DTA measure 1fazis1 Date: 20241015:112 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 857.21 s Mass = 100.000 mg data_number = 1066 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2073 -1.6939 203.0850 204.7789 260.5235 1.9993 -1.6869 203.3217 205.0086 260.5254 2.7910 -1.6855 203.5812 205.2667 260.5392 3.6133 -1.6796 203.8415 205.5212 260.5764 4.4048 -1.6780 204.0883 205.7663 260.5657 5.2268 -1.6747 204.3445 206.0193 260.5745 6.0190 -1.6730 204.5730 206.2460 260.5867 6.8105 -1.6687 204.8164 206.4851 260.6223 7.6630 -1.6624 205.0827 206.7452 260.6586 8.4248 -1.6576 205.3199 206.9775 260.6870 9.2475 -1.6535 205.5727 207.2262 260.7293 10.0400 -1.6516 205.8282 207.4798 260.8023 10.8315 -1.6483 206.0440 207.6923 260.8908 11.6845 -1.6444 206.3079 207.9524 260.9445 12.4468 -1.6392 206.5448 208.1840 261.0122 13.2670 -1.6324 206.7956 208.4280 261.0854 14.0553 -1.6323 207.0417 208.6741 261.1787 14.8430 -1.6313 207.2817 208.9129 261.2601 15.6913 -1.6302 207.5514 209.1816 261.3687 16.4493 -1.6279 207.7442 209.3721 261.4723 17.2690 -1.6270 207.9924 209.6194 261.6001 18.0875 -1.6201 208.2422 209.8624 261.7116 18.8450 -1.6177 208.4627 210.0803 261.8192 19.6948 -1.6158 208.6996 210.3154 261.9418 20.4835 -1.6121 208.9243 210.5363 262.0687 21.2738 -1.6123 209.1881 210.8004 262.2223 22.0950 -1.6126 209.4213 211.0339 262.3644 22.8568 -1.6081 209.6398 211.2479 262.5070 23.7090 -1.6043 209.8989 211.5032 262.6688 24.5010 -1.6035 210.1197 211.7232 262.8165 25.2928 -1.6044 210.3394 211.9438 263.0045 26.1153 -1.6046 210.5964 212.2010 263.1630 26.8765 -1.5990 210.8116 212.4105 263.3256 27.7363 -1.5955 211.0513 212.6468 263.4753 28.5000 -1.5983 211.2516 212.8499 263.6491 29.3218 -1.5997 211.5017 213.1014 263.8603 30.1163 -1.5974 211.7307 213.3281 264.0362 30.9085 -1.5914 211.9787 213.5700 264.1922 31.7610 -1.5914 212.2320 213.8234 264.3720 32.5228 -1.5936 212.4538 214.0474 264.5463 33.3448 -1.5969 212.6857 214.2826 264.7169 34.1670 -1.5934 212.8926 214.4860 264.9282 34.9285 -1.5924 213.1018 214.6941 265.1196 35.7810 -1.5885 213.3390 214.9275 265.3085 36.5428 -1.5882 213.5601 215.1483 265.4831 37.3648 -1.5892 213.7835 215.3727 265.6693 38.1870 -1.5912 214.0128 215.6041 265.8565 38.9485 -1.5904 214.2410 215.8314 266.0356 39.8015 -1.5928 214.4837 216.0765 266.2196 40.5938 -1.5894 214.7061 216.2955 266.4133 41.3865 -1.5884 214.9125 216.5008 266.5790 42.2088 -1.5914 215.1477 216.7391 266.7740 42.9705 -1.5901 215.3674 216.9576 266.9523 43.8228 -1.5931 215.6128 217.2059 267.1268 44.6145 -1.5935 215.8260 217.4195 267.3015 45.4040 -1.5937 216.0464 217.6401 267.4868 46.2220 -1.5932 216.2847 217.8779 267.6551 46.9800 -1.5941 216.4878 218.0818 267.8159 47.8283 -1.5957 216.7316 218.3274 267.9781 48.6160 -1.5939 216.9252 218.5191 268.1410 49.4040 -1.5971 217.1482 218.7453 268.2905 50.2223 -1.5971 217.3879 218.9850 268.4519 51.0100 -1.5944 217.5926 219.1869 268.5958 51.8290 -1.5926 217.8163 219.4089 268.7686 52.6178 -1.5954 218.0325 219.6279 268.9350 53.4083 -1.6046 218.2461 219.8508 269.0717 54.2298 -1.5989 218.4649 220.0638 269.2332 54.9915 -1.5904 218.6760 220.2663 269.3580 55.8440 -1.5855 218.9172 220.5028 269.5046 56.6360 -1.5906 219.1388 220.7294 269.6628 57.4275 -1.5956 219.3647 220.9603 269.7713 58.2500 -1.5993 219.5791 221.1784 269.9164 59.0115 -1.5974 219.7765 221.3738 270.0410 59.8640 -1.5931 220.0377 221.6308 270.2072 60.6258 -1.5996 220.2329 221.8325 270.3155 61.4478 -1.6068 220.4375 222.0443 270.4331 62.2700 -1.6086 220.6516 222.2602 270.5509 63.0315 -1.6047 220.8620 222.4667 270.6658 63.8840 -1.6051 221.0955 222.7007 270.8231 64.6455 -1.6066 221.2938 222.9004 270.9338 65.4678 -1.5988 221.5078 223.1065 271.0405 66.2898 -1.5914 221.7247 223.3162 271.1472 67.0515 -1.5954 221.9263 223.5217 271.2513 67.9038 -1.6298 222.1460 223.7758 271.3832 68.6655 -1.6540 222.3614 224.0154 271.5088 69.4878 -1.6581 222.5863 224.2444 271.6146 70.3098 -1.6581 222.8243 224.4824 271.6922 71.0715 -1.6587 223.0235 224.6822 271.7881 71.9235 -1.6594 223.2367 224.8961 271.8974 72.6855 -1.6690 223.4507 225.1197 271.9937 73.5075 -1.6699 223.6291 225.2989 272.1073 74.3298 -1.6418 223.8567 225.4984 272.2246 75.0933 -1.6174 224.0668 225.6843 272.3401 75.9460 -1.6144 224.2774 225.8918 272.4489 76.7070 -1.6170 224.4679 226.0849 272.5510 77.5245 -1.6188 224.6864 226.3052 272.6629 78.3440 -1.6208 224.9031 226.5239 272.7874 79.1020 -1.6190 225.1163 226.7353 272.8988 79.9488 -1.6220 225.3337 226.9558 272.9826 80.7083 -1.6208 225.5118 227.1326 273.0711 81.5270 -1.6204 225.7356 227.3559 273.2074 82.3453 -1.6230 225.9480 227.5711 273.3335 83.1040 -1.6288 226.1329 227.7617 273.4351 83.9525 -1.6285 226.3411 227.9696 273.5791 84.7420 -1.6213 226.5549 228.1763 273.6924 85.5318 -1.6288 226.7631 228.3919 273.8008 86.3508 -1.6295 226.9815 228.6110 273.9246 87.1118 -1.6267 227.1661 228.7929 274.0410 87.9638 -1.6259 227.3695 228.9954 274.2142 88.7555 -1.6215 227.5714 229.1930 274.3169 89.5475 -1.6212 227.7777 229.3990 274.4223 90.3695 -1.6221 227.9816 229.6036 274.5774 91.1315 -1.6239 228.1864 229.8103 274.7008 91.9835 -1.6258 228.3787 230.0045 274.8515 92.7758 -1.6269 228.5783 230.2052 274.9701 93.5675 -1.6287 228.7758 230.4045 275.0914 94.3895 -1.6505 228.9957 230.6462 275.2368 95.1515 -1.6779 229.2073 230.8851 275.3579 96.0035 -1.6906 229.4126 231.1033 275.5120 96.7955 -1.6953 229.6076 231.3029 275.6401 97.5875 -1.6963 229.8140 231.5103 275.7756 98.4095 -1.6984 229.9951 231.6935 275.9529 99.1715 -1.7023 230.1697 231.8721 276.0677 100.0235 -1.7031 230.3713 232.0745 276.2135 100.7855 -1.6720 230.5667 232.2387 276.3511 101.6075 -1.6596 230.7821 232.4416 276.4906 102.4295 -1.6843 230.9807 232.6650 276.6403 103.2515 -1.6995 231.1879 232.8874 276.7772 104.1335 -1.7015 231.3919 233.0934 276.9294 104.8955 -1.6991 231.5767 233.2759 277.0719 105.7480 -1.6967 231.7974 233.4941 277.2181 106.5105 -1.6816 231.9969 233.6785 277.3739 107.3325 -1.6574 232.2103 233.8676 277.5279 108.1545 -1.6491 232.3990 234.0481 277.6930 108.9155 -1.6493 232.5704 234.2197 277.8181 109.7603 -1.6477 232.7710 234.4187 277.9684 110.5193 -1.6493 232.9553 234.6046 278.1169 111.3383 -1.6592 233.1499 234.8091 278.2639 112.1268 -1.6619 233.3561 235.0180 278.4136 112.9145 -1.6578 233.5385 235.1963 278.5596 113.7640 -1.6574 233.7282 235.3856 278.7151 114.5220 -1.6615 233.9246 235.5861 278.8484 115.3400 -1.6636 234.1306 235.7941 278.9921 116.1583 -1.6661 234.3266 235.9927 279.1422 116.9170 -1.6703 234.5190 236.1893 279.2902 117.7675 -1.6742 234.6981 236.3723 279.4536 118.5278 -1.6746 234.8663 236.5409 279.5860 119.3495 -1.6702 235.0974 236.7676 279.7538 120.1705 -1.6734 235.2834 236.9568 279.8897 120.9325 -1.6767 235.4629 237.1396 280.0286 121.7845 -1.6778 235.6623 237.3401 280.1749 122.5465 -1.6821 235.8303 237.5124 280.3095 123.3685 -1.6846 236.0380 237.7227 280.4437 124.1605 -1.7150 236.2270 237.9420 280.5858 124.9525 -1.7437 236.4035 238.1472 280.7207 125.8055 -1.7447 236.6389 238.3836 280.8472 126.6290 -1.7306 236.8212 238.5517 280.9990 127.4225 -1.7175 237.0162 238.7337 281.1292 128.2445 -1.7113 237.2085 238.9198 281.2603 129.0365 -1.7043 237.3995 239.1038 281.4067 129.8310 -1.7009 237.5828 239.2837 281.5383 130.6603 -1.7005 237.7872 239.4877 281.6790 131.4225 -1.7056 237.9547 239.6603 281.7952 132.2745 -1.7106 238.1579 239.8685 281.9313 133.0363 -1.7160 238.3391 240.0550 282.0407 133.8583 -1.7135 238.5366 240.2501 282.1851 134.6805 -1.7175 238.7039 240.4214 282.3040 135.4420 -1.7172 238.8737 240.5909 282.4268 136.2945 -1.7159 239.0756 240.7915 282.5701 137.0870 -1.7201 239.2667 240.9869 282.6823 137.8795 -1.7216 239.4350 241.1566 282.7921 138.7020 -1.7273 239.6275 241.3548 282.9127 139.4635 -1.7233 239.7913 241.5147 283.0199 140.3160 -1.7228 240.0064 241.7292 283.1410 141.1080 -1.7249 240.1952 241.9201 283.2730 141.8998 -1.7282 240.3780 242.1062 283.3933 142.7170 -1.7265 240.5827 242.3092 283.5195 143.4760 -1.7312 240.7411 242.4723 283.6246 144.3230 -1.7310 240.9182 242.6492 283.7566 145.1125 -1.7334 241.1073 242.8407 283.8842 145.9003 -1.7352 241.2972 243.0325 283.9890 146.7190 -1.7362 241.4993 243.2355 284.1174 147.4775 -1.7418 241.6869 243.4286 284.2181 148.3273 -1.7456 241.8742 243.6198 284.3459 149.1158 -1.7529 242.0417 243.7946 284.4604 149.9058 -1.7609 242.2432 244.0041 284.6015 150.7275 -1.7621 242.4066 244.1687 284.7107 151.4893 -1.7660 242.5772 244.3432 284.8276 152.3415 -1.7625 242.7601 244.5226 284.9416 153.1035 -1.7663 242.9683 244.7346 285.0717 153.9253 -1.7664 243.1471 244.9135 285.2099 154.7175 -1.7685 243.3262 245.0947 285.3534 155.5090 -1.7669 243.4966 245.2635 285.4845 156.3313 -1.7568 243.6781 245.4349 285.5950 157.1230 -1.7540 243.8846 245.6386 285.7261 157.9453 -1.7524 244.0616 245.8140 285.8764 158.7373 -1.7561 244.2361 245.9922 285.9963 159.5288 -1.7533 244.4023 246.1556 286.1446 160.3513 -1.7718 244.5779 246.3497 286.2930 161.1430 -1.8141 244.7659 246.5800 286.3964 161.9650 -1.8134 244.9292 246.7426 286.5291 162.8170 -1.7857 245.1039 246.8896 286.6706 163.6090 -1.7744 245.2864 247.0608 286.8066 164.4005 -1.7744 245.4892 247.2636 286.9442 165.2230 -1.7700 245.6941 247.4641 287.0730 165.9845 -1.7725 245.8641 247.6366 287.1877 166.8370 -1.7816 246.0301 247.8118 287.3268 167.6290 -1.7817 246.1926 247.9743 287.4892 168.4215 -1.7877 246.3893 248.1770 287.6269 169.2443 -1.7897 246.5675 248.3572 287.7742 170.0065 -1.7860 246.7262 248.5123 287.8971 170.8648 -1.7819 246.9216 248.7034 288.0436 171.6338 -1.7875 247.0666 248.8541 288.1820 172.4558 -1.7940 247.2798 249.0738 288.3319 173.2478 -1.7956 247.4470 249.2426 288.4391 174.0368 -1.7954 247.5986 249.3940 288.5806 174.8860 -1.7984 247.7982 249.5967 288.7100 175.6440 -1.7984 247.9725 249.7709 288.8516 176.4620 -1.7965 248.1428 249.9393 288.9931 177.2505 -1.8017 248.3115 250.1132 289.1395 178.0390 -1.8045 248.4989 250.3035 289.2735 178.8870 -1.8097 248.6848 250.4945 289.4099 179.6453 -1.8089 248.8423 250.6512 289.5488 180.4648 -1.8093 249.0302 250.8395 289.6807 181.2538 -1.8119 249.2092 251.0211 289.8142 182.0430 -1.8165 249.3734 251.1899 289.9584 182.8940 -1.8170 249.5600 251.3771 290.0844 183.6550 -1.8174 249.7074 251.5248 290.2087 184.4768 -1.8184 249.8998 251.7182 290.3729 185.2690 -1.8241 250.0786 251.9027 290.5120 186.0605 -1.8245 250.2461 252.0706 290.6703 186.8830 -1.8242 250.4336 252.2577 290.7948 187.6748 -1.8310 250.5995 252.4305 290.9385 188.4968 -1.8315 250.7807 252.6122 291.0736 189.2890 -1.8350 250.9419 252.7769 291.2024 190.0805 -1.8342 251.1272 252.9614 291.3369 190.9030 -1.8336 251.2956 253.1292 291.4937 191.6948 -1.8320 251.4500 253.2820 291.6153 192.5168 -1.8328 251.6454 253.4782 291.7548 193.3090 -1.8364 251.8001 253.6365 291.9045 194.1005 -1.8388 251.9866 253.8254 292.0268 194.9230 -1.8378 252.1577 253.9955 292.1551 195.7160 -1.8436 252.3308 254.1744 292.2994 196.5410 -1.8452 252.5049 254.3502 292.4340 197.3330 -1.8483 252.6733 254.5216 292.5750 198.1245 -1.8500 252.8464 254.6964 292.6970 198.9470 -1.8531 253.0233 254.8764 292.8417 199.7385 -1.8546 253.1998 255.0544 292.9852 200.5608 -1.8588 253.3498 255.2087 293.1260 201.3525 -1.8597 253.5337 255.3934 293.2575 202.1445 -1.8617 253.7055 255.5672 293.3839 202.9968 -1.8631 253.8545 255.7177 293.5633 203.7585 -1.8688 254.0293 255.8981 293.6717 204.5805 -1.8679 254.2190 256.0869 293.7967 205.3725 -1.8736 254.3769 256.2506 293.9242 206.1638 -1.8763 254.5432 256.4195 294.0676 207.0120 -1.8773 254.7371 256.6144 294.2236 207.7700 -1.8793 254.9037 256.7830 294.3547 208.5880 -1.8788 255.0663 256.9451 294.4833 209.4060 -1.8780 255.2257 257.1036 294.6240 210.1640 -1.8825 255.3869 257.2693 294.7464 211.0128 -1.8844 255.5678 257.4523 294.8755 211.7710 -1.8879 255.7194 257.6073 295.0193 212.5898 -1.8903 255.8935 257.7838 295.1711 213.4098 -1.8941 256.0725 257.9666 295.3111 214.1703 -1.8909 256.2438 258.1347 295.4193 215.0218 -1.8943 256.4095 258.3038 295.5840 215.8133 -1.8994 256.5722 258.4716 295.7103 216.6045 -1.9044 256.7348 258.6392 295.8493 217.4270 -1.9066 256.9087 258.8153 295.9806 218.1885 -1.9087 257.0748 258.9834 296.1125 219.0410 -1.9086 257.2391 259.1478 296.2355 219.8330 -1.9095 257.4211 259.3306 296.3680 220.6245 -1.9115 257.5848 259.4963 296.5241 221.4468 -1.9143 257.7581 259.6724 296.6483 222.2138 -1.9212 257.9270 259.8482 296.7861 223.0688 -1.9305 258.0911 260.0215 296.9263 223.8308 -1.9444 258.2458 260.1902 297.0517 224.6528 -1.9522 258.4272 260.3794 297.1958 225.4745 -1.9531 258.5812 260.5342 297.3476 226.2368 -1.9528 258.7397 260.6925 297.4832 227.0885 -1.9519 258.9350 260.8869 297.6068 227.8505 -1.9549 259.0969 261.0518 297.7361 228.6725 -1.9460 259.2709 261.2169 297.8598 229.4945 -1.9416 259.4317 261.3732 298.0340 230.2565 -1.9442 259.5936 261.5378 298.1341 231.1090 -1.9432 259.7696 261.7128 298.2564 231.8728 -1.9403 259.9145 261.8548 298.3861 232.6975 -1.9397 260.0844 262.0241 298.5156 233.5198 -1.9459 260.2485 262.1944 298.6312 234.2825 -1.9471 260.4152 262.3623 298.7491 235.1345 -1.9480 260.5996 262.5476 298.8724 235.9000 -1.9484 260.7394 262.6878 298.9772 236.7243 -1.9526 260.9118 262.8644 299.1108 237.5165 -1.9608 261.0803 263.0411 299.2295 238.3058 -1.9626 261.2304 263.1931 299.3364 239.1223 -1.9635 261.4044 263.3678 299.4695 239.9120 -1.9685 261.5770 263.5455 299.6163 240.7300 -1.9699 261.7533 263.7232 299.7231 241.5180 -1.9695 261.8935 263.8630 299.8292 242.3060 -1.9699 262.0681 264.0380 299.9772 243.1308 -1.9767 262.2392 264.2159 300.0892 243.8900 -1.9807 262.3900 264.3707 300.2220 244.7385 -1.9804 262.5963 264.5767 300.3417 245.5280 -1.9806 262.7497 264.7302 300.4367 246.3195 -1.9820 262.8998 264.8818 300.5661 247.1410 -1.9852 263.0632 265.0484 300.6885 247.9025 -1.9909 263.2123 265.2033 300.8291 248.7545 -1.9914 263.3801 265.3714 300.9746 249.5165 -1.9938 263.5312 265.5250 301.0809 250.3385 -1.9984 263.7132 265.7117 301.2139 251.1318 -1.9987 263.8670 265.8657 301.3353 251.9245 -2.0042 264.0131 266.0173 301.4448 252.7765 -2.0072 264.2015 266.2087 301.5816 253.5385 -2.0079 264.3579 266.3658 301.6880 254.3605 -2.0133 264.5284 266.5417 301.8221 255.1525 -2.0151 264.6783 266.6934 301.9454 255.9445 -2.0150 264.8236 266.8386 302.0677 256.7665 -2.0169 264.9784 266.9953 302.2151 257.5585 -2.0195 265.1340 267.1536 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