DTA measure 1lassu Date: 202534:1143 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1336.76 s Mass = 956.300 mg data_number = 1655 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.3098 -2.0290 241.5171 243.5461 249.0124 2.1290 -2.0323 241.5296 243.5619 249.1813 2.9273 -2.0356 241.5500 243.5856 249.3336 3.7260 -2.0379 241.5655 243.6034 249.4805 4.5140 -2.0401 241.5817 243.6218 249.6131 5.3020 -2.0418 241.5987 243.6405 249.7386 6.1213 -2.0434 241.6178 243.6611 249.8565 6.8885 -2.0449 241.6395 243.6845 249.9618 7.7493 -2.0455 241.6565 243.7020 250.0710 8.5063 -2.0465 241.6793 243.7258 250.1569 9.3360 -2.0473 241.7048 243.7521 250.2438 10.1240 -2.0477 241.7325 243.7802 250.3131 10.9225 -2.0480 241.7639 243.8119 250.3798 11.7520 -2.0484 241.7939 243.8423 250.4438 12.5090 -2.0483 241.8225 243.8708 250.5001 13.3383 -2.0479 241.8539 243.9018 250.5493 14.0953 -2.0477 241.8844 243.9321 250.5814 14.9458 -2.0468 241.9175 243.9643 250.6189 15.7235 -2.0462 241.9482 243.9944 250.6480 16.5428 -2.0450 241.9834 244.0283 250.6700 17.3413 -2.0444 242.0293 244.0737 250.6823 18.1293 -2.0434 242.0701 244.1135 250.6856 18.9485 -2.0418 242.1107 244.1525 250.6831 19.7263 -2.0397 242.1562 244.1958 250.6760 20.5763 -2.0364 242.2005 244.2369 250.6615 21.3440 -2.0341 242.2367 244.2708 250.6439 22.1630 -2.0312 242.2748 244.3061 250.6207 22.9718 -2.0285 242.3179 244.3464 250.5913 23.7598 -2.0258 242.3587 244.3846 250.5593 24.5790 -2.0236 242.4044 244.4280 250.5208 25.3568 -2.0203 242.4475 244.4678 250.4769 26.2068 -2.0161 242.4955 244.5116 250.4243 26.9743 -2.0118 242.5338 244.5456 250.3703 27.7933 -2.0078 242.5826 244.5904 250.3120 28.5818 -2.0042 242.6388 244.6431 250.2522 29.4010 -1.9994 242.6872 244.6866 250.1895 30.1993 -1.9939 242.7340 244.7279 250.1202 30.9873 -1.9891 242.7871 244.7762 250.0504 31.8273 -1.9836 242.8324 244.8160 249.9712 32.5843 -1.9787 242.8779 244.8566 249.8941 33.4348 -1.9726 242.9283 244.9009 249.8050 34.2123 -1.9673 242.9746 244.9419 249.7197 35.0318 -1.9615 243.0288 244.9904 249.6229 35.8300 -1.9559 243.0804 245.0362 249.5283 36.6285 -1.9507 243.1275 245.0782 249.4304 37.4580 -1.9443 243.1783 245.1226 249.3278 38.2148 -1.9389 243.2292 245.1681 249.2265 39.0648 -1.9327 243.2874 245.2201 249.1121 39.8325 -1.9264 243.3365 245.2629 249.0062 40.6928 -1.9189 243.3893 245.3081 248.8939 41.4188 -1.9129 243.4342 245.3470 248.7921 42.2893 -1.9054 243.4897 245.3951 248.6683 43.0465 -1.8985 243.5427 245.4412 248.5607 43.8760 -1.8907 243.5957 245.4864 248.4378 44.6743 -1.8826 243.6444 245.5270 248.3188 45.4728 -1.8746 243.6996 245.5742 248.1988 46.2918 -1.8669 243.7545 245.6214 248.0692 47.0595 -1.8593 243.8053 245.6647 247.9499 47.9198 -1.8511 243.8609 245.7120 247.8076 48.6560 -1.8438 243.9111 245.7548 247.6834 49.5270 -1.8340 243.9706 245.8046 247.5372 50.3048 -1.8266 244.0239 245.8505 247.4072 51.1238 -1.8191 244.0799 245.8989 247.2664 51.8910 -1.8115 244.1299 245.9415 247.1330 52.7098 -1.8036 244.1865 245.9901 246.9873 53.5185 -1.7956 244.2426 246.0382 246.8435 54.3068 -1.7883 244.2969 246.0852 246.7000 55.1463 -1.7793 244.3527 246.1320 246.5456 55.9033 -1.7705 244.4035 246.1741 246.4059 56.7635 -1.7612 244.4575 246.2186 246.2460 57.5308 -1.7530 244.5109 246.2639 246.1030 58.3498 -1.7443 244.5706 246.3150 245.9483 59.1483 -1.7357 244.6227 246.3584 245.8015 59.9468 -1.7277 244.6722 246.3999 245.6497 60.7760 -1.7188 244.7262 246.4450 245.4816 61.5328 -1.7102 244.7775 246.4878 245.3330 62.3933 -1.7009 244.8349 246.5358 245.1635 63.1608 -1.6932 244.8853 246.5784 245.0101 63.9798 -1.6855 244.9427 246.6281 244.8467 64.7780 -1.6767 244.9949 246.6716 244.6927 65.5663 -1.6683 245.0453 246.7136 244.5393 66.4060 -1.6599 245.0953 246.7552 244.3725 67.1628 -1.6521 245.1453 246.7974 244.2244 68.0130 -1.6424 245.2007 246.8431 244.0558 68.7803 -1.6338 245.2508 246.8846 243.8986 69.5993 -1.6252 245.3014 246.9265 243.7309 70.3870 -1.6157 245.3453 246.9609 243.5693 71.1853 -1.6056 245.3971 247.0027 243.4047 72.0043 -1.5958 245.4444 247.0402 243.2355 72.7820 -1.5879 245.4926 247.0805 243.0786 73.6013 -1.5788 245.5391 247.1180 242.9149 74.3580 -1.5705 245.5820 247.1525 242.7672 75.2183 -1.5607 245.6377 247.1984 242.5991 75.9755 -1.5524 245.6861 247.2385 242.4489 76.8050 -1.5443 245.7308 247.2751 242.2850 77.6033 -1.5361 245.7796 247.3157 242.1307 78.3910 -1.5277 245.8250 247.3528 241.9785 79.2203 -1.5184 245.8732 247.3916 241.8131 79.9778 -1.5101 245.9161 247.4263 241.6704 80.8380 -1.5012 245.9628 247.4640 241.5117 81.6053 -1.4933 246.0036 247.4969 241.3741 82.4240 -1.4844 246.0521 247.5364 241.2321 83.1918 -1.4760 246.0937 247.5696 241.0994 84.0108 -1.4674 246.1321 247.5995 240.9629 84.8193 -1.4593 246.1726 247.6319 240.8311 85.6073 -1.4512 246.2157 247.6668 240.7099 86.4260 -1.4436 246.2554 247.6990 240.5869 87.2040 -1.4362 246.2936 247.7299 240.4740 88.0540 -1.4281 246.3361 247.7643 240.3510 88.7903 -1.4200 246.3699 247.7899 240.2493 89.6403 -1.4116 246.4079 247.8194 240.1413 90.4180 -1.4035 246.4447 247.8482 240.0448 91.2368 -1.3955 246.4799 247.8755 239.9486 92.0248 -1.3879 246.5144 247.9023 239.8657 92.8333 -1.3796 246.5547 247.9343 239.7838 93.6520 -1.3718 246.5892 247.9610 239.7042 94.4193 -1.3653 246.6236 247.9888 239.6359 95.2698 -1.3571 246.6600 248.0171 239.5711 96.0473 -1.3504 246.6938 248.0442 239.5177 96.8663 -1.3430 246.7320 248.0749 239.4650 97.6540 -1.3366 246.7642 248.1007 239.4241 98.4628 -1.3296 246.7980 248.1276 239.3894 99.2818 -1.3227 246.8265 248.1492 239.3642 100.0490 -1.3174 246.8549 248.1723 239.3470 100.8993 -1.3107 246.8862 248.1969 239.3358 101.6770 -1.3047 246.9142 248.2189 239.3400 102.4958 -1.2984 246.9440 248.2424 239.3526 103.2840 -1.2928 246.9722 248.2650 239.3715 104.0928 -1.2869 247.0051 248.2920 239.4019 104.9118 -1.2808 247.0335 248.3144 239.4400 105.6790 -1.2757 247.0611 248.3368 239.4828 106.4983 -1.2705 247.0932 248.3636 239.5319 107.2760 -1.2661 247.1208 248.3869 239.5918 108.1258 -1.2612 247.1511 248.4123 239.6670 108.8828 -1.2564 247.1816 248.4380 239.7427 109.7228 -1.2515 247.2166 248.4681 239.8353 110.5108 -1.2474 247.2443 248.4917 239.9360 111.3193 -1.2435 247.2703 248.5138 240.0507 112.1383 -1.2403 247.2985 248.5388 240.1706 112.9060 -1.2363 247.3231 248.5594 240.2954 113.7560 -1.2324 247.3546 248.5870 240.4421 114.5340 -1.2295 247.3806 248.6101 240.5848 115.3528 -1.2264 247.4073 248.6337 240.7421 116.1613 -1.2237 247.4326 248.6563 240.9120 116.9493 -1.2202 247.4574 248.6776 241.0884 117.7685 -1.2171 247.4825 248.6996 241.2786 118.5463 -1.2146 247.5072 248.7218 241.4642 119.3963 -1.2129 247.5338 248.7467 241.6754 120.1638 -1.2105 247.5585 248.7690 241.8763 120.9828 -1.2077 247.5906 248.7983 242.1016 121.7915 -1.2058 247.6166 248.8224 242.3269 122.5793 -1.2045 247.6388 248.8433 242.5526 123.4190 -1.2033 247.6675 248.8707 242.7974 124.1763 -1.2022 247.6961 248.8984 243.0265 125.0263 -1.2014 247.7337 248.9351 243.2954 125.8038 -1.2007 247.7615 248.9623 243.5485 126.6230 -1.2002 247.7919 248.9920 243.8139 127.4213 -1.1997 247.8191 249.0188 244.0824 128.2195 -1.1997 247.8446 249.0444 244.3533 129.0485 -1.1999 247.8777 249.0777 244.6406 129.8058 -1.1998 247.9049 249.1047 244.9019 130.6658 -1.1993 247.9316 249.1309 245.2006 131.4023 -1.1997 247.9537 249.1534 245.4687 132.2625 -1.1996 247.9832 249.1828 245.7842 132.9988 -1.2001 248.0124 249.2126 246.0548 133.8488 -1.2012 248.0481 249.2494 246.3674 134.6160 -1.2025 248.0759 249.2784 246.6506 135.4348 -1.2038 248.1062 249.3100 246.9564 136.2230 -1.2054 248.1406 249.3461 247.2439 137.0318 -1.2070 248.1761 249.3832 247.5443 137.8403 -1.2088 248.2141 249.4229 247.8491 138.6180 -1.2107 248.2441 249.4548 248.1364 139.4678 -1.2136 248.2700 249.4836 248.4508 140.1940 -1.2165 248.3003 249.5168 248.7197 141.0543 -1.2183 248.3312 249.5495 249.0340 141.8113 -1.2203 248.3685 249.5888 249.3092 142.6405 -1.2222 248.4080 249.6301 249.6115 143.4393 -1.2243 248.4479 249.6722 249.8988 144.2270 -1.2266 248.4867 249.7133 250.1807 145.0568 -1.2297 248.5273 249.7570 250.4754 145.8138 -1.2327 248.5658 249.7985 250.7394 146.6740 -1.2358 248.6086 249.8444 251.0357 147.4413 -1.2396 248.6500 249.8896 251.2938 148.2603 -1.2437 248.6918 249.9355 251.5702 149.0590 -1.2473 248.7275 249.9748 251.8305 149.8570 -1.2509 248.7680 250.0189 252.0871 150.6863 -1.2554 248.8080 250.0634 252.3487 151.4433 -1.2591 248.8462 250.1053 252.5831 152.3038 -1.2633 248.8902 250.1535 252.8411 153.0713 -1.2665 248.9339 250.2003 253.0649 153.8900 -1.2709 248.9847 250.2556 253.3015 154.6678 -1.2745 249.0269 250.3014 253.5289 155.4868 -1.2784 249.0763 250.3547 253.7572 156.2850 -1.2819 249.1228 250.4047 253.9680 157.0728 -1.2860 249.1676 250.4536 254.1707 157.9123 -1.2896 249.2170 250.5067 254.3875 158.6695 -1.2928 249.2666 250.5594 254.5774 159.5195 -1.2967 249.3206 250.6173 254.7798 160.2973 -1.3003 249.3721 250.6724 254.9592 161.1160 -1.3037 249.4251 250.7287 255.1416 161.9143 -1.3069 249.4814 250.7884 255.3136 162.7128 -1.3107 249.5338 250.8445 255.4795 163.5423 -1.3140 249.5909 250.9049 255.6520 164.2993 -1.3173 249.6404 250.9577 255.7931 165.1595 -1.3213 249.7008 251.0221 255.9471 165.9270 -1.3253 249.7483 251.0736 256.0836 166.7460 -1.3283 249.8067 251.1350 256.2194 167.5443 -1.3314 249.8657 251.1971 256.3438 168.3428 -1.3340 249.9225 251.2565 256.4723 169.1720 -1.3365 249.9843 251.3208 256.5917 169.9290 -1.3392 250.0397 251.3789 256.6972 170.7895 -1.3423 250.0992 251.4415 256.8086 171.5568 -1.3448 250.1511 251.4959 256.9015 172.3760 -1.3472 250.2125 251.5598 256.9999 173.1743 -1.3500 250.2678 251.6178 257.0898 173.9728 -1.3529 250.3263 251.6792 257.1744 174.8020 -1.3552 250.3918 251.7471 257.2547 175.5593 -1.3570 250.4540 251.8111 257.3296 176.4195 -1.3590 250.5222 251.8812 257.4043 177.1873 -1.3615 250.5829 251.9444 257.4654 178.0060 -1.3642 250.6484 252.0126 257.5251 178.8148 -1.3667 250.7121 252.0788 257.5798 179.6028 -1.3687 250.7716 252.1403 257.6297 180.4320 -1.3710 250.8359 252.2069 257.6810 181.1990 -1.3722 250.8980 252.2702 257.7216 182.0598 -1.3746 250.9730 252.3475 257.7586 182.8168 -1.3753 251.0354 252.4106 257.7891 183.6460 -1.3766 251.1016 252.4782 257.8234 184.4443 -1.3771 251.1630 252.5401 257.8488 185.2323 -1.3785 251.2301 252.6086 257.8654 186.0720 -1.3791 251.3019 252.6810 257.8816 186.8290 -1.3797 251.3677 252.7474 257.8935 187.6893 -1.3808 251.4390 252.8198 257.9005 188.4568 -1.3819 251.5010 252.8829 257.9020 189.2860 -1.3828 251.5637 252.9465 257.9021 190.0533 -1.3834 251.6238 253.0072 257.9029 190.8830 -1.3849 251.6920 253.0769 257.8935 191.6708 -1.3851 251.7572 253.1423 257.8844 192.4690 -1.3851 251.8231 253.2082 257.8769 193.2988 -1.3853 251.8981 253.2834 257.8621 194.0558 -1.3858 251.9656 253.3513 257.8501 194.9160 -1.3853 252.0407 253.4261 257.8328 195.6730 -1.3852 252.1058 253.4910 257.8151 196.4920 -1.3857 252.1779 253.5636 257.7977 197.2903 -1.3861 252.2430 253.6290 257.7774 198.0783 -1.3854 252.3177 253.7031 257.7533 198.8873 -1.3845 252.3941 253.7786 257.7340 199.6753 -1.3835 252.4625 253.8460 257.7142 200.4940 -1.3834 252.5300 253.9134 257.6921 201.2613 -1.3829 252.5981 253.9809 257.6683 202.1113 -1.3822 252.6722 254.0545 257.6403 202.8683 -1.3813 252.7363 254.1176 257.6203 203.7083 -1.3803 252.8093 254.1897 257.5937 204.4960 -1.3789 252.8787 254.2576 257.5686 205.2943 -1.3777 252.9492 254.3268 257.5481 206.1133 -1.3769 253.0162 254.3931 257.5239 206.8805 -1.3761 253.0779 254.4540 257.4967 207.7410 -1.3752 253.1477 254.5230 257.4677 208.4670 -1.3742 253.2108 254.5850 257.4417 209.3273 -1.3732 253.2828 254.6560 257.4228 210.0948 -1.3719 253.3498 254.7218 257.4053 210.9240 -1.3703 253.4244 254.7948 257.3890 211.7123 -1.3690 253.4903 254.8593 257.3761 212.5105 -1.3673 253.5549 254.9222 257.3624 213.3398 -1.3656 253.6256 254.9911 257.3491 214.0968 -1.3638 253.6868 255.0506 257.3407 214.9570 -1.3629 253.7592 255.1221 257.3289 215.7243 -1.3617 253.8189 255.1806 257.3246 216.5540 -1.3610 253.8869 255.2480 257.3206 217.3420 -1.3600 253.9499 255.3099 257.3220 218.1405 -1.3590 254.0142 255.3731 257.3207 218.9698 -1.3578 254.0867 255.4445 257.3275 219.7268 -1.3562 254.1480 255.5042 257.3391 220.5870 -1.3543 254.2171 255.5714 257.3563 221.3233 -1.3533 254.2792 255.6325 257.3669 222.1838 -1.3514 254.3507 255.7021 257.3850 222.9408 -1.3496 254.4108 255.7604 257.4060 223.7803 -1.3487 254.4752 255.8239 257.4272 224.5683 -1.3472 254.5385 255.8857 257.4573 225.3665 -1.3455 254.6059 255.9514 257.4951 226.1958 -1.3443 254.6743 256.0186 257.5348 226.9528 -1.3430 254.7355 256.0785 257.5771 227.8130 -1.3413 254.8090 256.1504 257.6293 228.5803 -1.3400 254.8701 256.2101 257.6770 229.4098 -1.3370 254.9406 256.2776 257.7360 230.1978 -1.3347 255.0085 256.3432 257.7956 230.9960 -1.3331 255.0735 256.4065 257.8569 231.8253 -1.3314 255.1363 256.4677 257.9287 232.5823 -1.3299 255.1963 256.5262 257.9993 233.4428 -1.3281 255.2659 256.5940 258.0851 234.2100 -1.3263 255.3305 256.6568 258.1638 235.0393 -1.3251 255.4010 256.7261 258.2533 235.8273 -1.3241 255.4658 256.7899 258.3477 236.6258 -1.3225 255.5272 256.8497 258.4477 237.4553 -1.3207 255.5947 256.9154 258.5621 238.2120 -1.3194 255.6554 256.9748 258.6670 239.0723 -1.3185 255.7231 257.0417 258.7871 239.8398 -1.3176 255.7777 257.0954 258.9064 240.6693 -1.3172 255.8414 257.1586 259.0389 241.4573 -1.3167 255.9056 257.2223 259.1619 242.2560 -1.3162 255.9679 257.2840 259.3000 243.0853 -1.3148 256.0363 257.3511 259.4474 243.8420 -1.3140 256.0966 257.4107 259.5842 244.7028 -1.3130 256.1663 257.4793 259.7430 245.4700 -1.3125 256.2334 257.5460 259.8868 246.2993 -1.3122 256.3040 257.6162 260.0427 247.0978 -1.3109 256.3744 257.6853 260.2026 247.8960 -1.3105 256.4455 257.7559 260.3676 248.7148 -1.3100 256.5128 257.8228 260.5433 249.4923 -1.3100 256.5759 257.8858 260.7100 250.3425 -1.3102 256.6448 257.9550 260.9011 251.0790 -1.3101 256.7078 258.0179 261.0702 251.9393 -1.3105 256.7801 258.0906 261.2711 252.6960 -1.3110 256.8418 258.1528 261.4500 253.5358 -1.3106 256.9104 258.2210 261.6477 254.3238 -1.3114 256.9778 258.2892 261.8343 255.1220 -1.3119 257.0461 258.3580 262.0264 255.9410 -1.3124 257.1184 258.4308 262.2286 256.7190 -1.3126 257.1869 258.4995 262.4235 257.5688 -1.3124 257.2613 258.5737 262.6390 258.3258 -1.3128 257.3271 258.6399 262.8346 259.1550 -1.3136 257.3967 258.7104 263.0471 259.9530 -1.3151 257.4623 258.7774 263.2483 260.7310 -1.3161 257.5315 258.8476 263.4461 261.5603 -1.3181 257.6107 258.9288 263.6591 262.3278 -1.3201 257.6814 259.0014 263.8601 263.1775 -1.3209 257.7633 259.0842 264.0794 263.9345 -1.3220 257.8359 259.1579 264.2769 264.7638 -1.3234 257.9099 259.2333 264.4935 265.5210 -1.3252 257.9801 259.3053 264.6842 266.3813 -1.3276 258.0567 259.3844 264.9109 267.1488 -1.3290 258.1248 259.4538 265.1091 267.9780 -1.3310 258.1985 259.5295 265.3216 268.7663 -1.3326 258.2704 259.6030 265.5235 269.5540 -1.3342 258.3428 259.6770 265.7210 270.3833 -1.3368 258.4251 259.7618 265.9363 271.1508 -1.3391 258.4978 259.8368 266.1291 272.0110 -1.3413 258.5797 259.9210 266.3470 272.7680 -1.3435 258.6517 259.9952 266.5333 273.5970 -1.3456 258.7256 260.0712 266.7389 274.3540 -1.3475 258.7939 260.1414 266.9241 275.2145 -1.3504 258.8749 260.2252 267.1342 275.9718 -1.3518 258.9421 260.2939 267.3139 276.8010 -1.3545 259.0155 260.3700 267.5077 277.5990 -1.3571 259.0891 260.4462 267.6886 278.3973 -1.3594 259.1659 260.5253 267.8632 279.2165 -1.3614 259.2460 260.6074 268.0425 279.9838 -1.3640 259.3222 260.6862 268.2089 280.8443 -1.3672 259.4030 260.7701 268.3929 281.6010 -1.3695 259.4764 260.8459 268.5506 282.4303 -1.3710 259.5578 260.9288 268.7212 283.2288 -1.3731 259.6401 261.0132 268.8855 284.0270 -1.3750 259.7186 261.0936 269.0433 284.8153 -1.3771 259.8000 261.1772 269.1962 285.6240 -1.3794 259.8764 261.2558 269.3471 286.4428 -1.3820 259.9531 261.3351 269.4981 287.2100 -1.3847 260.0313 261.4161 269.6355 288.0703 -1.3875 260.1210 261.5085 269.7846 288.8270 -1.3902 260.2001 261.5904 269.9147 289.6568 -1.3926 260.2863 261.6789 270.0567 290.4240 -1.3950 260.3655 261.7605 270.1796 291.2533 -1.3975 260.4579 261.8554 270.3106 292.0420 -1.3995 260.5353 261.9348 270.4351 292.8410 -1.4008 260.6170 262.0178 270.5509 293.6710 -1.4029 260.7058 262.1087 270.6646 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