DTA measure 1gyors_pb3 Date: 2026915:1135 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.45 s Mass = 1149.900 mg data_number = 1341 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2820 0.9942 195.2300 194.2358 247.8098 2.0485 0.9957 195.4976 194.5020 247.8223 2.8758 0.9935 195.7749 194.7814 247.8435 3.6728 0.9938 196.0531 195.0593 247.8418 4.4598 0.9928 196.3452 195.3525 247.8491 5.2873 0.9937 196.6356 195.6419 247.8572 6.0533 0.9944 196.8893 195.8948 247.8826 6.9120 0.9948 197.1904 196.1956 247.9159 7.6680 0.9941 197.4366 196.4425 247.9448 8.4953 0.9921 197.7229 196.7308 247.9491 9.3233 0.9926 197.9861 196.9936 247.9794 10.2948 0.9968 198.3073 197.3105 248.0023 11.0810 0.9976 198.5610 197.5634 248.0267 11.9088 0.9980 198.8322 197.8342 248.0809 12.6753 0.9992 199.0986 198.0994 248.1254 13.5335 0.9977 199.3917 198.3940 248.1716 14.2893 0.9949 199.6291 198.6342 248.2087 15.1173 0.9943 199.9050 198.9107 248.2436 15.9140 0.9937 200.1625 199.1688 248.2965 16.7005 0.9910 200.4186 199.4276 248.3348 17.5388 0.9905 200.6714 199.6809 248.3899 18.2950 0.9916 200.9275 199.9359 248.4362 19.1428 0.9910 201.1847 200.1937 248.5356 19.9193 0.9895 201.4353 200.4459 248.6301 20.7370 0.9889 201.7278 200.7388 248.7166 21.5340 0.9897 201.9933 201.0035 248.8050 22.3305 0.9918 202.2490 201.2573 248.8867 23.1483 0.9879 202.5121 201.5243 248.9716 23.9145 0.9860 202.7669 201.7810 249.0745 24.7725 0.9853 203.0327 202.0474 249.1917 25.5288 0.9839 203.2505 202.2667 249.2819 26.3568 0.9818 203.5010 202.5192 249.3831 27.1530 0.9816 203.7701 202.7885 249.5113 27.9503 0.9819 204.0209 203.0390 249.6221 28.7680 0.9801 204.2710 203.2909 249.7357 29.5338 0.9767 204.5260 203.5493 249.8615 30.3820 0.9758 204.7810 203.8051 249.9954 31.1485 0.9764 205.0316 204.0552 250.1206 32.0073 0.9761 205.3038 204.3277 250.2687 32.7730 0.9744 205.5289 204.5545 250.4015 33.5905 0.9730 205.7633 204.7903 250.5270 34.3878 0.9718 205.9923 205.0205 250.6772 35.1845 0.9706 206.2334 205.2627 250.8064 36.0018 0.9687 206.4838 205.5152 250.9388 36.7785 0.9673 206.7407 205.7733 251.0610 37.5963 0.9646 207.0083 206.0438 251.2025 38.3618 0.9590 207.2463 206.2872 251.3359 39.2205 0.9558 207.4899 206.5341 251.4876 39.9768 0.9538 207.7191 206.7653 251.6285 40.8353 0.9507 207.9725 207.0218 251.7671 41.6215 0.9488 208.2299 207.2811 251.9085 42.4188 0.9455 208.4805 207.5349 252.0474 43.2160 0.9430 208.7299 207.7870 252.1775 44.0023 0.9368 208.9622 208.0253 252.3279 44.8300 0.9342 209.2068 208.2726 252.4589 45.5965 0.9307 209.4307 208.5000 252.5807 46.4445 0.9284 209.6828 208.7544 252.7303 47.2105 0.9250 209.9054 208.9804 252.8737 48.0385 0.9227 210.1487 209.2259 253.0231 48.8358 0.9205 210.3692 209.4487 253.1609 49.6218 0.9191 210.5989 209.6797 253.3054 50.4600 0.9171 210.8427 209.9256 253.4553 51.2470 0.9179 211.0669 210.1490 253.6059 52.0638 0.9159 211.3325 210.4166 253.7400 52.8405 0.9140 211.5644 210.6504 253.8823 53.6890 0.9097 211.8332 210.9235 254.0432 54.4545 0.9064 212.0530 211.1465 254.1961 55.2825 0.9018 212.2828 211.3810 254.3742 56.0695 0.8965 212.5037 211.6072 254.5069 56.8665 0.8914 212.7170 211.8257 254.6271 57.6938 0.8876 212.9704 212.0828 254.7721 58.4500 0.8846 213.2100 212.3255 254.8962 59.3088 0.8819 213.4641 212.5822 255.0330 60.0745 0.8763 213.7032 212.8269 255.1714 60.9023 0.8705 213.9650 213.0944 255.3291 61.6995 0.8678 214.1908 213.3231 255.4710 62.4863 0.8634 214.4150 213.5516 255.6132 63.3135 0.8600 214.6460 213.7859 255.7370 64.0800 0.8563 214.8503 213.9939 255.8749 64.9285 0.8545 215.0785 214.2240 256.0099 65.7045 0.8507 215.3025 214.4517 256.1351 66.5220 0.8436 215.5239 214.6803 256.2860 67.3193 0.8398 215.7459 214.9061 256.4257 68.1158 0.8369 215.9682 215.1312 256.5601 68.9333 0.8298 216.1854 215.3556 256.7028 69.6998 0.8269 216.4271 215.6002 256.8345 70.5275 0.8229 216.6519 215.8290 256.9818 71.3138 0.8188 216.8688 216.0500 257.1232 72.1418 0.8122 217.0869 216.2748 257.2558 72.9080 0.8072 217.3038 216.4966 257.3926 73.7353 0.8048 217.5540 216.7492 257.5523 74.5223 0.7994 217.7779 216.9785 257.6987 75.3193 0.7920 217.9943 217.2023 257.8347 76.1465 0.7860 218.2189 217.4329 257.9626 76.9130 0.7843 218.4351 217.6508 258.0908 77.7615 0.7791 218.6762 217.8972 258.2610 78.5373 0.7742 218.8906 218.1165 258.4057 79.3550 0.7709 219.0992 218.3282 258.5433 80.1420 0.7664 219.3021 218.5357 258.6871 80.9490 0.7590 219.5308 218.7718 258.8185 81.7663 0.7539 219.7652 219.0112 258.9633 82.5840 0.7496 220.0033 219.2537 259.1135 83.3913 0.7484 220.2188 219.4705 259.2621 84.2185 0.7448 220.4562 219.7115 259.3911 84.9850 0.7397 220.6695 219.9298 259.5154 85.8333 0.7335 220.8940 220.1605 259.6572 86.6913 0.7278 221.1123 220.3845 259.8186 87.4475 0.7234 221.3147 220.5913 259.9549 88.2755 0.7157 221.5577 220.8419 260.0954 89.0720 0.7078 221.7741 221.0663 260.2347 89.8690 0.7053 222.0086 221.3032 260.3800 90.6868 0.7005 222.2261 221.5255 260.5207 91.4528 0.6966 222.4337 221.7371 260.6397 92.3110 0.6898 222.6647 221.9749 260.7906 93.0673 0.6852 222.8421 222.1569 260.9302 93.8948 0.6793 223.0591 222.3797 261.0816 94.7223 0.6755 223.2625 222.5870 261.2286 95.4785 0.6705 223.4794 222.8089 261.3561 96.3060 0.6637 223.6790 223.0154 261.4884 97.0720 0.6583 223.8945 223.2362 261.6093 97.9205 0.6542 224.1098 223.4556 261.7551 98.6973 0.6485 224.3276 223.6791 261.8833 99.5140 0.6421 224.5489 223.9069 262.0181 100.3113 0.6388 224.7756 224.1369 262.1644 101.1083 0.6334 224.9761 224.3428 262.3211 101.9253 0.6281 225.1823 224.5542 262.4501 102.6918 0.6205 225.3802 224.7597 262.5840 103.5505 0.6118 225.6125 225.0006 262.7278 104.3163 0.6047 225.8241 225.2194 262.8658 105.1338 0.5990 226.0323 225.4333 263.0008 105.9310 0.5963 226.2440 225.6476 263.1281 106.7280 0.5927 226.4603 225.8677 263.2626 107.5450 0.5843 226.6662 226.0819 263.3955 108.3115 0.5765 226.8614 226.2850 263.5253 109.1703 0.5699 227.1126 226.5427 263.6816 109.9258 0.5614 227.3253 226.7638 263.8318 110.7535 0.5579 227.5366 226.9787 263.9425 111.5508 0.5534 227.7466 227.1932 264.0730 112.3473 0.5468 227.9338 227.3871 264.2054 113.1648 0.5408 228.1482 227.6074 264.3511 113.9313 0.5363 228.3469 227.8106 264.4937 114.7898 0.5317 228.5775 228.0458 264.6520 115.5453 0.5265 228.7732 228.2466 264.7809 116.3733 0.5210 228.9892 228.4682 264.9317 117.1705 0.5141 229.1957 228.6816 265.0770 117.9570 0.5090 229.3916 228.8826 265.2024 118.7948 0.5033 229.6241 229.1208 265.3283 119.5510 0.5020 229.8245 229.3226 265.4657 120.3993 0.4977 230.0222 229.5245 265.6059 121.1753 0.4933 230.2118 229.7185 265.7379 121.9930 0.4895 230.3977 229.9082 265.8784 122.7903 0.4884 230.6027 230.1143 266.0170 123.6175 0.4858 230.8048 230.3190 266.1551 124.4043 0.4809 231.0110 230.5301 266.2954 125.2015 0.4751 231.2319 230.7568 266.4270 126.0290 0.4670 231.4416 230.9745 266.5642 126.7950 0.4633 231.6279 231.1646 266.6876 127.6435 0.4552 231.8384 231.3831 266.8318 128.4198 0.4469 232.0217 231.5748 266.9539 129.2370 0.4413 232.2215 231.7803 267.0975 130.0240 0.4358 232.4226 231.9868 267.2373 130.8315 0.4304 232.6165 232.1860 267.3845 131.6488 0.4273 232.8104 232.3831 267.5177 132.4353 0.4239 232.9963 232.5724 267.6460 133.2325 0.4150 233.2146 232.7996 267.7834 134.0293 0.4095 233.4312 233.0217 267.9296 134.8568 0.4048 233.6322 233.2274 268.0727 135.6233 0.3977 233.8258 233.4281 268.1907 136.4718 0.3909 234.0421 233.6512 268.3190 137.2375 0.3843 234.2536 233.8693 268.4517 138.0653 0.3790 234.4476 234.0686 268.6065 138.8625 0.3727 234.6505 234.2778 268.7484 139.6493 0.3665 234.8367 234.4702 268.8803 140.4765 0.3599 235.0254 234.6656 269.0080 141.2430 0.3567 235.1983 234.8416 269.1230 142.0915 0.3506 235.4020 235.0515 269.2688 142.8570 0.3465 235.6004 235.2539 269.3838 143.7055 0.3407 235.8156 235.4749 269.5151 144.4720 0.3346 236.0030 235.6683 269.6294 145.2998 0.3317 236.1913 235.8596 269.7353 146.0860 0.3287 236.3904 236.0617 269.8329 146.8935 0.3238 236.5830 236.2592 269.9299 147.7113 0.3158 236.7935 236.4777 270.0451 148.4665 0.3108 236.9915 236.6807 270.1830 149.3355 0.3047 237.2144 236.9096 270.2915 150.0918 0.2989 237.3914 237.0925 270.3713 150.9090 0.2927 237.6073 237.3145 270.4931 151.7160 0.2889 237.7974 237.5085 270.6255 152.5030 0.2831 238.0030 237.7199 270.7406 153.3308 0.2766 238.2247 237.9481 270.8750 154.0965 0.2708 238.3899 238.1192 270.9708 154.9553 0.2657 238.5886 238.3228 271.1118 155.7113 0.2597 238.7610 238.5012 271.2335 156.5385 0.2560 238.9467 238.6907 271.3466 157.3358 0.2512 239.1307 238.8795 271.4601 158.1328 0.2471 239.3194 239.0722 271.5789 158.9498 0.2462 239.5063 239.2601 271.6880 159.7163 0.2419 239.6940 239.4521 271.7904 160.5750 0.2364 239.8855 239.6490 271.9273 161.3305 0.2314 240.0707 239.8393 272.0376 162.1685 0.2235 240.2648 240.0412 272.1674 162.9658 0.2180 240.4629 240.2450 272.2906 163.7828 0.2122 240.6736 240.4614 272.4230 164.5695 0.2076 240.8757 240.6681 272.5554 165.3565 0.2035 241.0611 240.8576 272.6909 166.1945 0.1980 241.2566 241.0586 272.8188 166.9500 0.1941 241.4272 241.2331 272.9266 167.7985 0.1899 241.6374 241.4474 273.0782 168.5753 0.1856 241.8031 241.6176 273.1884 169.3920 0.1799 242.0065 241.8266 273.3369 170.1893 0.1739 242.1913 242.0174 273.4840 170.9865 0.1695 242.3756 242.2061 273.6307 171.8038 0.1650 242.5545 242.3895 273.7654 172.5698 0.1574 242.7364 242.5790 273.8899 173.4285 0.1506 242.9524 242.8018 274.0374 174.1945 0.1464 243.1430 242.9965 274.1851 175.0118 0.1412 243.3421 243.2009 274.3118 175.8090 0.1375 243.5249 243.3875 274.4443 176.6063 0.1340 243.7054 243.5714 274.5669 177.4338 0.1261 243.8917 243.7656 274.7038 178.1895 0.1213 244.0639 243.9426 274.8283 179.0585 0.1170 244.2566 244.1396 274.9611 179.8143 0.1098 244.4400 244.3302 275.0756 180.6315 0.1043 244.6379 244.5335 275.2118 181.4390 0.1010 244.8297 244.7287 275.3548 182.2255 0.0979 245.0312 244.9333 275.4827 183.0530 0.0957 245.2159 245.1202 275.6245 183.8400 0.0894 245.3804 245.2909 275.7537 184.6575 0.0812 245.5656 245.4843 275.8935 185.4233 0.0759 245.7384 245.6626 276.0255 186.2820 0.0708 245.9316 245.8608 276.1707 187.0383 0.0655 246.1074 246.0419 276.3028 187.8653 0.0601 246.2905 246.2305 276.4388 188.6625 0.0561 246.4787 246.4226 276.5765 189.4495 0.0525 246.6588 246.6063 276.7042 190.2768 0.0494 246.8538 246.8044 276.8599 191.0430 0.0459 247.0207 246.9748 276.9722 191.8915 0.0386 247.2067 247.1681 277.1131 192.6678 0.0339 247.3961 247.3622 277.2467 193.4850 0.0264 247.5937 247.5673 277.3958 194.2823 0.0227 247.7680 247.7454 277.5245 195.1000 0.0156 247.9619 247.9463 277.6555 195.8963 0.0087 248.1311 248.1224 277.7938 196.6935 0.0037 248.3240 248.3203 277.9274 197.5215 -0.0027 248.4983 248.5010 278.0670 198.2873 -0.0067 248.6582 248.6649 278.2036 199.1355 -0.0142 248.8428 248.8570 278.3427 199.9020 -0.0194 249.0105 249.0299 278.4742 200.7295 -0.0244 249.2114 249.2358 278.6258 201.5160 -0.0284 249.4018 249.4302 278.7658 202.3133 -0.0337 249.5853 249.6190 278.8977 203.1413 -0.0379 249.7668 249.8046 279.0413 203.9070 -0.0424 249.9257 249.9681 279.1777 204.7553 -0.0462 250.1288 250.1750 279.3176 205.5115 -0.0501 250.3095 250.3596 279.4293 206.3700 -0.0540 250.4929 250.5469 279.5681 207.1358 -0.0566 250.6573 250.7139 279.6887 207.9535 -0.0617 250.8265 250.8882 279.8290 208.7610 -0.0658 251.0131 251.0789 279.9417 209.5473 -0.0698 251.1994 251.2692 280.0492 210.3648 -0.0759 251.3585 251.4344 280.1895 211.1415 -0.0847 251.5306 251.6153 280.3131 211.9893 -0.0898 251.7284 251.8182 280.4455 212.7555 -0.0955 251.8969 251.9924 280.5492 213.5835 -0.1006 252.0783 252.1789 280.6773 214.3803 -0.1041 252.2674 252.3715 280.8157 215.1770 -0.1092 252.4424 252.5516 280.9662 215.9948 -0.1157 252.6116 252.7273 281.1142 216.7613 -0.1242 252.7692 252.8934 281.2258 217.6193 -0.1313 252.9516 253.0829 281.3546 218.3753 -0.1345 253.1292 253.2637 281.4579 219.2033 -0.1387 253.3019 253.4405 281.5900 220.0000 -0.1436 253.4806 253.6242 281.7009 220.7865 -0.1474 253.6631 253.8105 281.8378 221.6248 -0.1501 253.8406 253.9907 281.9822 222.3810 -0.1549 253.9990 254.1539 282.1043 223.2388 -0.1598 254.1635 254.3233 282.2359 224.0053 -0.1641 254.3306 254.4947 282.3567 224.8435 -0.1701 254.5220 254.6922 282.4991 225.6193 -0.1743 254.6912 254.8654 282.6109 226.4370 -0.1796 254.8568 255.0364 282.7375 227.2240 -0.1843 255.0280 255.2123 282.8571 228.0315 -0.1883 255.2168 255.4052 282.9850 228.8483 -0.1949 255.3932 255.5881 283.1008 229.6045 -0.1978 255.5775 255.7753 283.2194 230.4735 -0.2032 255.7692 255.9725 283.3523 231.2295 -0.2086 255.9417 256.1503 283.4775 232.0568 -0.2123 256.1270 256.3393 283.6004 232.8540 -0.2174 256.2942 256.5116 283.7123 233.6410 -0.2230 256.4745 256.6975 283.8266 234.4680 -0.2312 256.6588 256.8900 283.9789 235.2345 -0.2371 256.8355 257.0727 284.1095 236.0830 -0.2416 257.0233 257.2650 284.2553 236.8795 -0.2461 257.1738 257.4199 284.3652 237.6765 -0.2511 257.3387 257.5898 284.4800 238.5045 -0.2549 257.5100 257.7649 284.6266 239.2703 -0.2568 257.6674 257.9242 284.7293 240.1185 -0.2604 257.8467 258.1071 284.8438 240.8850 -0.2653 258.0078 258.2731 284.9813 241.7128 -0.2716 258.1800 258.4516 285.1029 242.4990 -0.2789 258.3368 258.6157 285.2125 243.2963 -0.2828 258.5180 258.8008 285.3472 244.1243 -0.2839 258.7048 258.9887 285.4829 244.8898 -0.2895 258.8669 259.1564 285.6024 245.7075 -0.2948 259.0305 259.3253 285.7341 246.4943 -0.2996 259.1970 259.4966 285.8469 247.3215 -0.3067 259.3769 259.6836 285.9802 248.0880 -0.3115 259.5362 259.8477 286.0897 248.9363 -0.3155 259.7104 260.0258 286.1982 249.7123 -0.3179 259.8967 260.2146 286.3084 250.5300 -0.3214 260.0854 260.4068 286.4305 251.3273 -0.3263 260.2554 260.5817 286.5558 252.1235 -0.3324 260.4327 260.7651 286.6876 252.9515 -0.3386 260.6151 260.9536 286.8239 253.7078 -0.3430 260.7844 261.1274 286.9463 254.5660 -0.3475 260.9756 261.3230 287.0870 255.3115 -0.3514 261.1156 261.4669 287.2119 256.1498 -0.3553 261.2912 261.6465 287.3635 256.9055 -0.3589 261.4598 261.8187 287.4983 257.7638 -0.3602 261.6356 261.9958 287.6342 258.5303 -0.3604 261.7937 262.1540 287.7488 259.3480 -0.3639 261.9751 262.3390 287.8770 260.1443 -0.3671 262.1460 262.5131 288.0172 260.9415 -0.3708 262.3029 262.6736 288.1416 261.7695 -0.3786 262.4743 262.8529 288.2700 262.5358 -0.3842 262.6305 263.0147 288.3971 263.3835 -0.3888 262.8039 263.1927 288.5622 264.1500 -0.3919 262.9725 263.3644 288.7172 264.9780 -0.3950 263.1458 263.5408 288.8734 265.7333 -0.3988 263.3191 263.7179 289.0195 266.5920 -0.4020 263.5009 263.9029 289.1665 267.3585 -0.4076 263.6549 264.0625 289.3119 268.1858 -0.4119 263.8430 264.2549 289.4583 268.9725 -0.4180 264.0026 264.4206 289.5923 269.7698 -0.4222 264.1647 264.5869 289.7323 270.5665 -0.4267 264.3301 264.7567 289.8809 271.3530 -0.4315 264.4853 264.9168 290.0050 272.1810 -0.4377 264.6625 265.1002 290.1387 272.9475 -0.4446 264.8202 265.2648 290.2576 273.7950 -0.4511 265.0194 265.4705 290.4162 274.5615 -0.4574 265.1881 265.6455 290.5453 275.3895 -0.4642 265.3396 265.8037 290.6824 276.1863 -0.4684 265.5089 265.9773 290.8120 276.9830 -0.4717 265.6798 266.1515 290.9413 277.8008 -0.4754 265.8446 266.3200 291.0849 278.5773 -0.4780 266.0007 266.4787 291.2208 279.4250 -0.4814 266.1676 266.6490 291.3805 280.1813 -0.4848 266.3341 266.8189 291.5223 281.0193 -0.4911 266.5049 266.9960 291.6871 281.7748 -0.4972 266.6486 267.1458 291.8184 282.5925 -0.4986 266.8290 267.3276 291.9617 283.4000 -0.5024 266.9819 267.4843 292.1004 284.1863 -0.5084 267.1299 267.6383 292.2315 285.0038 -0.5143 267.3035 267.8179 292.3897 285.7805 -0.5201 267.4668 267.9869 292.5387 286.6388 -0.5263 267.6268 268.1531 292.7033 287.3945 -0.5289 267.7725 268.3014 292.8214 288.2225 -0.5323 267.9763 268.5086 292.9733 289.0198 -0.5384 268.1386 268.6770 293.0994 289.8160 -0.5426 268.2807 268.8234 293.2434 290.6338 -0.5476 268.4368 268.9844 293.3876 291.4105 -0.5533 268.6067 269.1600 293.5280 292.2273 -0.5604 268.7803 269.3406 293.6505 292.9938 -0.5638 268.9421 269.5059 293.7649 293.8525 -0.5681 269.1092 269.6772 293.9042 294.6183 -0.5698 269.2735 269.8434 294.0339 295.4358 -0.5730 269.4226 269.9957 294.1612 296.2330 -0.5781 269.5719 270.1500 294.2835 297.0298 -0.5811 269.7468 270.3279 294.3940 297.8470 -0.5871 269.9331 270.5202 294.5079 298.6135 -0.5931 270.0911 270.6842 294.6321 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