DTA measure 1Pb251118-3.dat Date: 20251118:152 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.69 s Mass = 1094.200 mg data_number = 1268 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2195 0.0792 251.5654 251.4862 276.4551 1.9853 0.0813 251.7229 251.6417 276.6352 2.8128 0.0874 251.8568 251.7694 276.7319 3.5990 0.0905 252.0132 251.9227 276.8055 4.3853 0.0994 252.2045 252.1051 276.8771 5.2025 0.1023 252.3771 252.2749 276.8619 5.9580 0.1052 252.5341 252.4289 276.8191 6.7750 0.1060 252.7065 252.6005 276.8084 7.5513 0.1092 252.8562 252.7469 276.7463 8.3888 0.1169 253.0377 252.9208 276.6634 9.1443 0.1275 253.1961 253.0686 276.6136 9.9615 0.1337 253.3531 253.2194 276.5166 10.7375 0.1384 253.5373 253.3989 276.4052 11.5853 0.1427 253.7242 253.5815 276.2836 12.3410 0.1453 253.8811 253.7358 276.1518 13.1683 0.1491 254.0490 253.8999 275.9822 13.9650 0.1507 254.2213 254.0706 275.8283 14.7515 0.1559 254.3970 254.2411 275.7116 15.5888 0.1606 254.5579 254.3973 275.5878 16.3443 0.1655 254.6951 254.5296 275.5079 17.1618 0.1697 254.8566 254.6869 275.4285 17.9583 0.1734 255.0179 254.8445 275.3601 18.7755 0.1824 255.2012 255.0188 275.2830 19.5515 0.1861 255.3441 255.1580 275.2723 20.3993 0.1898 255.5102 255.3204 275.2669 21.1650 0.1927 255.6630 255.4703 275.2714 21.9925 0.1972 255.8407 255.6434 275.3409 22.7890 0.2044 256.0095 255.8051 275.4506 23.5858 0.2086 256.1661 255.9575 275.5921 24.4028 0.2111 256.3351 256.1239 275.7619 25.1788 0.2114 256.4993 256.2879 275.9662 25.9963 0.2125 256.6593 256.4469 276.2188 26.7618 0.2170 256.8417 256.6247 276.4820 27.6200 0.2241 257.0343 256.8102 276.8185 28.3758 0.2316 257.1910 256.9594 277.1472 29.2338 0.2349 257.3352 257.1003 277.5638 29.9998 0.2383 257.4772 257.2388 277.9323 30.8270 0.2422 257.6210 257.3788 278.3557 31.6135 0.2471 257.7507 257.5036 278.7557 32.4205 0.2520 257.9147 257.6627 279.1753 33.2373 0.2572 258.0692 257.8120 279.5902 34.0138 0.2573 258.2314 257.9741 280.0119 34.8615 0.2593 258.4021 258.1428 280.4443 35.6273 0.2637 258.5606 258.2970 280.8145 36.4445 0.2706 258.7316 258.4610 281.1953 37.2410 0.2763 258.9036 258.6274 281.5264 38.0375 0.2795 259.0358 258.7563 281.8608 38.8243 0.2801 259.1950 258.9149 282.1430 39.6513 0.2798 259.3595 259.0797 282.4090 40.4378 0.2802 259.5372 259.2571 282.6116 41.2345 0.2827 259.6681 259.3854 282.8144 42.0310 0.2825 259.8271 259.5446 282.9210 42.8278 0.2831 259.9764 259.6933 283.0456 43.6448 0.2833 260.1337 259.8505 283.1444 44.4208 0.2807 260.2950 260.0143 283.1664 45.2688 0.2774 260.4392 260.1618 283.1959 46.0345 0.2786 260.5807 260.3021 283.2123 46.8618 0.2801 260.7476 260.4675 283.2105 47.6585 0.2794 260.9324 260.6530 283.1676 48.4653 0.2787 261.0545 260.7758 283.1218 49.2620 0.2783 261.1915 260.9132 283.0218 50.0588 0.2833 261.3435 261.0602 282.8979 50.8860 0.2863 261.5121 261.2258 282.7700 51.6520 0.2864 261.6749 261.3885 282.6878 52.5100 0.2883 261.8786 261.5903 282.5865 53.2655 0.2867 262.0412 261.7546 282.4614 54.1035 0.2855 262.2030 261.9175 282.3002 54.8895 0.2879 262.3512 262.0633 282.1790 55.6863 0.2921 262.5101 262.2181 282.0825 56.5138 0.2979 262.6776 262.3797 281.9930 57.2795 0.2995 262.8260 262.5264 281.9683 58.1378 0.3019 262.9732 262.6713 281.9450 58.8933 0.3024 263.0782 262.7758 281.9191 59.7205 0.3043 263.2214 262.9171 281.9082 60.4868 0.3068 263.3777 263.0709 281.9408 61.3445 0.3109 263.5541 263.2432 282.0262 62.1103 0.3114 263.7108 263.3994 282.1040 62.9380 0.3147 263.8614 263.5467 282.2367 63.7240 0.3138 263.9871 263.6734 282.3726 64.5313 0.3164 264.1050 263.7886 282.5646 65.3483 0.3204 264.2826 263.9622 282.8299 66.1140 0.3220 264.4604 264.1384 283.1236 66.9723 0.3265 264.6088 264.2823 283.4557 67.7380 0.3280 264.7524 264.4245 283.7750 68.5548 0.3271 264.9453 264.6182 284.1954 69.3518 0.3271 265.0995 264.7724 284.5824 70.1483 0.3239 265.2577 264.9338 284.9840 70.9755 0.3211 265.4140 265.0929 285.4113 71.7313 0.3201 265.5523 265.2322 285.8068 72.5893 0.3219 265.7114 265.3895 286.2934 73.3550 0.3233 265.8514 265.5282 286.6949 74.1723 0.3210 265.9968 265.6758 287.1038 74.9790 0.3156 266.1773 265.8616 287.4782 75.7653 0.3162 266.3596 266.0435 287.8177 76.5825 0.3191 266.5021 266.1830 288.1631 77.3585 0.3173 266.6332 266.3159 288.4765 78.2063 0.3163 266.8156 266.4993 288.7629 78.9723 0.3151 267.0004 266.6853 288.9723 79.7995 0.3158 267.1532 266.8375 289.1624 80.5755 0.3177 267.3079 266.9902 289.3157 81.3928 0.3180 267.4178 267.0997 289.4457 82.1893 0.3147 267.5682 267.2534 289.5602 82.9858 0.3113 267.7267 267.4155 289.6522 83.8133 0.3081 267.8772 267.5692 289.6985 84.5790 0.3047 267.9684 267.6636 289.7150 85.4370 0.3064 268.1787 267.8723 289.7165 86.2030 0.3057 268.3425 268.0368 289.6836 87.0303 0.3042 268.5183 268.2141 289.6261 87.8270 0.3040 268.6526 268.3487 289.5841 88.6135 0.3000 268.7930 268.4931 289.5079 89.4508 0.2978 268.9712 268.6735 289.4019 90.2065 0.3002 269.1244 268.8241 289.2872 91.0648 0.2968 269.2752 268.9784 289.1429 91.8303 0.2957 269.4374 269.1417 289.0542 92.6578 0.2943 269.6184 269.3240 288.9300 93.4545 0.2951 269.7170 269.4219 288.8086 94.2405 0.2946 269.8479 269.5533 288.7071 95.0785 0.2907 270.0468 269.7562 288.6013 95.8340 0.2935 270.1949 269.9014 288.5147 96.6920 0.2943 270.3413 270.0471 288.4343 97.4580 0.2938 270.4970 270.2032 288.3871 98.2853 0.2929 270.6387 270.3458 288.3421 99.0820 0.2924 270.7736 270.4812 288.3417 99.8788 0.2950 270.9168 270.6218 288.4013 100.7058 0.2941 271.0824 270.7883 288.5116 101.4615 0.2957 271.2459 270.9502 288.6231 102.3198 0.2925 271.4203 271.1278 288.7939 103.0545 0.2952 271.5523 271.2572 288.9797 103.9028 0.2979 271.7021 271.4042 289.2312 104.6685 0.3026 271.8028 271.5002 289.4674 105.4958 0.3056 271.9654 271.6598 289.7649 106.2925 0.3071 272.1152 271.8081 290.0776 107.0788 0.3057 272.2511 271.9453 290.4248 107.9063 0.3093 272.4039 272.0946 290.8017 108.6723 0.3041 272.5440 272.2399 291.1626 109.5300 0.3049 272.7153 272.4104 291.6270 110.2755 0.3046 272.8575 272.5529 292.0042 111.1338 0.3002 273.0175 272.7173 292.4409 111.8995 0.3003 273.1388 272.8385 292.8434 112.7270 0.3009 273.2874 272.9865 293.2649 113.5235 0.3007 273.4349 273.1342 293.6554 114.3098 0.3006 273.6020 273.3014 294.0391 115.1475 0.2985 273.7634 273.4648 294.3568 115.9030 0.2973 273.9031 273.6057 294.6566 116.7715 0.2936 274.0426 273.7490 294.9823 117.5273 0.2929 274.2067 273.9138 295.2518 118.3645 0.2866 274.3497 274.0630 295.4826 119.1510 0.2853 274.5128 274.2275 295.6769 119.9580 0.2822 274.6708 274.3887 295.8370 120.7645 0.2782 274.8321 274.5539 295.9617 121.5510 0.2773 274.9749 274.6976 296.0057 122.3888 0.2760 275.1527 274.8767 296.0448 123.1440 0.2748 275.3358 275.0610 296.0682 124.0025 0.2742 275.4707 275.1966 296.0986 124.7683 0.2722 275.6194 275.3472 296.0679 125.6058 0.2670 275.7874 275.5204 296.0188 126.3923 0.2616 275.9186 275.6569 295.9298 127.1888 0.2620 276.0743 275.8123 295.8613 128.0160 0.2606 276.2051 275.9446 295.8025 128.7818 0.2577 276.3135 276.0558 295.7161 129.6400 0.2597 276.4763 276.2166 295.5816 130.3955 0.2607 276.6330 276.3723 295.5097 131.2333 0.2640 276.7642 276.5002 295.4002 132.0298 0.2640 276.9036 276.6396 295.2913 132.8263 0.2619 277.0756 276.8137 295.1788 133.6435 0.2592 277.2436 276.9844 295.0901 134.4093 0.2566 277.4232 277.1667 294.9988 135.2260 0.2549 277.5666 277.3117 294.8653 135.9920 0.2538 277.7111 277.4573 294.8104 136.8503 0.2580 277.8755 277.6175 294.8173 137.6160 0.2555 278.0416 277.7861 294.8359 138.4333 0.2538 278.1986 277.9448 294.8648 139.2400 0.2533 278.3806 278.1273 294.9290 140.0263 0.2535 278.5416 278.2881 295.0683 140.8435 0.2525 278.7021 278.4496 295.2309 141.6195 0.2539 278.8501 278.5962 295.3964 142.4673 0.2525 278.9784 278.7258 295.6013 143.2333 0.2517 279.1183 278.8666 295.8467 144.0605 0.2523 279.2793 279.0270 296.1353 144.8570 0.2513 279.4168 279.1655 296.4386 145.6538 0.2511 279.5662 279.3151 296.7772 146.4503 0.2521 279.7033 279.4512 297.1304 147.2465 0.2489 279.8395 279.5906 297.5171 148.0740 0.2491 280.0047 279.7556 297.8781 148.8400 0.2468 280.1437 279.8968 298.2542 149.6875 0.2465 280.2591 280.0126 298.6921 150.4638 0.2444 280.3927 280.1483 299.0742 151.2810 0.2466 280.5348 280.2883 299.4791 152.0773 0.2454 280.6704 280.4249 299.8658 152.8740 0.2409 280.8037 280.5628 300.2313 153.7015 0.2362 280.9479 280.7118 300.6006 154.4670 0.2318 281.0879 280.8561 300.9001 155.3150 0.2312 281.2832 281.0520 301.1941 156.0913 0.2284 281.4387 281.2103 301.4577 156.9083 0.2279 281.5824 281.3544 301.7270 157.7153 0.2276 281.7416 281.5140 301.9197 158.5015 0.2244 281.8979 281.6735 302.0956 159.3393 0.2214 282.0494 281.8280 302.2292 160.0950 0.2174 282.1698 281.9524 302.3204 160.9528 0.2153 282.3267 282.1114 302.4044 161.7185 0.2136 282.4927 282.2790 302.4429 162.5463 0.2130 282.6319 282.4189 302.4689 163.3425 0.2101 282.8161 282.6061 302.4430 164.1290 0.2084 282.9808 282.7724 302.4348 164.9668 0.2030 283.1244 282.9215 302.3945 165.7220 0.2016 283.2700 283.0684 302.3223 166.5703 0.1961 283.4261 283.2300 302.2204 167.3463 0.1937 283.5863 283.3927 302.1111 168.1633 0.1888 283.7396 283.5508 302.0007 168.9293 0.1890 283.8788 283.6898 301.8894 169.7565 0.1867 284.0193 283.8327 301.7846 170.5533 0.1887 284.1999 284.0112 301.6698 171.3500 0.1848 284.3265 284.1416 301.5720 172.1565 0.1836 284.4855 284.3018 301.5139 172.9430 0.1830 284.6590 284.4760 301.3900 173.7808 0.1815 284.8414 284.6600 301.3273 174.5360 0.1841 284.9702 284.7862 301.2949 175.3943 0.1828 285.0891 284.9063 301.2685 176.1603 0.1827 285.2266 285.0439 301.2602 176.9873 0.1861 285.4033 285.2172 301.2938 177.7740 0.1881 285.5530 285.3648 301.3595 178.5705 0.1852 285.6898 285.5047 301.4592 179.3978 0.1820 285.8469 285.6648 301.5981 180.1638 0.1808 286.0087 285.8279 301.7773 181.0115 0.1830 286.1434 285.9603 301.9780 181.7775 0.1846 286.2823 286.0977 302.1900 182.6358 0.1831 286.4475 286.2643 302.5207 183.4013 0.1812 286.5874 286.4061 302.8207 184.2290 0.1824 286.7438 286.5615 303.1395 185.0255 0.1842 286.8921 286.7080 303.4720 185.8118 0.1816 287.0303 286.8486 303.8044 186.6495 0.1796 287.2027 287.0231 304.2360 187.4153 0.1749 287.3521 287.1772 304.6417 188.2630 0.1721 287.5334 287.3613 305.0899 189.0290 0.1709 287.6214 287.4505 305.4755 189.8563 0.1696 287.7797 287.6101 305.9007 190.6528 0.1690 287.9421 287.7730 306.2554 191.4495 0.1671 288.0824 287.9153 306.6119 192.2665 0.1621 288.2345 288.0723 306.9544 193.0633 0.1579 288.4033 288.2454 307.3002 193.8908 0.1551 288.5418 288.3867 307.6295 194.6563 0.1553 288.6776 288.5223 307.9150 195.5145 0.1520 288.8286 288.6766 308.1421 196.2703 0.1459 288.9779 288.8320 308.3068 197.0973 0.1437 289.1237 288.9800 308.5000 197.8838 0.1453 289.2517 289.1065 308.6350 198.6805 0.1422 289.3516 289.2093 308.7512 199.5075 0.1393 289.5046 289.3653 308.8232 200.2735 0.1381 289.6380 289.4999 308.8481 201.1215 0.1341 289.8185 289.6844 308.8650 201.8870 0.1321 289.9520 289.8199 308.8510 202.7350 0.1272 290.1286 290.0015 308.8087 203.5010 0.1279 290.3029 290.1750 308.7671 204.3280 0.1243 290.4442 290.3199 308.7196 205.1145 0.1211 290.6018 290.4807 308.6448 205.9215 0.1165 290.7616 290.6450 308.5814 206.7383 0.1155 290.9261 290.8106 308.4795 207.5043 0.1119 291.0633 290.9513 308.3513 208.3625 0.1080 291.2114 291.1034 308.1998 209.1280 0.1070 291.3677 291.2607 308.0947 209.9555 0.1060 291.5509 291.4449 308.0154 210.7420 0.1038 291.7232 291.6193 307.8948 211.5485 0.1058 291.8682 291.7624 307.7808 212.3763 0.1048 292.0000 291.8952 307.7244 213.1625 0.1008 292.1533 292.0524 307.6755 213.9793 0.1028 292.3114 292.2086 307.6458 214.7455 0.1047 292.4597 292.3550 307.6400 215.6035 0.1063 292.6420 292.5357 307.6573 216.3693 0.1068 292.7753 292.6685 307.7510 217.1968 0.1054 292.9081 292.8027 307.8300 217.9933 0.1053 293.0665 292.9612 307.9734 218.7898 0.1049 293.2166 293.1116 308.1623 219.6173 0.0991 293.3765 293.2774 308.3749 220.3830 0.0949 293.5215 293.4265 308.5910 221.2308 0.0941 293.6528 293.5586 308.8987 222.0070 0.0931 293.7979 293.7048 309.1687 222.8240 0.0942 293.9623 293.8681 309.5043 223.6205 0.0961 294.0852 293.9891 309.8583 224.4175 0.0979 294.2224 294.1244 310.2632 225.2445 0.0973 294.3708 294.2736 310.6564 226.0105 0.0950 294.5498 294.4548 311.0578 226.8585 0.0940 294.6994 294.6054 311.5082 227.6343 0.0903 294.8520 294.7618 311.9158 228.4618 0.0863 295.0112 294.9249 312.3516 229.2585 0.0815 295.1407 295.0593 312.7695 230.0445 0.0764 295.2791 295.2026 313.1114 230.8720 0.0721 295.4415 295.3694 313.4568 231.6380 0.0704 295.5708 295.5004 313.7642 232.4855 0.0696 295.7200 295.6504 314.0858 233.2513 0.0691 295.8607 295.7916 314.3600 234.0688 0.0674 296.0253 295.9579 314.5910 234.8650 0.0625 296.1954 296.1328 314.7684 235.6620 0.0584 296.3535 296.2951 314.9312 236.4790 0.0569 296.4948 296.4379 315.0528 237.2448 0.0560 296.6272 296.5712 315.1343 238.1030 0.0531 296.7710 296.7179 315.2220 238.8688 0.0506 296.9123 296.8617 315.2452 239.6860 0.0516 297.0524 297.0007 315.2827 240.4930 0.0505 297.2355 297.1850 315.2344 241.2790 0.0472 297.3919 297.3447 315.1654 242.1170 0.0422 297.5635 297.5214 315.1378 242.8725 0.0412 297.6778 297.6366 315.0943 243.7408 0.0351 297.8592 297.8241 314.9797 244.4965 0.0316 297.9802 297.9486 314.8839 245.3238 0.0298 298.1144 298.0846 314.7564 246.1203 0.0324 298.2568 298.2244 314.6039 246.9173 0.0284 298.3984 298.3699 314.4745 247.7443 0.0217 298.5590 298.5373 314.3667 248.5000 0.0208 298.7279 298.7071 314.2505 249.3685 0.0188 298.9029 298.8841 314.1547 250.1238 0.0203 299.0579 299.0376 314.0853 250.9513 0.0189 299.2142 299.1953 314.0397 251.7173 0.0169 299.3572 299.3404 313.9966 252.5548 0.0170 299.5306 299.5136 313.9674 253.3720 0.0148 299.6783 299.6635 313.9846 254.1378 0.0142 299.8149 299.8007 314.0308 254.9958 0.0155 299.9840 299.9685 314.0829 255.7620 0.0150 300.1001 300.0852 314.2119 256.5890 0.0166 300.2296 300.2130 314.3039 257.3755 0.0168 300.3612 300.3444 314.5003 258.1825 0.0161 300.5184 300.5023 314.7343 258.9993 0.0164 300.6493 300.6329 314.9849 259.7758 0.0168 300.7819 300.7650 315.2594 260.6235 0.0166 300.9352 300.9186 315.5915 261.3995 0.0161 301.0879 301.0718 315.9376 262.2168 0.0128 301.2600 301.2472 316.3405 262.9723 0.0040 301.3894 301.3855 316.7266 263.8200 0.0025 301.5151 301.5126 317.1730 264.5860 0.0012 301.6519 301.6507 317.5779 265.4030 0.0006 301.7772 301.7766 318.0159 266.1995 0.0032 301.9180 301.9149 318.4151 266.9963 -0.0012 302.0543 302.0555 318.8456 267.8133 -0.0047 302.2148 302.2195 319.2601 268.5793 -0.0055 302.3685 302.3740 319.5818 269.4068 -0.0123 302.5387 302.5510 319.9614 270.1725 -0.0161 302.7046 302.7207 320.2789 271.0205 -0.0149 302.8732 302.8881 320.5949 271.7863 -0.0192 303.0299 303.0491 320.8415 272.6135 -0.0229 303.1813 303.2041 321.0595 273.4103 -0.0290 303.3323 303.3613 321.2238 274.2170 -0.0325 303.4658 303.4983 321.3628 275.0135 -0.0335 303.6337 303.6672 321.4788 275.8103 -0.0345 303.8143 303.8488 321.5750 276.6375 -0.0377 303.9610 303.9987 321.6408 277.4033 -0.0418 304.0869 304.1288 321.6532 278.2515 -0.0450 304.2643 304.3092 321.6524 279.0273 -0.0468 304.4082 304.4549 321.6196 279.8448 -0.0508 304.5689 304.6196 321.5426 280.6413 -0.0528 304.7204 304.7732 321.4815 281.4378 -0.0555 304.8742 304.9297 321.3906 282.2345 -0.0592 304.9879 305.0471 321.2840 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