DTA measure 1Pb251118-4.dat Date: 20251118:162 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.90 s Mass = 1094.200 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3681 0.1240 269.9903 269.8663 236.6529 3.9921 0.1207 269.8498 269.7291 236.4094 5.5956 0.1130 269.7302 269.6171 236.1931 7.2095 0.1091 269.6545 269.5454 235.9454 8.8179 0.1098 269.5683 269.4585 235.7329 10.4214 0.1057 269.4604 269.3547 235.4832 12.0198 0.0981 269.3105 269.2124 235.3012 13.6230 0.0924 269.1905 269.0982 235.0764 15.2111 0.0881 269.0886 269.0006 234.8738 16.8146 0.0887 268.9759 268.8872 234.6482 18.4333 0.0803 268.8404 268.7602 234.4356 20.0470 0.0775 268.7098 268.6323 234.2106 21.6506 0.0750 268.5820 268.5070 233.9879 23.2541 0.0699 268.4412 268.3713 233.7596 24.8626 0.0642 268.2922 268.2280 233.4915 26.4661 0.0610 268.1577 268.0967 233.3171 28.0749 0.0588 268.0379 267.9791 233.1325 29.6834 0.0565 267.9638 267.9073 232.9554 31.2919 0.0504 267.8289 267.7785 232.7664 32.9006 0.0420 267.6414 267.5993 232.5218 34.5093 0.0445 267.5127 267.4681 232.2622 36.1125 0.0406 267.3739 267.3333 232.0420 37.7213 0.0357 267.1974 267.1617 231.8506 39.3299 0.0342 266.9814 266.9472 231.6854 40.9386 0.0355 266.8600 266.8244 231.4913 42.5419 0.0292 266.7183 266.6891 231.2613 44.1556 0.0212 266.6018 266.5805 231.0599 45.7643 0.0149 266.4733 266.4584 230.8970 47.3470 0.0065 266.3401 266.3336 230.7492 48.9505 -0.0058 266.1882 266.1940 230.5066 50.5593 -0.0073 266.0416 266.0489 230.2949 52.1626 -0.0094 265.8607 265.8701 230.0710 53.7711 -0.0071 265.7269 265.7340 229.8532 55.3746 -0.0050 265.6255 265.6305 229.6958 56.9986 -0.0116 265.5023 265.5139 229.4843 58.6019 -0.0232 265.3191 265.3423 229.3162 60.2055 -0.0289 265.1314 265.1603 229.1423 61.8141 -0.0369 264.9943 265.0312 228.9458 63.4174 -0.0437 264.8259 264.8696 228.7832 65.0260 -0.0452 264.6792 264.7244 228.5563 66.6295 -0.0496 264.5722 264.6219 228.3083 68.2585 -0.0548 264.4284 264.4832 228.0965 69.8671 -0.0561 264.2751 264.3312 227.8899 71.4604 -0.0657 264.0706 264.1364 227.7007 73.0743 -0.0715 263.8817 263.9532 227.5492 74.6724 -0.0771 263.7038 263.7809 227.3712 76.2708 -0.0800 263.5404 263.6204 227.1844 77.8794 -0.0847 263.3745 263.4592 226.9694 79.4829 -0.0856 263.2186 263.3042 226.7725 81.2400 -0.0915 263.0413 263.1328 226.5811 82.8948 -0.1015 262.8768 262.9783 226.4216 84.4981 -0.1077 262.7073 262.8150 226.2905 86.1015 -0.1152 262.5200 262.6352 226.1755 87.7101 -0.1161 262.3484 262.4644 226.1310 89.3291 -0.1148 262.1565 262.2712 226.0986 90.9324 -0.1152 261.9931 262.1082 226.0999 92.5410 -0.1161 261.8707 261.9867 226.1814 94.1496 -0.1219 261.7445 261.8664 226.3502 95.7581 -0.1318 261.6063 261.7381 226.5736 97.3616 -0.1429 261.3772 261.5201 226.8732 98.9703 -0.1497 261.2056 261.3552 227.2208 100.5893 -0.1568 261.0152 261.1720 227.6164 102.2028 -0.1636 260.8401 261.0037 228.0408 103.8061 -0.1711 260.7071 260.8782 228.4773 105.4148 -0.1788 260.5502 260.7290 228.9703 107.0129 -0.1890 260.4344 260.6234 229.4100 108.6011 -0.1974 260.2659 260.4633 229.8040 110.2046 -0.2016 260.1129 260.3144 230.2070 111.8233 -0.2053 259.9335 260.1389 230.5436 113.4166 -0.2114 259.7740 259.9854 230.8689 115.0355 -0.2228 259.5787 259.8015 231.1389 116.6289 -0.2284 259.4151 259.6434 231.3741 118.2321 -0.2327 259.2839 259.5165 231.5199 119.8408 -0.2306 259.1422 259.3727 231.6297 121.4596 -0.2324 258.9918 259.2242 231.7210 123.0683 -0.2376 258.8781 259.1157 231.7854 124.6614 -0.2434 258.7515 258.9949 231.8540 126.2649 -0.2467 258.6093 258.8560 231.8946 127.8736 -0.2500 258.4758 258.7258 231.9501 129.4769 -0.2572 258.3270 258.5842 231.9717 131.0958 -0.2589 258.1669 258.4258 232.0309 132.7148 -0.2667 258.0080 258.2747 232.0969 134.3230 -0.2722 257.8598 258.1321 232.1923 135.9265 -0.2716 257.7303 258.0018 232.3007 137.5353 -0.2726 257.6131 257.8857 232.4280 139.1336 -0.2772 257.5025 257.7797 232.6246 140.7369 -0.2770 257.4140 257.6910 232.8499 142.3559 -0.2740 257.3045 257.5785 233.0710 143.9338 -0.2792 257.1746 257.4538 233.3795 145.5421 -0.2820 257.0724 257.3544 233.6655 147.1661 -0.2823 256.9445 257.2268 234.0047 148.7696 -0.2797 256.8692 257.1490 234.2898 150.3780 -0.2756 256.7953 257.0708 234.6113 151.9866 -0.2825 256.6827 256.9652 234.9605 153.5799 -0.2893 256.5662 256.8555 235.3303 155.1831 -0.2920 256.4643 256.7563 235.6828 156.7916 -0.2960 256.3914 256.6875 235.9244 158.3950 -0.3075 256.2729 256.5804 236.1951 160.0036 -0.3139 256.1615 256.4754 236.4482 161.6226 -0.3149 256.0245 256.3394 236.7061 163.2466 -0.3163 255.9086 256.2249 236.9296 164.8551 -0.3199 255.8356 256.1555 237.0967 166.4481 -0.3230 255.7602 256.0832 237.2242 168.0568 -0.3250 255.7058 256.0308 237.3454 169.6600 -0.3269 255.6336 255.9605 237.4751 171.2686 -0.3285 255.5412 255.8697 237.5299 172.8721 -0.3328 255.4511 255.7840 237.5756 174.4755 -0.3320 255.4334 255.7654 237.6493 176.0635 -0.3241 255.3576 255.6817 237.7571 177.6721 -0.3274 255.2435 255.5709 237.8656 179.2859 -0.3321 255.1598 255.4919 237.9767 180.8893 -0.3320 255.0868 255.4187 238.1298 182.4979 -0.3308 255.0091 255.3399 238.2870 184.1118 -0.3296 254.9023 255.2319 238.5100 185.7154 -0.3281 254.8490 255.1770 238.7423 187.3239 -0.3297 254.7978 255.1275 238.9862 188.9325 -0.3336 254.7297 255.0633 239.2546 190.5413 -0.3359 254.6810 255.0169 239.5558 192.1600 -0.3344 254.6367 254.9711 239.8771 193.7584 -0.3328 254.5466 254.8794 240.1909 195.3773 -0.3293 254.4805 254.8098 240.5419 196.9805 -0.3274 254.4247 254.7521 240.8852 198.5941 -0.3269 254.3305 254.6574 241.1986 200.1978 -0.3275 254.2972 254.6247 241.4931 201.8064 -0.3307 254.2813 254.6120 241.7686 203.4098 -0.3294 254.2900 254.6194 242.0346 204.9979 -0.3243 254.2483 254.5726 242.2542 206.5963 -0.3233 254.2242 254.5475 242.4425 208.2099 -0.3168 254.1970 254.5137 242.6171 209.8133 -0.3209 254.1774 254.4983 242.7548 211.4219 -0.3177 254.1351 254.4528 242.8598 213.0253 -0.3187 254.1138 254.4325 242.9608 214.6338 -0.3167 254.1107 254.4274 243.0611 216.2373 -0.3086 254.0712 254.3799 243.1188 217.8460 -0.3094 254.0040 254.3133 243.2253 219.4646 -0.3102 253.9319 254.2420 243.3177 221.0681 -0.3098 253.8993 254.2091 243.4461 222.6769 -0.3128 253.8479 254.1608 243.5571 224.2803 -0.3112 253.8707 254.1819 243.7278 225.8888 -0.3072 253.8770 254.1842 243.9505 227.4924 -0.3079 253.8420 254.1499 244.1755 229.1063 -0.3068 253.7906 254.0974 244.4338 230.6994 -0.3037 253.8151 254.1188 244.6701 232.3234 -0.2984 253.8269 254.1253 244.9667 233.9269 -0.2982 253.8612 254.1593 245.2677 235.5304 -0.2997 253.8808 254.1805 245.5816 237.1339 -0.2921 253.8685 254.1607 245.9311 238.7321 -0.2900 253.8485 254.1385 246.2538 240.3408 -0.2882 253.8584 254.1466 246.5780 241.9441 -0.2907 253.8441 254.1348 246.8987 243.5578 -0.2893 253.8252 254.1145 247.1351 245.1614 -0.2864 253.8051 254.0914 247.4264 246.7649 -0.2827 253.8622 254.1449 247.6515 248.3733 -0.2798 253.8870 254.1668 247.8341 249.9768 -0.2762 253.9061 254.1822 247.9945 251.5854 -0.2778 253.9492 254.2270 248.1495 253.1886 -0.2856 253.9675 254.2532 248.2988 254.8126 -0.2842 253.9935 254.2776 248.4587 256.4110 -0.2804 253.9994 254.2798 248.6131 258.0296 -0.2756 253.9480 254.2237 248.7164 259.6331 -0.2734 254.0054 254.2788 248.8022 261.2264 -0.2707 254.0518 254.3225 248.8913 262.8349 -0.2649 254.0967 254.3617 248.9809 264.4435 -0.2594 254.1613 254.4206 249.0625 266.0573 -0.2565 254.2344 254.4909 249.2099 267.6606 -0.2504 254.2408 254.4912 249.3754 269.2640 -0.2475 254.2803 254.5278 249.5797 270.8523 -0.2483 254.3018 254.5502 249.8195 272.4558 -0.2471 254.3069 254.5540 250.0763 274.0795 -0.2383 254.3664 254.6048 250.3949 275.6678 -0.2322 254.4280 254.6603 250.7318 277.2764 -0.2293 254.4752 254.7044 251.1075 278.8850 -0.2217 254.5272 254.7489 251.4558 280.4885 -0.2199 254.5726 254.7925 251.7366 282.0920 -0.2199 254.6348 254.8547 252.0676 283.6854 -0.2219 254.6919 254.9138 252.3967 285.3043 -0.2194 254.7552 254.9746 252.6683 286.9074 -0.2160 254.8015 255.0175 252.9192 288.5160 -0.2136 254.8862 255.0998 253.1202 290.1196 -0.2164 254.9305 255.1469 253.2782 291.7435 -0.2136 255.0058 255.2194 253.4209 293.3470 -0.2057 255.0511 255.2568 253.5404 294.9556 -0.2013 255.1127 255.3140 253.6588 296.5590 -0.2015 255.1593 255.3608 253.8042 298.1624 -0.2001 255.2225 255.4226 253.8948 299.7710 -0.1963 255.3207 255.5169 253.9861 301.3590 -0.1904 255.3363 255.5268 254.0717 302.9625 -0.1832 255.4129 255.5961 254.1771 304.5659 -0.1817 255.5134 255.6951 254.3545 306.1849 -0.1764 255.5679 255.7442 254.5018 307.7676 -0.1768 255.6591 255.8359 254.6498 309.3763 -0.1762 255.7168 255.8930 254.8718 310.9953 -0.1771 255.7967 255.9738 255.1135 312.6038 -0.1766 255.8484 256.0250 255.3849 314.2123 -0.1638 255.9303 256.0941 255.6386 315.8261 -0.1557 255.9737 256.1294 255.9456 317.4144 -0.1520 256.0449 256.1969 256.2970 319.0230 -0.1518 256.1347 256.2865 256.6370 320.6264 -0.1529 256.2612 256.4141 256.9493 322.2350 -0.1487 256.3855 256.5342 257.3124 323.8385 -0.1509 256.4869 256.6379 257.6275 325.4623 -0.1465 256.5730 256.7194 257.9259 327.0760 -0.1405 256.6745 256.8151 258.1772 328.6848 -0.1389 256.7547 256.8936 258.4048 330.2933 -0.1364 256.8273 256.9637 258.6113 331.8966 -0.1416 256.9498 257.0914 258.7860 333.4848 -0.1413 257.0255 257.1668 258.9158 335.0881 -0.1390 257.1335 257.2725 259.0391 336.7018 -0.1308 257.2346 257.3654 259.1091 338.2899 -0.1244 257.3300 257.4543 259.2238 339.8984 -0.1256 257.4503 257.5759 259.3022 341.4966 -0.1235 257.5683 257.6918 259.3732 343.1156 -0.1233 257.6578 257.7812 259.4895 344.7243 -0.1237 257.7732 257.8969 259.6245 346.3328 -0.1172 257.8690 257.9861 259.7596 347.9414 -0.1128 257.9623 258.0752 259.9328 349.5500 -0.1147 258.0517 258.1664 260.1301 351.1535 -0.1124 258.1518 258.2642 260.3536 352.7569 -0.1089 258.2225 258.3314 260.5436 354.3656 -0.1071 258.3287 258.4358 260.8173 355.9845 -0.1054 258.4532 258.5586 261.1369 357.5933 -0.0992 258.5801 258.6793 261.4517 359.1968 -0.0898 258.7248 258.8145 261.8000 360.8104 -0.0865 258.8768 258.9633 262.1586 362.4139 -0.0849 259.0087 259.0936 262.4879 364.0175 -0.0863 259.1274 259.2137 262.8486 365.6156 -0.0868 259.2734 259.3602 263.1477 367.2295 -0.0836 259.3923 259.4759 263.4131 368.8329 -0.0863 259.5279 259.6142 263.7151 370.4259 -0.0844 259.6440 259.7284 263.9262 372.0294 -0.0822 259.7500 259.8322 264.1311 373.6329 -0.0777 259.8621 259.9398 264.2862 375.2363 -0.0728 259.9819 260.0548 264.3907 376.8396 -0.0738 260.0782 260.1521 264.5164 378.4534 -0.0686 260.2038 260.2723 264.6148 380.0723 -0.0664 260.3759 260.4423 264.7172 381.6806 -0.0619 260.4771 260.5390 264.8060 383.2841 -0.0642 260.6142 260.6784 264.8728 384.8926 -0.0667 260.7451 260.8118 264.9490 386.4961 -0.0642 260.8937 260.9580 265.0513 388.1150 -0.0561 261.0705 261.1266 265.2148 389.7133 -0.0521 261.2215 261.2736 265.3826 391.3219 -0.0512 261.3420 261.3932 265.5870 392.9408 -0.0446 261.4849 261.5295 265.8589 394.5494 -0.0397 261.5765 261.6162 266.1354 396.1529 -0.0389 261.7008 261.7397 266.4812 397.7614 -0.0314 261.8499 261.8813 266.8245 399.3546 -0.0301 261.9944 262.0246 267.1366 400.9531 -0.0273 262.1740 262.2013 267.4760 402.5564 -0.0255 262.3423 262.3678 267.8288 404.1599 -0.0240 262.5318 262.5558 268.1895 405.7635 -0.0220 262.6728 262.6948 268.5102 407.3823 -0.0217 262.8558 262.8776 268.7847 408.9856 -0.0265 263.0177 263.0442 269.0226 410.5943 -0.0247 263.1449 263.1696 269.3049 412.1979 -0.0208 263.2824 263.3032 269.4723 413.8064 -0.0141 263.4223 263.4364 269.6053 415.4099 -0.0150 263.5923 263.6073 269.7448 417.0185 -0.0148 263.7292 263.7439 269.8240 418.6321 -0.0194 263.8859 263.9053 269.9092 420.2355 -0.0089 264.0715 264.0804 269.9747 421.8441 -0.0035 264.2449 264.2484 270.0321 423.4680 -0.0050 264.3998 264.4047 270.1425 425.0765 -0.0048 264.5547 264.5595 270.2656 426.6801 -0.0042 264.6956 264.6999 270.3557 428.2888 -0.0012 264.8244 264.8256 270.4760 429.8766 0.0044 264.9966 264.9922 270.6358 431.4853 0.0106 265.1449 265.1343 270.8344 433.0838 0.0171 265.3217 265.3045 271.0653 434.6871 0.0204 265.4736 265.4532 271.3346 436.2956 0.0236 265.6033 265.5797 271.6606 437.9094 0.0195 265.7687 265.7492 272.0031 439.5079 0.0136 265.9594 265.9458 272.3614 441.1216 0.0166 266.1077 266.0910 272.7179 442.7199 0.0174 266.2471 266.2297 273.0426 444.3235 0.0160 266.4117 266.3957 273.3973 445.9321 0.0177 266.5909 266.5732 273.7446 447.5354 0.0180 266.7623 266.7443 274.0700 449.1543 0.0178 266.9173 266.8995 274.3955 450.7630 0.0215 267.0842 267.0627 274.6073 452.3666 0.0235 267.2867 267.2633 274.8147 453.9955 0.0253 267.5095 267.4843 275.0143 455.5990 0.0211 267.6551 267.6340 275.1537 457.2129 0.0220 267.8118 267.7898 275.2593 458.8161 0.0201 267.9887 267.9686 275.3399 460.4196 0.0227 268.1783 268.1555 275.4070 462.0231 0.0245 268.3765 268.3520 275.4638 463.6265 0.0219 268.5515 268.5297 275.4667 465.2094 0.0261 268.6741 268.6479 275.4974 466.8129 0.0294 268.8583 268.8290 275.5704 468.4164 0.0316 269.0252 268.9936 275.7273 470.0351 0.0328 269.2266 269.1938 275.8890 471.6388 0.0365 269.4005 269.3640 276.0480 473.2474 0.0395 269.5768 269.5373 276.2823 474.8458 0.0440 269.7350 269.6910 276.5660 476.4544 0.0405 269.9260 269.8855 276.8957 478.0579 0.0394 270.0907 270.0513 277.2059 479.6716 0.0425 270.2592 270.2167 277.6093 481.2804 0.0397 270.4774 270.4377 278.0337 482.8838 0.0390 270.6670 270.6280 278.3978 484.4924 0.0391 270.8188 270.7797 278.7817 486.1164 0.0370 270.9991 270.9621 279.1671 487.7250 0.0331 271.1981 271.1649 279.5109 489.3335 0.0304 271.3722 271.3417 279.8003 490.9370 0.0324 271.5479 271.5155 280.0177 492.5456 0.0353 271.7591 271.7237 280.1982 494.1439 0.0376 271.9534 271.9159 280.3545 495.7423 0.0391 272.1123 272.0732 280.4780 497.3456 0.0393 272.2989 272.2597 280.5734 498.9489 0.0389 272.5204 272.4815 280.6607 500.5678 0.0378 272.7220 272.6842 280.7090 502.1456 0.0410 272.8959 272.8548 280.7600 503.7694 0.0444 273.0781 273.0337 280.7438 505.3780 0.0474 273.2476 273.2002 280.7648 506.9868 0.0469 273.4905 273.4435 280.7905 508.5901 0.0466 273.7133 273.6667 280.9011 510.1986 0.0496 273.9052 273.8555 281.0660 511.8021 0.0528 274.0734 274.0205 281.2712 513.4055 0.0514 274.2464 274.1950 281.5862 515.0140 0.0498 274.4253 274.3755 281.9289 516.6176 0.0519 274.6552 274.6033 282.3039 518.2365 0.0509 274.8608 274.8099 282.6352 519.8449 0.0571 275.0447 274.9876 282.9810 521.4484 0.0574 275.2323 275.1749 283.3584 523.0570 0.0568 275.4810 275.4241 283.7573 524.6605 0.0600 275.6512 275.5912 284.1583 526.2640 0.0604 275.8231 275.7627 284.5013 527.8674 0.0558 276.0407 275.9849 284.8024 529.4659 0.0545 276.2587 276.2042 285.0992 531.0694 0.0594 276.4493 276.3899 285.3546 532.6728 0.0514 276.6301 276.5787 285.5218 534.2764 0.0460 276.8266 276.7806 285.6650 535.8850 0.0488 277.0149 276.9661 285.7922 537.4883 0.0514 277.1870 277.1356 285.8420 539.0969 0.0542 277.4187 277.3645 285.9235 540.7005 0.0588 277.6331 277.5743 285.9618 542.3141 0.0555 277.8333 277.7779 285.9905 543.9175 0.0493 278.0225 277.9732 285.9899 545.5210 0.0509 278.2287 278.1778 286.0582 547.1293 0.0507 278.4411 278.3904 286.1321 548.7328 0.0565 278.6411 278.5846 286.2616 550.3414 0.0604 278.8716 278.8111 286.4256 551.9603 0.0644 279.0859 279.0215 286.6598 553.5585 0.0611 279.2504 279.1893 286.9322 555.1671 0.0569 279.4873 279.4304 287.2353 556.7859 0.0608 279.6938 279.6330 287.5866 558.3944 0.0542 279.9265 279.8723 287.9723 559.9825 0.0589 280.0781 280.0192 288.3382 561.5859 0.0609 280.2648 280.2039 288.7643 563.1893 0.0610 280.4411 280.3801 289.1586 564.7723 0.0607 280.7052 280.6445 289.5034 566.3808 0.0657 280.9352 280.8694 289.8388 567.9841 0.0609 281.0694 281.0084 290.1932 569.5928 0.0585 281.2591 281.2006 290.4876 571.1960 0.0525 281.4667 281.4143 290.7183 572.9891 0.0510 281.7177 281.6667 290.8853 574.6133 0.0519 281.9464 281.8944 290.9985 576.2219 0.0544 282.1825 282.1280 291.0536 577.8254 0.0568 282.3833 282.3265 291.0948 579.4493 0.0559 282.5346 282.4787 291.1238 581.0528 0.0503 282.7121 282.6618 291.1356 582.6614 0.0526 282.9501 282.8975 291.1417 584.2648 0.0559 283.1773 283.1214 291.1418 585.8734 0.0616 283.4155 283.3539 291.2384 587.4820 0.0629 283.6072 283.5443 291.3543 589.0853 0.0604 283.8215 283.7611 291.5160 590.6785 0.0565 284.0413 283.9848 291.6718 592.2923 0.0565 284.2391 284.1826 291.9143 593.9006 0.0577 284.4399 284.3822 292.2036 595.4888 0.0615 284.6727 284.6112 292.5386 597.0923 0.0636 284.8981 284.8345 292.9529 598.7006 0.0657 285.1219 285.0562 293.4228 600.3041 0.0603 285.3346 285.2744 293.8732 601.8974 0.0574 285.5531 285.4956 294.3658 603.5160 0.0585 285.7729 285.7144 294.7978 605.1246 0.0561 285.9782 285.9221 295.1512 606.7435 0.0529 286.2205 286.1676 295.4580 608.3520 0.0466 286.3847 286.3380 295.7044 609.9451 0.0460 286.5738 286.5278 295.9044 611.5538 0.0459 286.8060 286.7602 296.0998 613.1570 0.0457 287.0152 286.9695 296.1956 614.7708 0.0389 287.2143 287.1754 296.2401 616.3794 0.0373 287.4670 287.4297 296.2478 617.9826 0.0398 287.6648 287.6250 296.2283 619.5914 0.0437 287.9078 287.8641 296.2228 621.2103 0.0479 288.1582 288.1103 296.2165 622.8189 0.0440 288.3773 288.3333 296.2180 624.4170 0.0422 288.5937 288.5515 296.2855 626.0103 0.0409 288.8599 288.8189 296.3570 627.6190 0.0341 289.0393 289.0052 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