DTA measure 1elso Date: 20241016:929 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.06 s Mass = 100.000 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2983 -1.0466 233.8954 234.9419 265.9295 2.1475 -1.0441 233.8663 234.9105 265.8305 2.9365 -1.0405 234.0888 235.1292 265.7245 3.7250 -1.0361 234.4768 235.5130 265.9680 4.5445 -0.9853 234.8762 235.8616 266.0152 5.3358 -0.9679 235.0688 236.0367 266.1601 6.1568 -0.9658 235.3033 236.2691 266.3141 6.9490 -0.9472 235.4181 236.3653 266.1804 7.7405 -0.9587 235.7752 236.7339 266.1228 8.5645 -0.9481 236.0609 237.0089 266.1233 9.3265 -0.9338 236.2862 237.2200 266.1151 10.1800 -0.9526 236.5083 237.4609 265.9326 10.9425 -0.9208 236.6071 237.5279 266.1577 11.7648 -0.9041 236.5925 237.4966 266.4950 12.5568 -0.8710 236.6721 237.5430 266.4036 13.3498 -0.8641 236.7203 237.5844 266.3744 14.2095 -0.8585 236.9695 237.8281 266.4366 14.9715 -0.8411 236.9992 237.8403 266.4774 15.7938 -0.8414 237.2881 238.1296 266.6141 16.5858 -0.8241 237.6389 238.4630 266.7281 17.3775 -0.8316 237.6378 238.4694 266.9358 18.2013 -0.8155 237.6084 238.4239 266.9878 18.9935 -0.8548 238.0469 238.9017 267.1053 19.8155 -0.8737 238.2096 239.0833 267.4061 20.6085 -0.8589 238.5198 239.3787 267.6717 21.4015 -0.8812 238.9173 239.7985 267.9488 22.2245 -0.8850 239.1694 240.0543 268.3075 22.9875 -0.8566 239.2597 240.1164 268.5688 23.8395 -0.8455 239.5848 240.4303 268.7640 24.6315 -0.8061 240.1472 240.9533 269.0789 25.4235 -0.7806 240.2726 241.0532 269.3489 26.2748 -0.7765 240.2846 241.0612 269.3459 27.0325 -0.7792 240.4587 241.2380 269.5656 27.8528 -0.7450 240.5680 241.3130 269.6783 28.6425 -0.7521 240.8392 241.5913 269.9604 29.4310 -0.7462 241.0016 241.7478 270.1454 30.2493 -0.7311 241.0886 241.8198 270.2594 31.0080 -0.7017 241.4421 242.1439 270.4465 31.8578 -0.7052 241.5895 242.2947 270.5029 32.6460 -0.6906 241.8097 242.5004 270.9243 33.4350 -0.6531 242.1403 242.7934 271.1186 34.2475 -0.6456 242.4605 243.1061 271.1495 35.0498 -0.6627 242.5155 243.1782 271.3103 35.8695 -0.6614 242.7668 243.4282 271.2614 36.6308 -0.6122 243.0225 243.6347 271.5202 37.4815 -0.5858 243.2761 243.8619 271.6661 38.2723 -0.5949 243.3941 243.9890 271.2683 39.0635 -0.6151 243.5304 244.1455 271.0962 39.8855 -0.6160 243.8581 244.4741 271.4295 40.6475 -0.6043 244.0246 244.6289 271.7445 41.5005 -0.6402 244.0452 244.6854 271.8528 42.2625 -0.5837 244.1181 244.7019 271.8813 43.0845 -0.6191 244.0680 244.6871 271.6730 43.8765 -0.6280 244.3032 244.9312 271.8030 44.6685 -0.6314 244.5304 245.1618 271.8904 45.5205 -0.6313 244.6706 245.3019 272.0829 46.3125 -0.6510 244.8116 245.4626 271.9857 47.1035 -0.6614 244.9869 245.6483 272.1761 47.9265 -0.6598 245.0948 245.7546 272.5969 48.6888 -0.6633 245.3486 246.0120 272.6445 49.5408 -0.6589 245.5243 246.1832 272.7742 50.3033 -0.6622 245.4777 246.1399 273.0085 51.1268 -0.6645 245.8169 246.4813 273.0475 51.9488 -0.6688 245.9921 246.6609 273.3280 52.7105 -0.6727 246.1300 246.8027 273.3451 53.5628 -0.6606 246.2353 246.8958 273.3669 54.3898 -0.6597 246.3854 247.0451 273.3127 55.3490 -0.6654 246.5616 247.2270 273.3804 56.1405 -0.6782 246.5938 247.2719 273.4385 56.9928 -0.6547 246.9822 247.6369 273.5554 57.7548 -0.6627 247.4070 248.0697 273.7788 58.5750 -0.6461 247.8097 248.4557 274.0266 59.3635 -0.6398 248.1403 248.7801 274.3499 60.1530 -0.6324 248.3580 248.9904 274.9211 60.9715 -0.6593 248.5853 249.2445 274.7117 61.7300 -0.6491 248.6530 249.3022 274.9762 62.5800 -0.6479 248.7549 249.4029 275.4479 63.3683 -0.6161 249.0229 249.6390 275.8493 64.1570 -0.6371 249.1976 249.8347 276.0220 64.9688 -0.6104 249.5316 250.1421 276.0741 65.7670 -0.6035 249.8793 250.4828 276.4882 66.5863 -0.6678 250.0611 250.7289 276.4276 67.3750 -0.6424 250.1475 250.7899 276.6271 68.1948 -0.6415 250.2314 250.8729 276.8927 68.9845 -0.6010 250.2482 250.8492 276.8856 69.7753 -0.5991 250.4765 251.0755 277.0116 70.5958 -0.6144 250.5600 251.1744 276.9401 71.3873 -0.6245 250.7152 251.3397 277.0273 72.2088 -0.6219 250.9503 251.5722 277.4172 73.0018 -0.6179 251.2771 251.8950 277.6093 73.7945 -0.6446 251.4871 252.1317 277.5181 74.6173 -0.6430 251.6126 252.2556 277.7402 75.4095 -0.6683 251.6548 252.3231 277.7195 76.2315 -0.6832 251.7959 252.4791 277.8862 77.0235 -0.6902 252.1937 252.8838 278.1149 77.8155 -0.6719 252.2248 252.8966 278.2462 78.6375 -0.6733 252.4676 253.1409 278.2789 79.3995 -0.6648 252.6616 253.3264 278.3767 80.2525 -0.6636 252.8016 253.4651 278.4033 81.0445 -0.6843 253.0149 253.6992 278.4260 81.8365 -0.6490 253.1098 253.7588 278.6206 82.6585 -0.6511 253.3523 254.0034 278.9133 83.4205 -0.6212 253.4539 254.0751 278.7602 84.2745 -0.6061 253.6156 254.2217 278.8648 85.0715 -0.5840 253.8785 254.4625 279.0288 85.8775 -0.6190 254.0684 254.6874 279.0393 86.6695 -0.5912 254.2331 254.8243 279.3229 87.4605 -0.5977 254.1503 254.7480 279.2631 88.3130 -0.6282 254.4271 255.0553 279.4992 89.0753 -0.6546 254.7979 255.4525 279.3538 89.8988 -0.6304 254.8070 255.4375 279.5255 90.6880 -0.6327 254.8299 255.4626 279.7205 91.4763 -0.6047 255.1753 255.7801 279.9752 92.2948 -0.5819 255.3207 255.9026 280.0851 93.0825 -0.6101 255.4854 256.0955 280.3491 93.9008 -0.5761 255.5119 256.0880 280.5779 94.6888 -0.5718 255.7565 256.3283 280.5643 95.4788 -0.5739 256.0520 256.6259 280.6184 96.3035 -0.6254 256.2521 256.8775 280.7004 97.0930 -0.5497 256.5324 257.0821 280.9905 97.9118 -0.5354 256.5044 257.0398 281.0022 98.7013 -0.5592 256.8456 257.4048 281.1909 99.4920 -0.5748 256.9918 257.5665 281.2672 100.3103 -0.5599 257.0946 257.6545 281.2704 101.0710 -0.6070 257.3050 257.9119 280.6346 101.9245 -0.6284 257.4614 258.0898 281.1568 102.7165 -0.6077 257.4922 258.0999 281.6429 103.5083 -0.6091 257.5416 258.1507 281.7773 104.3310 -0.5995 257.7866 258.3861 282.0070 105.0928 -0.5944 258.0432 258.6376 282.1832 105.9648 -0.6048 258.0219 258.6266 282.0898 106.7015 -0.6099 258.0768 258.6867 282.4868 107.5540 -0.5942 258.2846 258.8789 282.6586 108.3458 -0.6278 258.2832 258.9110 282.9749 109.1375 -0.6304 258.4477 259.0781 283.1982 109.9608 -0.6241 258.6824 259.3065 283.1913 110.7225 -0.6413 258.7593 259.4006 283.1688 111.5748 -0.6600 258.8493 259.5093 283.2660 112.3368 -0.6783 259.0708 259.7491 283.1721 113.1588 -0.7186 259.4122 260.1308 283.3526 113.9808 -0.7044 259.5245 260.2289 283.6549 114.7425 -0.7113 259.7976 260.5088 283.7217 115.5948 -0.6946 260.0460 260.7406 284.0761 116.3875 -0.7421 260.2033 260.9455 284.1215 117.1795 -0.7598 260.2253 260.9851 284.2750 118.0015 -0.7610 260.4888 261.2498 284.3196 118.7635 -0.7680 260.8855 261.6535 284.4720 119.6165 -0.7723 261.1120 261.8844 284.6978 120.4085 -0.7970 261.3311 262.1280 284.8684 121.2005 -0.8060 261.5199 262.3259 284.9206 122.0240 -0.8167 261.7845 262.6012 284.9682 122.7865 -0.8022 261.8780 262.6802 285.2427 123.6360 -0.7995 262.1398 262.9394 285.5556 124.3940 -0.8345 262.3726 263.2072 285.9056 125.2128 -0.8175 262.4537 263.2712 285.9432 126.0018 -0.8236 262.5430 263.3666 286.2161 126.7910 -0.8377 262.9192 263.7569 286.4225 127.6398 -0.8320 263.0570 263.8890 286.6381 128.4283 -0.8386 263.1686 264.0072 286.9220 129.2170 -0.8080 263.3178 264.1258 287.1017 130.0353 -0.8179 263.2675 264.0854 287.0974 130.8240 -0.7990 263.4710 264.2701 287.0622 131.6433 -0.7934 263.4760 264.2694 287.2330 132.4320 -0.8172 263.6056 264.4229 287.3083 133.2215 -0.8061 263.7901 264.5962 287.3689 134.0708 -0.8008 263.9543 264.7551 287.4548 134.8325 -0.8184 264.1682 264.9866 287.6105 135.6545 -0.7923 264.2947 265.0871 287.5281 136.4273 -0.7980 264.5651 265.3631 287.7059 137.2635 -0.8070 264.6116 265.4187 287.8702 138.0563 -0.8278 264.9366 265.7645 287.9468 138.8505 -0.8377 265.2798 266.1175 287.9003 139.6725 -0.8025 265.4353 266.2378 288.0611 140.4645 -0.8000 265.5843 266.3843 288.0942 141.2865 -0.8166 265.8188 266.6354 288.1317 142.0790 -0.8477 266.0031 266.8508 288.1130 142.8715 -0.8579 266.2116 267.0695 288.3191 143.6935 -0.8632 266.4278 267.2910 288.5004 144.4555 -0.8312 266.4468 267.2780 288.6334 145.3085 -0.8038 266.6437 267.4475 288.7286 146.1000 -0.8194 266.5562 267.3757 288.8025 146.8915 -0.8578 266.7374 267.5952 288.9273 147.7140 -0.8600 266.9122 267.7723 289.0190 148.4755 -0.8379 267.2070 268.0448 288.9150 149.3290 -0.8281 267.5009 268.3290 289.3202 150.1208 -0.8304 267.6929 268.5233 289.2789 150.9125 -0.8171 267.7237 268.5408 289.6487 151.7348 -0.8316 267.9434 268.7750 289.7413 152.5265 -0.8033 268.0325 268.8358 289.9770 153.3495 -0.8131 268.2173 269.0304 290.3013 154.1423 -0.8507 268.4014 269.2521 290.4521 154.9343 -0.8506 268.4561 269.3068 290.5857 155.7533 -0.8399 268.4066 269.2466 290.7223 156.5410 -0.7986 268.7685 269.5671 290.9129 157.5363 -0.7963 269.0270 269.8233 290.9379 158.3550 -0.8201 269.3024 270.1226 291.0618 159.1438 -0.8314 269.4457 270.2770 291.2062 159.9330 -0.8328 269.4533 270.2861 291.1894 160.7815 -0.8375 269.5929 270.4305 291.3839 161.5403 -0.8592 269.8227 270.6819 291.4770 162.3610 -0.8368 269.9053 270.7421 291.6399 163.1503 -0.8318 270.0265 270.8583 291.7438 163.9400 -0.8378 270.2865 271.1243 291.8212 164.7900 -0.8167 270.3753 271.1920 291.8742 165.5510 -0.7984 270.5919 271.3903 292.1359 166.3715 -0.8052 270.8243 271.6295 292.3852 167.1448 -0.8158 271.0035 271.8193 292.5428 167.9818 -0.8364 271.1217 271.9581 292.7049 168.7730 -0.8451 271.2791 272.1242 292.7975 169.5645 -0.8449 271.2631 272.1080 292.7606 170.4168 -0.8253 271.4711 272.2963 292.9221 171.1788 -0.8559 271.4251 272.2810 293.1015 172.0008 -0.8612 271.6992 272.5603 293.2982 172.7928 -0.8487 271.9197 272.7684 293.4749 173.5845 -0.8630 271.9750 272.8380 293.5501 174.4083 -0.8824 272.2122 273.0946 293.7031 175.2005 -0.8812 272.3294 273.2105 293.8067 176.0228 -0.8673 272.5344 273.4016 293.9404 176.8145 -0.8645 272.5680 273.4325 294.0340 177.6065 -0.8948 272.7916 273.6865 294.2923 178.4300 -0.8841 273.1887 274.0728 294.3778 179.2225 -0.8978 273.5275 274.4253 294.6027 180.0445 -0.8977 273.5108 274.4085 294.6999 180.8368 -0.8940 273.6964 274.5904 294.9202 181.6295 -0.8886 273.7592 274.6478 295.1168 182.4530 -0.8808 273.7787 274.6595 295.1825 183.2465 -0.8945 274.0304 274.9249 295.3826 184.0685 -0.8790 274.0307 274.9097 295.4900 184.8610 -0.8782 274.2836 275.1619 295.6243 185.6538 -0.8804 274.4001 275.2806 295.8060 186.4763 -0.8668 274.5140 275.3807 295.9570 187.2668 -0.8677 274.6865 275.5542 296.0774 188.2613 -0.8684 275.0312 275.8996 296.2828 189.0820 -0.8614 275.3297 276.1912 296.5880 189.8705 -0.8871 275.4117 276.2988 296.7014 190.6598 -0.8855 275.4855 276.3710 296.8480 191.4790 -0.8775 275.7601 276.6376 296.9418 192.2680 -0.9011 275.7827 276.6838 296.9397 193.0868 -0.9365 275.9768 276.9133 297.0259 193.8753 -0.9419 275.9576 276.8995 297.0102 194.6650 -0.9568 276.2053 277.1621 297.1385 195.5138 -0.9304 276.5191 277.4496 297.2762 196.2730 -0.9157 276.7108 277.6265 297.3588 197.0930 -0.9276 276.7291 277.6567 297.3229 197.9828 -0.9442 276.8159 277.7601 297.3767 198.9038 -0.9416 276.9542 277.8958 297.4911 199.6653 -0.9521 277.2094 278.1615 297.7760 200.5175 -0.9295 277.3931 278.3226 297.7653 201.3095 -0.9395 277.5861 278.5256 297.8393 202.1015 -0.9699 277.8319 278.8017 297.9511 202.9235 -0.9580 277.9978 278.9558 298.2094 203.6848 -0.9635 278.1200 279.0835 298.2364 204.5380 -0.9977 278.1746 279.1724 298.1577 205.3300 -0.9947 278.3697 279.3644 298.0817 206.1215 -0.9939 278.5705 279.5644 298.4195 206.9440 -1.0259 278.7674 279.7933 298.6211 207.7355 -1.0190 278.8704 279.8894 298.8938 208.5773 -0.9965 278.8817 279.8782 299.2372 209.3393 -0.9853 279.1143 280.0996 299.3927 210.1628 -1.0213 279.2189 280.2402 299.3396 210.9548 -0.9794 279.5212 280.5006 299.7011 211.7465 -0.9883 279.5499 280.5383 299.9723 212.5988 -0.9745 279.6885 280.6630 300.1369 213.3605 -0.9804 279.8892 280.8696 300.1827 214.1828 -0.9906 279.9989 280.9895 300.4224 214.9748 -1.0117 280.3017 281.3134 300.6933 215.7665 -1.0281 280.3954 281.4234 300.7591 216.6185 -1.0172 280.6147 281.6319 300.9633 217.3805 -1.0228 280.8372 281.8600 301.0793 218.2025 -1.0294 280.8588 281.8881 301.2042 219.0243 -1.0724 280.9212 281.9936 301.3805 219.7830 -1.0512 281.3506 282.4018 301.5790 220.6320 -1.0572 281.4652 282.5224 301.4785 221.3903 -1.0629 281.6605 282.7234 301.6510 222.2090 -1.0549 281.7764 282.8312 301.7304 222.9985 -1.0635 281.8701 282.9336 302.0726 223.7880 -1.0540 281.9835 283.0375 302.2996 224.6388 -1.0786 282.1419 283.2205 302.4142 225.3973 -1.0574 282.2507 283.3080 302.6738 226.2168 -1.0601 282.3732 283.4333 302.4247 227.0355 -1.0507 282.5532 283.6039 302.9428 227.7940 -1.0632 282.8317 283.8949 303.1292 228.6570 -1.0735 282.8442 283.9177 303.0317 229.4025 -1.0605 283.0481 284.1086 303.3355 230.2535 -1.0591 283.2993 284.3584 303.3082 231.0445 -1.0431 283.4361 284.4793 303.4491 231.8353 -1.0313 283.7706 284.8019 303.4571 232.6583 -1.0712 283.7035 284.7747 303.5073 233.4205 -1.0525 283.7505 284.8030 303.7305 234.2725 -1.0504 284.0914 285.1418 303.8440 235.0350 -1.0340 284.2710 285.3051 303.8684 235.8575 -1.0365 284.3400 285.3765 303.6304 236.6795 -1.0628 284.4099 285.4727 303.3961 237.4415 -1.1056 284.6111 285.7167 302.8967 238.2935 -1.1292 284.6919 285.8212 302.9460 239.0855 -1.1320 284.7202 285.8521 302.9973 239.8775 -1.1380 284.8366 285.9745 303.1686 240.6995 -1.1623 284.8697 286.0320 303.4398 241.4915 -1.1232 284.9474 286.0706 303.5287 242.3135 -1.0914 284.9921 286.0834 303.7528 243.1063 -1.0913 285.2769 286.3682 303.9837 243.8993 -1.0670 285.5508 286.6178 304.1534 244.7210 -1.0588 285.7217 286.7804 304.4163 245.5140 -1.1061 285.9342 287.0404 304.9152 246.3378 -1.1146 286.0584 287.1730 305.1346 247.1310 -1.1308 286.2879 287.4187 305.5928 247.9235 -1.1416 286.3957 287.5372 306.0198 248.7458 -1.1747 286.3834 287.5581 306.1309 249.5293 -1.1835 286.3922 287.5757 305.9523 250.3533 -1.1713 286.7188 287.8901 305.9599 251.1455 -1.1760 286.8965 288.0725 306.3330 251.9675 -1.1907 286.9396 288.1303 306.4786 252.7568 -1.1889 287.1948 288.3837 306.7511 253.5450 -1.1900 287.3566 288.5466 307.0257 254.3643 -1.1894 287.5700 288.7594 307.1559 255.1530 -1.1610 287.7383 288.8993 307.4066 255.9723 -1.1451 287.9541 289.0992 307.5855 256.7613 -1.1729 287.9450 289.1179 307.6815 257.5513 -1.2071 288.2234 289.4305 307.9971 258.3718 -1.1889 288.3886 289.5775 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