DTA measure 2fazis1 Date: 20241015:1132 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1638.99 s Mass = 100.000 mg data_number = 1019 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4318 -4.5037 400.0914 404.5951 418.7554 4.0308 -4.5041 400.3516 404.8558 418.8199 5.6446 -4.5040 400.5657 405.0697 418.9141 7.2738 -4.5000 400.7980 405.2979 418.9751 8.8725 -4.5006 400.9960 405.4966 419.0108 10.4715 -4.5003 401.2286 405.7289 419.0448 12.0863 -4.4879 401.4631 405.9511 419.0474 13.6855 -4.4927 401.6509 406.1436 419.0540 15.3126 -4.4909 401.8734 406.3643 419.0185 16.9041 -4.4916 402.1110 406.6025 418.9657 18.4960 -4.4860 402.3131 406.7991 418.8732 20.1025 -4.4825 402.4938 406.9763 418.7757 21.6954 -4.4767 402.7015 407.1782 418.6412 23.3201 -4.4730 402.8979 407.3709 418.5056 24.9159 -4.4680 403.1055 407.5734 418.3496 26.5126 -4.4642 403.3180 407.7822 418.1734 28.1266 -4.4683 403.5107 407.9790 417.9820 29.7256 -4.4541 403.7178 408.1719 417.7549 31.3395 -4.4355 403.9076 408.3431 417.5312 32.9546 -4.4260 404.0872 408.5132 417.3002 34.5535 -4.4194 404.2649 408.6843 417.0518 36.1525 -4.4124 404.4533 408.8657 416.8359 37.7665 -4.4012 404.6644 409.0656 416.5906 39.3805 -4.3908 404.8268 409.2176 416.3208 40.9945 -4.3784 404.9807 409.3591 416.0674 42.5935 -4.3691 405.1511 409.5202 415.8099 44.1924 -4.3573 405.3309 409.6881 415.5661 45.8064 -4.3456 405.4917 409.8372 415.3249 47.4181 -4.3325 405.6481 409.9806 415.0781 49.0241 -4.3259 405.7917 410.1176 414.8521 50.6163 -4.3099 405.9537 410.2635 414.6102 52.2160 -4.3018 406.1052 410.4070 414.4056 53.8199 -4.2885 406.2593 410.5479 414.1837 55.4291 -4.2771 406.4085 410.6856 413.9514 57.0405 -4.2700 406.5297 410.7997 413.7518 58.6395 -4.2594 406.6580 410.9174 413.5672 60.2535 -4.2507 406.7984 411.0491 413.3488 61.8525 -4.2368 406.9326 411.1694 413.1623 63.4665 -4.2263 407.0548 411.2811 412.9973 65.0806 -4.2134 407.1850 411.3983 412.8155 66.6805 -4.2060 407.2944 411.5004 412.6318 68.2945 -4.1969 407.4098 411.6067 412.4715 69.8933 -4.1850 407.5253 411.7103 412.3049 71.5223 -4.1750 407.6340 411.8090 412.1447 73.1223 -4.1686 407.7419 411.9105 411.9634 74.7368 -4.1585 407.8450 412.0035 411.7863 76.3358 -4.1478 407.9419 412.0898 411.6189 77.9504 -4.1349 408.0480 412.1830 411.4575 79.5616 -4.1266 408.1468 412.2735 411.2970 81.1683 -4.1303 408.2435 412.3738 411.1271 82.7601 -4.1125 408.3028 412.4153 410.9333 84.3578 -4.1004 408.4159 412.5162 410.7877 85.9660 -4.0906 408.4940 412.5845 410.6100 87.5775 -4.0808 408.5900 412.6708 410.4089 89.1765 -4.0744 408.6510 412.7254 410.2616 90.7904 -4.0633 408.7313 412.7946 410.0685 92.3894 -4.0558 408.8025 412.8584 409.8919 93.9885 -4.0454 408.8778 412.9233 409.7190 95.6174 -4.0337 408.9575 412.9911 409.5318 97.2170 -4.0256 409.0300 413.0555 409.3448 98.8309 -4.0172 409.0707 413.0879 409.1457 100.4298 -4.0061 409.1212 413.1273 408.9621 102.0288 -3.9972 409.1869 413.1841 408.7887 103.6579 -3.9863 409.2568 413.2431 408.6079 105.2720 -3.9820 409.2874 413.2693 408.4134 106.8718 -3.9710 409.3531 413.3241 408.2291 108.4708 -3.9655 409.3885 413.3540 408.0360 110.0853 -3.9560 409.4363 413.3922 407.8375 111.6964 -3.9460 409.4737 413.4196 407.6223 113.2884 -3.9380 409.5092 413.4472 407.4331 114.8960 -3.9245 409.5517 413.4761 407.2256 116.4871 -3.9174 409.5593 413.4767 407.0294 118.0943 -3.9081 409.5917 413.4997 406.8425 119.7050 -3.8981 409.6263 413.5244 406.6276 121.3039 -3.8936 409.6599 413.5536 406.4425 122.9028 -3.8851 409.6734 413.5585 406.2537 124.5075 -3.8751 409.6887 413.5638 406.0524 126.1098 -3.8679 409.7023 413.5702 405.8702 127.7238 -3.8599 409.7325 413.5924 405.6767 129.3379 -3.8527 409.7551 413.6077 405.4969 130.9380 -3.8446 409.7476 413.5922 405.3066 132.5538 -3.8383 409.7610 413.5992 405.1169 134.1565 -3.8288 409.7488 413.5776 404.9385 135.7616 -3.8196 409.7575 413.5771 404.7455 137.3756 -3.8127 409.7399 413.5526 404.5447 138.9896 -3.8071 409.7405 413.5475 404.3325 140.5885 -3.7969 409.7543 413.5513 404.1460 142.2025 -3.7875 409.7409 413.5283 403.9560 143.8016 -3.7789 409.7358 413.5147 403.7561 145.3933 -3.7719 409.7227 413.4946 403.5546 147.0170 -3.7624 409.7205 413.4829 403.3645 148.6080 -3.7556 409.7068 413.4624 403.1473 150.2144 -3.7467 409.6872 413.4338 402.9496 151.8081 -3.7318 409.6510 413.3829 402.7707 153.4180 -3.7239 409.6323 413.3562 402.5809 155.0315 -3.7179 409.6152 413.3331 402.3964 156.6308 -3.7125 409.5900 413.3025 402.2177 158.2446 -3.7044 409.5543 413.2586 401.9942 159.8438 -3.6960 409.5370 413.2330 401.8193 161.4426 -3.6890 409.5044 413.1934 401.6366 163.0566 -3.6795 409.4562 413.1356 401.4323 164.6719 -3.6703 409.4586 413.1289 401.2385 166.2771 -3.6606 409.4052 413.0658 401.0442 167.8775 -3.6571 409.3576 413.0147 400.8458 169.4915 -3.6512 409.3285 412.9797 400.6387 171.0905 -3.6416 409.2914 412.9329 400.4546 172.7195 -3.6305 409.2342 412.8647 400.2403 174.3195 -3.6229 409.1867 412.8096 400.0398 175.9258 -3.6173 409.1473 412.7646 399.8514 177.5223 -3.6100 409.0860 412.6960 399.6554 179.1148 -3.6026 409.0513 412.6539 399.4567 180.7368 -3.5961 408.9816 412.5777 399.2656 182.3440 -3.5857 408.9429 412.5285 399.0516 183.9376 -3.5790 408.8740 412.4529 398.8563 185.5478 -3.5732 408.8025 412.3758 398.6674 187.1455 -3.5774 408.7562 412.3336 398.4868 188.7745 -3.5684 408.6868 412.2551 398.2889 190.3735 -3.5538 408.6158 412.1696 398.0845 191.9725 -3.5454 408.5455 412.0909 397.9192 193.5865 -3.5414 408.4951 412.0365 397.7342 195.1855 -3.5315 408.4333 411.9647 397.5415 196.8153 -3.5239 408.3565 411.8804 397.3362 198.4145 -3.5173 408.2729 411.7902 397.1364 200.0285 -3.5092 408.1958 411.7050 396.9334 201.6725 -3.5027 408.1184 411.6212 396.7391 203.2863 -3.4981 408.0531 411.5512 396.5309 204.8848 -3.4914 407.9643 411.4557 396.3221 206.4875 -3.4815 407.8880 411.3695 396.1294 208.0866 -3.4734 407.8104 411.2838 395.9390 209.7083 -3.4657 407.7247 411.1905 395.7503 211.2993 -3.4610 407.6495 411.1105 395.5608 212.9060 -3.4542 407.5548 411.0090 395.3500 214.4989 -3.4463 407.4684 410.9147 395.1586 216.0923 -3.4390 407.3830 410.8220 394.9562 217.7166 -3.4331 407.3004 410.7335 394.7552 219.3145 -3.4268 407.2100 410.6368 394.5719 220.9285 -3.4187 407.1140 410.5327 394.3662 222.5274 -3.4155 407.0290 410.4445 394.1946 224.1264 -3.4084 406.9487 410.3571 393.9950 225.7405 -3.4033 406.8384 410.2417 393.7762 227.3541 -3.3979 406.7369 410.1348 393.5983 228.9531 -3.3924 406.6382 410.0306 393.3949 230.5678 -3.3859 406.5322 409.9181 393.1939 232.1668 -3.3784 406.4238 409.8022 392.9778 233.7658 -3.3745 406.3357 409.7102 392.7825 235.3950 -3.3647 406.2436 409.6082 392.5562 236.9938 -3.3567 406.1468 409.5035 392.3537 238.5928 -3.3529 406.0205 409.3734 392.1666 240.2048 -3.3462 405.9066 409.2528 391.9521 241.7970 -3.3390 405.7963 409.1353 391.7538 243.4194 -3.3327 405.6941 409.0268 391.5316 245.0114 -3.3273 405.5708 408.8981 391.3275 246.6079 -3.3179 405.4596 408.7774 391.1222 248.2151 -3.3122 405.3485 408.6607 390.9387 249.8110 -3.3077 405.2573 408.5650 390.7344 251.4099 -3.3015 405.1451 408.4466 390.5338 253.0390 -3.2957 405.0196 408.3153 390.3316 254.6378 -3.2872 404.8897 408.1769 390.1336 256.2368 -3.2832 404.7635 408.0467 389.9200 257.8358 -3.2767 404.6543 407.9310 389.7325 259.4498 -3.2692 404.5412 407.8105 389.5384 261.0640 -3.2664 404.4349 407.7014 389.3473 262.6799 -3.2591 404.3130 407.5721 389.1356 264.2788 -3.2522 404.1926 407.4448 388.9669 265.8776 -3.2471 404.0710 407.3181 388.7721 267.4916 -3.2433 403.9480 407.1913 388.5567 269.1056 -3.2363 403.8131 407.0494 388.3473 270.7195 -3.2297 403.6875 406.9172 388.1679 272.3188 -3.2246 403.5397 406.7643 387.9661 273.9129 -3.2196 403.4109 406.6305 387.7568 275.5190 -3.2119 403.3012 406.5131 387.5702 277.1294 -3.2052 403.1726 406.3778 387.3563 278.7380 -3.2021 403.0454 406.2475 387.1557 280.3316 -3.1920 402.9054 406.0973 386.9712 281.9405 -3.1842 402.7708 405.9550 386.7515 283.5378 -3.1819 402.6482 405.8301 386.5527 285.1519 -3.1762 402.5067 405.6829 386.3389 286.7658 -3.1713 402.3769 405.5482 386.1252 288.3648 -3.1666 402.2426 405.4092 385.9094 289.9786 -3.1589 402.1203 405.2792 385.7197 291.5776 -3.1539 401.9787 405.1326 385.4931 293.2068 -3.1471 401.8408 404.9879 385.3030 294.8055 -3.1492 401.7021 404.8514 385.1083 296.4195 -3.1367 401.5558 404.6925 384.9064 298.0185 -3.1293 401.4124 404.5418 384.6999 299.6325 -3.1189 401.2805 404.3993 384.5089 301.2465 -3.1153 401.1446 404.2599 384.3090 302.8605 -3.1098 400.9701 404.0798 384.0985 304.4594 -3.1059 400.8318 403.9377 383.9114 306.0536 -3.1020 400.6808 403.7829 383.6994 307.6750 -3.0967 400.5510 403.6477 383.5059 309.2660 -3.0844 400.4119 403.4963 383.3101 310.8733 -3.0829 400.2815 403.3644 383.1133 312.4658 -3.0797 400.1265 403.2062 382.9232 314.0759 -3.0702 399.9901 403.0603 382.7313 315.6895 -3.0650 399.8418 402.9069 382.5227 317.2885 -3.0601 399.6851 402.7452 382.3277 318.8903 -3.0547 399.5382 402.5929 382.1302 320.5065 -3.0479 399.3885 402.4364 381.9115 322.1055 -3.0424 399.2375 402.2799 381.7112 323.7195 -3.0370 399.0756 402.1125 381.5155 325.3335 -3.0325 398.9331 401.9656 381.3079 326.9475 -3.0251 398.7767 401.8019 381.0879 328.5466 -3.0241 398.6370 401.6610 380.8778 330.1464 -3.0150 398.4906 401.5056 380.6857 331.7604 -3.0063 398.3197 401.3261 380.4684 333.3741 -3.0024 398.1551 401.1575 380.2653 334.9878 -2.9970 398.0119 401.0088 380.0634 336.5866 -2.9896 397.8654 400.8550 379.8351 338.1795 -2.9845 397.7236 400.7081 379.6383 339.7865 -2.9777 397.5606 400.5383 379.4256 341.3939 -2.9743 397.3900 400.3644 379.2250 342.9860 -2.9674 397.2428 400.2102 379.0169 344.5935 -2.9627 397.0861 400.0488 378.8001 346.1886 -2.9595 396.9077 399.8672 378.5998 347.7875 -2.9517 396.7710 399.7227 378.3962 349.4073 -2.9465 396.5896 399.5360 378.1951 351.0125 -2.9391 396.4421 399.3812 377.9802 352.6115 -2.9361 396.2858 399.2219 377.7953 354.2255 -2.9324 396.1139 399.0464 377.6011 355.8243 -2.9292 395.9448 398.8740 377.3978 357.4381 -2.9242 395.7938 398.7180 377.1876 359.0521 -2.9166 395.6341 398.5506 376.9751 360.6509 -2.9122 395.4665 398.3786 376.7923 362.2648 -2.9056 395.3003 398.2059 376.6153 363.8643 -2.9010 395.1239 398.0250 376.4053 365.4789 -2.8959 394.9724 397.8683 376.2110 367.0929 -2.8913 394.7968 397.6881 376.0208 368.6915 -2.8855 394.6471 397.5326 375.8045 370.2913 -2.8783 394.4969 397.3753 375.6022 371.8861 -2.8722 394.3197 397.1920 375.4015 373.4929 -2.8714 394.1529 397.0243 375.2106 375.1154 -2.8655 393.9616 396.8270 374.9949 376.7079 -2.8572 393.7966 396.6538 374.7992 378.3040 -2.8535 393.6372 396.4908 374.6001 379.9178 -2.8485 393.4618 396.3103 374.3863 381.5169 -2.8427 393.3069 396.1496 374.1649 383.1310 -2.8379 393.1311 395.9691 373.9649 384.7449 -2.8342 392.9671 395.8013 373.7560 386.3438 -2.8257 392.8096 395.6353 373.5495 387.9428 -2.8242 392.6373 395.4615 373.3621 389.5574 -2.8202 392.4447 395.2649 373.1375 391.1735 -2.8152 392.2790 395.0942 372.9240 392.7879 -2.8057 392.1165 394.9222 372.7313 394.3868 -2.8004 391.9354 394.7358 372.5128 395.9858 -2.7950 391.7685 394.5635 372.3105 397.5996 -2.7922 391.5966 394.3888 372.1315 399.2136 -2.7840 391.4378 394.2219 371.9130 400.8288 -2.7772 391.2640 394.0412 371.7058 402.4266 -2.7748 391.0838 393.8586 371.4898 404.0180 -2.7692 390.8960 393.6652 371.2960 405.6248 -2.7656 390.7324 393.4980 371.1019 407.2336 -2.7642 390.5484 393.3126 370.9263 408.8424 -2.7562 390.3813 393.1375 370.7081 410.4364 -2.7529 390.2035 392.9563 370.5229 412.0341 -2.7516 390.0200 392.7717 370.3224 413.6478 -2.7464 389.8413 392.5877 370.1314 415.2619 -2.7394 389.6629 392.4023 369.9316 416.8759 -2.7378 389.4854 392.2232 369.7377 418.4748 -2.7330 389.3090 392.0420 369.5501 420.0738 -2.7246 389.1527 391.8773 369.3440 421.6876 -2.7186 388.9774 391.6960 369.1533 423.3168 -2.7165 388.7904 391.5068 368.9510 424.9156 -2.7123 388.6123 391.3247 368.7531 426.5146 -2.7052 388.4396 391.1448 368.5653 428.1285 -2.7025 388.2579 390.9604 368.3619 429.7275 -2.7005 388.0815 390.7820 368.1616 431.3401 -2.7023 387.9042 390.6065 367.9561 432.9673 -2.6996 387.7179 390.4175 367.7515 434.5639 -2.6888 387.5414 390.2302 367.5419 436.1550 -2.6761 387.3598 390.0358 367.3527 437.7626 -2.6716 387.1903 389.8620 367.1371 439.3556 -2.6695 387.0198 389.6894 366.9367 440.9780 -2.6634 386.8315 389.4949 366.7050 442.5719 -2.6599 386.6341 389.2940 366.5204 444.1688 -2.6549 386.4745 389.1295 366.2942 445.7825 -2.6508 386.2875 388.9383 366.1065 447.3816 -2.6439 386.1023 388.7462 365.9005 449.0105 -2.6400 385.9383 388.5783 365.6939 450.6095 -2.6383 385.7348 388.3731 365.5054 452.2086 -2.6327 385.5657 388.1984 365.2899 453.8225 -2.6259 385.3885 388.0143 365.0881 455.4221 -2.6230 385.2029 387.8259 364.8952 457.0515 -2.6144 385.0143 387.6287 364.6877 458.6505 -2.6099 384.8324 387.4423 364.4677 460.2495 -2.6055 384.6598 387.2654 364.2718 461.8635 -2.6024 384.4729 387.0754 364.0836 463.4623 -2.5976 384.3056 386.9032 363.8712 465.0936 -2.5936 384.1030 386.6966 363.6697 466.6898 -2.5875 383.9231 386.5106 363.4658 468.2799 -2.5833 383.7505 386.3338 363.2624 469.8873 -2.5787 383.5591 386.1378 363.0303 471.4940 -2.5713 383.3728 385.9441 362.8315 473.1034 -2.5692 383.1900 385.7592 362.6272 474.7001 -2.5664 383.0170 385.5835 362.4271 476.3128 -2.5561 382.8092 385.3653 362.1975 477.9115 -2.5519 382.6648 385.2167 361.9829 479.5105 -2.5476 382.4609 385.0084 361.7778 481.1395 -2.5415 382.2609 384.8024 361.5637 482.7385 -2.5361 382.0739 384.6100 361.3461 484.3375 -2.5334 381.8978 384.4312 361.1329 485.9515 -2.5303 381.7147 384.2450 360.9119 487.5503 -2.5256 381.5196 384.0452 360.7068 489.1794 -2.5192 381.3325 383.8516 360.5033 490.7781 -2.5145 381.1458 383.6604 360.2844 492.3918 -2.5085 380.9750 383.4836 360.0801 493.9908 -2.5023 380.7646 383.2670 359.8608 495.6050 -2.5016 380.6049 383.1065 359.6330 497.2189 -2.4946 380.3999 382.8945 359.4214 498.8151 -2.4894 380.2104 382.6998 359.2133 500.4216 -2.4863 380.0253 382.5117 358.9993 502.0138 -2.4800 379.8411 382.3211 358.7975 503.6211 -2.4769 379.6528 382.1297 358.5837 505.2303 -2.4863 379.4642 381.9504 358.3666 506.8259 -2.4830 379.2765 381.7595 358.1734 508.4385 -2.4808 379.0839 381.5647 357.9577 510.0373 -2.4768 378.8943 381.3711 357.7564 511.6510 -2.4678 378.6977 381.1655 357.5445 513.2630 -2.4646 378.5224 380.9870 357.3297 514.8750 -2.4594 378.3224 380.7819 357.1361 516.4738 -2.4542 378.1462 380.6003 356.9324 518.0878 -2.4500 377.9578 380.4078 356.7233 519.6868 -2.4443 377.7667 380.2110 356.5190 521.3009 -2.4386 377.5756 380.0142 356.3195 522.9149 -2.4358 377.3740 379.8098 356.1080 524.5288 -2.4287 377.1791 379.6078 355.9130 526.1276 -2.4272 377.0033 379.4305 355.7018 527.7268 -2.4230 376.8062 379.2291 355.5114 529.3556 -2.4193 376.6023 379.0216 355.2916 530.9693 -2.4140 376.4488 378.8629 355.0831 532.5615 -2.4093 376.2281 378.6374 354.8907 534.1536 -2.4028 376.0289 378.4316 354.7065 535.7608 -2.3996 375.8494 378.2490 354.4965 537.3831 -2.3955 375.6556 378.0511 354.3033 538.9773 -2.3948 375.4673 377.8621 354.1162 540.5888 -2.3884 375.2877 377.6761 353.9229 542.1878 -2.3864 375.1091 377.4955 353.7177 543.8019 -2.3835 374.8805 377.2640 353.5217 545.4159 -2.3742 374.7031 377.0773 353.3133 547.0148 -2.3612 374.5205 376.8817 353.1268 548.6288 -2.3525 374.3069 376.6594 352.9295 550.2278 -2.3461 374.1144 376.4606 352.7179 551.8418 -2.3447 373.9321 376.2768 352.5239 553.4558 -2.3418 373.7420 376.0838 352.3296 555.0696 -2.3378 373.5452 375.8829 352.1353 556.6690 -2.3336 373.3486 375.6821 351.9321 558.2685 -2.3329 373.1716 375.5045 351.7291 559.8975 -2.3273 372.9780 375.3053 351.5183 561.5116 -2.3221 372.8006 375.1227 351.3196 563.1106 -2.3197 372.5998 374.9195 351.1213 564.7021 -2.3145 372.3913 374.7058 350.9101 566.3096 -2.3088 372.1942 374.5030 350.6922 567.9170 -2.3050 372.0209 374.3259 350.4858 569.5248 -2.3050 371.8317 374.1367 350.2757 571.1194 -2.2982 371.6246 373.9228 350.0808 572.7308 -2.2961 371.4519 373.7480 349.8774 574.3359 -2.2926 371.2609 373.5535 349.6808 575.9396 -2.2909 371.0560 373.3469 349.4784 577.5686 -2.2854 370.8532 373.1386 349.2813 579.1676 -2.2755 370.6711 372.9466 349.0782 580.7815 -2.2717 370.4791 372.7508 348.8813 582.3805 -2.2685 370.3034 372.5719 348.6796 583.9945 -2.2644 370.0921 372.3564 348.4908 585.6085 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