DTA measure 31.gyors Date: 2024101:1538 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.87 s Mass = 958.900 mg data_number = 1026 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3035 -4.8011 434.7005 439.5016 424.8917 3.9025 -4.8005 434.8130 439.6135 424.7880 5.5165 -4.8105 434.8560 439.6665 424.8475 7.1455 -4.8227 435.0010 439.8238 424.7287 8.7445 -4.8333 435.0681 439.9014 424.6945 10.3458 -4.8378 435.0514 439.8892 424.5344 11.9625 -4.8422 435.2018 440.0440 424.5117 13.5616 -4.8686 435.2563 440.1249 424.3351 15.1910 -4.8710 435.3483 440.2193 424.2333 16.7908 -4.8751 435.4825 440.3577 424.0803 18.3906 -4.8793 435.5333 440.4126 423.9337 20.0020 -4.8870 435.5733 440.4604 423.8416 21.5931 -4.8878 435.6578 440.5456 423.5650 23.1993 -4.8962 435.8516 440.7478 423.3097 24.8055 -4.8973 435.8258 440.7231 422.9906 26.3983 -4.9040 435.9820 440.8861 422.8599 28.0089 -4.9196 436.0526 440.9722 422.6521 29.6078 -4.9156 436.0668 440.9824 422.5829 31.2218 -4.9202 436.0304 440.9506 422.1670 32.8358 -4.9234 436.2058 441.1292 422.0188 34.4346 -4.9288 436.2192 441.1480 421.7933 36.0336 -4.9221 436.2070 441.1292 421.5985 37.6476 -4.9269 436.1888 441.1156 421.3139 39.2616 -4.9459 436.3664 441.3123 421.1093 40.8758 -4.9452 436.2158 441.1610 421.0073 42.4746 -4.9651 436.2308 441.1959 420.8374 44.0735 -4.9299 436.3804 441.3103 420.6018 45.6881 -4.9378 436.3277 441.2656 420.4732 47.3033 -4.9358 436.4167 441.3525 420.2499 48.9176 -4.9497 436.5553 441.5050 419.9979 50.5174 -4.9658 436.5466 441.5124 419.6758 52.1135 -4.9623 436.2480 441.2104 419.5278 53.7199 -4.9694 436.4932 441.4626 419.3054 55.3410 -4.9900 436.5593 441.5494 419.1258 56.9331 -4.9808 436.5413 441.5221 418.8831 58.5268 -4.9761 436.7042 441.6804 418.7379 60.1395 -4.9693 436.6097 441.5791 418.6915 61.7385 -4.9823 436.5094 441.4917 418.4505 63.3525 -4.9758 436.4079 441.3837 418.3378 64.9515 -4.9812 436.3290 441.3102 418.1529 66.5655 -4.9761 436.4214 441.3975 417.9789 68.1644 -4.9939 436.5369 441.5308 417.5413 69.7634 -4.9883 436.4231 441.4114 417.4657 71.3921 -4.9816 436.4880 441.4696 417.4402 72.9909 -5.0026 436.3843 441.3869 417.0620 74.5898 -4.9990 436.3034 441.3024 416.8410 76.2036 -5.0064 436.3436 441.3500 416.6466 77.8026 -5.0160 436.4732 441.4891 416.5079 79.4166 -5.0091 436.2596 441.2687 416.1490 81.0320 -4.9989 436.3438 441.3427 416.1033 82.6335 -5.0117 436.3245 441.3362 415.9717 84.2435 -5.0127 436.3878 441.4005 415.8754 85.8340 -5.0293 436.3480 441.3773 415.4448 87.4400 -5.0208 436.3195 441.3402 415.2975 89.0470 -5.0233 435.9975 441.0208 415.0987 90.6693 -5.0313 436.0262 441.0576 414.8208 92.4925 -5.0485 435.9541 441.0026 414.6110 94.0899 -5.0278 436.0061 441.0339 414.3899 95.7049 -5.0308 435.9613 440.9921 414.1748 97.3211 -5.0297 435.7626 440.7923 414.1606 98.9226 -5.0286 435.8122 440.8409 414.0006 100.5216 -5.0353 435.6736 440.7089 413.7397 102.1213 -5.0348 435.6976 440.7323 413.5150 103.7355 -5.0401 435.7312 440.7713 413.4578 105.3509 -5.0439 435.6828 440.7268 413.1683 106.9660 -5.0417 435.5830 440.6248 413.0053 108.5655 -5.0464 435.4337 440.4801 412.7965 110.1654 -5.0621 435.2738 440.3358 412.5380 111.7794 -5.0615 435.3404 440.4019 412.3734 113.3961 -5.0594 435.1415 440.2009 412.1534 114.9969 -5.0661 435.1012 440.1673 411.9635 116.6094 -5.0604 435.1466 440.2069 411.7500 118.2060 -5.0747 434.9562 440.0308 411.5440 119.7970 -5.0691 434.8744 439.9435 411.2849 121.4189 -5.0731 434.8689 439.9419 411.0636 123.0119 -5.0750 434.7365 439.8115 410.9203 124.6204 -5.0601 434.7154 439.7755 410.7092 126.2143 -5.0838 434.7162 439.8000 410.5495 127.8119 -5.0784 434.6574 439.7358 410.3304 129.4269 -5.0748 434.4098 439.4846 410.1653 131.0408 -5.0874 434.3357 439.4231 410.0001 132.6396 -5.0833 434.2422 439.3254 409.8751 134.2544 -5.0690 434.2303 439.2993 409.6247 135.8538 -5.0712 434.0657 439.1369 409.5298 137.4676 -5.0888 434.0275 439.1162 409.1036 139.0818 -5.0915 433.8675 438.9590 408.9191 140.6818 -5.0811 433.6854 438.7665 408.8010 142.2815 -5.0755 433.6996 438.7752 408.6880 143.8935 -5.0687 433.5506 438.6192 408.4427 145.4935 -5.0739 433.5233 438.5972 408.3222 147.1233 -5.0813 433.5182 438.5995 407.9863 148.7361 -5.0814 433.3963 438.4777 407.7887 150.3279 -5.0902 433.1775 438.2678 407.4913 151.9190 -5.0969 433.1220 438.2189 407.2062 153.5264 -5.0964 432.9958 438.0923 406.9712 155.1360 -5.0963 432.9038 438.0001 406.8134 156.7480 -5.0838 432.8336 437.9174 406.5772 158.3465 -5.0800 432.6650 437.7449 406.4726 159.9455 -5.0844 432.5357 437.6202 406.4226 161.5595 -5.0823 432.4047 437.4871 406.1977 163.1735 -5.0697 432.2207 437.2904 405.9412 164.7725 -5.0858 432.0805 437.1664 405.7150 166.3865 -5.0843 432.0628 437.1471 405.5238 167.9850 -5.0685 431.9041 436.9726 405.3941 169.5839 -5.0782 431.8456 436.9238 405.1298 171.2129 -5.0773 431.6356 436.7130 404.9121 172.8118 -5.0721 431.4309 436.5030 404.7701 174.4259 -5.0620 431.2657 436.3277 404.4050 176.0256 -5.0733 431.2903 436.3636 404.1849 177.6403 -5.0617 431.1636 436.2253 404.1724 179.2554 -5.0712 431.0133 436.0846 403.8213 180.8686 -5.0756 430.9351 436.0107 403.6245 182.4604 -5.0712 430.6961 435.7673 403.4693 184.0520 -5.0725 430.5677 435.6402 403.2674 185.6599 -5.0800 430.3458 435.4258 403.1338 187.2681 -5.0708 430.3235 435.3943 402.9405 188.8795 -5.0558 430.2541 435.3098 402.6644 190.4776 -5.0737 430.0385 435.1122 402.4811 192.0766 -5.0726 429.9038 434.9764 402.3283 193.6769 -5.0618 429.7355 434.7973 401.9296 195.3008 -5.0658 429.7571 434.8229 401.9778 196.9148 -5.0577 429.4685 434.5262 401.5749 198.5136 -5.0617 429.2967 434.3585 401.4935 200.1275 -5.0619 429.3175 434.3794 401.3468 201.7265 -5.0465 428.9660 434.0125 401.1338 203.3405 -5.0546 428.9068 433.9614 400.9380 204.9554 -5.0552 428.8518 433.9070 400.6356 206.5555 -5.0379 428.6370 433.6749 400.5072 208.1695 -5.0594 428.5190 433.5784 400.2866 209.7694 -5.0644 428.4855 433.5499 399.8498 211.3844 -5.0478 428.1750 433.2228 399.9060 212.9973 -5.0400 427.8822 432.9222 399.6162 214.5895 -5.0437 427.8199 432.8636 399.4496 216.1963 -5.0429 427.8683 432.9112 399.2182 217.7883 -5.0356 427.6121 432.6477 399.0533 219.3819 -5.0475 427.3904 432.4379 398.7721 221.0093 -5.0287 427.2393 432.2680 398.7324 222.6066 -5.0368 426.9807 432.0175 398.4650 224.2050 -5.0355 426.8898 431.9253 398.2968 225.8039 -5.0335 426.7492 431.7827 398.0693 227.4178 -5.0255 426.6263 431.6517 397.8479 229.0318 -5.0331 426.4322 431.4653 397.4833 230.6319 -5.0386 426.3434 431.3820 397.2195 232.2346 -5.0198 426.2716 431.2914 397.0637 233.8486 -5.0121 425.9197 430.9318 396.8230 235.4476 -5.0148 425.8794 430.8942 396.7522 237.0623 -5.0070 425.6443 430.6514 396.6951 238.6775 -5.0170 425.3679 430.3849 396.4851 240.2765 -5.0028 425.1806 430.1834 396.1071 241.8909 -4.9881 425.2113 430.1995 395.9662 243.4905 -4.9996 425.0167 430.0163 395.7616 245.1104 -4.9914 424.6705 429.6619 395.6059 246.7208 -4.9941 424.6739 429.6680 395.3161 248.3119 -4.9954 424.6492 429.6446 395.2263 249.9196 -4.9778 424.2822 429.2600 394.9920 251.5130 -4.9933 424.1295 429.1228 394.6550 253.1116 -4.9711 423.8912 428.8622 394.4979 254.7255 -4.9721 423.7902 428.7623 394.4817 256.3395 -4.9709 423.6673 428.6382 394.1977 257.9535 -4.9796 423.6054 428.5850 393.9422 259.5525 -4.9710 423.2994 428.2705 393.7527 261.1521 -4.9778 423.2156 428.1934 393.5832 262.7665 -4.9657 422.9904 427.9560 393.3279 264.3805 -4.9734 422.9032 427.8766 393.1081 265.9793 -4.9500 422.6432 427.5932 393.0291 267.5931 -4.9519 422.4774 427.4293 392.7943 269.1926 -4.9538 422.2551 427.2089 392.5353 270.8066 -4.9417 422.1348 427.0764 392.3113 272.4208 -4.9541 422.0806 427.0348 391.9784 274.0198 -4.9424 421.8652 426.8076 391.7721 275.6196 -4.9516 421.6171 426.5686 391.7171 277.2333 -4.9444 421.4519 426.3963 391.7079 278.8260 -4.9362 421.4473 426.3835 391.1377 280.4471 -4.9444 421.1408 426.0852 391.0433 282.0383 -4.9392 420.9656 425.9048 390.8351 283.6454 -4.9267 420.7454 425.6720 390.7921 285.2398 -4.9204 420.6014 425.5218 390.5811 286.8529 -4.9192 420.4183 425.3375 390.1326 288.4666 -4.9259 420.3530 425.2790 390.0574 290.0656 -4.9202 420.0884 425.0085 389.8413 291.6646 -4.9234 419.8662 424.7895 389.5909 293.2786 -4.9231 419.6448 424.5678 389.3822 294.8775 -4.9146 419.5360 424.4506 389.3511 296.5065 -4.9040 419.3663 424.2703 389.0260 298.1055 -4.9042 419.3228 424.2270 388.7200 299.7045 -4.8874 418.8475 423.7349 388.6398 301.3185 -4.8910 418.6065 423.4975 388.3326 302.9325 -4.8801 418.4465 423.3267 388.1960 304.5474 -4.8784 418.3259 423.2043 387.9204 306.1616 -4.8812 418.2051 423.0863 387.6459 307.7611 -4.8722 418.1512 423.0233 387.6549 309.3599 -4.8698 417.9158 422.7856 387.3678 310.9798 -4.8797 417.7926 422.6722 387.2516 312.5710 -4.8662 417.5627 422.4289 386.9336 314.1621 -4.8635 417.3374 422.2009 386.8389 315.7684 -4.8624 417.1905 422.0529 386.5878 317.3619 -4.8701 416.9800 421.8501 386.3306 318.9715 -4.8558 416.8382 421.6940 386.1925 320.5834 -4.8469 416.5472 421.3941 385.9152 322.1820 -4.8408 416.2080 421.0488 385.5963 323.7808 -4.8339 416.3168 421.1506 385.5026 325.3948 -4.8417 416.0933 420.9350 385.2084 326.9936 -4.8309 415.8470 420.6780 385.0946 328.6076 -4.8364 415.6944 420.5308 384.8446 330.2218 -4.8251 415.5289 420.3540 384.7268 331.8206 -4.8279 415.3963 420.2241 384.4107 333.4200 -4.8156 415.2407 420.0563 384.1195 335.0353 -4.8204 414.8913 419.7117 384.2536 336.6496 -4.8059 414.7848 419.5906 383.9039 338.2636 -4.8098 414.6319 419.4417 383.5805 339.8638 -4.7930 414.4616 419.2546 383.5675 341.4631 -4.8097 414.1862 418.9960 383.1867 343.0766 -4.8016 413.9102 418.7118 382.9632 344.6895 -4.7967 413.8893 418.6860 382.7903 346.3028 -4.7863 413.6769 418.4633 382.5697 347.9016 -4.7828 413.4818 418.2646 382.5568 349.5005 -4.7791 413.2136 417.9927 382.2152 351.0995 -4.7709 413.0318 417.8028 381.8886 352.7286 -4.7793 412.8845 417.6639 381.6969 354.3275 -4.7687 412.6847 417.4533 381.7334 355.9415 -4.7528 412.4954 417.2483 381.4612 357.5405 -4.7532 412.3069 417.0601 381.2476 359.1395 -4.7461 411.9960 416.7420 381.2092 360.7534 -4.7487 411.9426 416.6913 381.0100 362.3673 -4.7508 411.6660 416.4168 380.6083 363.9664 -4.7304 411.4266 416.1570 380.3538 365.5811 -4.7417 411.3645 416.1062 380.0909 367.1806 -4.7328 411.1871 415.9199 380.0579 368.7796 -4.7322 410.9424 415.6747 379.8660 370.4088 -4.7167 410.8479 415.5646 379.7195 372.0076 -4.7089 410.6267 415.3356 379.4080 373.6216 -4.7158 410.3468 415.0626 379.1436 375.2356 -4.7257 410.2491 414.9748 378.8781 376.8504 -4.7177 410.0151 414.7328 378.7037 378.4645 -4.7106 409.7709 414.4815 378.4943 380.0638 -4.7124 409.5617 414.2741 378.3440 381.6638 -4.6970 409.3172 414.0142 378.2476 383.2785 -4.6810 409.2183 413.8993 378.0536 384.8926 -4.6827 408.9622 413.6449 377.8640 386.5070 -4.6847 408.6289 413.3136 377.5013 388.1069 -4.6863 408.6174 413.3037 377.3433 389.7068 -4.6877 408.4084 413.0961 377.1148 391.3206 -4.6728 408.1872 412.8600 376.9081 392.9354 -4.6762 408.1076 412.7838 376.7465 394.5498 -4.6723 407.9103 412.5826 376.5420 396.1485 -4.6631 407.6809 412.3440 376.3650 397.7475 -4.6481 407.4606 412.1087 376.1591 399.3621 -4.6393 407.1420 411.7812 375.8567 400.9915 -4.6392 406.9799 411.6191 375.6495 402.5914 -4.6486 406.7473 411.3959 375.3200 404.1909 -4.6456 406.6848 411.3304 375.2784 405.8053 -4.6371 406.3931 411.0303 374.9996 407.4013 -4.6220 406.3199 410.9419 374.8431 409.0075 -4.6216 406.1504 410.7720 374.6819 410.6173 -4.6065 405.8346 410.4411 374.5829 412.2086 -4.6188 405.5897 410.2085 374.2558 413.8011 -4.6098 405.4437 410.0534 374.2597 415.3950 -4.6098 405.1013 409.7111 373.8057 417.0193 -4.6070 404.9534 409.5603 373.7478 418.6140 -4.5953 404.8832 409.4785 373.5537 420.2224 -4.5984 404.6820 409.2803 373.4001 421.8178 -4.5962 404.5121 409.1083 373.1826 423.4145 -4.5846 404.3489 408.9335 372.8861 425.0283 -4.5776 404.0822 408.6598 372.7687 426.6401 -4.5687 403.9972 408.5658 372.6277 428.2386 -4.5566 403.6291 408.1857 372.2800 429.8375 -4.5393 403.4165 407.9558 372.1102 431.4516 -4.5299 403.3736 407.9035 371.8580 433.0505 -4.5099 403.0814 407.5913 371.7319 434.6645 -4.4998 402.8241 407.3239 371.4427 436.2785 -4.4894 402.6978 407.1872 371.3517 437.8775 -4.4857 402.4525 406.9382 371.0792 439.4765 -4.4922 402.2357 406.7278 370.7969 441.0900 -4.5019 401.9076 406.4095 370.5392 442.7040 -4.4769 401.7882 406.2651 370.1859 444.3028 -4.4611 401.6836 406.1447 370.0080 445.9168 -4.4708 401.4820 405.9528 369.6724 447.5170 -4.5030 401.3528 405.8558 369.5273 449.1166 -4.5316 401.1121 405.6437 369.3547 450.7456 -4.5121 400.8254 405.3374 369.0064 452.3446 -4.4726 400.5496 405.0222 368.9488 453.9585 -4.4406 400.3215 404.7621 368.7333 455.5579 -4.4256 400.1715 404.5971 368.3699 457.1575 -4.4282 400.0738 404.5020 368.1867 458.7865 -4.4211 399.8915 404.3126 367.7942 460.3863 -4.4111 399.6460 404.0571 367.6098 461.9855 -4.4188 399.4666 403.8854 367.2144 463.6001 -4.4421 399.3849 403.8269 367.0071 465.2003 -4.4162 399.2058 403.6220 366.8594 466.8146 -4.4205 398.8860 403.3065 366.7560 468.4296 -4.5056 398.6933 403.1990 366.6341 470.0296 -4.4871 398.4108 402.8979 366.5163 471.6396 -4.4534 398.2497 402.7031 366.1988 473.2310 -4.4346 398.0217 402.4563 366.0378 474.8238 -4.4351 397.8917 402.3268 365.8536 476.4451 -4.4174 397.6280 402.0454 365.6732 478.0370 -4.4419 397.2984 401.7403 365.5549 479.6439 -4.4447 397.2401 401.6848 365.4303 481.2376 -4.3925 397.1146 401.5071 365.4560 482.8455 -4.3896 396.7478 401.1375 365.2156 484.4555 -4.3997 396.5383 400.9380 365.0513 486.0508 -4.4205 396.3998 400.8202 364.6888 487.6636 -4.4206 396.2138 400.6344 364.5618 489.2599 -4.4401 395.9744 400.4146 364.2554 490.8585 -4.4402 395.8563 400.2966 363.8364 492.4875 -4.4292 395.4382 399.8674 363.4726 494.0865 -4.4239 395.3927 399.8165 363.2784 495.6854 -4.4200 395.2019 399.6219 363.0355 497.2845 -4.4449 394.9150 399.3599 362.8310 498.8984 -4.4474 394.8031 399.2505 362.7134 500.5126 -4.4204 394.6242 399.0446 362.3458 502.1269 -4.4276 394.3720 398.7996 362.1799 503.7266 -4.4087 394.0946 398.5033 361.9526 505.3256 -4.4124 393.8858 398.2981 361.7448 506.9246 -4.4193 393.6058 398.0250 361.5112 508.5536 -4.4292 393.3904 397.8197 361.3336 510.1678 -4.4282 393.3002 397.7284 361.2722 511.7686 -4.4120 393.1633 397.5754 361.0832 513.3695 -4.4002 393.0145 397.4147 360.7460 514.9685 -4.4059 392.7534 397.1593 360.5151 516.5975 -4.4128 392.6547 397.0676 360.4082 518.1965 -4.4143 392.3072 396.7216 360.2081 519.8103 -4.4000 392.1362 396.5362 359.9950 521.4088 -4.3981 391.8361 396.2342 359.8120 523.0083 -4.3823 391.7119 396.0942 359.4958 524.6378 -4.4159 391.5980 396.0138 359.3444 526.2376 -4.3957 391.2990 395.6947 359.1343 527.8391 -4.4037 391.0250 395.4287 358.9988 529.4560 -4.3974 390.8745 395.2718 358.6929 531.0555 -4.4044 390.6331 395.0374 358.4871 532.6708 -4.4034 390.4355 394.8389 358.2915 534.2844 -4.3992 390.2132 394.6124 358.0909 535.8770 -4.3826 389.9791 394.3617 357.8712 537.4686 -4.3824 389.7749 394.1573 357.6239 539.0765 -4.3807 389.6657 394.0464 357.3970 540.6694 -4.3661 389.4199 393.7861 357.1885 542.2774 -4.3674 389.1454 393.5127 356.9728 543.8891 -4.3683 389.0402 393.4085 356.8913 545.4850 -4.3557 388.7630 393.1187 356.6181 547.0806 -4.3621 388.6703 393.0324 356.3590 548.6914 -4.3569 388.3040 392.6608 356.1655 550.3018 -4.3473 388.2180 392.5653 355.8948 551.8995 -4.3479 388.0477 392.3957 355.6974 553.5131 -4.3367 387.7994 392.1361 355.4651 555.1120 -4.3374 387.6883 392.0257 355.3409 556.7118 -4.3375 387.4072 391.7447 355.2022 558.3106 -4.3373 387.1594 391.4966 355.0172 559.9399 -4.3140 386.9853 391.2993 354.7814 561.5386 -4.3191 386.8948 391.2139 354.4935 563.1376 -4.2844 386.6298 390.9142 354.2333 564.7516 -4.3037 386.3327 390.6364 354.0964 566.3506 -4.3117 386.1795 390.4912 353.8469 567.9646 -4.3035 385.8724 390.1759 353.6541 569.5785 -4.2784 385.6438 389.9221 353.4770 571.1775 -4.2802 385.4932 389.7733 353.2239 572.7915 -4.2621 385.3960 389.6581 352.9867 574.3914 -4.2658 385.1551 389.4209 352.8536 576.0055 -4.2446 385.0108 389.2554 352.6469 577.6196 -4.2511 384.5944 388.8455 352.3720 579.2195 -4.2225 384.3135 388.5360 352.1454 580.8188 -4.2337 384.2237 388.4575 352.0055 582.4480 -4.2219 384.1026 388.3245 351.7740 584.0633 -4.2171 384.0193 388.2364 351.5851 585.6638 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