 284.4753 145.7318 -1.1032 281.5047 282.6079 284.5406 146.5238 -1.1092 281.4800 282.5891 284.7060 147.3155 -1.0963 281.4005 282.4968 284.5354 148.1378 -1.0818 281.6035 282.6852 284.5878 148.9295 -1.0653 281.6233 282.6886 284.6365 149.7518 -1.1132 281.7411 282.8543 284.7415 150.5438 -1.1194 281.7917 282.9111 284.7111 151.3355 -1.1688 281.9538 283.1226 284.9284 152.1575 -1.1681 281.9686 283.1367 285.0667 152.9495 -1.2134 282.0762 283.2896 285.2190 153.7715 -1.1996 282.1481 283.3476 285.4247 154.5635 -1.2215 282.2075 283.4290 285.4648 155.3565 -1.2152 282.3725 283.5877 285.5504 156.1785 -1.1899 282.4098 283.5997 285.7600 156.9705 -1.2117 282.4616 283.6733 285.9619 157.7925 -1.1944 282.5239 283.7183 286.2801 158.5845 -1.2026 282.5336 283.7361 286.4391 159.3775 -1.2243 282.7505 283.9748 286.6203 160.1993 -1.1922 282.7572 283.9494 286.7342 160.9913 -1.2135 282.8091 284.0226 286.8092 161.8135 -1.2046 282.8717 284.0763 286.9204 162.6058 -1.2461 282.8303 284.0764 287.0039 163.3985 -1.1801 283.0357 284.2158 287.4412 164.2208 -1.1675 283.1353 284.3028 287.6984 165.0125 -1.1459 283.1368 284.2827 287.8842 165.8348 -1.1675 283.2135 284.3810 288.0060 166.6268 -1.1260 283.3089 284.4349 288.2331 167.4195 -1.1160 283.4115 284.5275 288.0920 168.2420 -1.1056 283.3856 284.4912 288.1021 169.0198 -1.1007 283.6480 284.7486 288.0758 169.8468 -1.1126 283.6385 284.7511 288.1009 170.6385 -1.1547 283.7604 284.9151 288.2601 171.4608 -1.1874 283.8761 285.0634 288.3118 172.2528 -1.1838 283.7656 284.9494 288.2635 173.0445 -1.1955 283.8182 285.0137 288.3751 173.8675 -1.2040 283.9836 285.1875 288.5460 174.6595 -1.1999 284.1155 285.3154 288.5111 175.4823 -1.1780 284.2485 285.4266 288.7234 176.2735 -1.1790 284.2485 285.4275 288.7902 177.0620 -1.1194 284.3976 285.5170 289.0489 177.8803 -1.1356 284.3911 285.5267 289.2350 178.6390 -1.0766 284.4720 285.5486 289.1711 179.4868 -1.0867 284.4075 285.4943 289.2171 180.2750 -1.0276 284.5280 285.5556 289.2740 181.0628 -1.0286 284.5656 285.5942 289.4441 181.8815 -1.0685 284.6491 285.7175 289.6905 182.6700 -1.0461 284.8035 285.8497 289.8515 183.4890 -1.0454 284.7462 285.7916 289.9489 184.2770 -1.0193 284.7083 285.7276 290.2117 185.0660 -1.0306 284.7036 285.7342 290.4835 185.8843 -1.0364 284.7169 285.7533 290.6212 186.6730 -1.0443 284.7923 285.8365 290.8083 187.4928 -1.0631 284.8586 285.9217 290.8707 188.2810 -1.0756 284.9916 286.0671 290.6819 189.0790 -1.0889 284.9827 286.0716 290.4753 189.8940 -1.1118 285.0341 286.1459 290.4031 190.6840 -1.0829 285.1792 286.2621 290.5058 191.5045 -1.0676 285.1022 286.1698 290.6188 192.2658 -1.0742 285.2475 286.3217 290.7381 193.1175 -1.0993 285.2266 286.3259 290.8507 193.8790 -1.0767 285.4383 286.5150 290.9288 194.7003 -1.0703 285.4944 286.5647 291.0941 195.4925 -1.0786 285.5370 286.6156 291.3413 196.2835 -1.1206 285.6828 286.8034 291.3845 197.1360 -1.0957 285.5229 286.6187 291.5364 197.8980 -1.1401 285.6796 286.8197 291.8053 198.7198 -1.1310 285.9542 287.0852 291.9529 199.5118 -1.1872 285.9307 287.1179 291.9044 200.3035 -1.1706 285.9712 287.1418 292.0280 201.1258 -1.1538 285.9402 287.0940 292.1126 201.9175 -1.1749 286.1097 287.2846 292.0983 202.7398 -1.1880 286.2430 287.4309 292.1423 203.5318 -1.1702 286.3096 287.4798 292.2862 204.3235 -1.1931 286.4140 287.6071 292.4868 205.1458 -1.1866 286.4927 287.6793 292.5616 205.9375 -1.1728 286.4118 287.5847 292.7357 206.7598 -1.1443 286.5389 287.6832 292.8688 207.5518 -1.1295 286.7961 287.9255 292.9869 208.3435 -1.1402 286.8559 287.9961 293.1502 209.1655 -1.1431 286.9561 288.0992 293.3830 209.9430 -1.1044 286.9897 288.0941 293.3100 210.7733 -1.1163 287.0067 288.1230 293.4828 211.5655 -1.0955 287.2326 288.3282 293.5473 212.3875 -1.1176 287.2758 288.3934 293.6914 213.1795 -1.1116 287.2371 288.3487 293.8864 213.9715 -1.1198 287.3556 288.4754 294.0597 214.7935 -1.1371 287.5228 288.6600 294.1569 215.5855 -1.1282 287.5698 288.6980 294.1779 216.4075 -1.1431 287.6028 288.7459 294.3089 217.1995 -1.1339 287.7026 288.8365 294.4092 217.9925 -1.1394 287.9508 289.0902 294.5549 218.8143 -1.1711 288.0522 289.2233 294.6572 219.6060 -1.1761 288.2864 289.4625 294.7216 220.4285 -1.1700 288.2093 289.3793 294.6418 221.2210 -1.1366 288.2708 289.4074 294.7058 222.0135 -1.1766 288.2530 289.4296 294.8487 222.8358 -1.1771 288.3207 289.4978 294.8746 223.6275 -1.1723 288.3915 289.5638 294.8577 224.4498 -1.1942 288.5227 289.7168 295.1378 225.2418 -1.1920 288.5524 289.7444 295.1850 226.0335 -1.2045 288.7807 289.9852 295.4350 226.8558 -1.1846 288.8952 290.0798 295.4939 227.6475 -1.1655 289.0172 290.1827 295.6398 228.4705 -1.1272 289.1795 290.3066 295.8051 229.2628 -1.1301 289.1656 290.2957 295.9615 230.0555 -1.0899 289.2741 290.3640 296.0584 230.8775 -1.0954 289.3096 290.4050 296.1235 231.6695 -1.0890 289.3690 290.4580 296.2680 232.4925 -1.0891 289.6321 290.7211 296.3046 233.2845 -1.0928 289.7266 290.8194 296.3918 234.0765 -1.1197 289.6167 290.7364 296.5505 234.9290 -1.1348 289.7886 290.9234 296.7184 235.6915 -1.1469 289.9051 291.0520 296.7750 236.5143 -1.1651 289.9873 291.1524 296.8236 237.3065 -1.1693 290.1022 291.2714 296.9529 238.0985 -1.1880 290.2426 291.4306 296.9897 238.9203 -1.1978 290.3194 291.5173 297.0218 239.7118 -1.1881 290.3871 291.5752 297.0226 240.5325 -1.1697 290.4471 291.6168 297.1031 241.3200 -1.1907 290.5278 291.7185 297.0434 242.1083 -1.2135 290.7228 291.9363 297.0638 242.9270 -1.2111 290.8303 292.0414 297.1346 243.7150 -1.2130 290.8788 292.0918 297.3447 244.5333 -1.2307 290.9517 292.1823 297.4881 245.3215 -1.2237 291.0672 292.2910 297.4090 246.1105 -1.2247 291.0784 292.3031 297.4739 246.9283 -1.2245 291.1288 292.3533 297.6242 247.7163 -1.2452 291.2681 292.5133 297.6030 248.5353 -1.2458 291.3155 292.5613 297.7468 249.3235 -1.2662 291.4361 292.7023 297.8190 250.1110 -1.2658 291.5600 292.8258 298.0007 250.9598 -1.2679 291.7593 293.0272 298.1477 251.7180 -1.3106 291.6965 293.0071 298.1983 252.5378 -1.2603 291.7576 293.0179 298.4078 253.3285 -1.2616 291.9130 293.1746 298.4927 254.1185 -1.2586 292.0007 293.2593 298.8045 254.9688 -1.2781 292.0512 293.3293 299.0020 255.7278 -1.2380 292.2101 293.4482 299.1913 256.5485 -1.2219 292.3080 293.5299 299.3190 257.3398 -1.2692 292.3676 293.6368 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