DTA measure 21.gyors Date: 2024101:159 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.52 s Mass = 958.900 mg data_number = 1269 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2375 -0.5739 226.1628 226.7367 265.5682 2.0570 -0.5361 226.4313 226.9674 265.9712 2.8150 -0.5416 226.8296 227.3712 265.9507 3.6633 -0.5401 227.2032 227.7433 265.9190 4.4210 -0.5544 227.4340 227.9884 266.0812 5.2398 -0.5512 227.5786 228.1298 266.1774 6.0580 -0.5179 227.9263 228.4442 266.1461 6.8165 -0.5118 228.2160 228.7278 266.2271 7.6660 -0.4895 228.4310 228.9204 266.3129 8.4255 -0.4677 228.5913 229.0591 266.3210 9.2465 -0.4584 228.8680 229.3263 266.5803 10.0378 -0.4741 229.1656 229.6397 266.7924 10.8295 -0.4657 229.3150 229.7807 266.7866 11.6818 -0.4402 229.6733 230.1135 266.8575 12.4435 -0.4343 229.9988 230.4331 266.9927 13.2658 -0.4491 230.2632 230.7123 267.2496 14.0578 -0.4434 230.5534 230.9968 267.3761 14.8495 -0.4540 230.7800 231.2339 267.5163 15.6718 -0.4499 231.0105 231.4603 267.6874 16.4635 -0.4585 231.3229 231.7814 267.8177 17.2858 -0.4657 231.5719 232.0376 268.1018 18.0775 -0.4803 231.8743 232.3546 268.2708 18.8695 -0.4825 232.0421 232.5246 268.3224 19.6915 -0.5013 232.3241 232.8254 268.3070 20.4535 -0.5514 232.5716 233.1230 268.3283 21.3055 -0.4920 232.4653 232.9572 268.3434 22.0975 -0.5194 232.7137 233.2331 268.3370 22.8895 -0.5178 232.9791 233.4969 268.3135 23.7115 -0.5061 233.2066 233.7127 268.4291 24.4735 -0.4973 233.4593 233.9566 268.6667 25.3255 -0.4854 233.6570 234.1423 268.8019 26.1175 -0.4818 233.7992 234.2811 268.7433 26.9095 -0.4388 233.8595 234.2983 268.8931 27.7318 -0.4319 234.0421 234.4740 269.1323 28.4943 -0.4469 234.1289 234.5758 269.2579 29.3463 -0.4474 234.3433 234.7907 269.4452 30.1380 -0.4556 234.7470 235.2027 269.6374 30.9298 -0.4696 235.1042 235.5737 270.0208 31.7523 -0.4605 235.4715 235.9320 270.2758 32.5145 -0.4265 235.7060 236.1326 270.0886 33.3673 -0.4388 235.9709 236.4097 270.1669 34.1263 -0.4290 236.1882 236.6172 270.2602 34.9453 -0.4299 236.2234 236.6532 270.6485 35.7635 -0.3933 236.4175 236.8108 270.6781 36.5225 -0.4181 236.6254 237.0435 270.7292 37.3703 -0.4271 236.6195 237.0467 270.9136 38.1288 -0.4110 236.9442 237.3552 271.1153 38.9488 -0.4011 237.0288 237.4299 271.0463 39.7668 -0.3896 237.0617 237.4513 271.0139 40.5285 -0.3543 237.1156 237.4699 270.9454 41.3798 -0.3594 237.4377 237.7972 271.1089 42.1415 -0.3643 237.6456 238.0099 271.1994 42.9633 -0.3821 237.7732 238.1553 271.4973 43.7555 -0.3421 237.9393 238.2813 271.5054 44.5470 -0.3492 238.2501 238.5994 271.6224 45.3695 -0.3848 238.5555 238.9403 271.9130 46.1615 -0.3802 238.8542 239.2344 272.1885 46.9830 -0.4020 239.3123 239.7143 272.7409 47.7753 -0.3875 239.4064 239.7939 272.8012 48.5668 -0.3860 239.7111 240.0971 273.0344 49.3893 -0.3739 239.8850 240.2590 273.0247 50.1505 -0.3895 240.1520 240.5416 273.3129 51.0030 -0.4049 240.2466 240.6515 273.7389 51.7950 -0.3827 240.4407 240.8235 273.7558 52.5865 -0.4250 240.7461 241.1711 273.9536 53.4088 -0.4384 240.9201 241.3585 273.9822 54.1705 -0.4265 241.2782 241.7047 274.1164 55.0228 -0.4088 241.4653 241.8741 274.4689 55.8148 -0.4131 241.6181 242.0312 274.7750 56.6065 -0.4048 241.9914 242.3962 275.1781 57.4290 -0.4061 242.1120 242.5181 275.3272 58.1915 -0.4020 242.4663 242.8683 275.3628 59.0438 -0.4259 242.5968 243.0227 275.4816 59.8358 -0.4095 242.9807 243.3902 275.7125 60.6285 -0.4287 243.0994 243.5282 275.8147 61.4505 -0.4158 243.3073 243.7231 275.8384 62.2125 -0.3999 243.4979 243.8978 275.3436 63.0645 -0.3997 243.5928 243.9925 275.2328 63.8565 -0.4116 243.9210 244.3325 275.7764 64.6485 -0.4246 244.0387 244.4633 275.8439 65.4705 -0.4360 244.0559 244.4920 275.9269 66.2348 -0.4115 244.1310 244.5425 275.8820 67.0860 -0.4215 244.3108 244.7323 275.9292 67.8435 -0.4535 244.5150 244.9685 275.7943 68.6628 -0.4748 244.6516 245.1265 275.9852 69.4810 -0.4477 244.7628 245.2105 275.9417 70.2390 -0.4438 244.9377 245.3815 275.9694 71.0883 -0.4829 245.0705 245.5534 276.0874 71.8770 -0.4726 245.1644 245.6370 275.9547 72.6670 -0.4709 245.3343 245.8052 276.0588 73.4875 -0.4990 245.5719 246.0709 276.3319 74.2495 -0.4697 245.7597 246.2294 276.2753 75.1013 -0.4989 245.8539 246.3528 276.5015 75.8928 -0.4666 245.9821 246.4487 276.4682 76.6845 -0.4735 246.3795 246.8529 276.6935 77.5065 -0.4874 246.5965 247.0839 276.8483 78.2685 -0.4481 246.7280 247.1761 277.0149 79.1205 -0.4724 247.1784 247.6508 277.2342 79.8825 -0.4797 247.3667 247.8464 277.3343 80.7045 -0.4849 247.6633 248.1482 277.8608 81.5265 -0.4793 247.8849 248.3643 278.1153 82.2885 -0.4979 248.1610 248.6589 278.3113 83.1405 -0.5199 248.4977 249.0176 278.5386 83.9325 -0.5203 248.6995 249.2198 278.6029 84.7245 -0.5145 248.8271 249.3416 278.8358 85.5465 -0.5139 248.9547 249.4686 278.8578 86.3085 -0.5257 249.1278 249.6536 278.9340 87.1638 -0.5348 249.4494 249.9843 279.5162 87.9550 -0.5755 249.6014 250.1768 279.8087 88.7470 -0.5702 249.9291 250.4993 280.0322 89.5690 -0.5527 249.9837 250.5364 280.2725 90.3305 -0.5490 250.1241 250.6730 280.6636 91.1830 -0.5609 250.4368 250.9977 280.7835 91.9748 -0.5622 250.8700 251.4322 281.1690 92.7665 -0.5413 251.1561 251.6975 281.1776 93.5890 -0.5564 251.1133 251.6697 281.1047 94.3815 -0.5477 251.2666 251.8143 281.1842 95.2045 -0.5596 251.3025 251.8621 281.2801 95.9968 -0.5861 251.5475 252.1337 281.2792 96.7895 -0.6003 251.9030 252.5033 281.4516 97.6120 -0.5780 252.0701 252.6482 281.6497 98.4043 -0.5987 252.3211 252.9198 281.6649 99.2230 -0.5841 252.4607 253.0448 281.7361 100.0115 -0.5735 252.5883 253.1618 281.9299 100.8000 -0.5742 252.7785 253.3527 282.0232 101.6185 -0.6351 252.9164 253.5515 281.9959 102.4070 -0.5952 252.9957 253.5909 282.1339 103.2250 -0.5998 253.1754 253.7753 282.2349 104.0130 -0.6153 253.2680 253.8833 282.3730 104.8020 -0.6160 253.5206 254.1366 282.3048 105.6210 -0.5925 253.7532 254.3457 282.5279 106.4118 -0.5812 253.9847 254.5658 282.7410 107.2328 -0.5846 254.1659 254.7505 282.8052 108.0235 -0.6108 254.1643 254.7750 282.8389 108.8145 -0.6358 254.4278 255.0636 282.9640 109.6368 -0.6492 254.6909 255.3401 283.0573 110.3985 -0.6460 254.8884 255.5344 283.3301 111.2508 -0.6245 255.0461 255.6706 283.3973 112.0428 -0.6610 255.1947 255.8557 283.5487 112.8345 -0.6408 255.4902 256.1310 283.5772 113.6568 -0.6536 255.7531 256.4067 283.7809 114.4185 -0.6657 255.9534 256.6191 283.9779 115.2708 -0.6157 256.2081 256.8237 284.0009 116.0628 -0.7117 256.3089 257.0206 284.2004 116.8545 -0.7454 256.4035 257.1489 284.1401 117.6765 -0.7525 256.6540 257.4066 284.2050 118.4385 -0.7906 256.7983 257.5889 284.3485 119.2905 -0.7934 256.9917 257.7851 284.3654 120.0525 -0.8091 257.0944 257.9035 284.2196 120.8745 -0.7567 257.3219 258.0786 284.1373 121.6965 -0.7650 257.3732 258.1382 284.3102 122.4585 -0.7954 257.4645 258.2599 284.3565 123.3105 -0.7899 257.5381 258.3280 284.3910 124.0725 -0.7984 257.5943 258.3927 284.2985 124.8945 -0.7793 257.5366 258.3159 284.5485 125.7168 -0.7683 257.7054 258.4737 284.7012 126.4793 -0.8036 258.0313 258.8349 284.8347 127.3310 -0.7956 258.2970 259.0926 285.1127 128.0933 -0.8007 258.4869 259.2876 285.4347 128.9148 -0.7967 258.6484 259.4450 285.7808 129.7370 -0.8211 259.0705 259.8916 286.1915 130.4993 -0.7999 259.2730 260.0729 286.6216 131.3490 -0.8362 259.3411 260.1773 286.3029 132.1063 -0.8448 259.4846 260.3294 286.7476 132.9245 -0.8115 259.6467 260.4582 286.9940 133.7125 -0.8320 259.9890 260.8210 287.1458 134.5015 -0.8335 260.1317 260.9652 287.2379 135.3505 -0.8352 260.3742 261.2095 287.4562 136.1090 -0.8376 260.5893 261.4269 287.6210 136.9288 -0.8081 260.7000 261.5082 288.0349 137.7483 -0.7894 260.9806 261.7700 288.3186 138.5095 -0.7697 261.2414 262.0111 288.4735 139.3608 -0.8040 261.4932 262.2972 288.7669 140.1220 -0.8053 261.7054 262.5107 288.8648 140.9433 -0.7998 261.8787 262.6785 288.9864 141.7355 -0.8270 262.0931 262.9201 289.3674 142.5273 -0.7975 262.1559 262.9534 289.5762 143.3495 -0.8052 262.3789 263.1841 289.7727 144.1408 -0.8096 262.5248 263.3344 289.7611 144.9633 -0.8261 262.6986 263.5247 289.9505 145.7548 -0.8191 262.7301 263.5492 289.8499 146.5468 -0.8112 262.9850 263.7961 289.8384 147.3688 -0.8307 263.1778 264.0085 289.8267 148.1305 -0.8745 263.1545 264.0290 289.7450 148.9880 -0.8387 263.3682 264.2069 290.0817 149.7495 -0.8645 263.5266 264.3911 290.0466 150.5718 -0.8332 263.6995 264.5327 290.0768 151.3938 -0.8334 263.7296 264.5630 290.1279 152.1555 -0.8551 263.8741 264.7293 290.3475 153.0078 -0.8648 264.2437 265.1084 290.5389 153.7695 -0.8985 264.3444 265.2429 290.7739 154.5918 -0.8791 264.6788 265.5579 290.8916 155.4138 -0.8961 264.9341 265.8303 291.0036 156.1755 -0.8669 265.3584 266.2253 291.1907 157.0283 -0.8717 265.5289 266.4006 291.1898 157.7905 -0.8447 265.7495 266.5942 291.3189 158.6125 -0.8313 265.8205 266.6517 291.3719 159.4350 -0.8305 265.9426 266.7731 291.4210 160.1975 -0.8253 266.0826 266.9079 291.5188 161.0503 -0.8547 266.4089 267.2635 291.6248 161.8125 -0.8506 266.6150 267.4657 291.7190 162.6338 -0.8465 266.7337 267.5802 291.7001 163.4515 -0.8327 266.8752 267.7079 291.8464 164.2090 -0.8616 267.0686 267.9303 291.9146 165.0570 -0.8658 267.2359 268.1016 292.0344 165.8450 -0.8213 267.3024 268.1236 292.1516 166.6338 -0.8785 267.6181 268.4967 292.3823 167.4528 -0.8929 267.6114 268.5043 292.3318 168.2120 -0.8456 267.7795 268.6251 292.4436 169.0613 -0.8787 267.9518 268.8305 292.4621 169.8505 -0.8449 267.8823 268.7271 292.7387 170.6410 -0.8456 268.1879 269.0336 292.8771 171.4618 -0.8326 268.4482 269.2809 292.9864 172.2235 -0.8607 268.7563 269.6171 293.0831 173.0755 -0.8798 268.7615 269.6413 293.1364 173.8678 -0.8865 268.7530 269.6395 293.3617 174.6595 -0.9219 269.2391 270.1610 293.6150 175.4815 -0.9046 269.4315 270.3362 293.5322 176.2435 -0.8995 269.6187 270.5183 293.6976 177.0955 -0.9106 269.6056 270.5162 293.8175 177.8875 -0.8968 269.5983 270.4952 293.9717 178.6795 -0.8992 270.0443 270.9436 294.0436 179.5015 -0.9117 270.1170 271.0287 294.1427 180.2635 -0.9361 270.1372 271.0733 294.3165 181.1155 -0.9271 270.4691 271.3962 294.5345 181.9075 -0.9329 270.7662 271.6991 294.7235 182.6995 -0.9342 270.7564 271.6907 294.8606 183.5218 -0.9082 271.0204 271.9286 295.0361 184.2845 -0.9089 271.0663 271.9752 295.2923 185.1375 -0.9395 271.3819 272.3214 295.6479 185.9300 -0.9499 271.5995 272.5494 295.7111 186.7218 -0.9490 271.5518 272.5007 295.6885 187.5440 -0.9387 271.7245 272.6632 295.9056 188.3055 -0.9310 271.8250 272.7560 296.2910 189.1578 -0.9658 272.1306 273.0964 296.4249 189.9498 -0.9894 272.3277 273.3171 296.6457 190.7415 -1.0281 272.5356 273.5637 296.6874 191.5638 -1.0351 272.3894 273.4246 296.7916 192.3255 -1.0425 272.6213 273.6637 296.9627 193.1778 -1.0502 272.8088 273.8590 297.0746 193.9698 -0.9972 273.2531 274.2502 297.1246 194.7625 -1.0169 273.3827 274.3996 297.2506 195.6145 -1.0501 273.3504 274.4005 297.2534 196.4030 -1.0708 273.6555 274.7263 297.4079 197.1910 -1.0546 273.9336 274.9882 297.4640 198.0098 -1.0520 273.8623 274.9143 297.5370 198.7680 -1.0457 273.9342 274.9800 297.6317 199.6168 -1.0572 274.3184 275.3756 297.8109 200.4050 -1.0739 274.4677 275.5415 297.8884 201.1940 -1.0597 274.5527 275.6124 298.1421 202.0428 -1.0816 274.6007 275.6823 298.2036 202.8013 -1.1296 274.7145 275.8441 298.2965 203.6218 -1.1177 274.9556 276.0733 298.2924 204.4135 -1.1128 275.2647 276.3775 298.4509 205.2033 -1.0831 275.4199 276.5030 298.6293 206.0250 -1.1315 275.7432 276.8747 298.7572 206.8165 -1.1031 275.7927 276.8958 298.8889 207.6388 -1.0740 275.7870 276.8610 298.9671 208.4308 -1.0788 276.0696 277.1484 299.2062 209.2225 -1.0890 276.0731 277.1621 299.4434 210.0448 -1.0866 276.2969 277.3835 299.6005 210.8365 -1.0730 276.5403 277.6133 299.7542 211.6588 -1.0954 276.6161 277.7116 299.8595 212.4508 -1.0904 276.7827 277.8732 299.9314 213.2425 -1.1438 277.0908 278.2346 300.0195 214.0648 -1.1137 277.2150 278.3288 300.3673 214.8265 -1.1390 277.3426 278.4816 300.5359 215.6785 -1.1662 277.3796 278.5458 300.5550 216.4705 -1.1992 277.6146 278.8138 300.7045 217.2625 -1.1892 277.8812 279.0704 300.8886 218.0845 -1.1731 277.9479 279.1210 301.0736 218.8765 -1.2028 278.1492 279.3519 301.2665 219.6985 -1.2056 278.2869 279.4925 301.2624 220.4905 -1.2037 278.5901 279.7938 301.4965 221.2835 -1.2107 278.6350 279.8458 301.5326 222.1055 -1.2011 278.7522 279.9533 301.6825 222.8975 -1.2131 278.7885 280.0016 301.9456 223.7203 -1.1760 278.9011 280.0771 302.1129 224.5125 -1.2068 279.2273 280.4341 302.4666 225.3055 -1.2040 279.4215 280.6255 302.3978 226.1273 -1.2122 279.5222 280.7344 302.4004 226.9188 -1.1998 279.7305 280.9302 302.5655 227.7395 -1.2193 279.8537 281.0730 302.5460 228.5280 -1.1946 279.9468 281.1415 302.6541 229.3163 -1.1729 280.0139 281.1868 302.8614 230.1348 -1.2030 280.4184 281.6214 302.9733 230.9223 -1.2230 280.6210 281.8440 303.0800 231.7418 -1.2037 280.6592 281.8629 303.2573 232.5300 -1.2577 280.7799 282.0377 303.3584 233.3188 -1.2495 280.9982 282.2477 303.4820 234.1675 -1.2679 281.2343 282.5022 303.5853 234.9265 -1.2560 281.4633 282.7193 303.6178 235.7473 -1.2503 281.5544 282.8047 303.7629 236.5685 -1.2272 281.6329 282.8602 303.8691 237.3305 -1.2641 281.7412 283.0053 304.2059 238.1825 -1.2307 281.9618 283.1925 304.4415 238.9445 -1.2445 282.2162 283.4607 304.7084 239.7665 -1.2604 282.3461 283.6065 304.7744 240.5595 -1.2679 282.5707 283.8386 305.0158 241.3520 -1.2570 282.6052 283.8622 305.0465 242.2045 -1.2482 282.8291 284.0773 305.1906 242.9658 -1.2446 283.1326 284.3772 305.3427 243.7878 -1.2496 283.2763 284.5258 305.2760 244.5800 -1.2242 283.4981 284.7223 305.3501 245.3715 -1.2324 283.5763 284.8087 305.3514 246.2238 -1.2635 283.4452 284.7087 305.4823 246.9855 -1.2491 283.8336 285.0827 305.4134 247.8078 -1.2498 283.9136 285.1634 305.4576 248.6000 -1.2301 284.1175 285.3476 305.5266 249.3915 -1.2389 284.3163 285.5552 305.9674 250.2443 -1.2814 284.4973 285.7787 305.5697 251.0065 -1.3306 284.6092 285.9398 305.3734 251.8288 -1.3194 284.6094 285.9288 305.3639 252.6208 -1.3270 284.8444 286.1714 305.6260 253.4135 -1.3021 284.8678 286.1699 305.7192 254.2663 -1.2397 284.9260 286.1656 306.0557 255.0285 -1.2222 285.0228 286.2450 306.4908 255.8505 -1.2139 285.1431 286.3570 306.7273 256.6425 -1.2108 285.3057 286.5165 306.7984 257.4345 -1.2248 285.3206 286.5454 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378.5816 381.9768 390.8312 765.8155 -3.3856 378.6124 381.9980 390.8439 766.5775 -3.4036 378.7141 382.1177 390.9487 767.4300 -3.3902 378.9195 382.3097 390.9851 768.1925 -3.3879 379.0449 382.4328 391.2985 769.0145 -3.3991 379.0723 382.4714 391.6088 769.8365 -3.3946 379.2612 382.6558 391.5426 770.5985 -3.4180 379.3381 382.7561 391.6675 771.4505 -3.4355 379.5093 382.9448 391.8876 772.2425 -3.4235 379.8374 383.2609 391.9669 773.0340 -3.3934 379.8695 383.2629 392.0484 773.8563 -3.4218 379.9572 383.3790 392.2510 774.6175 -3.4322 380.2042 383.6364 392.3068 775.4698 -3.4068 380.3999 383.8067 392.4570 776.2583 -3.4161 380.5058 383.9219 392.5200 777.0475 -3.4275 380.7586 384.1861 392.5453 777.8660 -3.4510 380.9313 384.3824 392.8112 778.6245 -3.4412 380.9988 384.4400 392.8280 779.4735 -3.4270 380.8951 384.3220 393.0974 780.2315 -3.4365 381.1402 384.5766 393.2018 781.0505 -3.4306 381.4669 384.8975 393.3432 781.8703 -3.4450 381.5663 385.0114 393.5805 782.6300 -3.4570 381.7216 385.1786 393.7586 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