DTA measure 2Fazisatalakulas1 Date: 20251126:945 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.27 s Mass = 1172.2 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4144 -4.7481 459.8503 464.5984 433.3168 4.0074 -4.7599 459.8368 464.5967 433.5393 5.6006 -4.7695 459.8612 464.6307 433.6803 7.2039 -4.7770 459.8560 464.6330 433.7737 8.8023 -4.7836 459.8525 464.6361 433.7789 10.4109 -4.7966 459.8497 464.6463 433.6698 11.9936 -4.8045 459.8844 464.6889 433.5132 13.6023 -4.8155 459.8689 464.6844 433.2729 15.2210 -4.8256 459.8605 464.6861 432.9399 16.8243 -4.8335 459.8593 464.6928 432.5188 18.4329 -4.8381 459.9094 464.7475 432.0585 20.0258 -4.8436 459.9013 464.7449 431.6106 21.6344 -4.8471 459.9213 464.7684 431.1250 23.2379 -4.8462 459.8965 464.7427 430.5987 24.8463 -4.8480 459.9042 464.7523 430.1134 26.4496 -4.8467 459.9096 464.7563 429.6742 28.0735 -4.8493 459.9083 464.7577 429.2743 29.6769 -4.8477 459.8912 464.7389 428.9401 31.2804 -4.8525 459.8820 464.7345 428.6461 32.8940 -4.8519 459.8778 464.7298 428.4079 34.4820 -4.8553 459.8287 464.6841 428.2169 36.0906 -4.8552 459.7884 464.6436 428.1047 37.6941 -4.8574 459.7421 464.5995 427.9918 39.3026 -4.8573 459.7388 464.5961 427.9301 40.9265 -4.8551 459.7065 464.5615 427.9129 42.5350 -4.8557 459.6917 464.5474 427.9219 44.1384 -4.8577 459.6799 464.5377 427.9146 45.7521 -4.8594 459.6229 464.4822 427.8917 47.3555 -4.8635 459.5497 464.4132 427.8565 48.9691 -4.8689 459.4739 464.3428 427.8135 50.5726 -4.8730 459.4575 464.3305 427.7115 52.1709 -4.8735 459.4142 464.2878 427.5150 53.7948 -4.8778 459.3879 464.2657 427.2924 55.4034 -4.8812 459.3493 464.2305 427.0761 57.0119 -4.8890 459.2746 464.1636 426.8166 58.6204 -4.8873 459.2194 464.1067 426.5013 60.2239 -4.8929 459.1806 464.0735 426.1843 61.8375 -4.8953 459.1183 464.0135 425.8534 63.4409 -4.8989 459.0537 463.9526 425.5299 65.0598 -4.8953 459.0211 463.9163 425.1750 66.6631 -4.8889 458.9105 463.7994 424.8176 68.2614 -4.8890 458.8606 463.7496 424.4862 69.8649 -4.8901 458.8243 463.7144 424.1810 71.4680 -4.8888 458.7389 463.6277 423.9233 73.0663 -4.8869 458.6571 463.5440 423.6714 74.6594 -4.8896 458.5722 463.4618 423.4236 76.2626 -4.8890 458.4903 463.3793 423.2339 77.8814 -4.8907 458.4459 463.3366 423.0551 79.4898 -4.8887 458.3809 463.2696 422.8889 81.0933 -4.8896 458.3099 463.1995 422.8003 82.7018 -4.8921 458.2264 463.1185 422.6872 84.2896 -4.8929 458.1349 463.0279 422.5701 85.9033 -4.8884 458.0468 462.9352 422.4471 87.5066 -4.8895 457.9785 462.8680 422.3334 89.1151 -4.8935 457.9037 462.7971 422.1850 90.7340 -4.8975 457.8186 462.7161 422.0461 92.3373 -4.9014 457.6919 462.5933 421.9123 93.9306 -4.9018 457.5776 462.4794 421.7769 95.5341 -4.9019 457.4808 462.3827 421.5637 97.1425 -4.9027 457.4061 462.3088 421.3341 98.7461 -4.9062 457.2795 462.1857 421.0959 100.3548 -4.9078 457.1627 462.0705 420.8610 101.9579 -4.9026 457.0355 461.9382 420.5858 103.5768 -4.9013 456.9452 461.8466 420.3332 105.1854 -4.9054 456.8668 461.7721 420.0950 106.7939 -4.9101 456.7814 461.6914 419.8145 108.4024 -4.9134 456.6517 461.5651 419.5305 110.0111 -4.9110 456.5335 461.4446 419.2913 111.6040 -4.9130 456.3961 461.3091 419.0291 113.2126 -4.9160 456.2647 461.1807 418.7835 114.8213 -4.9137 456.1786 461.0924 418.5339 116.4450 -4.9114 456.0857 460.9971 418.2675 118.0536 -4.9086 455.9687 460.8773 418.0391 119.6571 -4.9061 455.8429 460.7490 417.8360 121.2655 -4.9078 455.7480 460.6558 417.5966 122.8741 -4.9073 455.5963 460.5037 417.4277 124.4673 -4.9072 455.4433 460.3505 417.2834 126.0756 -4.9081 455.2653 460.1734 417.1559 127.6843 -4.9121 455.1181 460.0303 416.9887 129.3031 -4.9105 454.9676 459.8781 416.8243 130.9014 -4.9100 454.8625 459.7726 416.6627 132.5048 -4.9143 454.7200 459.6343 416.5062 134.1031 -4.9119 454.5665 459.4784 416.3202 135.7014 -4.9106 454.4491 459.3596 416.1321 137.3099 -4.9123 454.3157 459.2280 415.9417 138.9084 -4.9085 454.2033 459.1118 415.7392 140.5270 -4.9113 454.0794 458.9907 415.5010 142.1356 -4.9109 453.9926 458.9036 415.2850 143.7236 -4.9150 453.8403 458.7553 415.0860 145.3321 -4.9122 453.6788 458.5909 414.8201 146.9356 -4.9047 453.5150 458.4197 414.5773 148.5443 -4.9057 453.3774 458.2831 414.3489 150.1475 -4.9031 453.2243 458.1274 414.1135 151.7613 -4.9007 453.0830 457.9838 413.8707 153.3800 -4.8971 452.9348 457.8319 413.6411 154.9833 -4.8931 452.7702 457.6633 413.3828 156.5919 -4.8864 452.6391 457.5255 413.1562 158.1953 -4.8885 452.5334 457.4220 412.9211 159.8038 -4.8919 452.3681 457.2599 412.7117 161.4073 -4.8946 452.2177 457.1123 412.5268 163.0156 -4.8912 452.0445 456.9357 412.3405 164.6395 -4.8923 451.9257 456.8180 412.0986 166.2480 -4.8951 451.8206 456.7157 411.9290 167.8513 -4.8920 451.6944 456.5863 411.7546 169.4548 -4.8890 451.5167 456.4057 411.5222 171.0633 -4.8856 451.3538 456.2394 411.3357 172.6819 -4.8827 451.1724 456.0551 411.1722 174.3110 -4.8785 450.9952 455.8737 410.9876 175.9143 -4.8726 450.8568 455.7294 410.8241 177.5230 -4.8704 450.6684 455.5387 410.6307 179.1264 -4.8718 450.4885 455.3603 410.4650 180.7399 -4.8670 450.2947 455.1618 410.2637 182.3434 -4.8621 450.1282 454.9903 410.1026 183.9418 -4.8592 449.9843 454.8435 409.8991 185.5449 -4.8609 449.8179 454.6789 409.6436 187.1740 -4.8576 449.6539 454.5115 409.3668 188.7774 -4.8565 449.5005 454.3570 409.0923 190.3910 -4.8530 449.3425 454.1955 408.8522 191.9996 -4.8542 449.1484 454.0027 408.6363 193.6080 -4.8546 448.9991 453.8537 408.4057 195.2011 -4.8539 448.8074 453.6612 408.1683 196.7996 -4.8476 448.6379 453.4855 407.9344 198.3928 -4.8389 448.5087 453.3476 407.7167 200.0063 -4.8355 448.3163 453.1517 407.4945 201.5945 -4.8351 448.1699 453.0050 407.2836 203.2079 -4.8321 447.9848 452.8169 407.0942 204.8063 -4.8282 447.8420 452.6701 406.8973 206.4149 -4.8261 447.6779 452.5040 406.7011 208.0130 -4.8279 447.4894 452.3173 406.4965 209.6165 -4.8294 447.2905 452.1199 406.3098 211.2098 -4.8276 447.1046 451.9322 406.1347 212.8131 -4.8217 446.9522 451.7740 405.9544 214.4370 -4.8187 446.7593 451.5780 405.7523 216.0404 -4.8139 446.5543 451.3681 405.5388 217.6436 -4.8107 446.3978 451.2085 405.3514 219.2370 -4.8075 446.2026 451.0101 405.1483 220.8405 -4.8032 446.0185 450.8217 404.9669 222.4489 -4.7993 445.8395 450.6388 404.7639 224.0525 -4.8009 445.6797 450.4806 404.5290 225.6714 -4.7978 445.4810 450.2789 404.3333 227.2901 -4.7985 445.2920 450.0905 404.1021 228.8986 -4.7934 445.1073 449.9007 403.8750 230.5021 -4.7858 444.9651 449.7510 403.6580 232.1004 -4.7805 444.7955 449.5760 403.4533 233.7038 -4.7729 444.5986 449.3715 403.2080 235.3124 -4.7715 444.4558 449.2273 402.9609 236.9209 -4.7665 444.2754 449.0418 402.7307 238.5294 -4.7582 444.0771 448.8353 402.5208 240.1483 -4.7549 443.8807 448.6356 402.2968 241.7619 -4.7509 443.7288 448.4797 402.0347 243.3653 -4.7491 443.5631 448.3122 401.8260 244.9790 -4.7458 443.3621 448.1080 401.6116 246.5826 -4.7411 443.1314 447.8725 401.4065 248.1961 -4.7397 442.9636 447.7033 401.1722 249.7996 -4.7367 442.7960 447.5327 400.9716 251.4185 -4.7326 442.5945 447.3271 400.7671 253.0320 -4.7293 442.3812 447.1105 400.5863 254.6354 -4.7316 442.1962 446.9279 400.3944 256.2490 -4.7272 442.0073 446.7346 400.2399 257.8474 -4.7238 441.8224 446.5462 400.0742 259.4560 -4.7242 441.6194 446.3437 399.8835 261.0544 -4.7196 441.4467 446.1664 399.6832 262.6679 -4.7166 441.2956 446.0122 399.5192 264.2764 -4.7134 441.1132 445.8267 399.2947 265.8644 -4.7129 440.9290 445.6419 399.0914 267.4626 -4.7068 440.7422 445.4489 398.8917 269.0713 -4.6990 440.5405 445.2395 398.6858 270.6745 -4.6933 440.3205 445.0139 398.4524 272.2830 -4.6850 440.1209 444.8059 398.1987 273.8865 -4.6815 439.9031 444.5846 397.9842 275.5051 -4.6764 439.6890 444.3654 397.7908 277.1086 -4.6650 439.4868 444.1518 397.5576 278.7119 -4.6629 439.2661 443.9290 397.3102 280.3204 -4.6590 439.0973 443.7562 397.0628 281.9239 -4.6542 438.8925 443.5467 396.8216 283.5320 -4.6534 438.6992 443.3527 396.5884 285.1355 -4.6404 438.5023 443.1427 396.3641 286.7440 -4.6383 438.3032 442.9415 396.1313 288.3524 -4.6378 438.1048 442.7426 395.9087 289.9608 -4.6333 437.9041 442.5374 395.7037 291.5693 -4.6301 437.7281 442.3583 395.5175 293.1728 -4.6261 437.5640 442.1901 395.2779 294.7815 -4.6193 437.3707 441.9900 395.0165 296.3898 -4.6133 437.1652 441.7786 394.8209 297.9830 -4.6117 436.9529 441.5646 394.6241 299.5915 -4.6026 436.7950 441.3976 394.4506 301.2154 -4.5995 436.6054 441.2049 394.2865 302.8240 -4.5943 436.3927 440.9870 394.1152 304.4325 -4.5938 436.1695 440.7633 393.9046 306.0205 -4.5888 435.9431 440.5319 393.7195 307.6291 -4.5850 435.7327 440.3177 393.5465 309.2326 -4.5817 435.5200 440.1018 393.3463 310.8410 -4.5763 435.3370 439.9132 393.1537 312.4496 -4.5755 435.1686 439.7442 392.9759 314.0735 -4.5735 435.0089 439.5824 392.7627 315.6820 -4.5673 434.8054 439.3727 392.5686 317.2753 -4.5671 434.5954 439.1625 392.3316 318.8838 -4.5627 434.3837 438.9464 392.1344 320.4923 -4.5526 434.2271 438.7797 391.8817 322.0958 -4.5430 434.0249 438.5679 391.6656 323.6939 -4.5424 433.8036 438.3459 391.4624 325.2973 -4.5347 433.5592 438.0939 391.2644 326.9008 -4.5356 433.3797 437.9153 391.0395 328.4989 -4.5265 433.1898 437.7163 390.7926 330.1075 -4.5212 432.9706 437.4918 390.5657 331.7110 -4.5179 432.7791 437.2970 390.3468 333.3143 -4.5095 432.6052 437.1147 390.1227 334.9178 -4.5021 432.4090 436.9112 389.8941 336.5213 -4.5015 432.1977 436.6992 389.6551 338.1296 -4.4947 431.9951 436.4898 389.4015 339.7176 -4.4903 431.8293 436.3196 389.1905 341.3415 -4.4838 431.6029 436.0867 388.9645 342.9448 -4.4781 431.3852 435.8633 388.7077 344.5483 -4.4749 431.1981 435.6729 388.5000 346.1566 -4.4744 430.9988 435.4732 388.3195 347.7601 -4.4736 430.7629 435.2364 388.0966 349.3738 -4.4673 430.5239 434.9911 387.8918 350.9770 -4.4599 430.2942 434.7541 387.6728 352.6010 -4.4547 430.0976 434.5524 387.5135 354.2044 -4.4445 429.8965 434.3409 387.3162 355.8129 -4.4393 429.7065 434.1458 387.1011 357.4214 -4.4355 429.5020 433.9375 386.9291 359.0298 -4.4334 429.2795 433.7129 386.7471 360.6333 -4.3980 429.0919 433.4900 386.5717 362.2419 -4.3575 428.9112 433.2687 386.4009 363.8503 -4.3593 428.7137 433.0730 386.2087 365.4691 -4.3511 428.5237 432.8747 386.0018 367.0826 -4.3325 428.3151 432.6475 385.7967 368.6706 -4.3067 428.1062 432.4129 385.5776 370.2793 -4.3066 427.9026 432.2093 385.3701 371.8828 -4.2937 427.7019 431.9956 385.1452 373.5066 -4.2940 427.4599 431.7539 384.9187 375.1306 -4.2881 427.2401 431.5282 384.6560 376.7238 -4.2797 427.0666 431.3463 384.4349 378.3425 -4.2690 426.8559 431.1249 384.2190 379.9511 -4.2637 426.6269 430.8906 384.0002 381.5444 -4.2605 426.4332 430.6937 383.7934 383.1528 -4.2479 426.1999 430.4478 383.5703 384.7614 -4.2556 425.9985 430.2540 383.3596 386.3698 -4.2402 425.8110 430.0512 383.1544 387.9834 -4.2424 425.6218 429.8642 382.9443 389.5715 -4.2206 425.4064 429.6270 382.7274 391.1746 -4.1327 425.1810 429.3138 382.5369 392.7730 -4.0700 424.9312 429.0012 382.3309 394.3765 -4.0252 424.6945 428.7197 382.0977 395.9695 -3.9974 424.5381 428.5355 381.9147 397.5679 -3.9756 424.3282 428.3038 381.7455 399.1713 -3.9553 424.1077 428.0630 381.5339 400.7796 -3.9431 423.8910 427.8341 381.2572 402.3984 -3.9426 423.6868 427.6293 381.0642 404.0068 -3.9399 423.4753 427.4152 380.8528 405.5949 -3.9344 423.2879 427.2224 380.6589 407.2033 -3.9336 423.0757 427.0093 380.4614 408.8116 -3.9353 422.8754 426.8107 380.2331 410.4203 -3.9407 422.6762 426.6169 380.0220 412.0235 -3.9419 422.4785 426.4204 379.8244 413.6270 -3.9363 422.2735 426.2099 379.5948 415.2508 -3.9306 422.0663 425.9969 379.3682 416.8541 -3.9263 421.8650 425.7913 379.1405 418.4628 -3.9225 421.6429 425.5654 378.9270 420.0713 -3.9245 421.4404 425.3649 378.7135 421.6798 -3.9168 421.2300 425.1468 378.4904 423.2831 -3.9145 421.0199 424.9343 378.2866 424.8914 -3.9175 420.8281 424.7456 378.0688 426.5104 -3.9125 420.5864 424.4990 377.8363 428.1240 -3.9016 420.3477 424.2493 377.5995 429.7274 -3.8970 420.1391 424.0362 377.3844 431.3360 -3.8896 419.9447 423.8343 377.2077 432.9446 -3.8773 419.7365 423.6138 377.0104 434.5479 -3.8747 419.5429 423.4176 376.8073 436.1616 -3.9303 419.3360 423.2664 376.5867 437.7805 -3.9438 419.1098 423.0537 376.3939 439.3890 -3.9056 418.8994 422.8050 376.2194 440.9976 -3.8893 418.7162 422.6055 376.0109 442.6061 -3.8732 418.4951 422.3683 375.7566 444.2145 -3.8592 418.2934 422.1526 375.5085 445.8231 -3.8498 418.0811 421.9309 375.3012 447.4318 -3.8315 417.8613 421.6928 375.1070 449.0555 -3.8197 417.6321 421.4518 374.9167 450.6436 -3.8120 417.4079 421.2199 374.7353 452.2524 -3.8055 417.2305 421.0360 374.5218 453.8504 -3.8037 417.0214 420.8251 374.3206 455.4488 -3.7975 416.8073 420.6048 374.1467 457.0574 -3.7911 416.6107 420.4018 373.9650 458.6453 -3.7819 416.3873 420.1692 373.7559 460.2435 -3.7754 416.1603 419.9357 373.5765 461.8519 -3.7671 415.9499 419.7171 373.3734 463.4654 -3.7617 415.7314 419.4931 373.1509 465.0738 -3.7534 415.5093 419.2627 372.9405 466.6771 -3.7467 415.3028 419.0495 372.7612 468.2805 -3.7457 415.0862 418.8319 372.5776 469.8889 -3.7443 414.9046 418.6489 372.3480 471.4924 -3.7386 414.7124 418.4510 372.0859 473.1009 -3.7311 414.5309 418.2620 371.8509 474.7195 -3.7233 414.3039 418.0272 371.5890 476.3281 -3.7173 414.0642 417.7815 371.3330 477.9314 -3.7151 413.8236 417.5387 371.0955 479.5451 -3.7088 413.5815 417.2904 370.8815 481.1486 -3.7002 413.3842 417.0844 370.6556 482.7518 -3.6922 413.2118 416.9041 370.4379 484.3604 -3.6907 413.0052 416.6960 370.2247 485.9790 -3.6932 412.7835 416.4767 369.9708 487.5875 -3.6918 412.5727 416.2645 369.7414 489.1959 -3.6878 412.3700 416.0578 369.5184 490.8043 -3.6756 412.1722 415.8478 369.3181 492.4078 -3.6653 411.9621 415.6274 369.1463 494.0161 -3.6649 411.7359 415.4008 368.9846 495.6248 -3.6640 411.5162 415.1802 368.7592 497.2488 -3.6549 411.2856 414.9405 368.5735 498.8573 -3.6449 411.0748 414.7198 368.3703 500.4658 -3.6358 410.8825 414.5183 368.2010 502.0744 -3.6305 410.6816 414.3120 367.9788 503.6879 -3.6261 410.4324 414.0585 367.7668 505.2913 -3.6233 410.2199 413.8433 367.6198 506.8998 -3.6199 410.0477 413.6676 367.4305 508.5185 -3.5985 409.8571 413.4556 367.2170 510.1323 -3.5718 409.6276 413.1994 367.0169 511.7356 -3.5517 409.3990 412.9507 366.7908 513.3491 -3.5388 409.1978 412.7365 366.5621 514.9475 -3.5336 408.9769 412.5104 366.3707 516.5509 -3.5260 408.7475 412.2735 366.1598 518.1543 -3.5317 408.5500 412.0818 365.9585 519.7528 -3.5332 408.3555 411.8887 365.7276 521.3563 -3.5242 408.1440 411.6682 365.5077 522.9646 -3.5153 407.9342 411.4494 365.2543 524.5681 -3.5140 407.7144 411.2284 365.0194 526.1665 -3.5140 407.4941 411.0081 364.7752 527.7750 -3.5108 407.2607 410.7715 364.5469 529.3784 -3.5088 407.0418 410.5506 364.3272 530.9870 -3.4974 406.8474 410.3448 364.0942 532.5749 -3.4936 406.6315 410.1251 363.8534 534.1989 -3.4953 406.4246 409.9199 363.6410 535.8023 -3.4832 406.2236 409.7068 363.4498 537.4056 -3.4735 405.9601 409.4336 363.2413 539.0143 -3.4574 405.7519 409.2093 363.0444 540.6176 -3.4445 405.5685 409.0130 362.8434 542.2261 -3.4354 405.3937 408.8291 362.6507 543.8501 -3.4283 405.1721 408.6004 362.4292 545.4686 -3.4223 404.9275 408.3499 362.2369 547.0721 -3.4148 404.7001 408.1149 362.0760 548.6808 -3.4087 404.4887 407.8974 361.8883 550.2839 -3.4030 404.2779 407.6809 361.6886 551.8976 -3.3939 404.0442 407.4380 361.4767 553.5010 -3.3899 403.8327 407.2225 361.2654 555.1145 -3.3894 403.6353 407.0247 361.0624 556.7331 -3.3783 403.4417 406.8200 360.8601 558.3468 -3.3695 403.2160 406.5855 360.6467 559.9400 -3.3589 402.9577 406.3167 360.4222 561.5538 -3.3546 402.7606 406.1152 360.2178 563.1570 -3.3568 402.5335 405.8903 360.0347 564.7655 -3.3467 402.3534 405.7001 359.8275 566.3739 -3.3503 402.1716 405.5219 359.6048 567.9825 -3.3458 401.9932 405.3390 359.3872 569.6014 -3.3422 401.7406 405.0828 359.1755 571.2149 -3.3454 401.5225 404.8679 358.9736 572.8183 -3.3397 401.3134 404.6530 358.7374 574.4268 -3.3341 401.0703 404.4045 358.5176 576.0301 -3.3191 400.8627 404.1818 358.3029 577.6388 -3.3091 400.6116 403.9208 358.0750 579.2421 -3.2975 400.4027 403.7002 357.8545 580.8558 -3.2895 400.2261 403.5156 357.6031 582.4644 -3.2973 400.0174 403.3146 357.3703 584.0625 -3.2983 399.7936 403.0919 357.1782 585.6609 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