DTA measure 1gyors Date: 202534:1050 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 919.27 s Mass = 956.3 mg data_number = 1139 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1850 0.0144 225.4479 225.4335 270.9073 2.0043 0.0151 225.7362 225.7211 270.7765 2.7820 0.0156 226.0118 225.9961 270.6442 3.6318 0.0163 226.3067 226.2904 270.4936 4.3890 0.0179 226.5756 226.5577 270.3611 5.2288 0.0190 226.8698 226.8508 270.2089 6.0168 0.0199 227.1461 227.1262 270.0638 6.8150 0.0217 227.4244 227.4026 269.9171 7.6343 0.0239 227.7113 227.6874 269.7647 8.4120 0.0269 227.9851 227.9582 269.6170 9.2620 0.0297 228.2859 228.2562 269.4516 10.0190 0.0313 228.5482 228.5169 269.3021 10.8590 0.0329 228.8390 228.8061 269.1357 11.6470 0.0348 229.1105 229.0757 268.9808 12.4558 0.0368 229.3882 229.3514 268.8257 13.2748 0.0384 229.6675 229.6291 268.6671 14.0423 0.0406 229.9250 229.8844 268.5178 14.8613 0.0430 230.2036 230.1606 268.3538 15.6390 0.0447 230.4613 230.4166 268.2040 16.4890 0.0468 230.7436 230.6968 268.0438 17.2665 0.0483 231.0018 230.9535 267.8954 18.0858 0.0504 231.2720 231.2216 267.7436 18.8840 0.0526 231.5367 231.4841 267.5993 19.6825 0.0549 231.8022 231.7473 267.4572 20.5015 0.0570 232.0732 232.0163 267.3159 21.2793 0.0583 232.3313 232.2731 267.1781 22.1290 0.0608 232.6036 232.5428 267.0303 22.8653 0.0628 232.8407 232.7780 266.9120 23.7258 0.0646 233.1150 233.0505 266.7777 24.4933 0.0667 233.3577 233.2909 266.6700 25.3123 0.0694 233.6121 233.5426 266.5570 26.1210 0.0716 233.8614 233.7898 266.4489 26.9088 0.0741 234.1094 234.0354 266.3563 27.7485 0.0763 234.3628 234.2865 266.2609 28.5055 0.0774 234.5944 234.5170 266.1792 29.3558 0.0792 234.8551 234.7759 266.0950 30.1333 0.0808 235.0923 235.0115 266.0270 30.9525 0.0831 235.3459 235.2628 265.9675 31.7510 0.0851 235.5831 235.4980 265.9181 32.5388 0.0868 235.8187 235.7319 265.8775 33.3783 0.0891 236.0663 235.9772 265.8425 34.1358 0.0903 236.2902 236.1999 265.8236 34.9858 0.0919 236.5437 236.4518 265.8112 35.7220 0.0931 236.7618 236.6686 265.8110 36.5723 0.0947 237.0047 236.9100 265.8213 37.3290 0.0962 237.2227 237.1265 265.8452 38.1583 0.0973 237.4601 237.3628 265.8820 38.9258 0.0988 237.6744 237.5755 265.9264 39.7758 0.1008 237.9085 237.8077 265.9833 40.5535 0.1020 238.1233 238.0212 266.0483 41.3728 0.1028 238.3558 238.2530 266.1309 42.1710 0.1019 238.5805 238.4786 266.2206 42.9588 0.1016 238.7952 238.6936 266.3191 43.7778 0.1019 239.0208 238.9189 266.4280 44.5450 0.1015 239.2347 239.1333 266.5410 45.3953 0.1010 239.4729 239.3719 266.6839 46.1730 0.1000 239.6877 239.5877 266.8221 46.9920 0.0990 239.9184 239.8193 266.9746 47.7490 0.0979 240.1264 240.0285 267.1323 48.5788 0.0978 240.3538 240.2560 267.3206 49.3770 0.0971 240.5642 240.4670 267.5090 50.1753 0.0954 240.7763 240.6809 267.7070 50.9943 0.0934 240.9934 240.9000 267.9209 51.7513 0.0922 241.1972 241.1050 268.1307 52.6120 0.0890 241.4219 241.3329 268.3835 53.3790 0.0864 241.6263 241.5399 268.6162 54.2083 0.0839 241.8396 241.7557 268.8765 54.9963 0.0810 242.0490 241.9680 269.1406 55.7950 0.0775 242.2565 242.1790 269.4156 56.6243 0.0736 242.4711 242.3975 269.7080 57.3810 0.0693 242.6681 242.5988 269.9786 58.2413 0.0649 242.8873 242.8224 270.3016 59.0090 0.0609 243.0865 243.0256 270.5963 59.8383 0.0564 243.3029 243.2464 270.9245 60.6263 0.0526 243.5119 243.4593 271.2441 61.4245 0.0477 243.7192 243.6715 271.5694 62.2543 0.0426 243.9307 243.8881 271.9132 63.0110 0.0377 244.1245 244.0868 272.2272 63.8718 0.0311 244.3471 244.3160 272.5891 64.6390 0.0253 244.5412 244.5160 272.9198 65.4683 0.0191 244.7525 244.7333 273.2819 66.2563 0.0127 244.9466 244.9339 273.6268 67.0545 0.0065 245.1468 245.1403 273.9870 67.9153 -0.0013 245.3592 245.3605 274.3775 68.7650 -0.0099 245.5776 245.5875 274.7631 69.7183 -0.0186 245.8184 245.8369 275.1973 70.5683 -0.0264 246.0305 246.0569 275.5889 71.4498 -0.0346 246.2537 246.2882 275.9950 72.2480 -0.0424 246.4543 246.4967 276.3588 73.0770 -0.0501 246.6627 246.7128 276.7321 73.9068 -0.0586 246.8735 246.9320 277.1057 74.7568 -0.0666 247.0840 247.1506 277.4846 75.5343 -0.0747 247.2745 247.3492 277.8369 76.3533 -0.0833 247.4796 247.5630 278.2064 77.1413 -0.0922 247.6828 247.7750 278.5589 77.9503 -0.1009 247.8873 247.9882 278.9118 78.8000 -0.1110 248.1005 248.2115 279.2805 79.5778 -0.1193 248.2981 248.4174 279.6132 80.3968 -0.1293 248.5065 248.6357 279.9603 81.1950 -0.1396 248.7051 248.8447 280.2886 81.9828 -0.1496 248.9016 249.0512 280.6089 82.8430 -0.1602 249.1231 249.2833 280.9536 83.5798 -0.1698 249.3081 249.4778 281.2443 84.4298 -0.1798 249.5269 249.7067 281.5702 85.2900 -0.1916 249.7499 249.9415 281.8925 86.0570 -0.2019 249.9417 250.1435 282.1816 86.8868 -0.2127 250.1514 250.3641 282.4793 87.6748 -0.2233 250.3504 250.5737 282.7540 88.4735 -0.2332 250.5510 250.7842 283.0221 89.2718 -0.2434 250.7504 250.9938 283.2889 90.0598 -0.2550 250.9488 251.2038 283.5399 90.8890 -0.2653 251.1597 251.4250 283.7945 91.6568 -0.2745 251.3599 251.6343 284.0249 92.5170 -0.2847 251.5841 251.8687 284.2691 93.2840 -0.2944 251.7796 252.0740 284.4843 94.1133 -0.3047 251.9912 252.2959 284.7075 94.9013 -0.3145 252.1866 252.5011 284.9173 95.6995 -0.3253 252.3919 252.7172 285.1193 96.5293 -0.3361 252.5981 252.9342 285.3225 97.2963 -0.3453 252.7944 253.1397 285.5001 98.1258 -0.3558 253.0044 253.3602 285.6799 98.8828 -0.3658 253.1943 253.5600 285.8380 99.7430 -0.3765 253.4073 253.7838 286.0171 100.5000 -0.3866 253.5954 253.9820 286.1591 101.3190 -0.3972 253.8011 254.1983 286.3096 102.1173 -0.4073 254.0037 254.4110 286.4483 102.9053 -0.4168 254.2050 254.6218 286.5803 103.7240 -0.4264 254.4144 254.8409 286.7121 104.4913 -0.4360 254.6098 255.0458 286.8259 105.3413 -0.4456 254.8224 255.2680 286.9468 106.1190 -0.4549 255.0213 255.4762 287.0478 106.9380 -0.4642 255.2340 255.6982 287.1534 107.6950 -0.4731 255.4263 255.8994 287.2433 108.5243 -0.4820 255.6393 256.1213 287.3264 109.3225 -0.4905 255.8455 256.3361 287.4021 110.1210 -0.4990 256.0453 256.5442 287.4699 110.9398 -0.5076 256.2533 256.7610 287.5359 111.6970 -0.5162 256.4508 256.9670 287.5857 112.5573 -0.5249 256.6695 257.1944 287.6404 113.3248 -0.5327 256.8658 257.3985 287.6843 114.1543 -0.5414 257.0753 257.6167 287.7217 114.9423 -0.5501 257.2777 257.8278 287.7525 115.7405 -0.5578 257.4816 258.0394 287.7798 116.5698 -0.5663 257.6960 258.2623 287.8018 117.3270 -0.5728 257.8924 258.4651 287.8170 118.1873 -0.5805 258.1097 258.6902 287.8266 118.9548 -0.5876 258.3085 258.8961 287.8329 119.7840 -0.5959 258.5186 259.1145 287.8400 120.5720 -0.6027 258.7186 259.3213 287.8365 121.3705 -0.6100 258.9197 259.5297 287.8381 122.1688 -0.6168 259.1222 259.7391 287.8323 122.9568 -0.6229 259.3174 259.9403 287.8277 123.7860 -0.6289 259.5249 260.1538 287.8162 124.5535 -0.6346 259.7229 260.3574 287.7957 125.4138 -0.6412 259.9436 260.5848 287.7755 126.1708 -0.6466 260.1315 260.7781 287.7542 127.0000 -0.6524 260.3340 260.9864 287.7238 127.7983 -0.6579 260.5304 261.1883 287.6889 128.5860 -0.6636 260.7253 261.3890 287.6575 129.4153 -0.6689 260.9265 261.5954 287.6243 130.1830 -0.6742 261.1188 261.7930 287.5985 131.0433 -0.6806 261.3344 262.0150 287.5598 131.8003 -0.6854 261.5172 262.2026 287.5309 132.6298 -0.6908 261.7181 262.4089 287.4984 133.4283 -0.6952 261.9151 262.6103 287.4618 134.2160 -0.6994 262.1054 262.8049 287.4260 135.0458 -0.7040 262.3075 263.0115 287.3879 135.8130 -0.7086 262.4893 263.1979 287.3534 136.6733 -0.7140 262.6963 263.4103 287.3187 137.3993 -0.7178 262.8678 263.5856 287.2871 138.2600 -0.7216 263.0767 263.7983 287.2525 139.0273 -0.7258 263.2585 263.9842 287.2260 139.8468 -0.7302 263.4501 264.1803 287.1962 140.6553 -0.7344 263.6438 264.3781 287.1681 141.4430 -0.7378 263.8245 264.5622 287.1433 142.2723 -0.7406 264.0205 264.7611 287.1191 143.0398 -0.7436 264.2016 264.9453 287.0985 143.9000 -0.7483 264.4019 265.1502 287.0873 144.6570 -0.7518 264.5792 265.3310 287.0809 145.4865 -0.7559 264.7722 265.5281 287.0754 146.2848 -0.7602 264.9570 265.7172 287.0758 147.0728 -0.7639 265.1334 265.8973 287.0771 147.9020 -0.7679 265.3177 266.0856 287.0778 148.6695 -0.7708 265.4903 266.2611 287.0832 149.4990 -0.7735 265.6801 266.4536 287.0959 150.2558 -0.7764 265.8536 266.6300 287.1146 151.1263 -0.7801 266.0495 266.8296 287.1417 151.8833 -0.7838 266.2180 267.0018 287.1674 152.7128 -0.7867 266.4003 267.1870 287.2026 153.5113 -0.7902 266.5741 267.3642 287.2497 154.2990 -0.7931 266.7497 267.5428 287.2950 155.1283 -0.7955 266.9334 267.7289 287.3469 155.8958 -0.7986 267.1032 267.9018 287.4041 156.7560 -0.8021 267.2901 268.0922 287.4813 157.5130 -0.8056 267.4553 268.2609 287.5499 158.3425 -0.8092 267.6434 268.4526 287.6360 159.1408 -0.8122 267.8208 268.6330 287.7247 159.9288 -0.8159 267.9893 268.8052 287.8175 160.7580 -0.8186 268.1664 268.9849 287.9250 161.5258 -0.8225 268.3259 269.1485 288.0306 162.3860 -0.8257 268.4986 269.3243 288.1487 163.1428 -0.8289 268.6552 269.4841 288.2603 163.9618 -0.8329 268.8311 269.6640 288.3873 164.7600 -0.8355 269.0023 269.8378 288.5198 165.5480 -0.8388 269.1678 270.0066 288.6613 166.3670 -0.8428 269.3396 270.1824 288.8150 167.1343 -0.8466 269.4952 270.3418 288.9632 167.9843 -0.8516 269.6741 270.5257 289.1341 168.7623 -0.8559 269.8392 270.6950 289.3009 169.5810 -0.8602 270.0149 270.8751 289.4844 170.3690 -0.8644 270.1812 271.0456 289.6598 171.1673 -0.8693 270.3470 271.2163 289.8433 171.9863 -0.8741 270.5182 271.3923 290.0393 172.7535 -0.8777 270.6779 271.5556 290.2308 173.6140 -0.8825 270.8583 271.7409 290.4553 174.3710 -0.8872 271.0082 271.8954 290.6550 175.2003 -0.8917 271.1749 272.0666 290.8765 175.9883 -0.8967 271.3399 272.2367 291.0890 176.7868 -0.9017 271.5079 272.4096 291.3111 177.6163 -0.9080 271.6806 272.5886 291.5485 178.3730 -0.9126 271.8349 272.7476 291.7727 179.2333 -0.9189 272.0127 272.9316 292.0283 179.9908 -0.9241 272.1624 273.0865 292.2550 180.8200 -0.9301 272.3299 273.2599 292.5142 181.6183 -0.9360 272.4877 273.4237 292.7739 182.4063 -0.9426 272.6473 273.5899 293.0309 183.2358 -0.9479 272.8151 273.7630 293.3068 184.0030 -0.9533 272.9752 273.9286 293.5569 184.8323 -0.9597 273.1498 274.1095 293.8326 185.5893 -0.9662 273.3017 274.2680 294.0830 186.4495 -0.9738 273.4770 274.4508 294.3715 187.2170 -0.9806 273.6308 274.6114 294.6319 188.0360 -0.9878 273.7919 274.7796 294.9039 188.8343 -0.9941 273.9509 274.9451 295.1774 189.6328 -1.0009 274.1213 275.1222 295.4473 190.4620 -1.0083 274.2935 275.3018 295.7250 191.2188 -1.0145 274.4441 275.4587 295.9797 192.0790 -1.0221 274.6215 275.6436 296.2724 192.8463 -1.0292 274.7820 275.8112 296.5320 193.6653 -1.0367 274.9492 275.9859 296.8142 194.4638 -1.0438 275.1097 276.1535 297.0866 195.2620 -1.0513 275.2725 276.3238 297.3587 196.0603 -1.0592 275.4350 276.4942 297.6242 196.8483 -1.0666 275.5954 276.6621 297.8856 197.6880 -1.0746 275.7734 276.8480 298.1670 198.4453 -1.0809 275.9305 277.0114 298.4131 199.2950 -1.0892 276.1082 277.1975 298.6877 200.0730 -1.0967 276.2678 277.3645 298.9314 200.8920 -1.1046 276.4381 277.5427 299.1829 201.6903 -1.1117 276.5968 277.7085 299.4237 202.4888 -1.1203 276.7575 277.8778 299.6653 203.3180 -1.1289 276.9281 278.0570 299.9111 204.0748 -1.1361 277.0830 278.2191 300.1340 204.9355 -1.1446 277.2631 278.4077 300.3843 205.7028 -1.1522 277.4190 278.5712 300.6031 206.5218 -1.1606 277.5859 278.7464 300.8317 207.3200 -1.1682 277.7487 278.9169 301.0525 208.1180 -1.1766 277.9147 279.0913 301.2622 208.9473 -1.1853 278.0855 279.2708 301.4763 209.7148 -1.1931 278.2481 279.4412 301.6711 210.5443 -1.2014 278.4215 279.6228 301.8806 211.3013 -1.2090 278.5792 279.7883 302.0630 212.1615 -1.2183 278.7583 279.9766 302.2630 212.9290 -1.2259 278.9195 280.1454 302.4390 213.7585 -1.2339 279.0926 280.3265 302.6211 214.5568 -1.2414 279.2570 280.4983 302.7950 215.3448 -1.2489 279.4204 280.6693 302.9620 216.1843 -1.2571 279.6000 280.8571 303.1322 216.9415 -1.2640 279.7586 281.0226 303.2754 217.8018 -1.2720 279.9365 281.2085 303.4436 218.5690 -1.2789 280.0939 281.3728 303.5836 219.3983 -1.2867 280.2689 281.5556 303.7325 220.1865 -1.2932 280.4413 281.7345 303.8691 220.9850 -1.3005 280.6091 281.9096 304.0050 221.8143 -1.3078 280.7833 282.0911 304.1381 222.5710 -1.3135 280.9482 282.2617 304.2511 223.4315 -1.3210 281.1379 282.4589 304.3770 224.1988 -1.3277 281.3053 282.6330 304.4816 225.0280 -1.3354 281.4808 282.8162 304.5905 225.8265 -1.3419 281.6522 282.9941 304.6968 226.6248 -1.3485 281.8155 283.1639 304.8001 227.4438 -1.3554 281.9903 283.3457 304.8943 228.2008 -1.3620 282.1478 283.5098 304.9761 229.0610 -1.3696 282.3308 283.7004 305.0591 229.8180 -1.3758 282.4908 283.8666 305.1335 230.6370 -1.3817 282.6564 284.0381 305.2110 231.4353 -1.3874 282.8259 284.2134 305.2789 232.2233 -1.3932 282.9905 284.3837 305.3399 233.0318 -1.3986 283.1618 284.5603 305.4025 233.8198 -1.4047 283.3325 284.7371 305.4606 234.6388 -1.4105 283.5052 284.9157 305.5205 235.4060 -1.4157 283.6682 285.0839 305.5719 236.2558 -1.4212 283.8417 285.2629 305.6211 237.0233 -1.4264 284.0000 285.4264 305.6658 237.8528 -1.4316 284.1723 285.6039 305.7130 238.6408 -1.4372 284.3342 285.7714 305.7582 239.4393 -1.4426 284.5004 285.9430 305.7951 240.2273 -1.4464 284.6625 286.1089 305.8285 241.0255 -1.4505 284.8304 286.2809 305.8589 241.8548 -1.4551 285.0066 286.4617 305.8938 242.6118 -1.4594 285.1584 286.6178 305.9270 243.4723 -1.4648 285.3339 286.7987 305.9548 244.2398 -1.4690 285.4894 286.9584 305.9822 245.0690 -1.4734 285.6583 287.1317 306.0119 245.8568 -1.4779 285.8206 287.2985 306.0353 246.6550 -1.4818 285.9828 287.4646 306.0573 247.4848 -1.4859 286.1509 287.6368 306.0862 248.2418 -1.4906 286.2990 287.7896 306.1066 249.0710 -1.4946 286.4664 287.9609 306.1277 249.8388 -1.4982 286.6246 288.1228 306.1426 250.6990 -1.5027 286.8035 288.3062 306.1659 251.4558 -1.5062 286.9598 288.4659 306.1916 252.2850 -1.5097 287.1289 288.6386 306.2192 253.0835 -1.5128 287.2924 288.8052 306.2444 253.8718 -1.5159 287.4586 288.9745 306.2695 254.7010 -1.5191 287.6251 289.1442 306.2949 255.4680 -1.5223 287.7762 289.2985 306.3186 256.3283 -1.5251 287.9492 289.4743 306.3493 257.0545 -1.5279 288.0916 289.6195 306.3746 257.9150 -1.5318 288.2662 289.7980 306.4065 258.6823 -1.5347 288.4284 289.9632 306.4371 259.5010 -1.5371 288.5943 290.1314 306.4751 260.3098 -1.5402 288.7601 290.3003 306.5181 261.0978 -1.5436 288.9178 290.4614 306.5518 261.9270 -1.5462 289.0819 290.6281 306.5927 262.6940 -1.5496 289.2368 290.7864 306.6367 263.5545 -1.5523 289.4079 290.9603 306.6870 264.3118 -1.5548 289.5543 291.1091 306.7371 265.1410 -1.5580 289.7190 291.2770 306.7943 265.9393 -1.5612 289.8777 291.4389 306.8525 266.7375 -1.5635 290.0336 291.5971 306.9203 267.5668 -1.5670 290.1964 291.7633 306.9965 268.3238 -1.5692 290.3460 291.9151 307.0684 269.1840 -1.5724 290.5153 292.0877 307.1533 269.9205 -1.5747 290.6558 292.2305 307.2269 270.7805 -1.5777 290.8184 292.3961 307.3267 271.5378 -1.5794 290.9675 292.5469 307.4084 272.3670 -1.5821 291.1260 292.7081 307.5013 273.1963 -1.5849 291.2831 292.8681 307.5990 273.9533 -1.5869 291.4279 293.0149 307.6926 274.7830 -1.5895 291.5840 293.1735 307.8017 275.5500 -1.5922 291.7243 293.3164 307.9058 276.4103 -1.5954 291.8892 293.4846 308.0276 277.1778 -1.5986 292.0380 293.6366 308.1433 278.0070 -1.6023 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