DTA measure 1pbupdown3 Date: 20251022:857 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.18 s Mass = 959.300 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1478 0.8954 229.6965 228.8012 274.0719 1.9755 0.9009 229.9873 229.0865 273.7917 2.7720 0.9035 230.2483 229.3448 273.5274 3.5685 0.9048 230.5401 229.6353 273.2940 4.3960 0.9055 230.8342 229.9287 273.0654 5.1618 0.9074 231.1102 230.2028 272.9092 6.0198 0.9136 231.4196 230.5060 272.7511 6.7963 0.9151 231.6691 230.7541 272.6151 7.6130 0.9183 231.9502 231.0318 272.5157 8.3790 0.9211 232.2268 231.3057 272.4473 9.2065 0.9193 232.5043 231.5850 272.4452 10.0028 0.9224 232.7572 231.8348 272.4995 10.7995 0.9243 233.0150 232.0907 272.6185 11.6270 0.9255 233.3050 232.3795 272.8283 12.3925 0.9286 233.5588 232.6302 273.0380 13.2510 0.9344 233.8400 232.9055 273.3490 14.0168 0.9345 234.0676 233.1331 273.6960 14.8338 0.9319 234.3300 233.3981 274.1126 15.6408 0.9313 234.5929 233.6615 274.5865 16.4373 0.9292 234.8440 233.9148 275.0857 17.2645 0.9312 235.0893 234.1581 275.6402 18.0203 0.9353 235.3423 234.4071 276.1670 18.8885 0.9323 235.6307 234.6984 276.7495 19.6440 0.9313 235.8708 234.9395 277.2803 20.4818 0.9321 236.1348 235.2027 277.8448 21.2680 0.9332 236.3855 235.4524 278.3594 22.0645 0.9334 236.6301 235.6967 278.8653 22.8510 0.9306 236.8760 235.9454 279.3305 23.6475 0.9270 237.1409 236.2139 279.7837 24.4645 0.9233 237.4051 236.4818 280.1880 25.2205 0.9237 237.6132 236.6895 280.4963 26.0783 0.9247 237.8875 236.9629 280.7864 26.8340 0.9220 238.1264 237.2043 281.0216 27.6615 0.9191 238.4170 237.4979 281.2242 28.4578 0.9162 238.6896 237.7735 281.3843 29.2443 0.9131 238.9590 238.0459 281.4675 30.0718 0.9096 239.2452 238.3356 281.5358 30.8373 0.9069 239.5006 238.5937 281.5331 31.6955 0.9088 239.7340 238.8252 281.5251 32.4205 0.9070 239.9551 239.0482 281.5359 33.2888 0.9053 240.2415 239.3362 281.4643 34.0445 0.9014 240.4839 239.5825 281.3621 34.8718 0.8986 240.7181 239.8195 281.2592 35.6683 0.8996 240.9704 240.0707 281.1159 36.4548 0.8994 241.2117 240.3124 280.9405 37.2820 0.8938 241.4889 240.5951 280.7449 38.0480 0.8891 241.7354 240.8463 280.5649 38.9165 0.8876 241.9897 241.1021 280.3745 39.6718 0.8857 242.1948 241.3091 280.2016 40.4995 0.8848 242.4576 241.5728 279.9806 41.2960 0.8833 242.7033 241.8200 279.7687 42.0925 0.8838 242.9678 242.0839 279.5914 42.9200 0.8823 243.2183 242.3360 279.4226 43.6755 0.8797 243.4712 242.5914 279.3029 44.5438 0.8768 243.7323 242.8555 279.1813 45.2998 0.8770 243.9664 243.0894 279.0894 46.1268 0.8774 244.2045 243.3271 279.0314 46.9235 0.8789 244.4434 243.5645 279.0577 47.7305 0.8794 244.6730 243.7936 279.0904 48.5475 0.8781 244.8992 244.0211 279.1919 49.3135 0.8796 245.1290 244.2494 279.3419 50.1715 0.8799 245.3926 244.5127 279.5858 50.9475 0.8762 245.6303 244.7541 279.8342 51.7650 0.8689 245.8563 244.9874 280.1416 52.5613 0.8660 246.0956 245.2296 280.5046 53.3580 0.8650 246.2920 245.4271 280.8985 54.1855 0.8643 246.5653 245.7010 281.3735 54.9510 0.8616 246.7894 245.9278 281.7942 55.7990 0.8549 246.9989 246.1440 282.2854 56.5750 0.8498 247.2352 246.3854 282.7758 57.4023 0.8516 247.4808 246.6292 283.3030 58.1988 0.8514 247.7225 246.8712 283.8216 58.9855 0.8503 247.9522 247.1019 284.3557 59.8228 0.8466 248.1773 247.3306 284.8612 60.5888 0.8456 248.3944 247.5488 285.3023 61.4470 0.8415 248.6670 247.8255 285.7854 62.2023 0.8377 248.8727 248.0351 286.1506 63.0400 0.8319 249.1090 248.2771 286.5038 63.8368 0.8226 249.3421 248.5195 286.8106 64.6330 0.8218 249.5677 248.7459 287.0956 65.4503 0.8184 249.7998 248.9814 287.3197 66.2265 0.8169 250.0446 249.2277 287.4776 67.0740 0.8074 250.2751 249.4678 287.6195 67.8503 0.8036 250.4831 249.6795 287.6987 68.6675 0.7988 250.7479 249.9490 287.7527 69.4740 0.7889 250.9960 250.2071 287.7672 70.2608 0.7847 251.2006 250.4159 287.7183 71.0880 0.7813 251.4472 250.6659 287.6345 71.8538 0.7812 251.6828 250.9016 287.5783 72.7223 0.7776 251.9317 251.1540 287.4706 73.4470 0.7731 252.1527 251.3796 287.3368 74.3153 0.7704 252.3995 251.6291 287.1474 75.0915 0.7679 252.6469 251.8790 286.9674 75.9085 0.7646 252.8931 252.1285 286.7596 76.7153 0.7623 253.1412 252.3789 286.5593 77.5018 0.7597 253.3496 252.5899 286.3902 78.3393 0.7544 253.5959 252.8415 286.2087 79.0950 0.7492 253.7944 253.0452 286.0621 79.9633 0.7493 254.0157 253.2663 285.8990 80.7188 0.7464 254.2168 253.4704 285.7627 81.5460 0.7437 254.4410 253.6973 285.6698 82.3428 0.7456 254.6831 253.9374 285.5631 83.1495 0.7437 254.9124 254.1687 285.4821 83.9358 0.7417 255.1265 254.3849 285.4550 84.7428 0.7390 255.3509 254.6119 285.4633 85.5598 0.7378 255.5735 254.8356 285.5287 86.3358 0.7377 255.7703 255.0326 285.6177 87.1838 0.7324 255.9869 255.2546 285.8145 87.9495 0.7295 256.1941 255.4646 286.0014 88.7770 0.7270 256.4297 255.7028 286.2733 89.5225 0.7248 256.6501 255.9253 286.5317 90.3495 0.7160 256.8441 256.1281 286.8846 91.1360 0.7162 257.0502 256.3340 287.2385 91.9225 0.7154 257.2534 256.5380 287.6617 92.7495 0.7173 257.4505 256.7332 288.0917 93.5155 0.7122 257.6739 256.9617 288.5123 94.3635 0.7120 257.8882 257.1762 289.0358 95.1290 0.7064 258.1066 257.4002 289.4734 95.9565 0.7013 258.3241 257.6228 289.9589 96.7225 0.6997 258.5180 257.8183 290.4027 97.5495 0.6918 258.7802 258.0884 290.8892 98.3465 0.6880 258.9642 258.2762 291.2930 99.1328 0.6851 259.1621 258.4771 291.6677 99.9600 0.6824 259.4059 258.7235 292.0615 100.7260 0.6755 259.6153 258.9398 292.3873 101.5840 0.6723 259.8515 259.1792 292.7291 102.3395 0.6720 260.0407 259.3686 292.9890 103.1773 0.6673 260.2638 259.5964 293.2711 103.9635 0.6604 260.5000 259.8396 293.5034 104.7705 0.6533 260.7540 260.1007 293.6551 105.5570 0.6474 260.9571 260.3096 293.7490 106.3635 0.6444 261.1506 260.5063 293.8082 107.1810 0.6387 261.3170 260.6784 293.8339 107.9468 0.6316 261.5140 260.8824 293.8138 108.8048 0.6276 261.7226 261.0951 293.7703 109.5710 0.6237 261.9223 261.2986 293.7404 110.3980 0.6203 262.1244 261.5042 293.6556 111.1950 0.6140 262.3493 261.7353 293.5493 111.9915 0.6114 262.5720 261.9605 293.4403 112.8188 0.6117 262.7857 262.1741 293.2786 113.5848 0.6098 263.0050 262.3952 293.1327 114.4325 0.6065 263.2533 262.6469 292.9280 115.2085 0.6019 263.4153 262.8134 292.7617 116.0258 0.6002 263.6487 263.0485 292.6006 116.8018 0.5946 263.8603 263.2657 292.4214 117.6188 0.5854 264.0901 263.5047 292.2636 118.4258 0.5877 264.2996 263.7119 292.1200 119.2120 0.5876 264.4675 263.8799 291.9844 120.0393 0.5847 264.6580 264.0733 291.8946 120.8053 0.5822 264.8586 264.2765 291.8094 121.6735 0.5791 265.0912 264.5122 291.7748 122.4290 0.5716 265.2829 264.7113 291.7993 123.2568 0.5699 265.5070 264.9372 291.8659 124.0530 0.5674 265.6996 265.1322 291.9801 124.8600 0.5616 265.9020 265.3404 292.1303 125.6773 0.5598 266.1245 265.5647 292.3418 126.4428 0.5576 266.3183 265.7607 292.5769 127.3010 0.5589 266.5224 265.9636 292.8781 128.0773 0.5555 266.7031 266.1476 293.1761 128.8943 0.5523 266.9341 266.3819 293.5509 129.6910 0.5476 267.1552 266.6076 293.9498 130.4875 0.5481 267.3392 266.7911 294.3568 131.3150 0.5467 267.5400 266.9933 294.7991 132.0810 0.5438 267.7393 267.1954 295.2089 132.9390 0.5384 267.9591 267.4208 295.7016 133.7048 0.5373 268.1100 267.5727 296.1110 134.5323 0.5323 268.3155 267.7832 296.5533 135.3288 0.5251 268.5115 267.9864 296.9805 136.1258 0.5214 268.7236 268.2022 297.3633 136.9528 0.5195 268.9498 268.4303 297.8045 137.7188 0.5146 269.1602 268.6456 298.1655 138.5770 0.5034 269.3486 268.8451 298.5270 139.3428 0.4953 269.5411 269.0458 298.8200 140.1703 0.4937 269.7372 269.2435 299.1050 140.9668 0.4942 269.9221 269.4279 299.3235 141.7633 0.4894 270.1112 269.6218 299.5195 142.5910 0.4870 270.3193 269.8323 299.6551 143.3565 0.4819 270.5150 270.0330 299.7814 144.2150 0.4805 270.7281 270.2476 299.8823 144.9808 0.4778 270.9197 270.4419 299.9160 145.7978 0.4687 271.1302 270.6616 299.9392 146.6045 0.4620 271.3574 270.8954 299.8995 147.4013 0.4536 271.5662 271.1126 299.8245 148.2283 0.4460 271.8089 271.3628 299.7394 148.9840 0.4419 272.0366 271.5947 299.6480 149.8525 0.4381 272.2587 271.8206 299.5753 150.6183 0.4359 272.4649 272.0291 299.4645 151.4458 0.4334 272.6450 272.2116 299.3307 152.2423 0.4294 272.8028 272.3734 299.1709 153.0285 0.4294 272.9904 272.5611 298.9975 153.8150 0.4236 273.1838 272.7601 298.8245 154.6115 0.4207 273.3644 272.9436 298.6874 155.4288 0.4166 273.5430 273.1264 298.5538 156.1845 0.4147 273.7456 273.3309 298.4229 157.0423 0.4174 273.9696 273.5522 298.2939 157.7980 0.4128 274.1512 273.7384 298.2264 158.6255 0.4099 274.3409 273.9311 298.1805 159.3910 0.4054 274.5133 274.1079 298.1635 160.2185 0.4012 274.7159 274.3147 298.1572 161.0050 0.3971 274.9132 274.5162 298.2449 161.8013 0.3895 275.0888 274.6993 298.3373 162.6290 0.3886 275.2648 274.8762 298.4818 163.3845 0.3906 275.4703 275.0797 298.6629 164.2528 0.3874 275.7199 275.3325 298.9400 165.0088 0.3864 275.9114 275.5251 299.2149 165.8460 0.3804 276.0853 275.7049 299.5113 166.6120 0.3764 276.2491 275.8726 299.8344 167.4395 0.3749 276.4074 276.0325 300.2102 168.2358 0.3720 276.6041 276.2321 300.5968 169.0328 0.3670 276.8139 276.4469 301.0237 169.8498 0.3647 277.0243 276.6595 301.5021 170.6258 0.3636 277.1929 276.8293 301.9540 171.4740 0.3547 277.3638 277.0092 302.4277 172.2395 0.3498 277.5328 277.1830 302.8497 173.0670 0.3480 277.7197 277.3717 303.2923 173.8638 0.3437 277.9055 277.5618 303.7255 174.6603 0.3408 278.1093 277.7684 304.1267 175.4878 0.3369 278.3060 277.9691 304.5090 176.2535 0.3311 278.4831 278.1520 304.8279 177.1115 0.3271 278.6689 278.3418 305.1194 177.8775 0.3216 278.8437 278.5221 305.3576 178.6945 0.3198 279.0442 278.7244 305.5756 179.4705 0.3141 279.2089 278.8948 305.7516 180.2980 0.3067 279.4099 279.1032 305.8934 181.0945 0.2981 279.6112 279.3131 306.0016 181.8808 0.2924 279.8270 279.5346 306.0837 182.7188 0.2861 280.0188 279.7327 306.0970 183.4740 0.2804 280.1963 279.9159 306.0977 184.3320 0.2687 280.4346 280.1659 306.0774 185.0983 0.2639 280.6512 280.3873 306.0007 185.9253 0.2630 280.8393 280.5763 305.9544 186.7220 0.2628 280.9820 280.7192 305.8429 187.5188 0.2598 281.1260 280.8661 305.7261 188.3460 0.2558 281.3227 281.0669 305.5977 189.1220 0.2498 281.5053 281.2555 305.4745 189.9700 0.2462 281.6899 281.4437 305.2968 190.7355 0.2448 281.8483 281.6035 305.1455 191.5630 0.2395 282.0429 281.8034 304.9909 192.3598 0.2354 282.2089 281.9735 304.8498 193.1560 0.2305 282.4030 282.1725 304.7020 193.9835 0.2295 282.6457 282.4162 304.6076 194.7495 0.2288 282.8410 282.6122 304.4941 195.5765 0.2291 283.0206 282.7915 304.4502 196.3425 0.2280 283.1808 282.9527 304.4398 197.1905 0.2247 283.3923 283.1676 304.4689 197.9560 0.2225 283.5642 283.3418 304.5090 198.8043 0.2224 283.7711 283.5487 304.5974 199.5803 0.2163 283.9450 283.7287 304.7230 200.3970 0.2128 284.1331 283.9202 304.8922 201.2043 0.2096 284.3085 284.0989 305.0858 201.9905 0.2057 284.4699 284.2642 305.3049 202.8278 0.2011 284.6600 284.4590 305.6084 203.5838 0.1962 284.8077 284.6114 305.9202 204.4520 0.1929 285.0011 284.8082 306.2811 205.1768 0.1930 285.1588 284.9658 306.6073 206.0453 0.1949 285.3980 285.2032 307.0571 206.8008 0.1931 285.5777 285.3846 307.4699 207.6385 0.1940 285.7429 285.5489 307.9482 208.4250 0.1927 285.9164 285.7237 308.3946 209.2315 0.1911 286.1057 285.9146 308.8117 210.0590 0.1855 286.2910 286.1055 309.2394 210.8250 0.1824 286.4825 286.3001 309.6210 211.6725 0.1762 286.6649 286.4887 310.0102 212.4488 0.1704 286.8158 286.6454 310.3567 213.2660 0.1644 286.9623 286.7979 310.7031 214.0728 0.1597 287.1388 286.9791 311.0240 214.8593 0.1561 287.3330 287.1769 311.3138 215.6968 0.1502 287.5413 287.3911 311.5472 216.4525 0.1496 287.7044 287.5548 311.7298 217.3108 0.1508 287.9183 287.7675 311.9021 218.0455 0.1476 288.0611 287.9135 312.0199 218.8935 0.1419 288.2796 288.1376 312.1020 219.6493 0.1380 288.4374 288.2994 312.1206 220.4765 0.1317 288.6418 288.5100 312.1492 221.2630 0.1256 288.8099 288.6843 312.1591 222.0595 0.1206 288.9794 288.8589 312.1354 222.8765 0.1173 289.1524 289.0351 312.0857 223.6323 0.1138 289.3344 289.2206 312.0092 224.5005 0.1095 289.5287 289.4191 311.9121 225.2253 0.1041 289.7052 289.6011 311.8144 226.0735 0.0991 289.8856 289.7865 311.7108 226.8493 0.0968 290.0512 289.9544 311.5913 227.6665 0.0918 290.2440 290.1522 311.4606 228.4633 0.0859 290.4229 290.3370 311.3377 229.2595 0.0850 290.6233 290.5383 311.2164 230.0870 0.0818 290.7810 290.6992 311.0765 230.8530 0.0817 290.9573 290.8756 310.9245 231.7005 0.0779 291.1561 291.0782 310.8247 232.4768 0.0775 291.3165 291.2390 310.7508 233.2940 0.0721 291.5064 291.4343 310.7015 234.0905 0.0706 291.6783 291.6077 310.6463 234.8873 0.0738 291.8423 291.7685 310.6367 235.7145 0.0749 292.0121 291.9372 310.7120 236.4803 0.0725 292.1552 292.0828 310.8284 237.3385 0.0686 292.3364 292.2678 310.9766 238.0838 0.0663 292.4838 292.4175 311.1303 238.9418 0.0656 292.6836 292.6180 311.3680 239.7075 0.0643 292.8782 292.8139 311.6355 240.5350 0.0595 293.0277 292.9681 311.9225 241.3210 0.0541 293.2319 293.1778 312.2313 242.1283 0.0432 293.4374 293.3942 312.6032 242.9453 0.0421 293.6160 293.5738 312.9810 243.7213 0.0399 293.7526 293.7127 313.3650 244.5693 0.0369 293.9158 293.8789 313.7835 245.3453 0.0358 294.0953 294.0595 314.2084 246.1623 0.0344 294.3199 294.2855 314.6540 246.9590 0.0329 294.4914 294.4585 315.0749 247.7555 0.0286 294.6624 294.6339 315.5016 248.5930 0.0283 294.8287 294.8004 315.8939 249.3488 0.0265 294.9978 294.9712 316.2445 250.2170 0.0186 295.1671 295.1486 316.6245 250.9725 0.0126 295.3335 295.3209 316.9417 251.8100 0.0076 295.5177 295.5101 317.2492 252.5965 0.0065 295.7063 295.6999 317.4711 253.4033 0.0043 295.8658 295.8615 317.6928 254.2205 -0.0013 296.0897 296.0910 317.8727 254.9965 -0.0071 296.2697 296.2768 317.9857 255.8443 -0.0109 296.4242 296.4351 318.1117 256.5898 -0.0166 296.5813 296.5979 318.1846 257.4375 -0.0215 296.7508 296.7723 318.2647 258.2135 -0.0251 296.9074 296.9325 318.3062 259.0308 -0.0301 297.0836 297.1137 318.3043 259.8375 -0.0320 297.2875 297.3195 318.2545 260.6238 -0.0319 297.4662 297.4981 318.1832 261.4615 -0.0358 297.6706 297.7064 318.1068 262.2170 -0.0394 297.8448 297.8842 317.9987 263.0855 -0.0431 298.0273 298.0704 317.8622 263.8413 -0.0472 298.1770 298.2241 317.7534 264.6785 -0.0521 298.3456 298.3976 317.6272 265.4650 -0.0564 298.5233 298.5797 317.5190 266.2720 -0.0604 298.6730 298.7333 317.3870 267.0888 -0.0633 298.8219 298.8852 317.2142 267.8650 -0.0646 298.9946 299.0592 317.1008 268.7130 -0.0660 299.2139 299.2800 316.9690 269.4785 -0.0690 299.3693 299.4383 316.8841 270.3060 -0.0733 299.5255 299.5988 316.8532 271.1130 -0.0755 299.7182 299.7937 316.8633 271.8990 -0.0780 299.8955 299.9735 316.8895 272.7265 -0.0779 300.0514 300.1292 316.9099 273.4925 -0.0781 300.2237 300.3018 317.0134 274.3605 -0.0842 300.4010 300.4852 317.1426 275.1163 -0.0851 300.5782 300.6633 317.2957 275.9435 -0.0838 300.7025 300.7863 317.4873 276.7400 -0.0838 300.8426 300.9264 317.7261 277.5470 -0.0849 301.0240 301.1089 317.9947 278.3643 -0.0852 301.2116 301.2968 318.2989 279.1298 -0.0851 301.3794 301.4645 318.6436 279.9883 -0.0855 301.5726 301.6581 319.0527 280.7335 -0.0871 301.7176 301.8046 319.4224 281.5813 -0.0918 301.8822 301.9740 319.8556 282.3473 -0.0968 302.0208 302.1176 320.2802 283.1643 -0.0986 302.2337 302.3323 320.6858 283.9508 -0.1038 302.4266 302.5304 321.0818 284.7475 -0.1068 302.6031 302.7099 321.4989 285.5643 -0.1108 302.7606 302.8714 321.9124 286.3200 -0.1181 302.9012 303.0192 322.2750 287.1783 -0.1239 303.0916 303.2155 322.6550 287.9130 -0.1231 303.2324 303.3555 322.9458 288.7610 -0.1279 303.3988 303.5267 323.2569 289.5270 -0.1331 303.5657 303.6988 323.5000 290.3543 -0.1367 303.7221 303.8587 323.7368 291.1408 -0.1380 303.9013 304.0393 323.9275 291.9475 -0.1409 304.0956 304.2365 324.0862 292.7338 -0.1465 304.2516 304.3981 324.2126 293.5308 -0.1472 304.4121 304.5593 324.3277 294.3578 -0.1488 304.5896 304.7384 324.3896 295.1238 -0.1498 304.7647 304.9145 324.3940 295.9820 -0.1515 304.9368 305.0883 324.4355 296.7375 -0.1591 305.0861 305.2452 324.4052 297.5753 -0.1637 305.2773 305.4410 324.3574 298.3308 -0.1680 305.4065 305.5745 324.2835 299.1580 -0.1746 305.5999 305.7746 324.1985 299.9550 -0.1784 305.7446 305.9230 324.0883 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