DTA measure 2pbupdown3 Date: 20251022:927 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1648.29 s Mass = 959.300 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2963 -2.7218 459.3166 462.0384 434.0515 3.8946 -2.7286 459.3535 462.0821 434.5197 5.5030 -2.7343 459.4162 462.1505 434.9043 7.1114 -2.7419 459.5092 462.2511 435.1582 8.7200 -2.7501 459.5361 462.2861 435.3282 10.3284 -2.7628 459.5454 462.3082 435.3342 11.9369 -2.7725 459.6203 462.3928 435.2043 13.5608 -2.7778 459.6257 462.4035 434.9258 15.1538 -2.7842 459.6626 462.4468 434.5485 16.7624 -2.7949 459.7034 462.4983 434.0614 18.3706 -2.8002 459.7449 462.5451 433.4952 19.9793 -2.7996 459.7667 462.5663 432.9364 21.5875 -2.8001 459.8157 462.6158 432.3060 23.1910 -2.8012 459.8499 462.6510 431.6639 24.7839 -2.8046 459.8763 462.6808 431.0556 26.3666 -2.8060 459.9054 462.7114 430.4151 27.9803 -2.8066 459.9405 462.7471 429.8228 29.5835 -2.8048 459.9785 462.7833 429.2991 31.1819 -2.8050 459.9557 462.7607 428.8489 32.7800 -2.8077 459.9994 462.8071 428.4723 34.3886 -2.8083 460.0316 462.8399 428.2135 35.9921 -2.8073 460.0388 462.8461 428.0615 37.5851 -2.8076 460.0477 462.8553 428.0203 39.1886 -2.8103 460.0050 462.8153 428.0428 40.8073 -2.8086 460.0018 462.8104 428.1213 42.4158 -2.8114 459.9819 462.7933 428.1975 44.0193 -2.8179 459.9828 462.8007 428.3104 45.6278 -2.8202 460.0001 462.8203 428.4474 47.2311 -2.8238 459.9829 462.8067 428.5639 48.8449 -2.8225 459.9620 462.7846 428.6561 50.4481 -2.8228 459.9133 462.7361 428.5993 52.0720 -2.8277 459.9134 462.7411 428.5253 53.6806 -2.8305 459.9044 462.7349 428.3714 55.2941 -2.8309 459.8672 462.6981 428.1715 56.8975 -2.8382 459.8284 462.6666 427.8718 58.5109 -2.8509 459.7880 462.6389 427.5389 60.1143 -2.8523 459.7829 462.6352 427.1813 61.7226 -2.8505 459.7790 462.6295 426.7597 63.3465 -2.8552 459.7362 462.5914 426.3068 64.9550 -2.8520 459.6976 462.5496 425.8634 66.5634 -2.8510 459.6245 462.4755 425.4129 68.1720 -2.8486 459.5700 462.4185 424.9957 69.7804 -2.8484 459.5280 462.3764 424.5658 71.3889 -2.8538 459.4926 462.3464 424.1904 72.9921 -2.8552 459.5130 462.3683 423.8198 74.6213 -2.8510 459.4518 462.3028 423.5315 76.2246 -2.8547 459.4097 462.2643 423.3114 77.8383 -2.8515 459.3527 462.2043 423.1168 79.4416 -2.8475 459.2559 462.1034 422.9912 81.0400 -2.8483 459.1699 462.0182 422.8945 82.6483 -2.8474 459.1060 461.9534 422.8911 84.2569 -2.8514 459.0538 461.9051 422.9169 85.8601 -2.8535 458.9887 461.8422 422.9244 87.4840 -2.8477 458.9089 461.7567 422.9265 89.0823 -2.8479 458.8500 461.6979 422.9441 90.6599 -2.8547 458.7639 461.6186 422.9178 92.2634 -2.8566 458.7360 461.5926 422.8178 93.8615 -2.8554 458.7070 461.5624 422.6463 95.4598 -2.8592 458.6276 461.4869 422.4875 97.0633 -2.8642 458.5261 461.3903 422.3274 98.6563 -2.8648 458.4903 461.3551 422.0549 100.2596 -2.8680 458.3754 461.2434 421.7505 101.8785 -2.8753 458.2688 461.1440 421.3999 103.4868 -2.8716 458.1781 461.0497 421.0801 105.0750 -2.8700 458.0958 460.9658 420.7551 106.6836 -2.8704 458.0601 460.9306 420.3851 108.2869 -2.8701 457.9492 460.8193 420.0210 109.8955 -2.8689 457.8558 460.7247 419.6507 111.5040 -2.8680 457.7981 460.6661 419.3403 113.1125 -2.8656 457.6964 460.5620 419.0443 114.7314 -2.8651 457.5962 460.4613 418.7626 116.3349 -2.8661 457.4798 460.3460 418.4835 117.9484 -2.8688 457.3973 460.2662 418.2298 119.5519 -2.8703 457.2957 460.1660 417.9919 121.1605 -2.8705 457.1946 460.0651 417.7953 122.7586 -2.8748 457.0964 459.9712 417.6125 124.3673 -2.8691 456.9832 459.8523 417.4462 125.9809 -2.8676 456.8589 459.7265 417.3786 127.5995 -2.8710 456.7323 459.6032 417.3194 129.2081 -2.8719 456.6112 459.4831 417.2277 130.8166 -2.8669 456.5348 459.4016 417.1226 132.4251 -2.8684 456.4886 459.3570 417.0127 134.0338 -2.8718 456.3711 459.2429 416.8876 135.6420 -2.8688 456.2422 459.1109 416.7804 137.2353 -2.8718 456.1086 458.9804 416.6362 138.8488 -2.8731 455.9753 458.8484 416.4777 140.4675 -2.8736 455.8400 458.7135 416.3064 142.0761 -2.8686 455.7546 458.6232 416.0988 143.6844 -2.8682 455.6459 458.5142 415.8297 145.2929 -2.8675 455.5178 458.3852 415.5741 146.9014 -2.8637 455.3678 458.2316 415.2897 148.5099 -2.8640 455.2353 458.0993 415.0397 150.1185 -2.8577 455.0975 457.9552 414.7687 151.7373 -2.8588 455.0151 457.8739 414.4712 153.3405 -2.8624 454.9100 457.7724 414.1766 154.9184 -2.8672 454.7682 457.6354 413.9110 156.5165 -2.8659 454.6550 457.5209 413.5982 158.1096 -2.8632 454.5157 457.3788 413.3099 159.7183 -2.8593 454.3675 457.2268 413.0629 161.3113 -2.8564 454.2758 457.1322 412.7944 162.9148 -2.8501 454.1138 456.9639 412.5340 164.5386 -2.8518 453.9680 456.8197 412.2874 166.1266 -2.8562 453.8149 456.6712 412.1299 167.7351 -2.8566 453.6530 456.5096 411.9532 169.3384 -2.8532 453.5554 456.4086 411.8074 170.9418 -2.8502 453.4336 456.2838 411.6500 172.5503 -2.8522 453.3106 456.1628 411.5181 174.1536 -2.8511 453.1274 455.9786 411.4063 175.7673 -2.8533 452.9638 455.8171 411.2843 177.3858 -2.8531 452.8545 455.7076 411.1102 178.9995 -2.8502 452.6899 455.5401 410.9522 180.6025 -2.8487 452.5188 455.3675 410.8195 182.2111 -2.8455 452.3879 455.2334 410.6273 183.8196 -2.8435 452.2653 455.1087 410.4316 185.4281 -2.8399 452.1215 454.9614 410.1930 187.0368 -2.8366 451.9463 454.7828 409.9777 188.6606 -2.8374 451.7972 454.6346 409.7845 190.2691 -2.8432 451.6406 454.4838 409.5569 191.8778 -2.8399 451.4243 454.2642 409.2794 193.4810 -2.8396 451.2705 454.1102 409.0167 195.0896 -2.8361 451.1249 453.9610 408.7557 196.6983 -2.8340 450.9936 453.8275 408.4832 198.3068 -2.8323 450.8575 453.6897 408.2299 199.9255 -2.8274 450.7485 453.5759 407.9794 201.5393 -2.8226 450.5956 453.4182 407.7071 203.1324 -2.8200 450.4142 453.2342 407.4623 204.7511 -2.8215 450.2588 453.0803 407.2397 206.3596 -2.8246 450.1027 452.9273 407.0064 207.9679 -2.8198 449.9616 452.7813 406.8073 209.5765 -2.8149 449.8218 452.6366 406.5957 211.1849 -2.8151 449.6249 452.4400 406.4324 212.7780 -2.8109 449.5128 452.3236 406.2371 214.4019 -2.8091 449.3357 452.1449 406.0456 216.0103 -2.8062 449.1462 451.9525 405.8429 217.6189 -2.8027 448.9410 451.7438 405.6210 219.2066 -2.8046 448.7517 451.5563 405.4419 220.7948 -2.8042 448.5706 451.3748 405.2930 222.3929 -2.7961 448.4036 451.1997 405.1281 223.9963 -2.7905 448.2276 451.0181 404.9466 225.5946 -2.7936 448.1012 450.8947 404.8091 227.1878 -2.7896 447.9668 450.7564 404.6648 228.8014 -2.7880 447.8106 450.5986 404.4525 230.4049 -2.7846 447.6374 450.4220 404.2532 232.0134 -2.7852 447.4423 450.2276 404.0309 233.6168 -2.7860 447.3138 450.0998 403.8029 235.2253 -2.7848 447.1429 449.9276 403.5897 236.8285 -2.7863 446.9377 449.7239 403.3733 238.4218 -2.7877 446.7733 449.5610 403.1384 240.0304 -2.7820 446.6215 449.4036 402.8953 241.6490 -2.7751 446.4534 449.2285 402.6651 243.2576 -2.7776 446.2926 449.0702 402.4111 244.8663 -2.7763 446.1256 448.9019 402.1963 246.4746 -2.7777 445.9521 448.7298 401.9782 248.0781 -2.7746 445.7759 448.5505 401.7825 249.6868 -2.7708 445.5897 448.3605 401.5559 251.2954 -2.7664 445.4474 448.2138 401.3167 252.9191 -2.7593 445.2764 448.0358 401.0818 254.5279 -2.7613 445.1155 447.8768 400.8071 256.1361 -2.7587 444.9163 447.6750 400.5473 257.7396 -2.7562 444.7599 447.5160 400.2993 259.3380 -2.7577 444.5305 447.2882 400.0779 260.9566 -2.7585 444.2945 447.0530 399.8710 262.5499 -2.7523 444.1350 446.8873 399.6337 264.1534 -2.7429 444.0084 446.7513 399.4713 265.7873 -2.7399 443.8144 446.5543 399.3144 267.3908 -2.7376 443.6055 446.3431 399.1478 269.0044 -2.7333 443.4483 446.1816 399.0093 270.6076 -2.7317 443.2439 445.9756 398.8225 272.2213 -2.7299 443.0109 445.7407 398.6437 273.8245 -2.7281 442.8202 445.5483 398.4384 275.4330 -2.7260 442.6868 445.4128 398.2570 277.0568 -2.7236 442.4787 445.2023 398.0281 278.6704 -2.7205 442.3184 445.0389 397.8345 280.2739 -2.7187 442.1413 444.8600 397.6323 281.8874 -2.7176 441.9299 444.6474 397.4300 283.4806 -2.7134 441.7381 444.4515 397.2048 285.0789 -2.7093 441.5579 444.2672 396.9648 286.6566 -2.7068 441.4145 444.1213 396.7511 288.2651 -2.7053 441.2250 443.9303 396.4870 289.8736 -2.7011 441.0666 443.7677 396.2329 291.4771 -2.6992 440.8551 443.5543 395.9714 293.0704 -2.6958 440.6804 443.3763 395.7583 294.6686 -2.6888 440.4661 443.1548 395.5545 296.2719 -2.6884 440.2526 442.9410 395.3573 297.8805 -2.6837 440.0881 442.7718 395.1092 299.4838 -2.6756 439.8792 442.5548 394.8848 301.0923 -2.6689 439.7210 442.3899 394.6575 302.7110 -2.6684 439.5433 442.2117 394.4572 304.3245 -2.6698 439.3911 442.0610 394.2477 305.9329 -2.6673 439.1892 441.8566 394.0455 307.5413 -2.6635 438.9883 441.6518 393.8664 309.1499 -2.6572 438.7661 441.4232 393.6792 310.7429 -2.6529 438.5660 441.2189 393.5001 312.3463 -2.6531 438.3898 441.0429 393.2986 313.9599 -2.6487 438.2247 440.8733 393.0961 315.5785 -2.6435 438.0183 440.6618 392.9191 317.1871 -2.6450 437.7957 440.4407 392.7280 318.7904 -2.6442 437.5863 440.2305 392.5144 320.3939 -2.6408 437.3624 440.0032 392.3148 322.0076 -2.6365 437.1363 439.7728 392.0849 323.6109 -2.6342 436.9458 439.5800 391.8768 325.2245 -2.6333 436.7453 439.3786 391.6532 326.8279 -2.6318 436.5069 439.1387 391.4232 328.4415 -2.6285 436.3175 438.9460 391.2120 330.0450 -2.6261 436.1498 438.7759 391.0021 331.6534 -2.6238 435.9594 438.5832 390.7793 333.2619 -2.6125 435.7674 438.3800 390.5235 334.8704 -2.6112 435.6124 438.2236 390.3107 336.4839 -2.6067 435.4294 438.0361 390.1190 338.0770 -2.6025 435.2544 437.8569 389.8992 339.6905 -2.5996 435.0325 437.6321 389.6993 341.3093 -2.5987 434.8642 437.4629 389.5299 342.9175 -2.5925 434.6471 437.2396 389.2992 344.5261 -2.5916 434.4202 437.0118 389.0585 346.1348 -2.5891 434.1832 436.7724 388.8378 347.7379 -2.5881 433.9399 436.5280 388.6639 349.3209 -2.5829 433.7577 436.3406 388.4777 350.9140 -2.5758 433.5681 436.1438 388.2405 352.5174 -2.5700 433.3814 435.9514 388.0210 354.1004 -2.5624 433.2330 435.7954 387.8098 355.7191 -2.5553 433.0273 435.5826 387.5522 357.3224 -2.5477 432.8091 435.3568 387.3304 358.9208 -2.5442 432.6507 435.1949 387.0993 360.5291 -2.5407 432.4176 434.9583 386.8395 362.1326 -2.5371 432.2222 434.7593 386.5851 363.7413 -2.5376 432.0458 434.5835 386.3827 365.3445 -2.5335 431.8206 434.3541 386.2155 366.9531 -2.5390 431.6183 434.1573 385.9972 368.5463 -2.5364 431.4057 433.9421 385.8107 370.1649 -2.5299 431.1898 433.7197 385.6397 371.7735 -2.5244 430.9968 433.5211 385.4411 373.3819 -2.5165 430.7898 433.3063 385.2103 374.9904 -2.5109 430.5767 433.0876 385.0155 376.5990 -2.5096 430.3476 432.8571 384.8143 378.2073 -2.5063 430.1300 432.6362 384.6169 379.8108 -2.5042 429.9499 432.4541 384.4480 381.4089 -2.5067 429.7546 432.2612 384.2495 383.0276 -2.5048 429.5674 432.0722 384.0371 384.6413 -2.5039 429.3689 431.8728 383.8530 386.2445 -2.4990 429.1842 431.6833 383.6057 387.8533 -2.4937 429.0181 431.5118 383.3804 389.4616 -2.4908 428.8145 431.3053 383.1827 391.0701 -2.4888 428.6140 431.1028 383.0133 392.6736 -2.4887 428.3836 430.8723 382.7780 394.2821 -2.4819 428.1394 430.6213 382.5611 395.9009 -2.4742 427.9490 430.4233 382.3522 397.4889 -2.4769 427.7581 430.2350 382.1070 399.1126 -2.4700 427.5795 430.0495 381.8781 400.7161 -2.4684 427.4221 429.8905 381.6481 402.3296 -2.4701 427.1944 429.6646 381.4266 403.9330 -2.4685 426.9401 429.4086 381.2189 405.5468 -2.4654 426.7232 429.1886 381.0139 407.1499 -2.4527 426.5086 428.9613 380.7985 408.7789 -2.4436 426.3443 428.7879 380.5792 410.3823 -2.4411 426.0972 428.5382 380.3855 411.9958 -2.4427 425.8906 428.3333 380.1907 413.5890 -2.4360 425.6913 428.1273 380.0029 415.1768 -2.4324 425.5080 427.9404 379.8295 416.7700 -2.4290 425.2177 427.6467 379.6451 418.3734 -2.4245 425.0173 427.4419 379.4320 419.9715 -2.4268 424.8403 427.2671 379.2386 421.5596 -2.4259 424.6541 427.0800 379.0014 423.1833 -2.4265 424.4693 426.8959 378.7858 424.7818 -2.4219 424.2587 426.6807 378.5541 426.3850 -2.4159 424.0639 426.4798 378.3680 427.9935 -2.4101 423.8461 426.2562 378.1555 429.5970 -2.4115 423.6411 426.0526 377.9608 431.2104 -2.4076 423.3978 425.8053 377.7772 432.8139 -2.4023 423.2098 425.6121 377.5335 434.4379 -2.3948 423.0370 425.4318 377.2720 436.0411 -2.3878 422.8452 425.2329 377.0774 437.6548 -2.3819 422.6140 424.9959 376.8898 439.2580 -2.3777 422.4015 424.7792 376.6392 440.8715 -2.3720 422.1864 424.5585 376.4288 442.4749 -2.3601 421.9498 424.3099 376.1855 444.0834 -2.3561 421.7157 424.0717 375.9380 445.7073 -2.3521 421.4693 423.8214 375.7217 447.3156 -2.3525 421.2351 423.5876 375.4999 448.8986 -2.3464 421.0579 423.4043 375.2843 450.5276 -2.3402 420.8945 423.2347 375.0558 452.1514 -2.3355 420.6485 422.9840 374.8208 453.7600 -2.3332 420.4419 422.7751 374.5926 455.3631 -2.3294 420.2567 422.5861 374.4160 456.9768 -2.3226 420.0615 422.3841 374.2064 458.5646 -2.3154 419.8752 422.1906 373.9832 460.2039 -2.3137 419.6424 421.9561 373.7530 461.8123 -2.3117 419.4401 421.7518 373.5153 463.4208 -2.3134 419.2562 421.5696 373.3388 465.0294 -2.3109 419.0604 421.3713 373.1471 466.6376 -2.3091 418.8619 421.1710 372.9511 468.2463 -2.3062 418.6706 420.9768 372.7370 469.8549 -2.3041 418.4256 420.7297 372.5232 471.4788 -2.2956 418.2060 420.5017 372.2933 473.0821 -2.2952 417.9842 420.2795 372.1280 474.6959 -2.2919 417.7733 420.0653 371.8940 476.2991 -2.2884 417.5596 419.8480 371.7063 477.9026 -2.2830 417.3434 419.6264 371.4987 479.4959 -2.2773 417.1065 419.3839 371.2860 481.0786 -2.2734 416.9052 419.1785 371.0839 482.6821 -2.2699 416.6628 418.9327 370.9071 484.2959 -2.2649 416.4643 418.7292 370.7449 485.8990 -2.2601 416.3178 418.5778 370.5200 487.4974 -2.2536 416.1106 418.3642 370.3125 489.1059 -2.2522 415.8854 418.1376 370.1013 490.6939 -2.2449 415.6770 417.9219 369.9171 492.3025 -2.2391 415.4483 417.6875 369.7242 493.9110 -2.2334 415.2090 417.4425 369.5141 495.5195 -2.2300 414.9920 417.2220 369.2981 497.1435 -2.2251 414.7830 417.0081 369.0479 498.7518 -2.2232 414.5376 416.7608 368.8333 500.3553 -2.2190 414.3286 416.5476 368.6161 501.9689 -2.2167 414.1438 416.3605 368.3869 503.5721 -2.2133 413.9744 416.1877 368.1614 505.1808 -2.2080 413.7809 415.9889 367.9265 506.7840 -2.2110 413.5348 415.7458 367.7133 508.4181 -2.2034 413.3001 415.5034 367.5172 510.0265 -2.1975 413.1105 415.3080 367.3232 511.6350 -2.1920 412.9084 415.1004 367.0913 513.2385 -2.1901 412.7005 414.8905 366.8641 514.8468 -2.1838 412.5370 414.7208 366.6159 516.4554 -2.1837 412.3167 414.5005 366.3865 518.0639 -2.1776 412.0906 414.2682 366.1760 519.6826 -2.1759 411.8320 414.0079 365.9723 521.2963 -2.1656 411.5986 413.7642 365.7518 522.8841 -2.1666 411.4073 413.5738 365.5776 524.5131 -2.1628 411.1859 413.3488 365.3744 526.1164 -2.1615 410.9906 413.1521 365.1652 527.7145 -2.1544 410.7992 412.9536 364.9891 529.3230 -2.1544 410.6030 412.7574 364.7975 530.9314 -2.1514 410.3830 412.5344 364.5656 532.5503 -2.1460 410.1889 412.3349 364.3198 534.1639 -2.1405 409.9591 412.0995 364.0610 535.7671 -2.1392 409.7300 411.8693 363.8771 537.3806 -2.1370 409.4967 411.6338 363.6537 538.9840 -2.1318 409.2888 411.4206 363.4811 540.5978 -2.1297 409.1139 411.2436 363.2637 542.2011 -2.1272 408.8803 411.0075 363.0261 543.7839 -2.1199 408.6314 410.7513 362.8144 545.3976 -2.1120 408.4159 410.5279 362.6032 546.9958 -2.1077 408.2367 410.3444 362.4449 548.5941 -2.1015 408.0259 410.1275 362.2425 550.1924 -2.0969 407.8017 409.8986 362.0339 551.7855 -2.0893 407.6113 409.7005 361.8289 553.3890 -2.0848 407.3808 409.4656 361.6112 554.9975 -2.0885 407.1408 409.2293 361.3957 556.6008 -2.0849 406.9546 409.0394 361.1803 558.2196 -2.0864 406.7218 408.8082 360.9758 559.8280 -2.0912 406.4858 408.5770 360.7784 561.4314 -2.0799 406.2322 408.3121 360.5447 563.0399 -2.0761 406.0343 408.1104 360.2886 564.6329 -2.0784 405.8164 407.8948 360.1175 566.2413 -2.0736 405.6088 407.6824 359.8571 567.8445 -2.0701 405.3896 407.4597 359.6412 569.4583 -2.0724 405.1590 407.2314 359.4123 571.0770 -2.0642 404.9416 407.0059 359.1712 572.6855 -2.0545 404.7549 406.8094 358.9452 574.2993 -2.0470 404.5506 406.5976 358.7357 575.9075 -2.0410 404.3275 406.3684 358.5283 577.5110 -2.0395 404.1341 406.1736 358.3231 579.1246 -2.0356 403.9252 405.9608 358.1330 580.7279 -2.0328 403.6920 405.7248 357.9055 582.3569 -2.0267 403.4822 405.5090 357.6487 583.9603 -2.0248 403.2857 405.3106 357.4973 585.5738 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