DTA measure 2gyors Date: 202534:1119 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1614.53 s Mass = 956.3 mg data_number = 1004 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.2800 -5.2263 428.2767 433.5030 428.9356 3.8770 -5.2321 428.4945 433.7267 428.8194 5.4688 -5.2373 428.7038 433.9411 428.6795 7.0761 -5.2424 428.9024 434.1448 428.5107 8.6729 -5.2465 429.1048 434.3513 428.3285 10.2698 -5.2501 429.3095 434.5596 428.1162 11.8770 -5.2541 429.5099 434.7640 427.8727 13.4998 -5.2562 429.7067 434.9629 427.6131 15.0966 -5.2587 429.9029 435.1616 427.3432 16.7086 -5.2596 430.0997 435.3593 427.0484 18.3003 -5.2604 430.2929 435.5533 426.7366 19.9023 -5.2621 430.4777 435.7398 426.4089 21.5045 -5.2630 430.6542 435.9172 426.0697 23.1170 -5.2635 430.8314 436.0949 425.7153 24.7190 -5.2634 431.0108 436.2742 425.3560 26.3416 -5.2639 431.1846 436.4485 424.9733 27.9490 -5.2632 431.3524 436.6156 424.5856 29.5511 -5.2606 431.5128 436.7734 424.1961 31.1636 -5.2586 431.6592 436.9178 423.7993 32.7656 -5.2561 431.8106 437.0667 423.3934 34.3781 -5.2539 431.9578 437.2118 422.9783 35.9803 -5.2517 432.1062 437.3579 422.5656 37.6033 -5.2492 432.2464 437.4956 422.1428 39.2105 -5.2468 432.3822 437.6290 421.7205 40.8125 -5.2442 432.5284 437.7726 421.3031 42.4250 -5.2413 432.6520 437.8934 420.8843 44.0270 -5.2376 432.7705 438.0081 420.4660 45.6395 -5.2342 432.8858 438.1200 420.0528 47.2418 -5.2321 432.9940 438.2261 419.6435 48.8644 -5.2299 433.0941 438.3241 419.2336 50.4716 -5.2283 433.1856 438.4140 418.8318 52.0841 -5.2262 433.2779 438.5041 418.4420 53.6860 -5.2246 433.3621 438.5867 418.0638 55.2829 -5.2226 433.4419 438.6645 417.6961 56.8954 -5.2209 433.5171 438.7380 417.3363 58.4973 -5.2194 433.5809 438.8002 416.9839 60.1096 -5.2175 433.6390 438.8565 416.6458 61.7323 -5.2159 433.6925 438.9085 416.3200 63.3344 -5.2163 433.7487 438.9650 416.0079 64.9466 -5.2159 433.7952 439.0111 415.7187 66.5438 -5.2149 433.8362 439.0511 415.4406 68.1404 -5.2129 433.8720 439.0849 415.1800 69.7424 -5.2142 433.9071 439.1213 414.9339 71.3391 -5.2158 433.9323 439.1481 414.7073 72.9465 -5.2171 433.9603 439.1774 414.4918 74.5435 -5.2198 433.9697 439.1896 414.2890 76.1610 -5.2219 433.9818 439.2037 414.1094 77.7681 -5.2239 433.9850 439.2089 413.9401 79.3600 -5.2273 433.9928 439.2201 413.7819 80.9673 -5.2313 434.0018 439.2331 413.6358 82.5694 -5.2357 434.0087 439.2445 413.5021 84.1661 -5.2388 434.0034 439.2423 413.3883 85.7786 -5.2420 433.9897 439.2317 413.2772 87.3806 -5.2449 433.9749 439.2198 413.1769 88.9878 -5.2490 433.9654 439.2143 413.0897 90.6104 -5.2559 433.9477 439.2035 413.0056 92.2175 -5.2616 433.9276 439.1892 412.9368 93.8091 -5.2670 433.8966 439.1637 412.8711 95.4216 -5.2725 433.8707 439.1432 412.8065 97.0338 -5.2785 433.8419 439.1204 412.7423 98.6359 -5.2847 433.8188 439.1035 412.6829 100.2483 -5.2901 433.7872 439.0773 412.6222 101.8556 -5.2965 433.7561 439.0527 412.5660 103.4625 -5.3036 433.7250 439.0286 412.5012 105.0595 -5.3104 433.6939 439.0042 412.4413 106.6666 -5.3175 433.6621 438.9796 412.3810 108.2945 -5.3257 433.6272 438.9529 412.3222 109.9015 -5.3315 433.5911 438.9226 412.2534 111.5089 -5.3382 433.5524 438.8906 412.1769 113.1159 -5.3450 433.5074 438.8525 412.0921 114.7128 -5.3518 433.4619 438.8136 412.0036 116.3251 -5.3581 433.4082 438.7663 411.9057 117.9273 -5.3643 433.3636 438.7279 411.8074 119.5345 -5.3702 433.3204 438.6907 411.6960 121.1571 -5.3759 433.2659 438.6418 411.5683 122.7645 -5.3825 433.2125 438.5950 411.4398 124.3719 -5.3880 433.1543 438.5423 411.3003 125.9741 -5.3928 433.1059 438.4987 411.1527 127.5864 -5.3979 433.0552 438.4531 410.9961 129.1833 -5.4032 433.0011 438.4042 410.8331 130.7855 -5.4086 432.9471 438.3557 410.6611 132.4029 -5.4122 432.8950 438.3072 410.4794 134.0049 -5.4163 432.8361 438.2524 410.2994 135.6069 -5.4202 432.7737 438.1940 410.1080 137.2089 -5.4236 432.7158 438.1393 409.9031 138.8056 -5.4268 432.6551 438.0819 409.6916 140.4130 -5.4307 432.5945 438.0252 409.4692 142.0148 -5.4337 432.5230 437.9567 409.2377 143.6375 -5.4367 432.4484 437.8851 409.0011 145.2444 -5.4394 432.3817 437.8211 408.7502 146.8516 -5.4420 432.3093 437.7514 408.5045 148.4539 -5.4443 432.2296 437.6739 408.2548 150.0506 -5.4469 432.1511 437.5980 407.9883 151.6524 -5.4487 432.0790 437.5277 407.7230 153.2598 -5.4502 431.9995 437.4497 407.4435 154.8618 -5.4517 431.9156 437.3673 407.1659 156.4846 -5.4523 431.8335 437.2858 406.8878 158.0870 -5.4532 431.7468 437.2001 406.6100 159.6995 -5.4539 431.6643 437.1182 406.3215 161.3016 -5.4543 431.5763 437.0306 406.0430 162.9088 -5.4539 431.4897 436.9436 405.7606 164.5058 -5.4524 431.4037 436.8561 405.4739 166.1079 -5.4511 431.3085 436.7596 405.1794 167.7200 -5.4507 431.2109 436.6616 404.8840 169.3426 -5.4501 431.1116 436.5617 404.5935 170.9446 -5.4488 431.0045 436.4534 404.3097 172.5570 -5.4476 430.8976 436.3452 404.0231 174.1593 -5.4469 430.7913 436.2382 403.7387 175.7664 -5.4456 430.6824 436.1280 403.4510 177.3736 -5.4440 430.5680 436.0119 403.1669 178.9811 -5.4428 430.4588 435.9016 402.8864 180.6038 -5.4415 430.3388 435.7803 402.6139 182.2161 -5.4400 430.2204 435.6604 402.3375 183.8180 -5.4386 430.0974 435.5359 402.0705 185.4301 -5.4376 429.9778 435.4154 401.8015 187.0426 -5.4349 429.8534 435.2883 401.5377 188.6449 -5.4330 429.7268 435.1598 401.2814 190.2571 -5.4309 429.6082 435.0392 401.0269 191.8796 -5.4291 429.4829 434.9120 400.7787 193.4870 -5.4282 429.3525 434.7807 400.5288 195.0786 -5.4272 429.2235 434.6507 400.2894 196.6758 -5.4260 429.0965 434.5226 400.0571 198.2673 -5.4252 428.9559 434.3811 399.8328 199.8746 -5.4231 428.8193 434.2424 399.6042 201.4714 -5.4214 428.6855 434.1069 399.3831 203.0734 -5.4196 428.5449 433.9645 399.1776 204.6961 -5.4188 428.4070 433.8257 398.9672 206.2826 -5.4175 428.2697 433.6872 398.7718 207.8793 -5.4162 428.1293 433.5455 398.5786 209.4916 -5.4154 427.9948 433.4102 398.3741 211.0935 -5.4146 427.8520 433.2666 398.1869 212.7006 -5.4131 427.7033 433.1165 398.0078 214.3076 -5.4119 427.5522 432.9641 397.8323 215.9150 -5.4104 427.3954 432.8059 397.6590 217.5328 -5.4081 427.2423 432.6504 397.4927 219.1400 -5.4071 427.0910 432.4981 397.3243 220.7318 -5.4069 426.9441 432.3509 397.1664 222.3336 -5.4053 426.7944 432.1997 397.0130 223.9461 -5.4037 426.6392 432.0429 396.8574 225.5485 -5.4029 426.4943 431.8972 396.7003 227.1609 -5.4012 426.3386 431.7398 396.5462 228.7629 -5.3996 426.1918 431.5914 396.3997 230.3908 -5.3989 426.0370 431.4360 396.2482 231.9980 -5.3978 425.8821 431.2800 396.0995 233.6051 -5.3973 425.7164 431.1137 395.9436 235.2124 -5.3971 425.5584 430.9555 395.7918 236.8195 -5.3968 425.4014 430.7982 395.6361 238.4269 -5.3963 425.2441 430.6404 395.4760 240.0343 -5.3952 425.0928 430.4880 395.3157 241.6571 -5.3937 424.9306 430.3243 395.1514 243.2590 -5.3925 424.7719 430.1643 394.9919 244.8714 -5.3909 424.6158 430.0067 394.8345 246.4736 -5.3897 424.4565 429.8462 394.6696 248.0859 -5.3892 424.2974 429.6866 394.5106 249.6930 -5.3881 424.1361 429.5242 394.3469 251.3004 -5.3871 423.9809 429.3679 394.1755 252.9233 -5.3848 423.8226 429.2074 394.0025 254.5150 -5.3826 423.6669 429.0495 393.8277 256.1224 -5.3803 423.5017 428.8821 393.6600 257.7294 -5.3787 423.3384 428.7171 393.4840 259.3263 -5.3762 423.1767 428.5529 393.3115 260.9281 -5.3738 423.0118 428.3856 393.1200 262.5303 -5.3714 422.8544 428.2258 392.9291 264.1323 -5.3697 422.6865 428.0562 392.7395 265.7343 -5.3679 422.5213 427.8892 392.5451 267.3415 -5.3650 422.3658 427.7308 392.3526 268.9488 -5.3625 422.2064 427.5689 392.1501 270.5454 -5.3599 422.0405 427.4005 391.9439 272.1579 -5.3579 421.8846 427.2425 391.7318 273.7544 -5.3559 421.7229 427.0788 391.5207 275.3616 -5.3540 421.5593 426.9132 391.3089 276.9688 -5.3515 421.4044 426.7559 391.0971 278.5658 -5.3481 421.2475 426.5956 390.8793 280.1829 -5.3439 421.0823 426.4263 390.6576 281.7901 -5.3410 420.9125 426.2535 390.4364 283.3975 -5.3374 420.7437 426.0811 390.2086 284.9994 -5.3343 420.5777 425.9120 389.9709 286.6119 -5.3309 420.4090 425.7398 389.7403 288.2140 -5.3268 420.2413 425.5681 389.5091 289.8265 -5.3215 420.0705 425.3920 389.2733 291.4491 -5.3182 419.9008 425.2190 389.0404 293.0511 -5.3143 419.7273 425.0417 388.7984 294.6634 -5.3095 419.5543 424.8639 388.5539 296.2653 -5.3058 419.3859 424.6917 388.3128 297.8724 -5.3012 419.2125 424.5137 388.0734 299.4796 -5.2965 419.0422 424.3387 387.8242 301.0715 -5.2919 418.8682 424.1601 387.5752 302.6838 -5.2870 418.6885 423.9756 387.3240 304.3066 -5.2818 418.5067 423.7885 387.0746 305.9134 -5.2785 418.3301 423.6085 386.8245 307.5206 -5.2747 418.1488 423.4235 386.5779 309.1330 -5.2702 417.9699 423.2401 386.3303 310.7246 -5.2650 417.7883 423.0533 386.0884 312.3319 -5.2608 417.6073 422.8681 385.8492 313.9393 -5.2560 417.4260 422.6820 385.6092 315.5466 -5.2514 417.2416 422.4931 385.3702 317.1746 -5.2466 417.0560 422.3026 385.1298 318.7818 -5.2404 416.8808 422.1212 384.8907 320.3891 -5.2359 416.7017 421.9377 384.6487 321.9910 -5.2302 416.5253 421.7556 384.4155 323.5880 -5.2250 416.3437 421.5687 384.1794 325.1901 -5.2200 416.1578 421.3778 383.9464 326.8025 -5.2162 415.9770 421.1932 383.7109 328.4146 -5.2109 415.7937 421.0046 383.4806 329.9960 -5.2053 415.6073 420.8126 383.2571 331.5981 -5.2007 415.4170 420.6176 383.0347 333.2053 -5.1956 415.2308 420.4264 382.8147 334.8071 -5.1916 415.0514 420.2431 382.5969 336.4089 -5.1866 414.8627 420.0493 382.3830 338.0161 -5.1824 414.6793 419.8617 382.1652 339.6178 -5.1778 414.4828 419.6606 381.9491 341.2404 -5.1725 414.2812 419.4537 381.7337 342.8424 -5.1684 414.0906 419.2590 381.5238 344.4546 -5.1636 413.9010 419.0646 381.3115 346.0568 -5.1587 413.7137 418.8724 381.1099 347.6636 -5.1540 413.5175 418.6715 380.9091 349.2709 -5.1498 413.3268 418.4766 380.7074 350.8783 -5.1453 413.1346 418.2799 380.5045 352.4753 -5.1409 412.9431 418.0840 380.3085 354.0928 -5.1369 412.7474 417.8844 380.1127 355.7000 -5.1322 412.5475 417.6797 379.9138 357.3124 -5.1281 412.3618 417.4899 379.7186 358.9139 -5.1230 412.1711 417.2941 379.5358 360.5213 -5.1182 411.9757 417.0938 379.3509 362.1183 -5.1130 411.7829 416.8959 379.1689 363.7254 -5.1087 411.5886 416.6973 378.9839 365.3326 -5.1041 411.3929 416.4971 378.8040 366.9553 -5.0995 411.1987 416.2982 378.6171 368.5571 -5.0950 411.0002 416.0952 378.4397 370.1695 -5.0908 410.8010 415.8917 378.2591 371.7819 -5.0874 410.6032 415.6905 378.0808 373.3681 -5.0842 410.4145 415.4987 377.9009 374.9804 -5.0800 410.2222 415.3021 377.7175 376.5878 -5.0760 410.0386 415.1146 377.5360 378.1949 -5.0722 409.8453 414.9175 377.3441 379.8175 -5.0674 409.6467 414.7142 377.1635 381.4246 -5.0629 409.4496 414.5125 376.9782 383.0266 -5.0584 409.2584 414.3168 376.7956 384.6390 -5.0535 409.0729 414.1264 376.6083 386.2514 -5.0491 408.8755 413.9246 376.4261 387.8479 -5.0447 408.6838 413.7285 376.2451 389.4500 -5.0404 408.4873 413.5277 376.0576 391.0470 -5.0351 408.2913 413.3264 375.8706 392.6438 -5.0306 408.0911 413.1218 375.6815 394.2560 -5.0255 407.8983 412.9238 375.4958 395.8579 -5.0219 407.7052 412.7270 375.3063 397.4549 -5.0184 407.5093 412.5277 375.1084 399.0674 -5.0139 407.3175 412.3315 374.9052 400.6641 -5.0093 407.1237 412.1331 374.7083 402.2714 -5.0040 406.9255 411.9295 374.5044 403.8630 -4.9999 406.7285 411.7283 374.3030 405.4805 -4.9950 406.5344 411.5294 374.1042 407.0879 -4.9897 406.3410 411.3307 373.9060 408.6953 -4.9847 406.1441 411.1288 373.6982 410.2975 -4.9794 405.9489 410.9284 373.4903 411.9098 -4.9746 405.7458 410.7204 373.2843 413.5119 -4.9694 405.5525 410.5220 373.0849 415.1243 -4.9648 405.3610 410.3258 372.8839 416.7470 -4.9597 405.1661 410.1258 372.6715 418.3490 -4.9551 404.9753 409.9304 372.4659 419.9614 -4.9514 404.7746 409.7260 372.2541 421.5634 -4.9469 404.5768 409.5238 372.0375 423.1759 -4.9414 404.3856 409.3270 371.8226 424.7829 -4.9353 404.1803 409.1156 371.6071 426.3901 -4.9294 403.9846 408.9140 371.3921 428.0128 -4.9256 403.7889 408.7145 371.1683 429.6198 -4.9213 403.5982 408.5195 370.9511 431.2220 -4.9168 403.4063 408.3231 370.7317 432.8344 -4.9112 403.2091 408.1203 370.5078 434.4466 -4.9061 403.0137 407.9198 370.2776 436.0489 -4.9005 402.8106 407.7111 370.0575 437.6563 -4.8955 402.6078 407.5033 369.8309 439.2789 -4.8909 402.4113 407.3022 369.6039 440.8861 -4.8864 402.2159 407.1023 369.3727 442.4934 -4.8817 402.0124 406.8941 369.1387 444.1058 -4.8769 401.8140 406.6909 368.9102 445.7076 -4.8709 401.6207 406.4916 368.6852 447.3204 -4.8653 401.4231 406.2884 368.4536 448.9278 -4.8597 401.2221 406.0819 368.2306 450.5454 -4.8534 401.0221 405.8755 368.0052 452.1475 -4.8485 400.8313 405.6799 367.7791 453.7341 -4.8430 400.6343 405.4773 367.5546 455.3414 -4.8374 400.4334 405.2708 367.3260 456.9384 -4.8323 400.2339 405.0662 367.1037 458.5405 -4.8273 400.0365 404.8637 366.8786 460.1424 -4.8216 399.8418 404.6634 366.6571 461.7496 -4.8160 399.6506 404.4666 366.4358 463.3620 -4.8101 399.4558 404.2659 366.2139 464.9741 -4.8045 399.2590 404.0635 365.9992 466.5764 -4.7981 399.0609 403.8590 365.7811 468.1888 -4.7935 398.8619 403.6554 365.5643 469.7905 -4.7867 398.6552 403.4419 365.3511 471.3979 -4.7813 398.4602 403.2415 365.1362 473.0050 -4.7758 398.2560 403.0319 364.9207 474.6225 -4.7716 398.0536 402.8252 364.7059 476.2349 -4.7660 397.8523 402.6183 364.4978 477.8370 -4.7603 397.6548 402.4151 364.2860 479.4493 -4.7550 397.4577 402.2126 364.0746 481.0515 -4.7497 397.2532 402.0029 363.8598 482.6589 -4.7445 397.0502 401.7947 363.6467 484.2660 -4.7391 396.8505 401.5896 363.4406 485.8784 -4.7334 396.6427 401.3761 363.2292 487.4803 -4.7293 396.4361 401.1654 363.0217 489.0928 -4.7241 396.2338 400.9579 362.8122 490.6950 -4.7193 396.0320 400.7513 362.6002 492.3073 -4.7141 395.8268 400.5409 362.3931 493.9145 -4.7093 395.6295 400.3388 362.1928 495.5270 -4.7041 395.4327 400.1368 361.9920 497.1345 -4.6994 395.2333 399.9328 361.7959 498.7415 -4.6942 395.0276 399.7219 361.5937 500.3641 -4.6890 394.8166 399.5056 361.3932 501.9765 -4.6848 394.6051 399.2899 361.1854 503.5785 -4.6794 394.3984 399.0779 360.9865 505.1909 -4.6728 394.1952 398.8680 360.7927 506.7929 -4.6681 393.9862 398.6543 360.5978 508.4000 -4.6622 393.7854 398.4476 360.4036 510.0125 -4.6564 393.5953 398.2516 360.2064 511.6350 -4.6513 393.3896 398.0409 360.0122 513.2423 -4.6452 393.1799 397.8251 359.8146 514.8445 -4.6396 392.9802 397.6197 359.6129 516.4466 -4.6345 392.7813 397.4158 359.4217 518.0488 -4.6297 392.5944 397.2241 359.2297 519.6510 -4.6251 392.3901 397.0151 359.0330 521.2321 -4.6189 392.1904 396.8093 358.8388 522.8395 -4.6132 391.9795 396.5927 358.6467 524.4569 -4.6069 391.7770 396.3839 358.4443 526.0639 -4.6011 391.5801 396.1812 358.2428 527.6710 -4.5959 391.3806 395.9764 358.0452 529.2679 -4.5906 391.1805 395.7711 357.8464 530.8804 -4.5854 390.9727 395.5581 357.6533 532.4771 -4.5800 390.7729 395.3529 357.4585 534.0843 -4.5731 390.5674 395.1406 357.2587 535.7068 -4.5670 390.3670 394.9340 357.0611 537.3140 -4.5612 390.1674 394.7286 356.8595 538.9156 -4.5562 389.9733 394.5295 356.6708 540.5281 -4.5509 389.7681 394.3190 356.4756 542.1146 -4.5456 389.5605 394.1061 356.2786 543.7376 -4.5405 389.3499 393.8903 356.0688 545.3294 -4.5349 389.1482 393.6831 355.8712 546.9675 -4.5298 388.9415 393.4713 355.6650 548.5748 -4.5240 388.7378 393.2618 355.4575 550.1769 -4.5181 388.5432 393.0612 355.2585 551.7891 -4.5124 388.3440 392.8563 355.0557 553.3914 -4.5078 388.1405 392.6483 354.8495 554.9986 -4.5030 387.9354 392.4383 354.6456 556.6059 -4.4971 387.7364 392.2335 354.4414 558.2336 -4.4904 387.5317 392.0221 354.2381 559.8408 -4.4853 387.3252 391.8105 354.0432 561.4480 -4.4805 387.1257 391.6062 353.8422 563.0500 -4.4749 386.9173 391.3921 353.6441 564.6624 -4.4697 386.7151 391.1848 353.4336 566.2644 -4.4646 386.5078 390.9724 353.2274 567.8715 -4.4587 386.2991 390.7578 353.0184 569.4946 -4.4535 386.0921 390.5456 352.8094 571.0866 -4.4482 385.8898 390.3380 352.6013 572.7095 -4.4426 385.6854 390.1279 352.3935 574.3116 -4.4368 385.4844 389.9212 352.1812 575.9240 -4.4312 385.2812 389.7124 351.9686 577.5361 -4.4261 385.0856 389.5117 351.7490 579.1178 -4.4204 384.8950 389.3154 351.5326 580.7353 -4.4146 384.6964 389.1109 351.3184 582.3374 -4.4088 384.4964 388.9052 351.1055 583.9444 -4.4032 384.2937 388.6969 350.8896 585.5361 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