DTA measure 3Pb251118-3.dat Date: 20251118:1529 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1519.71 s Mass = 1094.200 mg data_number = 1890 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2608 -2.3903 453.8113 456.2016 433.1580 2.0063 -2.3928 453.8173 456.2101 433.4169 2.8745 -2.3978 453.8524 456.2502 433.7537 3.6403 -2.4019 453.9312 456.3331 434.0342 4.4678 -2.4109 453.9707 456.3816 434.3148 5.2540 -2.4153 454.0209 456.4362 434.5212 6.0605 -2.4213 454.1113 456.5326 434.7791 6.8778 -2.4276 454.1987 456.6263 434.9892 7.6438 -2.4340 454.2943 456.7284 435.1485 8.5015 -2.4373 454.3618 456.7991 435.3010 9.2675 -2.4379 454.3967 456.8346 435.3789 10.0948 -2.4442 454.4319 456.8761 435.4232 10.8810 -2.4465 454.4833 456.9298 435.4471 11.6878 -2.4528 454.5476 457.0005 435.4352 12.5050 -2.4556 454.6037 457.0593 435.3728 13.2810 -2.4573 454.6353 457.0926 435.3065 14.1285 -2.4649 454.6765 457.1414 435.1987 14.9048 -2.4693 454.7259 457.1952 435.0403 15.7218 -2.4763 454.7597 457.2360 434.8401 16.4875 -2.4818 454.8059 457.2877 434.6488 17.3148 -2.4856 454.8418 457.3274 434.4070 18.1218 -2.4838 454.9054 457.3892 434.1678 18.9080 -2.4832 454.9552 457.4384 433.9160 19.7350 -2.4852 455.0167 457.5019 433.6341 20.5010 -2.4904 455.0481 457.5385 433.3642 21.3590 -2.4578 455.1040 457.5618 433.0034 22.1145 -2.4518 455.1787 457.6304 432.6633 22.9520 -2.4589 455.2283 457.6872 432.2741 23.7180 -2.4641 455.2754 457.7395 431.9322 24.5453 -2.4700 455.2971 457.7671 431.5872 25.3315 -2.4733 455.3076 457.7809 431.2699 26.1283 -2.4753 455.3341 457.8094 430.9268 26.9555 -2.4811 455.3982 457.8794 430.6095 27.7213 -2.4846 455.4612 457.9458 430.3134 28.5693 -2.4872 455.4930 457.9802 429.9963 29.3453 -2.4868 455.5364 458.0232 429.7320 30.1620 -2.4911 455.5674 458.0585 429.4460 30.9280 -2.4897 455.5896 458.0793 429.1879 31.7553 -2.4885 455.6372 458.1257 428.9101 32.5415 -2.4871 455.6501 458.1372 428.6792 33.3688 -2.4902 455.6905 458.1807 428.4743 34.1555 -2.4928 455.7065 458.1993 428.3219 34.9518 -2.4951 455.7428 458.2379 428.1644 35.7790 -2.4967 455.7673 458.2640 428.0423 36.5553 -2.4946 455.8084 458.3030 427.9563 37.4030 -2.4917 455.8734 458.3651 427.8761 38.1483 -2.4905 455.8910 458.3815 427.8069 38.9963 -2.4930 455.9001 458.3930 427.7614 39.7723 -2.4901 455.9195 458.4096 427.7469 40.5890 -2.4909 455.9689 458.4598 427.7384 41.3858 -2.4963 456.0339 458.5302 427.7880 42.1825 -2.4989 456.0594 458.5583 427.8237 43.0095 -2.5007 456.0915 458.5922 427.8856 43.7958 -2.5024 456.1119 458.6142 427.9667 44.6230 -2.5076 456.1029 458.6105 428.0644 45.3890 -2.5150 456.1179 458.6329 428.1632 46.2468 -2.5134 456.1315 458.6449 428.2619 47.0128 -2.5143 456.1555 458.6699 428.3402 47.8403 -2.5161 456.1725 458.6886 428.4281 48.6365 -2.5196 456.1732 458.6929 428.5044 49.4230 -2.5213 456.1754 458.6967 428.5412 50.2605 -2.5265 456.1835 458.7100 428.6015 51.0160 -2.5310 456.2091 458.7401 428.5887 51.8843 -2.5335 456.2350 458.7685 428.5756 52.6400 -2.5356 456.2193 458.7549 428.5530 53.4673 -2.5371 456.2432 458.7803 428.4929 54.2535 -2.5416 456.2919 458.8335 428.4475 55.0500 -2.5429 456.3003 458.8432 428.3744 55.8468 -2.5440 456.3007 458.8447 428.2634 56.6328 -2.5470 456.3152 458.8622 428.1609 57.4603 -2.5502 456.3545 458.9048 427.9950 58.2263 -2.5545 456.3613 458.9158 427.8722 59.0840 -2.5569 456.3686 458.9255 427.7167 59.8398 -2.5591 456.3867 458.9458 427.5629 60.6673 -2.5628 456.3984 458.9613 427.3681 61.4635 -2.5663 456.4166 458.9829 427.1678 62.2500 -2.5649 456.4075 458.9724 426.9528 63.0875 -2.5653 456.4106 458.9759 426.7312 63.8430 -2.5679 456.4155 458.9834 426.5505 64.7010 -2.5679 456.4331 459.0011 426.3071 65.4670 -2.5681 456.4520 459.0201 426.0879 66.2943 -2.5721 456.4491 459.0212 425.8778 67.0908 -2.5737 456.4419 459.0155 425.6651 67.8775 -2.5703 456.4335 459.0038 425.4397 68.7148 -2.5674 456.4271 458.9944 425.2139 69.4705 -2.5683 456.4123 458.9806 425.0046 70.3288 -2.5679 456.4082 458.9761 424.7910 71.0943 -2.5688 456.4003 458.9691 424.6143 71.9218 -2.5717 456.3867 458.9584 424.4269 72.6878 -2.5725 456.3977 458.9702 424.2153 73.5148 -2.5737 456.3884 458.9621 423.9918 74.3010 -2.5740 456.3919 458.9659 423.8345 75.1183 -2.5739 456.4236 458.9976 423.6806 75.9250 -2.5773 456.4272 459.0045 423.5295 76.7113 -2.5789 456.4039 458.9828 423.4113 77.5388 -2.5790 456.3885 458.9675 423.2775 78.3045 -2.5793 456.3896 458.9688 423.1860 79.1625 -2.5752 456.3939 458.9691 423.0888 79.9285 -2.5707 456.4030 458.9737 423.0106 80.7455 -2.5670 456.3916 458.9586 422.9214 81.5520 -2.5634 456.3762 458.9396 422.8747 82.3385 -2.5594 456.3721 458.9315 422.8159 83.1763 -2.5649 456.3746 458.9395 422.8000 83.9315 -2.5695 456.3461 458.9156 422.8008 84.8000 -2.5723 456.3337 458.9060 422.7697 85.5558 -2.5745 456.2946 458.8691 422.7592 86.3725 -2.5760 456.2603 458.8363 422.7302 87.1690 -2.5788 456.2262 458.8050 422.7202 87.9658 -2.5830 456.2004 458.7834 422.6949 88.7520 -2.5846 456.1983 458.7830 422.6909 89.5585 -2.5872 456.1807 458.7679 422.7132 90.3758 -2.5900 456.1556 458.7456 422.7173 91.1315 -2.5926 456.1298 458.7224 422.7003 91.9995 -2.5996 456.1552 458.7547 422.6626 92.7553 -2.6027 456.1441 458.7468 422.6451 93.5825 -2.6094 456.1270 458.7365 422.6098 94.3790 -2.6150 456.1297 458.7448 422.5698 95.1753 -2.6192 456.1404 458.7596 422.5196 96.0028 -2.6195 456.1366 458.7561 422.4434 96.7585 -2.6195 456.0928 458.7124 422.3619 97.6163 -2.6203 456.0329 458.6532 422.2784 98.3823 -2.6219 456.0008 458.6226 422.1887 99.1995 -2.6227 455.9838 458.6065 422.0576 100.0060 -2.6272 455.9344 458.5616 421.9342 100.8025 -2.6310 455.9005 458.5315 421.7753 101.6300 -2.6308 455.8697 458.5005 421.5651 102.3855 -2.6322 455.8357 458.4679 421.4261 103.2535 -2.6340 455.8320 458.4660 421.3026 104.0093 -2.6371 455.8080 458.4451 421.1417 104.8368 -2.6384 455.7952 458.4337 420.9580 105.6330 -2.6409 455.7539 458.3948 420.8163 106.4298 -2.6410 455.7361 458.3771 420.6772 107.2573 -2.6403 455.7207 458.3610 420.4903 108.0125 -2.6400 455.6923 458.3323 420.3249 108.8810 -2.6374 455.6672 458.3045 420.1613 109.6365 -2.6331 455.6251 458.2582 419.9919 110.4638 -2.6370 455.6103 458.2473 419.8358 111.2603 -2.6404 455.5595 458.1999 419.6920 112.0673 -2.6473 455.5144 458.1616 419.5076 112.8843 -2.6480 455.4482 458.0962 419.3425 113.6500 -2.6455 455.4068 458.0523 419.1753 114.5083 -2.6461 455.3954 458.0415 419.0165 115.2535 -2.6449 455.3952 458.0401 418.8763 116.1115 -2.6455 455.3729 458.0184 418.7039 116.8773 -2.6472 455.3382 457.9855 418.5706 117.6945 -2.6504 455.3089 457.9592 418.4301 118.4908 -2.6503 455.2736 457.9239 418.3087 119.2875 -2.6492 455.2507 457.8999 418.1947 120.1045 -2.6495 455.2318 457.8814 418.0837 120.8805 -2.6502 455.2084 457.8586 417.9980 121.7283 -2.6581 455.1711 457.8292 417.8941 122.4940 -2.6580 455.1178 457.7758 417.8105 123.3215 -2.6592 455.0696 457.7289 417.7021 124.1075 -2.6608 455.0196 457.6805 417.6215 124.9145 -2.6618 454.9651 457.6269 417.5567 125.7110 -2.6634 454.9113 457.5747 417.5281 126.5075 -2.6587 454.8992 457.5578 417.4710 127.3348 -2.6602 454.8925 457.5527 417.4277 128.1008 -2.6603 454.8708 457.5311 417.3839 128.9485 -2.6560 454.8452 457.5011 417.3121 129.7243 -2.6573 454.7990 457.4564 417.2880 130.5415 -2.6624 454.7083 457.3706 417.2270 131.3383 -2.6626 454.6680 457.3306 417.1611 132.1345 -2.6650 454.6201 457.2851 417.1117 132.9415 -2.6683 454.5788 457.2471 417.0798 133.7280 -2.6699 454.5348 457.2048 417.0320 134.5550 -2.6696 454.4679 457.1374 416.9927 135.3310 -2.6732 454.4181 457.0913 416.9360 136.1790 -2.6789 454.4066 457.0855 416.9001 136.9345 -2.6792 454.3604 457.0396 416.8488 137.8025 -2.6760 454.3117 456.9877 416.7473 138.5583 -2.6803 454.2635 456.9438 416.6751 139.3858 -2.6819 454.2002 456.8821 416.5886 140.1823 -2.6840 454.1239 456.8079 416.5121 140.9788 -2.6881 454.0716 456.7597 416.4005 141.8063 -2.6880 454.0315 456.7195 416.2691 142.5718 -2.6900 453.9880 456.6780 416.1712 143.4298 -2.6883 453.9567 456.6450 416.0550 144.1958 -2.6901 453.9187 456.6087 415.9414 145.0230 -2.6898 453.8732 456.5630 415.8134 145.7988 -2.6862 453.8306 456.5168 415.6593 146.6365 -2.6843 453.7820 456.4663 415.4909 147.4230 -2.6856 453.7409 456.4265 415.3244 148.2295 -2.6884 453.6926 456.3811 415.1568 149.0465 -2.6903 453.6237 456.3140 414.9815 149.8125 -2.6920 453.5839 456.2759 414.8455 150.6705 -2.6942 453.5468 456.2410 414.6835 151.4260 -2.6923 453.4835 456.1758 414.5218 152.2433 -2.6910 453.4053 456.0962 414.3546 153.0193 -2.6925 453.3358 456.0282 414.2264 153.8360 -2.6966 453.3173 456.0139 414.0603 154.6328 -2.6991 453.3175 456.0166 413.8960 155.4295 -2.7023 453.2758 455.9781 413.7718 156.2463 -2.7058 453.2145 455.9204 413.6389 157.0428 -2.7068 453.1299 455.8367 413.5135 157.8703 -2.7083 453.0615 455.7698 413.3905 158.6360 -2.7134 453.0169 455.7303 413.2728 159.4530 -2.7162 452.9639 455.6801 413.1833 160.2293 -2.7134 452.8812 455.5946 413.0647 161.0770 -2.7204 452.8424 455.5628 412.9104 161.8428 -2.7201 452.8168 455.5369 412.7983 162.6700 -2.7191 452.7603 455.4794 412.6919 163.4668 -2.7131 452.7308 455.4439 412.6188 164.2630 -2.7063 452.6817 455.3880 412.5337 165.0803 -2.7069 452.6215 455.3284 412.4235 165.8668 -2.7056 452.4950 455.2006 412.3367 166.6938 -2.7032 452.4330 455.1363 412.2485 167.4698 -2.7053 452.3855 455.0908 412.1603 168.3178 -2.7044 452.3225 455.0269 412.1019 169.0835 -2.7050 452.2668 454.9718 412.0158 169.9105 -2.7045 452.1913 454.8958 411.9402 170.7070 -2.7058 452.1148 454.8206 411.8647 171.5038 -2.7089 452.0520 454.7609 411.7913 172.3208 -2.7117 451.9933 454.7050 411.7176 173.0965 -2.7179 451.9397 454.6576 411.6383 173.9445 -2.7175 451.8544 454.5719 411.5790 174.7208 -2.7164 451.8193 454.5357 411.5344 175.5375 -2.7152 451.7800 454.4951 411.5102 176.2933 -2.7137 451.7434 454.4570 411.4750 177.1513 -2.7151 451.6304 454.3456 411.3903 177.9273 -2.7150 451.5321 454.2471 411.3167 178.7443 -2.7177 451.4690 454.1867 411.2472 179.5513 -2.7164 451.4091 454.1255 411.1650 180.3375 -2.7178 451.3443 454.0622 411.0763 181.1748 -2.7165 451.2709 453.9874 410.9561 181.9308 -2.7151 451.2157 453.9308 410.8632 182.7785 -2.7150 451.1799 453.8949 410.7366 183.5543 -2.7181 451.1289 453.8470 410.6058 184.3715 -2.7192 451.0903 453.8095 410.4769 185.1578 -2.7176 451.0236 453.7411 410.3682 185.9645 -2.7187 450.9339 453.6526 410.2627 186.7303 -2.7178 450.8964 453.6142 410.1434 187.5783 -2.7191 450.8240 453.5431 410.0296 188.3645 -2.7209 450.7397 453.4606 409.9002 189.1610 -2.7223 450.6860 453.4084 409.7597 189.9883 -2.7251 450.6046 453.3297 409.6022 190.7543 -2.7259 450.5168 453.2426 409.4482 191.6018 -2.7262 450.4487 453.1749 409.2935 192.3675 -2.7253 450.3910 453.1163 409.1469 193.1950 -2.7266 450.2937 453.0202 409.0240 193.9915 -2.7292 450.2184 452.9476 408.9055 194.7775 -2.7302 450.1641 452.8943 408.7978 195.6153 -2.7287 450.0896 452.8182 408.7110 196.3710 -2.7254 450.0369 452.7623 408.5996 197.2288 -2.7269 449.9711 452.6980 408.4580 197.9945 -2.7313 449.9202 452.6514 408.3140 198.8425 -2.7303 449.8657 452.5961 408.1670 199.6083 -2.7304 449.7859 452.5164 408.0673 200.4458 -2.7344 449.7172 452.4516 407.9413 201.2118 -2.7317 449.6539 452.3857 407.8267 202.0390 -2.7298 449.5515 452.2813 407.7168 202.8250 -2.7280 449.4848 452.2128 407.6191 203.6320 -2.7288 449.4271 452.1559 407.5185 204.4595 -2.7299 449.3520 452.0819 407.3814 205.2455 -2.7293 449.2933 452.0226 407.2876 206.0730 -2.7246 449.2155 451.9401 407.1956 206.8698 -2.7233 449.1386 451.8619 407.0980 207.6660 -2.7231 449.0668 451.7900 407.0211 208.4833 -2.7237 448.9923 451.7159 406.9494 209.2595 -2.7218 448.9210 451.6428 406.8412 210.1070 -2.7216 448.8373 451.5589 406.7433 210.8728 -2.7211 448.7382 451.4593 406.6610 211.7003 -2.7174 448.6374 451.3548 406.5602 212.5070 -2.7195 448.5771 451.2966 406.4522 213.2933 -2.7198 448.5288 451.2486 406.3336 214.1205 -2.7188 448.4575 451.1763 406.2245 214.8865 -2.7186 448.3764 451.0949 406.1727 215.7340 -2.7200 448.2952 451.0151 406.0928 216.4998 -2.7224 448.2105 450.9329 405.9958 217.3375 -2.7227 448.1175 450.8402 405.8997 218.1033 -2.7215 448.0129 450.7343 405.8154 218.9305 -2.7199 447.9558 450.6757 405.7424 219.7168 -2.7200 447.8926 450.6126 405.6419 220.5135 -2.7209 447.8097 450.5306 405.5470 221.3405 -2.7214 447.7644 450.4858 405.4593 222.1063 -2.7252 447.6901 450.4153 405.3723 222.9543 -2.7245 447.5760 450.3005 405.2768 223.7303 -2.7207 447.4722 450.1928 405.2136 224.5473 -2.7199 447.3765 450.0964 405.0759 225.3440 -2.7168 447.3157 450.0324 404.9449 226.1405 -2.7131 447.2427 449.9558 404.7989 226.9678 -2.7110 447.1561 449.8672 404.7363 227.7540 -2.7075 447.0599 449.7674 404.6484 228.5713 -2.7061 446.9717 449.6778 404.5237 229.3368 -2.7071 446.8922 449.5993 404.3759 230.1950 -2.7093 446.8249 449.5342 404.2835 230.9610 -2.7086 446.7652 449.4738 404.1854 231.7880 -2.6972 446.6967 449.3939 404.0737 232.5745 -2.6895 446.6278 449.3173 403.9694 233.3815 -2.6882 446.5701 449.2583 403.8790 234.1983 -2.6915 446.5067 449.1982 403.7602 234.9643 -2.6927 446.3996 449.0923 403.6202 235.8225 -2.6916 446.3509 449.0425 403.4835 236.5880 -2.6929 446.2771 448.9700 403.3587 237.4153 -2.6943 446.1862 448.8806 403.2382 238.2120 -2.6959 446.0787 448.7745 403.0865 239.0290 -2.6937 446.0154 448.7091 402.9727 239.8253 -2.6921 445.9532 448.6452 402.8617 240.6220 -2.6941 445.8882 448.5823 402.7679 241.4595 -2.6952 445.7900 448.4852 402.6660 242.2150 -2.6998 445.7166 448.4164 402.5419 243.0833 -2.7018 445.6172 448.3190 402.4309 243.8390 -2.7036 445.5074 448.2110 402.3492 244.6765 -2.7005 445.4099 448.1105 402.2399 245.4625 -2.7002 445.3333 448.0335 402.1314 246.2593 -2.7010 445.2676 447.9686 402.0274 247.0868 -2.7029 445.2135 447.9164 401.8896 247.8523 -2.7054 445.1691 447.8746 401.7780 248.6590 -2.7047 445.0818 447.7865 401.6544 249.4558 -2.6996 444.9979 447.6975 401.5361 250.2728 -2.6987 444.9096 447.6083 401.4266 251.0385 -2.6962 444.8302 447.5264 401.3130 251.8968 -2.6976 444.7512 447.4488 401.1975 252.6523 -2.6999 444.6833 447.3832 401.0981 253.4895 -2.6975 444.5760 447.2735 400.9712 254.2760 -2.6959 444.4914 447.1873 400.8597 255.0725 -2.6967 444.4273 447.1241 400.7743 255.8998 -2.6862 444.3447 447.0309 400.6888 256.6655 -2.6846 444.2448 446.9294 400.6094 257.5238 -2.6851 444.1742 446.8592 400.5207 258.2690 -2.6846 444.1061 446.7907 400.4500 259.1373 -2.6816 443.9983 446.6799 400.3525 259.8930 -2.6793 443.9001 446.5793 400.2676 260.7305 -2.6814 443.8002 446.4816 400.1952 261.5168 -2.6846 443.6936 446.3781 400.0984 262.3135 -2.6847 443.5941 446.2788 400.0204 263.1408 -2.6848 443.5422 446.2270 399.9408 263.9065 -2.6849 443.4649 446.1498 399.8384 264.7645 -2.6802 443.3538 446.0339 399.7223 265.5203 -2.6762 443.2776 445.9538 399.6456 266.3575 -2.6739 443.1723 445.8462 399.5286 267.1543 -2.6749 443.0770 445.7519 399.4267 267.9508 -2.6722 442.9769 445.6490 399.3396 268.7473 -2.6726 442.8847 445.5573 399.2559 269.5640 -2.6712 442.7916 445.4629 399.2153 270.3608 -2.6694 442.7051 445.3744 399.1277 271.1573 -2.6686 442.6211 445.2897 399.0134 271.9845 -2.6696 442.5485 445.2181 398.8823 272.7505 -2.6683 442.4658 445.1341 398.7627 273.5983 -2.6636 442.3672 445.0307 398.6479 274.3743 -2.6610 442.2726 444.9336 398.5734 275.2015 -2.6638 442.2249 444.8888 398.4384 275.9980 -2.6652 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373.0818 371.5921 323.6618 843.6638 1.4263 372.9048 371.4785 323.5786 844.4605 1.3680 372.7186 371.3506 323.4834 845.2465 1.3133 372.5471 371.2338 323.3643 846.0843 1.2514 372.3641 371.1127 323.2526 846.8503 1.1995 372.1777 370.9782 323.1536 847.7080 1.1410 371.9588 370.8178 323.0369 848.4635 1.0879 371.7964 370.7085 322.9310 849.3013 1.0345 371.6123 370.5777 322.7634 850.0875 0.9851 371.4651 370.4801 322.6656 850.8840 0.9338 371.3111 370.3772 322.5666 851.7113 0.8829 371.1693 370.2864 322.4836 852.4773 0.8362 371.0285 370.1922 322.3888 853.3350 0.7865 370.8472 370.0606 322.2874 854.0908 0.7423 370.6787 369.9364 322.2008 854.9283 0.7000 370.5495 369.8495 322.1081 855.7248 0.6587 370.3962 369.7375 321.9870 856.5213 0.6174 370.2352 369.6178 321.8982 857.3385 0.5784 370.0943 369.5159 321.8058 858.1145 0.5407 369.9594 369.4187 321.7120 858.9620 0.5026 369.7770 369.2745 321.5870 859.7280 0.4622 369.6100 369.1478 321.4720 860.5555 0.4229 369.4298 369.0070 321.3868 861.3415 0.3816 369.2949 368.9133 321.2965 862.1278 0.3410 369.1042 368.7632 321.2027 862.9348 0.3025 368.9237 368.6213 321.0983 863.7210 0.2646 368.7727 368.5081 320.9995 864.5380 0.2264 368.6243 368.3979 320.8692 865.3140 0.1891 368.5104 368.3213 320.7742 866.1620 0.1555 368.3496 368.1941 320.6980 866.9275 0.1242 368.2119 368.0877 320.5746 867.7550 0.0936 368.0593 367.9657 320.4445 868.5515 0.0631 367.8776 367.8145 320.3648 869.3480 0.0311 367.7258 367.6947 320.2897 870.1650 -0.0021 367.5549 367.5570 320.1492 870.9410 -0.0270 367.3964 367.4234 320.0271 871.7890 -0.0543 367.2528 367.3071 319.8916 872.5545 -0.0802 367.1048 367.1850 319.7932 873.3820 -0.1081 366.9663 367.0743 319.6952 874.1785 -0.1336 366.8366 366.9703 319.6105 874.9750 -0.1584 366.6733 366.8317 319.4935 875.7920 -0.1709 366.4827 366.6536 319.3917 876.5680 -0.1819 366.3222 366.5041 319.3019 877.4160 -0.2012 366.1825 366.3837 319.1864 878.1815 -0.2175 366.0765 366.2940 319.0944 879.0090 -0.2355 365.9313 366.1669 318.9658 879.8058 -0.2498 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