DTA measure 1kkk Date: 20251118:1541 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.95 s Mass = 100.000 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1785 -7.8174 184.4976 192.3151 246.7807 2.0475 -7.8207 184.7758 192.5965 246.7210 2.8033 -7.8185 184.9893 192.8078 246.6694 3.6205 -7.8219 185.2027 193.0246 246.6217 4.4178 -7.8212 185.4016 193.2228 246.5512 5.2145 -7.8217 185.5972 193.4189 246.4935 6.0318 -7.8213 185.8246 193.6460 246.4246 6.7983 -7.8227 186.0295 193.8521 246.3756 7.6465 -7.8184 186.2633 194.0817 246.3175 8.4123 -7.8183 186.4786 194.2968 246.2642 9.2403 -7.8232 186.6932 194.5164 246.1933 10.0273 -7.8229 186.9152 194.7381 246.1577 10.8235 -7.8232 187.1126 194.9358 246.1096 11.6515 -7.8245 187.3406 195.1651 246.0442 12.4075 -7.8241 187.5832 195.4073 246.0098 13.2655 -7.8213 187.7889 195.6102 245.9808 14.0218 -7.8194 187.9804 195.7997 245.9676 14.8495 -7.8181 188.2236 196.0417 245.9339 15.6460 -7.8142 188.4752 196.2894 245.8579 16.4330 -7.8129 188.6855 196.4984 245.8225 17.2608 -7.8133 188.8683 196.6816 245.8093 18.0265 -7.8149 189.0906 196.9055 245.7931 18.8750 -7.8144 189.3228 197.1372 245.7575 19.6413 -7.8119 189.5101 197.3220 245.7630 20.4685 -7.8110 189.7416 197.5526 245.7956 21.2658 -7.8123 189.9261 197.7384 245.8095 22.0628 -7.8106 190.1243 197.9349 245.8232 22.8798 -7.8031 190.3628 198.1659 245.8268 23.6565 -7.8012 190.5559 198.3571 245.8553 24.5048 -7.8007 190.7975 198.5982 245.8811 25.2603 -7.7964 191.0453 198.8417 245.9208 26.0985 -7.7908 191.2465 199.0373 245.9458 26.8855 -7.7854 191.4390 199.2243 245.9954 27.6818 -7.7812 191.6593 199.4404 246.0425 28.5098 -7.7767 191.8280 199.6047 246.0866 29.2660 -7.7717 192.0254 199.7971 246.1483 30.1238 -7.7678 192.2246 199.9924 246.1968 30.8903 -7.7639 192.4194 200.1832 246.2471 31.7183 -7.7634 192.6384 200.4019 246.3496 32.5145 -7.7570 192.8379 200.5949 246.4394 33.3015 -7.7524 193.0553 200.8077 246.5003 34.1395 -7.7488 193.3158 201.0646 246.5913 34.8950 -7.7435 193.4881 201.2315 246.6836 35.7538 -7.7358 193.7021 201.4378 246.7866 36.5203 -7.7287 193.8738 201.6025 246.9162 37.3473 -7.7252 194.0884 201.8136 247.0405 38.1445 -7.7201 194.2852 202.0053 247.1544 38.9315 -7.7162 194.4889 202.2050 247.2554 39.7688 -7.7116 194.7015 202.4131 247.3829 40.5250 -7.7088 194.8642 202.5730 247.4741 41.3838 -7.7007 195.0916 202.7924 247.6244 42.1495 -7.7008 195.3038 203.0046 247.7878 42.9978 -7.6936 195.5222 203.2158 247.9247 43.7333 -7.6925 195.7005 203.3930 248.0376 44.6015 -7.6848 195.9371 203.6219 248.2296 45.3578 -7.6796 196.1107 203.7903 248.3785 46.1858 -7.6753 196.2864 203.9617 248.5240 46.9820 -7.6700 196.5020 204.1720 248.6937 47.7793 -7.6645 196.6969 204.3614 248.8464 48.6073 -7.6575 196.8893 204.5468 249.0153 49.3625 -7.6517 197.0863 204.7381 249.1779 50.2315 -7.6413 197.2886 204.9299 249.3558 50.9878 -7.6333 197.4419 205.0752 249.5281 51.8148 -7.6271 197.6376 205.2648 249.6978 52.6120 -7.6259 197.8625 205.4884 249.8848 53.4093 -7.6206 198.0638 205.6844 250.0600 54.2363 -7.6121 198.2709 205.8830 250.2630 54.9925 -7.6069 198.4330 206.0399 250.4439 55.8615 -7.6019 198.6609 206.2628 250.6345 56.6168 -7.5984 198.8682 206.4666 250.8171 57.4448 -7.5947 199.0375 206.6322 251.0376 58.2420 -7.5919 199.2097 206.8016 251.2128 59.0383 -7.5883 199.4111 206.9993 251.3754 59.8663 -7.5777 199.6140 207.1917 251.5903 60.6225 -7.5687 199.7684 207.3371 251.7920 61.4905 -7.5600 199.9992 207.5592 252.0310 62.2468 -7.5558 200.1919 207.7477 252.2350 63.0748 -7.5539 200.4063 207.9602 252.4543 63.8710 -7.5491 200.5942 208.1433 252.6502 64.6683 -7.5450 200.7869 208.3319 252.8379 65.4963 -7.5405 201.0092 208.5497 253.0260 66.2515 -7.5315 201.1970 208.7285 253.2021 67.1103 -7.5286 201.4042 208.9328 253.3964 67.8663 -7.5280 201.5596 209.0876 253.5561 68.6935 -7.5245 201.7394 209.2639 253.7429 69.4908 -7.5203 201.8947 209.4150 253.9518 70.2773 -7.5127 202.0758 209.5885 254.1397 71.1048 -7.5046 202.2993 209.8038 254.3456 71.8610 -7.4983 202.4669 209.9652 254.5105 72.7090 -7.4895 202.6498 210.1393 254.6920 73.4853 -7.4825 202.8218 210.3043 254.8602 74.3030 -7.4791 203.0100 210.4891 255.0303 75.0893 -7.4733 203.1876 210.6609 255.2032 75.8965 -7.4684 203.3841 210.8525 255.3923 76.7143 -7.4619 203.5569 211.0189 255.5716 77.4700 -7.4543 203.7372 211.1915 255.7335 78.3078 -7.4446 203.9496 211.3942 255.9268 79.0640 -7.4391 204.1661 211.6053 256.0627 79.9118 -7.4395 204.3675 211.8070 256.2513 80.6883 -7.4374 204.5812 212.0186 256.4628 81.5060 -7.4411 204.7732 212.2143 256.6034 82.3025 -7.4358 204.9314 212.3672 256.7579 83.0995 -7.4302 205.1332 212.5633 256.8912 83.9275 -7.4264 205.3562 212.7826 257.0406 84.6828 -7.4233 205.5440 212.9672 257.2144 85.5415 -7.4164 205.7696 213.1860 257.3551 86.3080 -7.4088 205.9519 213.3606 257.4919 87.1353 -7.4036 206.1539 213.5575 257.6547 87.8913 -7.3963 206.3243 213.7206 257.7809 88.7193 -7.3915 206.5004 213.8919 257.9297 89.5463 -7.3918 206.6888 214.0807 258.0644 90.3025 -7.3883 206.8554 214.2437 258.2380 91.1613 -7.3833 207.0502 214.4335 258.3995 91.8963 -7.3778 207.2255 214.6033 258.5350 92.7445 -7.3736 207.4246 214.7981 258.6826 93.5213 -7.3690 207.5891 214.9581 258.8181 94.3388 -7.3711 207.7585 215.1295 258.9522 95.1353 -7.3623 207.9342 215.2965 259.0764 95.9325 -7.3493 208.0886 215.4379 259.2227 96.7605 -7.3494 208.2573 215.6066 259.3549 97.5260 -7.3482 208.4367 215.7849 259.4854 98.3745 -7.3487 208.6339 215.9826 259.6377 99.1510 -7.3446 208.7895 216.1341 259.7852 99.9680 -7.3374 208.9759 216.3132 259.8938 100.7755 -7.3304 209.1546 216.4851 260.0218 101.5723 -7.3285 209.3406 216.6691 260.1399 102.3998 -7.3254 209.5348 216.8601 260.2477 103.1560 -7.3236 209.7142 217.0378 260.3244 104.0145 -7.3207 209.9248 217.2455 260.4651 104.7803 -7.3182 210.0936 217.4118 260.5768 105.6083 -7.3110 210.2859 217.5970 260.6991 106.4055 -7.3055 210.4891 217.7946 260.8012 107.1915 -7.3008 210.6767 217.9775 260.9058 107.9990 -7.2976 210.8961 218.1937 261.0034 108.7858 -7.2905 211.1221 218.4127 261.1220 109.6233 -7.2821 211.3038 218.5859 261.2266 110.3795 -7.2765 211.4752 218.7517 261.3577 111.2483 -7.2700 211.6083 218.8782 261.4550 112.0038 -7.2660 211.7458 219.0119 261.5785 112.8318 -7.2578 211.9122 219.1700 261.7057 113.6288 -7.2546 212.1033 219.3580 261.8013 114.4253 -7.2588 212.2900 219.5488 261.9239 115.2533 -7.2518 212.4836 219.7353 262.0191 116.0190 -7.2470 212.6449 219.8919 262.1112 116.8775 -7.2434 212.8468 220.0902 262.2547 117.6440 -7.2379 213.0213 220.2593 262.3575 118.4715 -7.2322 213.2313 220.4635 262.4653 119.2580 -7.2280 213.4048 220.6328 262.5388 120.0655 -7.2253 213.6045 220.8298 262.6501 120.8833 -7.2293 213.7840 221.0132 262.8044 121.6488 -7.2268 213.9496 221.1764 262.9413 122.5075 -7.2201 214.1134 221.3334 263.0728 123.2740 -7.2143 214.2644 221.4786 263.1784 124.1013 -7.2141 214.4317 221.6458 263.2663 124.8675 -7.2086 214.5912 221.7998 263.3294 125.7058 -7.2000 214.7734 221.9734 263.4277 126.5023 -7.1948 214.9652 222.1600 263.5670 127.2993 -7.1899 215.1325 222.3224 263.6820 128.1273 -7.1856 215.3156 222.5012 263.7980 128.8928 -7.1846 215.4706 222.6552 263.9126 129.7515 -7.1770 215.6540 222.8310 264.0178 130.4870 -7.1751 215.8125 222.9876 264.1126 131.3348 -7.1656 216.0162 223.1817 264.2284 132.1013 -7.1633 216.1841 223.3474 264.3564 132.9190 -7.1600 216.3234 223.4834 264.4986 133.7153 -7.1590 216.5139 223.6729 264.6592 134.5125 -7.1622 216.6869 223.8492 264.7708 135.3303 -7.1628 216.8410 224.0037 264.8913 136.0858 -7.1606 216.9946 224.1551 264.9901 136.9443 -7.1534 217.1973 224.3507 265.1002 137.7108 -7.1491 217.3639 224.5130 265.2297 138.5278 -7.1401 217.5542 224.6943 265.3088 139.3248 -7.1379 217.7369 224.8749 265.4523 140.1220 -7.1334 217.9256 225.0590 265.5856 140.9390 -7.1305 218.0789 225.2094 265.6987 141.7053 -7.1281 218.2440 225.3720 265.8027 142.5640 -7.1285 218.4457 225.5742 265.9651 143.3200 -7.1312 218.6223 225.7535 266.0838 144.1473 -7.1324 218.7659 225.8982 266.2084 144.9445 -7.1323 218.9268 226.0591 266.3362 145.7620 -7.1299 219.1017 226.2316 266.5021 146.5175 -7.1271 219.2478 226.3749 266.6647 147.3455 -7.1242 219.4267 226.5509 266.7724 148.1425 -7.1182 219.5612 226.6794 266.8943 148.9390 -7.1176 219.7299 226.8475 267.0380 149.7568 -7.1138 219.9377 227.0514 267.1700 150.5333 -7.1170 220.1263 227.2433 267.2663 151.3810 -7.1100 220.3221 227.4322 267.3894 152.1475 -7.1021 220.4691 227.5712 267.5323 152.9753 -7.0954 220.6516 227.7470 267.7057 153.7718 -7.0872 220.8272 227.9143 267.8428 154.5588 -7.0822 220.9858 228.0679 267.9933 155.3965 -7.0736 221.1545 228.2281 268.1158 156.1830 -7.0655 221.3163 228.3818 268.2534 156.9700 -7.0662 221.4916 228.5578 268.4046 157.7768 -7.0645 221.6526 228.7171 268.5280 158.5943 -7.0603 221.8186 228.8789 268.6516 159.3608 -7.0555 222.0105 229.0660 268.8125 160.2188 -7.0533 222.1942 229.2474 268.9585 160.9850 -7.0497 222.3785 229.4282 269.1219 161.8028 -7.0387 222.5631 229.6017 269.2792 162.5993 -7.0288 222.7242 229.7530 269.4395 163.3963 -7.0185 222.8950 229.9135 269.5713 164.2243 -7.0120 223.0857 230.0978 269.7360 164.9800 -7.0102 223.2451 230.2553 269.8350 165.8485 -7.0019 223.4328 230.4348 269.9893 166.6048 -6.9975 223.5975 230.5950 270.1234 167.4323 -6.9936 223.8036 230.7972 270.2851 168.2290 -6.9905 223.9635 230.9540 270.4386 169.0263 -6.9904 224.1390 231.1295 270.5760 169.8845 -6.9910 224.3129 231.3039 270.7148 170.6403 -6.9889 224.4940 231.4829 270.8411 171.4785 -6.9883 224.6590 231.6473 270.9766 172.2653 -6.9875 224.8290 231.8165 271.1233 173.0618 -6.9843 224.9820 231.9663 271.2808 173.8898 -6.9813 225.1503 232.1316 271.4500 174.6560 -6.9803 225.2938 232.2741 271.6068 175.5140 -6.9729 225.4422 232.4152 271.7643 176.2703 -6.9679 225.5384 232.5063 271.8826 177.1083 -6.9626 225.7031 232.6657 272.0088 177.8945 -6.9612 225.8646 232.8258 272.1417 178.7020 -6.9598 226.0518 233.0116 272.3008 179.5193 -6.9640 226.2449 233.2089 272.4641 180.2955 -6.9657 226.4056 233.3713 272.5905 181.1440 -6.9641 226.5888 233.5529 272.7328 181.9100 -6.9585 226.7031 233.6615 272.8709 182.7375 -6.9447 226.8994 233.8441 272.9916 183.5348 -6.9377 227.0239 233.9616 273.0962 184.3315 -6.9291 227.1834 234.1126 273.2302 185.1488 -6.9237 227.3589 234.2826 273.3535 185.9255 -6.9225 227.5143 234.4368 273.4822 186.7733 -6.9183 227.6585 234.5768 273.6317 187.5395 -6.9124 227.8085 234.7209 273.7354 188.3675 -6.9089 227.9686 234.8775 273.8786 189.1745 -6.9083 228.1516 235.0598 274.0085 189.9610 -6.9098 228.3352 235.2450 274.1560 190.7890 -6.9080 228.4939 235.4020 274.2991 191.5550 -6.9081 228.6232 235.5312 274.4484 192.4133 -6.9070 228.8344 235.7414 274.5995 193.1798 -6.9059 229.0091 235.9150 274.7314 193.9973 -6.9039 229.2032 236.1071 274.8730 194.8040 -6.9039 229.3818 236.2856 275.0066 195.5910 -6.9034 229.5288 236.4323 275.1220 196.4190 -6.9024 229.7036 236.6060 275.2734 197.1948 -6.8965 229.8454 236.7419 275.4088 197.9920 -6.8940 229.9916 236.8856 275.5215 198.7790 -6.8909 230.1763 237.0671 275.6466 199.5960 -6.8865 230.3469 237.2335 275.7646 200.3725 -6.8868 230.5066 237.3934 275.8605 201.2210 -6.8837 230.6754 237.5590 275.9871 201.9870 -6.8775 230.8626 237.7402 276.0907 202.8145 -6.8746 231.0051 237.8797 276.2147 203.6015 -6.8749 231.1293 238.0042 276.3185 204.3883 -6.8734 231.2660 238.1393 276.4462 205.2258 -6.8747 231.4157 238.2904 276.5645 205.9820 -6.8713 231.5834 238.4547 276.6790 206.8408 -6.8721 231.7928 238.6649 276.7850 207.5858 -6.8687 231.9198 238.7886 276.8886 208.4445 -6.8671 232.0827 238.9498 276.9714 209.2110 -6.8611 232.2466 239.1077 277.0568 210.0385 -6.8585 232.3924 239.2509 277.1859 210.8250 -6.8608 232.5505 239.4113 277.3144 211.6223 -6.8573 232.7412 239.5985 277.4276 212.4188 -6.8588 232.9299 239.7887 277.5340 213.2158 -6.8540 233.0914 239.9454 277.6736 214.0438 -6.8497 233.2642 240.1140 277.7637 214.7995 -6.8511 233.4007 240.2518 277.8531 215.6578 -6.8449 233.5649 240.4097 277.9784 216.4243 -6.8419 233.7122 240.5541 278.0894 217.2623 -6.8431 233.8896 240.7327 278.2202 218.0383 -6.8409 234.0678 240.9086 278.3232 218.8560 -6.8378 234.2353 241.0731 278.4565 219.6530 -6.8342 234.3764 241.2106 278.5782 220.4495 -6.8290 234.5702 241.3992 278.6937 221.2775 -6.8255 234.7551 241.5805 278.8261 222.0435 -6.8223 234.9072 241.7295 278.9348 222.8915 -6.8162 235.0698 241.8859 279.0683 223.6683 -6.8140 235.2063 242.0203 279.2179 224.4860 -6.8184 235.3408 242.1592 279.3586 225.2823 -6.8197 235.5055 242.3252 279.4814 226.0795 -6.8194 235.6436 242.4630 279.6176 226.9075 -6.8152 235.8206 242.6358 279.7421 227.6935 -6.8095 236.0033 242.8129 279.8538 228.5113 -6.8069 236.1567 242.9636 280.0190 229.2778 -6.8020 236.2825 243.0845 280.1714 230.1358 -6.7978 236.4441 243.2418 280.2532 230.9020 -6.7943 236.6193 243.4136 280.3638 231.7300 -6.7923 236.8062 243.5985 280.4952 232.5160 -6.7893 236.9168 243.7061 280.5859 233.3235 -6.7889 237.0557 243.8446 280.7036 234.1105 -6.7879 237.1972 243.9850 280.8045 234.9070 -6.7892 237.3506 244.1397 280.9429 235.7348 -6.7878 237.5545 244.3423 281.0980 236.5013 -6.7875 237.6975 244.4850 281.2517 237.3595 -6.7839 237.8722 244.6562 281.4156 238.1255 -6.7818 238.0212 244.8030 281.5571 238.9740 -6.7722 238.1869 244.9591 281.7048 239.7400 -6.7729 238.3444 245.1172 281.8459 240.5675 -6.7726 238.5015 245.2741 282.0012 241.3340 -6.7716 238.6667 245.4383 282.1220 242.1618 -6.7688 238.8513 245.6201 282.2565 242.9480 -6.7629 239.0001 245.7631 282.3892 243.7555 -6.7619 239.1436 245.9055 282.5378 244.5730 -6.7595 239.2841 246.0435 282.6268 245.3490 -6.7602 239.4491 246.2094 282.7266 246.1975 -6.7570 239.5857 246.3427 282.8082 246.9740 -6.7542 239.6994 246.4536 282.9414 247.7910 -6.7548 239.8643 246.6191 283.0969 248.5883 -6.7514 240.0441 246.7954 283.2446 249.3853 -6.7505 240.1949 246.9453 283.3704 250.2125 -6.7502 240.3775 247.1276 283.5034 250.9790 -6.7496 240.5492 247.2987 283.6402 251.8273 -6.7518 240.7624 247.5142 283.7709 252.6033 -6.7523 240.9113 247.6636 283.8570 253.4313 -6.7534 241.0596 247.8130 283.9944 254.2283 -6.7531 241.2039 247.9570 284.1072 255.0145 -6.7534 241.3507 248.1041 284.2767 255.8528 -6.7478 241.4793 248.2271 284.4455 256.6085 -6.7456 241.6164 248.3620 284.6048 257.4668 -6.7440 241.7833 248.5273 284.7619 258.2333 -6.7405 241.9223 248.6628 284.9223 259.0608 -6.7367 242.0613 248.7979 285.0335 259.8473 -6.7352 242.2252 248.9604 285.1431 260.6445 -6.7352 242.3717 249.1069 285.2948 261.4720 -6.7307 242.5343 249.2651 285.4468 262.2278 -6.7231 242.6806 249.4038 285.6059 263.0558 -6.7214 242.8192 249.5406 285.7587 263.8113 -6.7192 242.9373 249.6565 285.8705 264.6595 -6.7136 243.0689 249.7825 285.9830 265.4363 -6.7089 243.2124 249.9213 286.1079 266.2530 -6.7066 243.3964 250.1031 286.2529 267.0400 -6.7002 243.5578 250.2580 286.3599 267.8475 -6.6961 243.7163 250.4123 286.5189 268.6335 -6.6909 243.8804 250.5713 286.6592 269.4205 -6.6899 244.0018 250.6916 286.7733 270.2588 -6.6894 244.1645 250.8539 286.9167 271.0140 -6.6865 244.3469 251.0334 287.0326 271.8625 -6.6855 244.5345 251.2200 287.1818 272.6393 -6.6855 244.6768 251.3624 287.3349 273.4563 -6.6861 244.8286 251.5147 287.4612 274.2533 -6.6852 244.9587 251.6439 287.5947 275.0505 -6.6869 245.0987 251.7856 287.7120 275.8368 -6.6842 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360.5565 368.8378 396.1406 945.6993 -8.2830 360.7269 369.0099 396.2754 946.4555 -8.2822 360.8740 369.1562 396.3638 947.3245 -8.2785 361.0411 369.3196 396.5110 948.0500 -8.2722 361.1850 369.4573 396.6441 948.9088 -8.2645 361.3496 369.6141 396.7762 949.6763 -8.2600 361.5448 369.8048 396.9153 950.5043 -8.2609 361.7069 369.9678 397.0614 951.3015 -8.2565 361.8878 370.1442 397.1615 952.0885 -8.2502 362.0187 370.2690 397.2597 952.9268 -8.2418 362.1498 370.3916 397.3724 953.6830 -8.2360 362.2926 370.5286 397.4935 954.5623 -8.2305 362.4650 370.6955 397.6038 955.2980 -8.2273 362.5789 370.8062 397.7141 956.1568 -8.2192 362.7411 370.9603 397.8792 956.9233 -8.2146 362.8672 371.0818 398.0063 957.7513 -8.2112 363.0397 371.2509 398.1159 958.5485 -8.2125 363.1962 371.4087 398.2184 959.3355 -8.2092 363.3152 371.5244 398.3022 960.1738 -8.2057 363.4268 371.6325 398.4467 960.9300 -8.2049 363.5555 371.7604 398.5491 961.7888 -8.1990 363.7533 371.9523 398.6587 962.5563 -8.1887 363.9020 372.0907 398.7839 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