DTA measure 1fazisatalakulas Date: 2025923:154 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.03 s Mass = 1333.800 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3128 -0.3637 235.9082 236.2719 275.6311 2.1408 -0.3700 236.1726 236.5426 275.6729 2.9380 -0.3734 236.4644 236.8378 275.6969 3.7353 -0.3699 236.7265 237.0964 275.6789 4.5633 -0.3701 236.9645 237.3346 275.6378 5.3188 -0.3720 237.2306 237.6026 275.5540 6.1875 -0.3730 237.5044 237.8774 275.4298 6.9335 -0.3676 237.7717 238.1393 275.3445 7.7820 -0.3663 238.0589 238.4253 275.1763 8.5485 -0.3663 238.3131 238.6794 275.0273 9.3765 -0.3678 238.6134 238.9812 274.8537 10.1738 -0.3704 238.8767 239.2471 274.7125 10.9700 -0.3689 239.1459 239.5148 274.5425 11.7878 -0.3683 239.4161 239.7844 274.3463 12.5645 -0.3713 239.6893 240.0606 274.2143 13.3823 -0.3703 239.9696 240.3399 274.0809 14.1488 -0.3674 240.2071 240.5745 273.9484 15.0073 -0.3658 240.4944 240.8602 273.8357 15.7730 -0.3688 240.7235 241.0923 273.7403 16.6010 -0.3687 240.9645 241.3332 273.6819 17.3983 -0.3693 241.2014 241.5708 273.6095 18.1955 -0.3666 241.4399 241.8065 273.5897 19.0235 -0.3631 241.6898 242.0530 273.6351 19.7893 -0.3587 241.8936 242.2523 273.6753 20.6068 -0.3542 242.1687 242.5229 273.7947 21.3835 -0.3492 242.4141 242.7633 273.9371 22.2320 -0.3460 242.6465 242.9925 274.1151 22.9985 -0.3466 242.8704 243.2171 274.3292 23.8265 -0.3432 243.1219 243.4651 274.6303 24.6230 -0.3471 243.3612 243.7083 274.9261 25.4200 -0.3498 243.5645 243.9143 275.2560 26.2378 -0.3480 243.7847 244.1328 275.6494 27.0145 -0.3482 244.0150 244.3632 276.0448 27.8630 -0.3526 244.2863 244.6389 276.4671 28.6398 -0.3524 244.4982 244.8506 276.8738 29.4575 -0.3556 244.7205 245.0761 277.3368 30.2640 -0.3564 244.9466 245.3030 277.8059 31.0510 -0.3591 245.1993 245.5584 278.2336 31.8790 -0.3656 245.4529 245.8184 278.6571 32.6455 -0.3716 245.6638 246.0354 279.0365 33.5043 -0.3742 245.9208 246.2950 279.4743 34.2708 -0.3760 246.1370 246.5130 279.8567 35.0883 -0.3808 246.3527 246.7336 280.2054 35.8950 -0.3879 246.5907 246.9786 280.5126 36.6820 -0.3916 246.8150 247.2066 280.7885 37.4895 -0.3956 247.0840 247.4796 281.0528 38.2868 -0.4009 247.3192 247.7201 281.2884 39.1148 -0.4061 247.5566 247.9627 281.4984 39.8805 -0.4173 247.7587 248.1760 281.6425 40.7390 -0.4239 248.0185 248.4425 281.7536 41.4953 -0.4252 248.2177 248.6429 281.8241 42.3335 -0.4299 248.4450 248.8748 281.8787 43.1205 -0.4360 248.6492 249.0852 281.9063 43.9178 -0.4369 248.8832 249.3201 281.8824 44.7448 -0.4408 249.1359 249.5767 281.8392 45.5010 -0.4462 249.3755 249.8216 281.7796 46.3188 -0.4530 249.6155 250.0684 281.7165 47.0955 -0.4618 249.8254 250.2871 281.6265 47.9440 -0.4686 250.0508 250.5195 281.5103 48.6995 -0.4717 250.2678 250.7395 281.4263 49.5273 -0.4698 250.5242 250.9939 281.2751 50.3143 -0.4753 250.7537 251.2290 281.1309 51.1115 -0.4790 250.9661 251.4451 280.9977 51.9395 -0.4796 251.2125 251.6921 280.8760 52.6955 -0.4768 251.4215 251.8983 280.7539 53.5540 -0.4777 251.6710 252.1487 280.6432 54.2893 -0.4796 251.8796 252.3591 280.5327 55.1378 -0.4793 252.1404 252.6197 280.4497 55.9043 -0.4773 252.3588 252.8361 280.3844 56.7323 -0.4738 252.5780 253.0518 280.3812 57.5193 -0.4726 252.7717 253.2444 280.3948 58.3160 -0.4688 252.9969 253.4657 280.4288 59.1435 -0.4662 253.2385 253.7047 280.4394 59.9100 -0.4672 253.4140 253.8812 280.4970 60.7585 -0.4694 253.6115 254.0809 280.6582 61.5353 -0.4704 253.7878 254.2583 280.8334 62.3530 -0.4752 254.0216 254.4967 281.0663 63.1503 -0.4782 254.2486 254.7268 281.3361 63.9475 -0.4820 254.4328 254.9148 281.6145 64.7643 -0.4847 254.6417 255.1264 281.9106 65.5308 -0.4870 254.8643 255.3514 282.2249 66.3895 -0.4901 255.1202 255.6102 282.6561 67.1560 -0.4915 255.3324 255.8239 283.0237 67.9943 -0.4978 255.5459 256.0437 283.4157 68.7290 -0.5004 255.7524 256.2529 283.7713 69.5878 -0.5088 255.9632 256.4720 284.2103 70.3543 -0.5121 256.1620 256.6741 284.6521 71.1720 -0.5212 256.3569 256.8781 285.0941 71.9795 -0.5290 256.5865 257.1154 285.4931 72.7665 -0.5372 256.7873 257.3245 285.8655 73.6043 -0.5500 256.9989 257.5488 286.2185 74.3600 -0.5551 257.1951 257.7502 286.5395 75.2188 -0.5610 257.4107 257.9717 286.8840 75.9853 -0.5683 257.6322 258.2004 287.1393 76.8133 -0.5782 257.8178 258.3959 287.3835 77.6105 -0.5855 258.0158 258.6012 287.5833 78.4180 -0.5914 258.2443 258.8357 287.7573 79.2143 -0.5972 258.4658 259.0631 287.8786 80.0115 -0.6004 258.6680 259.2684 287.9825 80.8088 -0.6062 258.8599 259.4661 288.0698 81.6060 -0.6131 259.0769 259.6900 288.1264 82.4238 -0.6156 259.2831 259.8987 288.2019 83.2005 -0.6192 259.4747 260.0939 288.1952 84.0483 -0.6247 259.7436 260.3683 288.1491 84.8145 -0.6316 259.9402 260.5718 288.1140 85.6425 -0.6381 260.1450 260.7831 288.0579 86.4398 -0.6448 260.3281 260.9729 287.9619 87.2370 -0.6533 260.5174 261.1708 287.8744 88.0650 -0.6620 260.7315 261.3934 287.7742 88.8515 -0.6654 260.9451 261.6105 287.6797 89.6790 -0.6681 261.1649 261.8330 287.5259 90.4455 -0.6685 261.3602 262.0287 287.4308 91.3043 -0.6729 261.5743 262.2471 287.3367 92.0400 -0.6741 261.7732 262.4473 287.2611 92.8885 -0.6774 261.9757 262.6532 287.1543 93.6653 -0.6771 262.1492 262.8262 287.0718 94.4825 -0.6766 262.3529 263.0295 287.0321 95.2793 -0.6794 262.5352 263.2147 287.0141 96.0765 -0.6797 262.7542 263.4339 286.9868 96.9045 -0.6869 262.9209 263.6078 286.9955 97.6710 -0.6920 263.1172 263.8092 287.0378 98.5195 -0.6964 263.3379 264.0344 287.1390 99.2963 -0.7014 263.5295 264.2309 287.2684 100.1138 -0.6995 263.7611 264.4606 287.4206 100.9103 -0.6949 263.9669 264.6618 287.6075 101.7075 -0.6981 264.1461 264.8442 287.8219 102.5355 -0.7026 264.3520 265.0547 288.0984 103.3020 -0.7097 264.5397 265.2495 288.3651 104.1505 -0.7145 264.7547 265.4692 288.6614 104.9273 -0.7162 264.9161 265.6322 288.9769 105.7445 -0.7162 265.0775 265.7938 289.3609 106.5413 -0.7232 265.3003 266.0235 289.6895 107.3385 -0.7328 265.5128 266.2456 290.0791 108.1665 -0.7378 265.7143 266.4520 290.5035 108.9330 -0.7455 265.8704 266.6159 290.9040 109.7608 -0.7531 266.0676 266.8206 291.2696 110.5265 -0.7582 266.2644 267.0225 291.5947 111.3853 -0.7670 266.4913 267.2583 291.9828 112.1415 -0.7737 266.6562 267.4299 292.2899 112.9695 -0.7851 266.8470 267.6321 292.6050 113.7668 -0.7946 267.0715 267.8661 292.8879 114.5535 -0.7996 267.2634 268.0630 293.1718 115.3808 -0.8081 267.4510 268.2591 293.4164 116.1473 -0.8142 267.5851 268.3993 293.6023 116.9958 -0.8196 267.7456 268.5653 293.7843 117.7315 -0.8206 267.9216 268.7421 293.9463 118.5903 -0.8283 268.1601 268.9884 294.0685 119.3558 -0.8352 268.3558 269.1910 294.1541 120.1838 -0.8418 268.5305 269.3722 294.2195 120.9810 -0.8506 268.7001 269.5507 294.2897 121.7680 -0.8586 268.9033 269.7619 294.3197 122.5960 -0.8641 269.1243 269.9884 294.3152 123.3625 -0.8693 269.2823 270.1516 294.3162 124.2105 -0.8744 269.4832 270.3576 294.2560 124.9765 -0.8791 269.6729 270.5521 294.1937 125.8045 -0.8818 269.8604 270.7422 294.1662 126.6018 -0.8872 270.0474 270.9346 294.0891 127.3990 -0.8956 270.2195 271.1152 294.0139 128.2168 -0.9015 270.3784 271.2799 293.9222 128.9823 -0.9022 270.5744 271.4766 293.8772 129.8410 -0.9046 270.7848 271.6894 293.7859 130.5973 -0.9077 270.9470 271.8547 293.7134 131.4355 -0.9114 271.1625 272.0739 293.6581 132.1918 -0.9144 271.3295 272.2439 293.6302 133.0095 -0.9137 271.5070 272.4207 293.6030 133.8170 -0.9158 271.6917 272.6075 293.5955 134.6033 -0.9154 271.8583 272.7737 293.6348 135.4310 -0.9184 272.0564 272.9748 293.6496 136.1975 -0.9192 272.2569 273.1761 293.6971 137.0563 -0.9231 272.4544 273.3775 293.7990 137.8228 -0.9256 272.6688 273.5945 293.9142 138.6405 -0.9287 272.9160 273.8448 294.0453 139.4370 -0.9374 273.0908 274.0282 294.2125 140.2340 -0.9401 273.2166 274.1567 294.3958 141.0518 -0.9463 273.3683 274.3146 294.6059 141.8285 -0.9481 273.5379 274.4860 294.8337 142.6770 -0.9518 273.7257 274.6775 295.1296 143.4435 -0.9565 273.8866 274.8431 295.4180 144.2715 -0.9660 274.0787 275.0448 295.7285 145.0688 -0.9707 274.2707 275.2413 296.0284 145.8658 -0.9713 274.4631 275.4345 296.3963 146.6828 -0.9770 274.6189 275.5959 296.7748 147.4595 -0.9830 274.7557 275.7388 297.1039 148.3080 -0.9923 274.9751 275.9675 297.4294 149.0745 -0.9930 275.1796 276.1727 297.7818 149.9128 -0.9965 275.3585 276.3550 298.1288 150.6895 -1.0021 275.5379 276.5400 298.4519 151.5165 -1.0032 275.7010 276.7042 298.7669 152.3138 -1.0114 275.8694 276.8808 299.0655 153.1110 -1.0242 276.0338 277.0580 299.3220 153.9390 -1.0422 276.2518 277.2941 299.5517 154.7055 -1.0521 276.4535 277.5056 299.7614 155.5540 -1.0583 276.6160 277.6744 299.9324 156.3203 -1.0645 276.7449 277.8094 300.1112 157.1475 -1.0620 276.9251 277.9870 300.2561 157.9448 -1.0617 277.1222 278.1839 300.3731 158.7420 -1.0654 277.3063 278.3717 300.4789 159.5598 -1.0690 277.4829 278.5519 300.4987 160.3365 -1.0757 277.6496 278.7253 300.5092 161.1850 -1.0751 277.8186 278.8937 300.5447 161.9508 -1.0784 277.9669 279.0453 300.5816 162.7785 -1.0863 278.1153 279.2017 300.5789 163.5553 -1.0902 278.3115 279.4017 300.5619 164.3730 -1.0946 278.5329 279.6275 300.5396 165.1703 -1.0975 278.7377 279.8353 300.4805 165.9675 -1.1003 278.9055 280.0058 300.4484 166.7945 -1.1039 279.1111 280.2150 300.4220 167.5610 -1.1071 279.2973 280.4044 300.3396 168.4095 -1.1088 279.4646 280.5734 300.3015 169.1863 -1.1166 279.6522 280.7688 300.2833 170.0040 -1.1211 279.8099 280.9311 300.2423 170.8105 -1.1241 279.9793 281.1034 300.2060 171.6078 -1.1255 280.1653 281.2908 300.1720 172.4358 -1.1247 280.3464 281.4711 300.1487 173.1920 -1.1229 280.4893 281.6121 300.1670 174.0405 -1.1252 280.6621 281.7873 300.2160 174.7855 -1.1296 280.8171 281.9467 300.2560 175.6340 -1.1372 280.9905 282.1277 300.3470 176.3903 -1.1375 281.1624 282.2999 300.4368 177.2183 -1.1365 281.3379 282.4744 300.5435 178.0155 -1.1336 281.5118 282.6453 300.6895 178.8025 -1.1335 281.6507 282.7842 300.8476 179.6305 -1.1343 281.8406 282.9749 301.0251 180.3960 -1.1392 281.9800 283.1192 301.2274 181.2343 -1.1462 282.1437 283.2899 301.4937 181.9905 -1.1489 282.3222 283.4710 301.7421 182.8493 -1.1568 282.5113 283.6681 302.0481 183.6158 -1.1620 282.6842 283.8462 302.3540 184.4333 -1.1675 282.8428 284.0102 302.6863 185.2298 -1.1710 282.9897 284.1607 302.9980 186.0270 -1.1775 283.1426 284.3201 303.3206 186.8448 -1.1851 283.3029 284.4880 303.6949 187.6113 -1.1879 283.4825 284.6705 304.0234 188.4393 -1.1953 283.6664 284.8617 304.3490 189.1955 -1.2024 283.8208 285.0232 304.6414 190.0643 -1.2065 283.9987 285.2052 304.9927 190.7890 -1.2107 284.1636 285.3743 305.2722 191.6785 -1.2163 284.3651 285.5814 305.5521 192.4348 -1.2225 284.5204 285.7429 305.7702 193.2628 -1.2300 284.7095 285.9396 305.9612 194.0600 -1.2317 284.8889 286.1206 306.1541 194.8470 -1.2346 285.0755 286.3101 306.3264 195.6440 -1.2365 285.2288 286.4653 306.4585 196.4405 -1.2436 285.3805 286.6241 306.5846 197.2685 -1.2518 285.5468 286.7986 306.7139 198.0350 -1.2593 285.6827 286.9421 306.7962 198.8835 -1.2662 285.8807 287.1470 306.8596 199.6603 -1.2704 286.0661 287.3366 306.9116 200.4883 -1.2786 286.2838 287.5624 306.9334 201.2650 -1.2832 286.4351 287.7183 306.9166 202.0920 -1.2899 286.6035 287.8934 306.9157 202.8585 -1.2940 286.7633 288.0573 306.9083 203.6865 -1.2939 286.9215 288.2154 306.8632 204.4838 -1.2956 287.0675 288.3631 306.7990 205.2810 -1.3005 287.2187 288.5192 306.7465 206.0988 -1.3089 287.3987 288.7076 306.7010 206.8753 -1.3113 287.5947 288.9059 306.6820 207.7230 -1.3167 287.8069 289.1236 306.6178 208.4895 -1.3196 287.9615 289.2811 306.5607 209.3175 -1.3214 288.1454 289.4669 306.5317 210.1148 -1.3254 288.3342 289.6596 306.5550 210.9120 -1.3286 288.5188 289.8474 306.5637 211.7195 -1.3280 288.6811 290.0091 306.5904 212.5270 -1.3287 288.8024 290.1311 306.6426 213.3438 -1.3390 288.9548 290.2938 306.6915 214.1205 -1.3383 289.0864 290.4247 306.7481 214.9485 -1.3395 289.2484 290.5880 306.8348 215.7150 -1.3398 289.4120 290.7518 306.9757 216.5635 -1.3372 289.5812 290.9184 307.1176 217.3403 -1.3386 289.7349 291.0735 307.2856 218.1570 -1.3427 289.8282 291.1709 307.5206 218.9543 -1.3511 289.9713 291.3225 307.7704 219.7515 -1.3503 290.1532 291.5035 308.0312 220.5795 -1.3545 290.2963 291.6508 308.3024 221.3460 -1.3579 290.4715 291.8293 308.5974 222.1843 -1.3606 290.6583 292.0190 308.9167 222.9395 -1.3640 290.8018 292.1658 309.1904 223.8085 -1.3705 291.0548 292.4253 309.5667 224.5648 -1.3740 291.2011 292.5751 309.8789 225.3928 -1.3784 291.3954 292.7738 310.2109 226.1900 -1.3831 291.5631 292.9462 310.5121 226.9868 -1.3875 291.7077 293.0952 310.8411 227.8143 -1.3888 291.8534 293.2422 311.1419 228.5705 -1.3936 292.0074 293.4009 311.4038 229.4395 -1.4018 292.2189 293.6207 311.6994 230.2060 -1.4061 292.3818 293.7879 311.9133 231.0340 -1.4126 292.5777 293.9903 312.1250 231.8210 -1.4198 292.7158 294.1356 312.3414 232.6280 -1.4255 292.8588 294.2843 312.5467 233.4145 -1.4304 293.0228 294.4532 312.6865 234.2118 -1.4345 293.1940 294.6285 312.8134 235.0398 -1.4405 293.3282 294.7686 312.9335 235.8063 -1.4469 293.4980 294.9450 313.0100 236.6650 -1.4522 293.6686 295.1208 313.0659 237.4213 -1.4567 293.8071 295.2638 313.1347 238.2488 -1.4606 293.9571 295.4177 313.1861 239.0353 -1.4620 294.1471 295.6092 313.1976 239.8325 -1.4659 294.3341 295.8000 313.2213 240.6605 -1.4693 294.5046 295.9739 313.2228 241.4168 -1.4700 294.6608 296.1308 313.1842 242.2540 -1.4744 294.8260 296.3004 313.1240 243.0205 -1.4759 294.9839 296.4598 313.0593 243.8690 -1.4810 295.1489 296.6298 313.0352 244.6355 -1.4874 295.3003 296.7877 313.0132 245.4635 -1.4889 295.4464 296.9352 312.9824 246.2190 -1.4911 295.5939 297.0850 312.9469 247.0468 -1.4912 295.7577 297.2489 312.8971 247.8440 -1.4923 295.8618 297.3541 312.8469 248.6413 -1.4922 295.9904 297.4825 312.8784 249.4590 -1.4890 296.1494 297.6384 312.8954 250.2253 -1.4866 296.3335 297.8202 312.9080 251.0833 -1.4953 296.5237 298.0190 312.9429 251.8395 -1.5046 296.6684 298.1730 312.9897 252.6880 -1.5054 296.8281 298.3335 313.0936 253.4443 -1.5073 296.9811 298.4884 313.1908 254.2825 -1.5128 297.1713 298.6841 313.3450 255.0695 -1.5162 297.3363 298.8525 313.5012 255.8660 -1.5149 297.5113 299.0262 313.7002 256.6938 -1.5146 297.6688 299.1834 313.9410 257.4500 -1.5173 297.7951 299.3124 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