DTA measure 2pbupdown4 Date: 20251022:102 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.99 s Mass = 959.300 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5199 0.0559 237.8451 237.7892 223.0132 4.1298 0.0678 237.9094 237.8416 222.6408 5.7336 0.0797 237.9179 237.8382 222.2996 7.3383 0.0914 237.9459 237.8545 221.9787 8.9481 0.1023 237.9610 237.8587 221.7515 10.5528 0.1089 237.9676 237.8588 221.4532 12.1618 0.1193 237.9944 237.8751 221.1618 13.7665 0.1277 237.9833 237.8556 220.8687 15.3764 0.1378 237.9925 237.8547 220.5476 16.9806 0.1489 238.0174 237.8685 220.3029 18.6003 0.1605 238.0628 237.9023 220.0175 20.2255 0.1708 238.0649 237.8941 219.7126 21.8303 0.1816 238.0611 237.8795 219.4026 23.4401 0.1861 238.0945 237.9084 219.1197 25.0440 0.1959 238.0933 237.8974 218.8846 26.6538 0.2038 238.0982 237.8944 218.6113 28.2739 0.2142 238.1027 237.8885 218.3826 29.8786 0.2225 238.1030 237.8806 218.1629 31.4928 0.2264 238.1201 237.8938 218.0376 33.0974 0.2344 238.1285 237.8942 217.9665 34.7073 0.2376 238.1552 237.9175 217.9898 36.3120 0.2447 238.1576 237.9129 218.0600 37.9215 0.2553 238.1348 237.8796 218.1942 39.5461 0.2586 238.1226 237.8640 218.4590 41.1560 0.2592 238.0921 237.8329 218.8275 42.7608 0.2596 238.0867 237.8270 219.2951 44.3701 0.2637 238.0906 237.8269 219.8213 45.9744 0.2614 238.0626 237.8012 220.3475 47.5894 0.2641 238.0205 237.7564 220.9110 49.1941 0.2674 238.0104 237.7430 221.4910 50.8031 0.2744 238.0171 237.7427 222.0356 52.3821 0.2721 238.0008 237.7287 222.5371 53.9818 0.2650 238.0069 237.7420 222.9503 55.5810 0.2570 238.0186 237.7616 223.3220 57.1800 0.2523 238.0310 237.7787 223.6106 58.7796 0.2554 238.0009 237.7455 223.8604 60.3895 0.2564 237.9702 237.7138 224.0694 61.9883 0.2536 237.9720 237.7184 224.2104 63.5929 0.2538 237.9825 237.7287 224.2872 65.2028 0.2501 237.9387 237.6886 224.3073 66.8069 0.2466 237.9275 237.6808 224.2900 68.4164 0.2430 237.9025 237.6595 224.2942 70.0211 0.2405 237.8859 237.6454 224.2471 71.6358 0.2359 237.8696 237.6338 224.2353 73.2399 0.2326 237.8793 237.6467 224.2116 74.8498 0.2309 237.8313 237.6005 224.1879 76.4386 0.2289 237.8413 237.6124 224.2194 78.0583 0.2292 237.8518 237.6226 224.2163 79.6681 0.2282 237.8649 237.6367 224.2974 81.2779 0.2245 237.8602 237.6357 224.4561 82.8869 0.2235 237.8132 237.5897 224.6397 84.4916 0.2171 237.7742 237.5571 224.8801 86.1013 0.2139 237.7695 237.5555 225.1463 87.7053 0.2090 237.7829 237.5739 225.5019 89.3305 0.2053 237.7689 237.5636 225.8808 90.9353 0.2028 237.8111 237.6083 226.2840 92.5340 0.2035 237.8219 237.6184 226.6876 94.1386 0.1999 237.8392 237.6393 227.1141 95.7434 0.1964 237.8748 237.6784 227.5134 97.3584 0.1941 237.8725 237.6784 227.9009 98.9628 0.1888 237.8814 237.6926 228.2884 100.5720 0.1843 237.9185 237.7342 228.6304 102.1921 0.1786 237.8561 237.6775 228.9010 103.8020 0.1720 237.8569 237.6850 229.1599 105.4065 0.1689 237.8329 237.6639 229.3597 107.0156 0.1647 237.8108 237.6462 229.4988 108.6204 0.1598 237.8015 237.6417 229.6376 110.2301 0.1528 237.7934 237.6406 229.7313 111.8391 0.1477 237.8090 237.6614 229.7649 113.4285 0.1453 237.8099 237.6647 229.7965 115.0486 0.1395 237.8464 237.7069 229.8309 116.6431 0.1327 237.8804 237.7477 229.8019 118.2369 0.1336 237.9238 237.7902 229.8323 119.8363 0.1328 237.9565 237.8237 229.8907 121.4359 0.1317 237.9827 237.8510 229.9663 123.0400 0.1239 238.0098 237.8860 230.0822 124.6393 0.1256 238.0454 237.9199 230.2120 126.2491 0.1207 238.0280 237.9072 230.4343 127.8533 0.1125 238.0231 237.9106 230.7053 129.4576 0.1082 238.0776 237.9695 230.9763 131.0675 0.1057 238.1106 238.0049 231.3228 132.6715 0.1061 238.1812 238.0750 231.6936 134.2811 0.1008 238.2238 238.1230 232.0997 135.8859 0.0976 238.2302 238.1326 232.5239 137.4950 0.0957 238.2529 238.1572 232.8822 139.1149 0.0880 238.2941 238.2061 233.2592 140.7248 0.0829 238.3160 238.2331 233.6132 142.3341 0.0801 238.3784 238.2983 233.9426 143.9384 0.0786 238.4053 238.3266 234.2242 145.5534 0.0768 238.4550 238.3781 234.4469 147.1581 0.0705 238.4453 238.3748 234.6615 148.7671 0.0680 238.4674 238.3994 234.8058 150.3871 0.0644 238.4543 238.3899 234.8924 151.9970 0.0651 238.5119 238.4468 235.0071 153.6018 0.0621 238.5679 238.5058 235.0640 155.2116 0.0589 238.6034 238.5445 235.1105 156.8211 0.0542 238.5962 238.5420 235.1715 158.4304 0.0476 238.6237 238.5761 235.2383 160.0351 0.0467 238.7029 238.6563 235.3131 161.6550 0.0495 238.7429 238.6934 235.3619 163.2641 0.0501 238.8141 238.7640 235.4601 164.8689 0.0502 238.9080 238.8579 235.5930 166.4836 0.0472 238.9512 238.9040 235.7614 168.0774 0.0442 238.9934 238.9492 235.9709 169.6873 0.0425 239.0795 239.0370 236.2489 171.2920 0.0443 239.1254 239.0812 236.5662 172.9060 0.0426 239.1972 239.1545 236.8698 174.5261 0.0366 239.2924 239.2558 237.1842 176.1360 0.0371 239.4287 239.3916 237.4974 177.7451 0.0373 239.4817 239.4444 237.8637 179.3394 0.0336 239.4959 239.4623 238.2480 180.9288 0.0341 239.5274 239.4933 238.6195 182.5233 0.0298 239.6018 239.5720 238.9510 184.1220 0.0266 239.6963 239.6697 239.2721 185.7164 0.0258 239.7703 239.7444 239.5485 187.3058 0.0259 239.8474 239.8215 239.8175 188.9259 0.0190 239.8920 239.8730 240.0240 190.5246 0.0156 239.9482 239.9326 240.2037 192.1344 0.0202 240.0197 239.9995 240.3758 193.7340 0.0114 240.0968 240.0855 240.4631 195.3381 0.0082 240.1869 240.1787 240.5451 196.9476 0.0071 240.2423 240.2352 240.6015 198.5370 -0.0008 240.3434 240.3442 240.6502 200.1464 0.0026 240.4321 240.4295 240.6917 201.7660 0.0038 240.4897 240.4859 240.7574 203.3759 0.0006 240.5395 240.5389 240.8424 204.9800 0.0025 240.5998 240.5973 240.9732 206.5895 0.0047 240.6426 240.6379 241.1093 208.1840 0.0077 240.7553 240.7476 241.2536 209.7886 0.0047 240.8674 240.8627 241.4693 211.3976 0.0036 240.9835 240.9799 241.7138 213.0024 0.0083 241.0768 241.0685 241.9896 214.6273 0.0098 241.1585 241.1487 242.3110 216.2314 0.0078 241.2387 241.2309 242.6380 217.8464 0.0063 241.2881 241.2818 242.9773 219.4510 0.0019 241.3742 241.3723 243.3408 221.0651 -0.0004 241.4714 241.4718 243.7370 222.6699 -0.0025 241.5561 241.5585 244.1307 224.2798 -0.0015 241.6475 241.6490 244.4470 225.8990 -0.0044 241.7708 241.7752 244.7304 227.5036 -0.0032 241.8818 241.8850 245.0017 229.1186 -0.0042 241.9882 241.9924 245.2298 230.7229 -0.0068 242.0909 242.0977 245.4671 232.3323 -0.0102 242.2498 242.2601 245.6378 233.9216 -0.0097 242.3544 242.3642 245.7555 235.5469 -0.0137 242.4313 242.4450 245.8793 237.1506 -0.0107 242.5342 242.5449 245.9788 238.7759 -0.0180 242.6478 242.6659 246.0369 240.3858 -0.0205 242.7510 242.7715 246.0920 241.9950 -0.0223 242.8772 242.8996 246.1552 243.5994 -0.0196 242.9685 242.9881 246.2397 245.1990 -0.0182 243.0912 243.1094 246.3070 246.7986 -0.0187 243.2034 243.2220 246.3920 248.3823 -0.0167 243.2985 243.3152 246.5455 249.9969 -0.0113 243.4203 243.4316 246.7365 251.5965 -0.0055 243.5859 243.5914 246.9418 253.1851 -0.0011 243.6836 243.6846 247.1886 254.7845 0.0033 243.7626 243.7594 247.4667 256.3893 0.0023 243.8471 243.8448 247.7774 257.9988 0.0045 243.9538 243.9494 248.1487 259.6029 0.0023 244.0816 244.0793 248.4978 261.2128 -0.0015 244.2001 244.2016 248.8499 262.8021 -0.0046 244.3597 244.3643 249.1958 264.4215 -0.0058 244.4924 244.4982 249.5547 266.0311 -0.0061 244.5688 244.5749 249.9116 267.6410 -0.0092 244.7087 244.7179 250.2565 269.2406 -0.0099 244.8398 244.8497 250.5359 270.8451 -0.0045 245.0094 245.0139 250.7675 272.4543 -0.0000 245.1559 245.1559 251.0021 274.0590 0.0045 245.2896 245.2851 251.1713 275.6689 0.0039 245.4299 245.4260 251.3108 277.2884 0.0000 245.5811 245.5810 251.4288 278.8979 -0.0034 245.7209 245.7243 251.5056 280.5026 -0.0002 245.7979 245.7981 251.5538 282.1071 -0.0007 245.9219 245.9225 251.6214 283.7009 -0.0019 246.0493 246.0512 251.6693 285.3056 0.0035 246.1970 246.1935 251.6874 286.9155 0.0029 246.3345 246.3316 251.8060 288.5199 0.0046 246.4658 246.4612 251.9351 290.1445 0.0028 246.6240 246.6211 252.0198 291.7493 -0.0007 246.7331 246.7338 252.1380 293.3638 0.0031 246.8362 246.8332 252.4045 294.9680 0.0042 247.0244 247.0201 252.7100 296.5830 0.0073 247.1902 247.1828 253.0131 298.1874 0.0037 247.3193 247.3156 253.2795 299.7915 0.0060 247.4626 247.4565 253.6208 301.3860 0.0107 247.6395 247.6288 254.0709 303.0113 0.0097 247.8242 247.8144 254.4418 304.6201 0.0094 247.9560 247.9466 254.7977 306.2249 0.0092 248.0910 248.0818 255.1770 307.8348 0.0019 248.2195 248.2176 255.5547 309.4391 0.0043 248.4040 248.3997 255.8345 311.0330 0.0118 248.5813 248.5696 256.1151 312.6326 0.0166 248.7104 248.6937 256.3941 314.2476 0.0199 248.8632 248.8433 256.5490 315.8258 0.0174 249.0251 249.0077 256.6694 317.4408 0.0155 249.1603 249.1447 256.7955 319.0250 0.0176 249.3218 249.3042 256.8600 320.6298 0.0160 249.5125 249.4964 256.8989 322.2335 0.0146 249.7154 249.7008 256.9269 323.8434 0.0124 249.8697 249.8572 256.9674 325.4481 0.0179 250.0267 250.0088 257.0030 327.0629 0.0226 250.1718 250.1492 257.0956 328.6720 0.0267 250.3179 250.2911 257.1695 330.2768 0.0228 250.4908 250.4680 257.2924 331.8866 0.0223 250.6024 250.5801 257.4689 333.4908 0.0225 250.7122 250.6897 257.6770 335.0951 0.0259 250.8634 250.8375 257.8967 336.7050 0.0291 251.0442 251.0151 258.1831 338.3251 0.0265 251.2296 251.2031 258.5172 339.9344 0.0242 251.4161 251.3919 258.9052 341.5439 0.0288 251.5625 251.5337 259.3281 343.1538 0.0321 251.7194 251.6872 259.7422 344.7576 0.0366 251.9027 251.8661 260.1455 346.3674 0.0342 252.0969 252.0627 260.5101 347.9720 0.0327 252.2896 252.2569 260.8687 349.6015 0.0346 252.4376 252.4030 261.2230 351.2063 0.0309 252.6409 252.6100 261.4909 352.8108 0.0289 252.8096 252.7806 261.7522 354.4250 0.0295 252.9762 252.9468 261.9580 356.0298 0.0292 253.1801 253.1509 262.0849 357.6396 0.0274 253.3462 253.3188 262.1848 359.2434 0.0284 253.5091 253.4807 262.2377 360.8686 0.0294 253.7057 253.6763 262.2713 362.4785 0.0304 253.8900 253.8596 262.3080 364.0878 0.0315 254.0795 254.0480 262.3484 365.6921 0.0343 254.2549 254.2206 262.3667 367.3020 0.0373 254.3996 254.3623 262.4026 368.9066 0.0392 254.5853 254.5462 262.4533 370.5156 0.0366 254.7715 254.7349 262.5673 372.1409 0.0371 254.9254 254.8883 262.7154 373.7354 0.0360 255.1106 255.0746 262.8912 375.3391 0.0377 255.2807 255.2429 263.1427 376.9285 0.0390 255.4577 255.4187 263.4326 378.5279 0.0416 255.6413 255.5997 263.7927 380.1216 0.0444 255.8115 255.7671 264.1659 381.7161 0.0443 255.9626 255.9183 264.5334 383.3158 0.0455 256.1590 256.1135 265.0180 384.9144 0.0465 256.3524 256.3059 265.4513 386.5396 0.0455 256.5415 256.4960 265.9074 388.1290 0.0461 256.7565 256.7104 266.2590 389.7286 0.0418 256.9748 256.9330 266.6263 391.3375 0.0431 257.1595 257.1164 266.8946 392.9423 0.0405 257.3429 257.3024 267.1251 394.5521 0.0410 257.4658 257.4248 267.3170 396.1561 0.0395 257.6596 257.6201 267.4183 397.7658 0.0369 257.8391 257.8022 267.5306 399.3859 0.0358 258.0647 258.0289 267.5785 400.9746 0.0333 258.2391 258.2058 267.5668 402.5841 0.0310 258.4126 258.3816 267.5794 404.1940 0.0325 258.6061 258.5736 267.5090 405.8036 0.0350 258.8071 258.7722 267.5137 407.4076 0.0328 258.9971 258.9644 267.5306 409.0175 0.0321 259.2048 259.1727 267.6140 410.6223 0.0364 259.3800 259.3436 267.7170 412.2473 0.0393 259.5874 259.5481 267.8883 413.8513 0.0388 259.7947 259.7559 268.1616 415.4560 0.0438 260.0076 259.9638 268.4495 417.0659 0.0496 260.1716 260.1220 268.7844 418.6704 0.0522 260.3503 260.2981 269.1618 420.2949 0.0517 260.5209 260.4692 269.5717 421.9150 0.0506 260.6831 260.6325 270.0228 423.5249 0.0521 260.8726 260.8205 270.4885 425.1290 0.0458 261.1038 261.0580 270.9261 426.7385 0.0438 261.2970 261.2532 271.3249 428.3484 0.0394 261.4410 261.4016 271.7281 429.9531 0.0434 261.6341 261.5907 272.0935 431.5626 0.0440 261.9013 261.8573 272.3606 433.1821 0.0458 262.1220 262.0762 272.5092 434.7920 0.0418 262.3169 262.2751 272.6898 436.3968 0.0409 262.5480 262.5071 272.8019 438.0065 0.0397 262.7582 262.7185 272.8172 439.6053 0.0384 262.9773 262.9389 272.8336 441.2049 0.0381 263.1804 263.1423 272.8277 442.7994 0.0338 263.4046 263.3707 272.8175 444.3831 0.0393 263.5852 263.5459 272.7615 446.0130 0.0449 263.7854 263.7404 272.7138 447.6178 0.0441 263.9988 263.9547 272.7177 449.2020 0.0393 264.2410 264.2017 272.8224 450.8059 0.0352 264.4571 264.4220 272.9461 452.4105 0.0360 264.6387 264.6027 273.1112 454.0204 0.0397 264.8454 264.8058 273.3432 455.6243 0.0432 265.0532 265.0100 273.6419 457.2443 0.0447 265.2668 265.2221 274.0244 458.8541 0.0450 265.4294 265.3845 274.4651 460.4584 0.0416 265.5983 265.5567 274.9626 462.0678 0.0399 265.7633 265.7235 275.4590 463.6725 0.0431 265.9653 265.9222 275.9247 465.2820 0.0398 266.1456 266.1058 276.3900 466.8861 0.0381 266.3100 266.2720 276.8013 468.5063 0.0350 266.5515 266.5165 277.1583 470.1161 0.0340 266.8101 266.7761 277.4805 471.7203 0.0325 267.0574 267.0249 277.7445 473.3246 0.0315 267.2469 267.2155 277.9104 474.9550 0.0296 267.4348 267.4052 278.0434 476.5596 0.0282 267.6644 267.6362 278.1092 478.1738 0.0301 267.8765 267.8464 278.1187 479.7785 0.0295 268.0904 268.0609 278.0719 481.4038 0.0297 268.3078 268.2782 278.0448 483.0131 0.0325 268.5142 268.4817 278.0314 484.6225 0.0334 268.7039 268.6704 277.9674 486.2273 0.0326 268.8910 268.8583 277.9891 487.8365 0.0303 269.1074 269.0771 278.0372 489.4409 0.0320 269.3117 269.2797 278.1146 491.0508 0.0268 269.5275 269.5007 278.2583 492.6709 0.0287 269.7158 269.6871 278.4759 494.2753 0.0290 269.9390 269.9100 278.8007 495.8896 0.0300 270.1580 270.1280 279.1396 497.4944 0.0250 270.3861 270.3611 279.5051 499.1039 0.0264 270.5730 270.5466 279.9288 500.7131 0.0287 270.7748 270.7462 280.3745 502.3230 0.0289 270.9845 270.9556 280.8314 503.9431 0.0254 271.2502 271.2249 281.3071 505.5426 0.0217 271.4617 271.4400 281.7345 507.1260 0.0235 271.6553 271.6319 282.1244 508.7205 0.0145 271.8743 271.8599 282.4781 510.3096 0.0064 272.1119 272.1055 282.7799 511.9085 0.0026 272.2947 272.2921 282.9966 513.5133 0.0055 272.5439 272.5385 283.1367 515.1121 0.0062 272.7589 272.7527 283.2444 516.7218 0.0070 273.0083 273.0013 283.2492 518.3265 0.0083 273.1626 273.1543 283.2589 519.9309 0.0072 273.3542 273.3470 283.2453 521.5401 0.0092 273.5852 273.5760 283.1851 523.1449 0.0133 273.8370 273.8237 283.1889 524.7544 0.0123 274.0415 274.0292 283.1762 526.3585 0.0094 274.2434 274.2340 283.2250 527.9684 0.0102 274.4748 274.4646 283.2600 529.5729 0.0103 274.7373 274.7270 283.3905 531.1923 0.0091 274.9574 274.9483 283.5571 532.8021 0.0104 275.1845 275.1741 283.8276 534.4069 0.0078 275.3873 275.3795 284.1416 536.0163 0.0072 275.5873 275.5801 284.5107 537.6205 0.0053 275.8039 275.7986 284.9436 539.2304 0.0023 276.0069 276.0046 285.4061 540.8350 0.0039 276.2039 276.2000 285.8345 542.4594 -0.0016 276.3859 276.3874 286.3048 544.0693 -0.0029 276.6468 276.6497 286.7387 545.6740 -0.0058 276.8981 276.9038 287.1450 547.2833 -0.0112 277.1515 277.1627 287.5455 548.8876 -0.0125 277.3499 277.3624 287.8408 550.4975 -0.0174 277.5643 277.5817 288.0571 552.1023 -0.0198 277.7720 277.7918 288.2719 553.7266 -0.0197 277.9604 277.9801 288.4058 555.3313 -0.0213 278.1538 278.1751 288.4769 556.9360 -0.0214 278.4039 278.4252 288.4768 558.5609 -0.0238 278.6528 278.6766 288.4595 560.1701 -0.0234 278.8845 278.9079 288.4125 561.7646 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293.6438 598.6874 -0.0720 284.2944 284.3665 293.6501 600.2921 -0.0749 284.5152 284.5901 293.6235 601.9123 -0.0725 284.7196 284.7921 293.5909 603.5214 -0.0735 284.9340 285.0075 293.5274 605.1259 -0.0764 285.1620 285.2384 293.5357 606.7409 -0.0773 285.4093 285.4866 293.5689 608.3455 -0.0750 285.6442 285.7192 293.6929 609.9545 -0.0800 285.8634 285.9434 293.8996 611.5593 -0.0825 286.0543 286.1368 294.2235 613.1896 -0.0870 286.2356 286.3226 294.5899 614.7935 -0.0871 286.4900 286.5771 294.9965 616.4033 -0.0908 286.7135 286.8042 295.4633 618.0080 -0.0957 286.9479 287.0435 295.9421 619.6223 -0.0946 287.2221 287.3167 296.4620 621.2114 -0.0985 287.4352 287.5338 296.9431 622.8161 -0.0943 287.6557 287.7500 297.4024 624.4251 -0.0955 287.9091 288.0046 297.8015 626.0605 -0.1003 288.1059 288.2062 298.1706 627.6704 -0.1092 288.3205 288.4297 298.4784 629.2598 -0.1122 288.5515 288.6637 298.6798 630.8696 -0.1128 288.7793 288.8921 298.8123 632.4898 -0.1116 289.0332 289.1448 298.8621 634.0786 -0.1094 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