DTA measure 3Pb251118-4.dat Date: 20251118:1633 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1749.59 s Mass = 1094.200 mg data_number = 1088 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3488 -2.6914 457.2487 459.9400 434.4130 3.9480 -2.7046 457.3196 460.0243 434.6267 5.5521 -2.7166 457.4237 460.1403 434.7339 7.1569 -2.7305 457.4689 460.1994 434.7424 8.7659 -2.7423 457.5299 460.2722 434.7247 10.3603 -2.7525 457.5627 460.3152 434.5437 11.9846 -2.7646 457.6483 460.4129 434.3524 13.5893 -2.7672 457.7189 460.4860 434.0679 15.1983 -2.7741 457.7898 460.5639 433.7194 16.8029 -2.7843 457.8005 460.5848 433.3200 18.4071 -2.7901 457.8179 460.6081 432.9015 20.0165 -2.7943 457.9128 460.7071 432.3875 21.6213 -2.8043 458.0110 460.8153 431.9033 23.2458 -2.8092 458.0167 460.8259 431.5090 24.8400 -2.8110 458.0505 460.8615 431.1601 26.4495 -2.8159 458.0990 460.9149 430.8276 28.0639 -2.8257 458.1852 461.0109 430.5152 29.6684 -2.8278 458.2676 461.0955 430.3214 31.2724 -2.8319 458.3096 461.1415 430.2402 32.8771 -2.8341 458.3173 461.1514 430.2441 34.4809 -2.8378 458.3238 461.1616 430.3123 36.0959 -2.8429 458.3673 461.2102 430.3883 37.6743 -2.8433 458.4009 461.2442 430.4927 39.2788 -2.8489 458.4148 461.2638 430.6507 40.8985 -2.8594 458.4473 461.3067 430.7897 42.5026 -2.8704 458.4748 461.3452 430.9361 44.1069 -2.8838 458.4824 461.3661 431.0323 45.7163 -2.8899 458.4636 461.3536 431.1121 47.3159 -2.8917 458.4719 461.3635 431.1259 48.9198 -2.8936 458.4995 461.3930 431.0259 50.5295 -2.9022 458.5242 461.4264 430.8370 52.1338 -2.9131 458.5572 461.4703 430.6042 53.7585 -2.9197 458.5621 461.4817 430.3217 55.3631 -2.9286 458.5887 461.5172 430.0061 56.9721 -2.9376 458.5996 461.5372 429.7338 58.5820 -2.9421 458.5782 461.5203 429.3567 60.1860 -2.9433 458.5631 461.5064 428.9948 61.7956 -2.9499 458.5630 461.5129 428.6587 63.4000 -2.9516 458.5685 461.5202 428.3443 64.9939 -2.9591 458.5633 461.5224 428.0315 66.6038 -2.9609 458.6195 461.5804 427.7939 68.2075 -2.9621 458.6145 461.5766 427.5930 69.8123 -2.9650 458.6096 461.5745 427.4476 71.4164 -2.9683 458.5646 461.5329 427.3819 73.0156 -2.9740 458.5573 461.5313 427.3533 74.6253 -2.9778 458.5766 461.5543 427.3487 76.2293 -2.9823 458.5854 461.5677 427.3932 77.8388 -2.9898 458.5709 461.5607 427.4438 79.4429 -2.9976 458.5610 461.5586 427.5058 81.0579 -3.0026 458.5394 461.5419 427.5641 82.6616 -3.0144 458.5149 461.5293 427.5708 84.2715 -3.0245 458.4927 461.5172 427.5479 85.8809 -3.0225 458.4637 461.4863 427.5130 87.4851 -3.0259 458.4063 461.4322 427.4313 89.0950 -3.0247 458.3534 461.3781 427.2717 90.7141 -3.0285 458.3048 461.3333 427.1362 92.3240 -3.0362 458.3215 461.3577 426.9558 93.9284 -3.0413 458.3295 461.3708 426.7246 95.5325 -3.0472 458.2965 461.3437 426.5251 97.1420 -3.0537 458.2826 461.3363 426.3102 98.7308 -3.0591 458.2844 461.3436 426.0175 100.3355 -3.0619 458.2586 461.3205 425.7524 101.9344 -3.0607 458.2285 461.2892 425.4778 103.5389 -3.0607 458.2315 461.2921 425.2561 105.1585 -3.0648 458.1651 461.2299 425.0219 106.7833 -3.0721 458.0800 461.1521 424.8031 108.5570 -3.0789 458.0113 461.0902 424.5695 110.1660 -3.0827 457.9181 461.0008 424.4344 111.7861 -3.0843 457.8506 460.9349 424.3165 113.3950 -3.0893 457.8212 460.9105 424.2150 114.9998 -3.0951 457.8138 460.9089 424.1753 116.6088 -3.0967 457.7893 460.8859 424.1235 118.2134 -3.0976 457.7450 460.8427 424.1242 119.8178 -3.1004 457.7046 460.8050 424.1605 121.4270 -3.1101 457.6535 460.7636 424.1789 123.0471 -3.1172 457.6339 460.7512 424.1620 124.6560 -3.1171 457.5828 460.6999 424.1192 126.2608 -3.1197 457.4880 460.6077 424.0551 127.8699 -3.1232 457.4388 460.5621 423.9484 129.4590 -3.1247 457.4078 460.5326 423.8331 131.0580 -3.1334 457.3585 460.4919 423.6950 132.6675 -3.1351 457.2335 460.3686 423.5175 134.2671 -3.1391 457.1637 460.3028 423.3419 135.8863 -3.1471 457.0792 460.2263 423.1437 137.4960 -3.1525 457.0308 460.1832 422.9501 139.0999 -3.1528 456.9880 460.1408 422.7390 140.7046 -3.1538 456.9642 460.1180 422.4762 142.3086 -3.1535 456.8836 460.0372 422.2477 143.9183 -3.1557 456.8350 459.9907 421.9848 145.5228 -3.1603 456.7776 459.9378 421.7741 147.1319 -3.1611 456.7200 459.8811 421.6252 148.7469 -3.1605 456.6085 459.7690 421.4527 150.3404 -3.1586 456.5661 459.7247 421.2837 151.9656 -3.1609 456.4676 459.6284 421.1758 153.5698 -3.1635 456.4211 459.5846 421.0850 155.1844 -3.1606 456.3400 459.5006 420.9906 156.7885 -3.1663 456.2337 459.4000 420.9431 158.4031 -3.1693 456.2043 459.3737 420.8556 159.9970 -3.1692 456.1737 459.3429 420.8116 161.5963 -3.1704 456.1047 459.2751 420.7476 163.1955 -3.1695 456.0246 459.1940 420.6982 164.7996 -3.1690 455.8973 459.0663 420.6176 166.4198 -3.1769 455.7861 458.9630 420.4943 168.0184 -3.1790 455.7057 458.8847 420.4159 169.6231 -3.1809 455.6613 458.8422 420.3339 171.2271 -3.1820 455.5637 458.7457 420.2359 172.8368 -3.1844 455.4758 458.6603 420.1586 174.4411 -3.1842 455.4013 458.5855 420.0269 176.0504 -3.1850 455.3080 458.4930 419.8895 177.6549 -3.1912 455.2611 458.4523 419.6835 179.2743 -3.1890 455.1676 458.3566 419.5118 180.8688 -3.1947 455.0818 458.2765 419.3500 182.4880 -3.1973 455.0564 458.2537 419.1351 184.0926 -3.1960 454.9853 458.1813 418.9531 185.7020 -3.1959 454.8853 458.0812 418.7629 187.3114 -3.1925 454.8209 458.0134 418.5917 188.9206 -3.2022 454.7214 457.9236 418.3791 190.5250 -3.2022 454.6272 457.8293 418.1654 192.1343 -3.1985 454.5311 457.7296 418.0035 193.7181 -3.2011 454.4221 457.6231 417.8396 195.3328 -3.2003 454.3182 457.5185 417.7061 196.9369 -3.1967 454.2282 457.4249 417.6212 198.5416 -3.2030 454.1754 457.3784 417.5453 200.1404 -3.2067 454.0883 457.2949 417.4875 201.7501 -3.2082 454.0111 457.2194 417.4329 203.3541 -3.2069 453.9115 457.1184 417.3732 204.9638 -3.2042 453.7890 456.9932 417.2555 206.5831 -3.2027 453.6970 456.8997 417.1801 208.1876 -3.1977 453.6039 456.8016 417.0668 209.7814 -3.1979 453.5203 456.7181 416.9431 211.3859 -3.2012 453.4318 456.6330 416.8582 212.9951 -3.2034 453.3253 456.5286 416.7644 214.5995 -3.2032 453.2065 456.4098 416.6235 216.2090 -3.2035 453.1121 456.3156 416.4259 217.8131 -3.2043 453.0085 456.2127 416.3174 219.4333 -3.2060 452.8926 456.0986 416.1551 221.0423 -3.2115 452.7830 455.9946 416.0158 222.6469 -3.2132 452.6810 455.8942 415.8148 224.2561 -3.2134 452.5873 455.8007 415.6575 225.8554 -3.2141 452.4986 455.7127 415.4815 227.4548 -3.2146 452.3962 455.6108 415.2955 229.0588 -3.2167 452.2874 455.5041 415.1090 230.6738 -3.2129 452.1913 455.4042 414.9424 232.2879 -3.2102 452.1155 455.3257 414.8056 233.8925 -3.2077 452.0220 455.2297 414.6420 235.4964 -3.2063 451.8844 455.0906 414.4805 237.1010 -3.2048 451.7604 454.9652 414.3704 238.7104 -3.2061 451.6694 454.8756 414.2644 240.3249 -3.2074 451.5486 454.7560 414.1662 241.9143 -3.2114 451.4364 454.6478 414.1140 243.5180 -3.2144 451.3196 454.5340 414.0563 245.1279 -3.2132 451.2641 454.4774 414.0253 246.7475 -3.2106 451.1430 454.3535 413.9131 248.3569 -3.2067 451.0296 454.2362 413.8529 249.9614 -3.2083 450.8776 454.0859 413.7504 251.5756 -3.2076 450.7756 453.9831 413.6181 253.1803 -3.2113 450.6674 453.8787 413.4920 254.7893 -3.2110 450.5817 453.7928 413.3382 256.3940 -3.2123 450.4878 453.7000 413.1756 257.9981 -3.2161 450.3873 453.6034 413.0206 259.5820 -3.2121 450.2578 453.4699 412.8363 261.2018 -3.2117 450.1723 453.3839 412.6666 262.7956 -3.2136 450.0588 453.2724 412.4817 264.4003 -3.2125 449.9641 453.1767 412.2985 266.0041 -3.2061 449.8591 453.0652 412.1500 267.6089 -3.1955 449.7771 452.9726 411.9684 269.2178 -3.1944 449.6846 452.8790 411.7673 270.8276 -3.1902 449.5736 452.7638 411.6228 272.4265 -3.1876 449.4203 452.6079 411.4645 274.0361 -3.1844 449.2510 452.4354 411.3479 275.6403 -3.1850 449.0809 452.2659 411.2210 277.2498 -3.1936 448.9664 452.1601 411.1048 278.8696 -3.1955 448.8614 452.0569 411.0144 280.4583 -3.1917 448.7446 451.9363 410.9217 282.0784 -3.1898 448.6267 451.8165 410.8121 283.6874 -3.1882 448.5339 451.7221 410.7207 285.3023 -3.1843 448.3971 451.5815 410.6243 286.9064 -3.1836 448.2547 451.4383 410.5629 288.5108 -3.1843 448.1328 451.3171 410.4287 290.0998 -3.1839 448.0240 451.2079 410.2788 291.7090 -3.1842 447.9341 451.1183 410.1718 293.3086 -3.1841 447.7927 450.9768 410.0434 294.9126 -3.1817 447.6852 450.8668 409.9111 296.5376 -3.1856 447.6120 450.7976 409.8263 298.1370 -3.1863 447.4993 450.6856 409.6905 299.7359 -3.1853 447.4098 450.5951 409.5045 301.3458 -3.1846 447.3217 450.5063 409.3575 302.9341 -3.1792 447.2060 450.3852 409.2012 304.5440 -3.1758 447.0561 450.2319 409.0461 306.1480 -3.1767 446.9071 450.0838 408.8709 307.7986 -3.1769 446.7985 449.9754 408.7162 309.4541 -3.1758 446.6954 449.8712 408.5448 311.0584 -3.1719 446.5865 449.7583 408.3984 312.6780 -3.1671 446.4247 449.5918 408.2929 314.2823 -3.1590 446.2871 449.4460 408.1227 315.8818 -3.1582 446.1520 449.3102 407.9925 317.4959 -3.1604 446.0118 449.1722 407.8770 319.1058 -3.1667 445.9121 449.0787 407.7326 320.7150 -3.1667 445.7765 448.9432 407.5880 322.3194 -3.1649 445.6750 448.8399 407.4591 323.9135 -3.1623 445.5575 448.7197 407.3170 325.4971 -3.1642 445.4748 448.6390 407.2650 327.1018 -3.1606 445.4278 448.5885 407.1448 328.6954 -3.1578 445.2907 448.4485 407.0184 330.3206 -3.1592 445.1292 448.2884 406.9089 331.9198 -3.1632 445.0061 448.1692 406.7641 333.5291 -3.1560 444.8797 448.0357 406.6814 335.1389 -3.1541 444.7735 447.9276 406.5585 336.7479 -3.1556 444.6521 447.8077 406.4638 338.3424 -3.1536 444.5181 447.6717 406.3366 339.9464 -3.1474 444.4516 447.5990 406.1843 341.5560 -3.1410 444.3652 447.5062 406.0408 343.1758 -3.1366 444.1880 447.3246 405.9335 344.7850 -3.1390 444.0667 447.2057 405.8042 346.3898 -3.1393 443.9749 447.1143 405.6892 347.9988 -3.1369 443.8799 447.0168 405.5759 349.6034 -3.1308 443.7609 446.8917 405.4067 351.2074 -3.1275 443.6122 446.7397 405.2256 352.8221 -3.1268 443.4549 446.5817 405.0467 354.4214 -3.1266 443.2795 446.4061 404.9063 356.0153 -3.1273 443.1605 446.2878 404.7689 357.6303 -3.1280 442.9968 446.1248 404.6154 359.2391 -3.1221 442.8825 446.0047 404.4583 360.8388 -3.1216 442.7520 445.8736 404.3014 362.4428 -3.1170 442.6152 445.7321 404.1798 364.0473 -3.1173 442.5052 445.6225 404.0660 365.6514 -3.1144 442.3736 445.4879 403.9219 367.2506 -3.1155 442.2776 445.3931 403.7943 368.8548 -3.1114 442.1554 445.2668 403.6821 370.4796 -3.1067 442.0260 445.1327 403.5447 372.0840 -3.1004 441.9128 445.0133 403.4283 373.6933 -3.0924 441.7996 444.8919 403.2746 375.3031 -3.0877 441.6780 444.7656 403.1950 376.9018 -3.0899 441.5923 444.6821 403.0591 378.5065 -3.0903 441.4410 444.5313 402.9631 380.1155 -3.0868 441.2568 444.3435 402.8509 381.7201 -3.0852 441.1299 444.2152 402.7665 383.3445 -3.0853 441.0084 444.0936 402.6502 384.9543 -3.0841 440.8946 443.9786 402.5140 386.5535 -3.0851 440.7534 443.8384 402.3568 388.1423 -3.0817 440.5978 443.6795 402.2434 389.7520 -3.0763 440.4791 443.5554 402.1021 391.3405 -3.0743 440.3682 443.4425 401.9299 392.9555 -3.0728 440.2315 443.3043 401.7885 394.5699 -3.0753 440.0757 443.1510 401.6366 396.1589 -3.0747 439.9368 443.0114 401.4869 397.7789 -3.0764 439.7936 442.8700 401.3245 399.3879 -3.0695 439.6645 442.7340 401.1686 400.9926 -3.0645 439.4873 442.5518 401.0209 402.5811 -3.0577 439.3569 442.4146 400.8750 404.2165 -3.0508 439.2940 442.3448 400.7110 405.8105 -3.0554 439.1914 442.2469 400.5281 407.4096 -3.0508 439.0660 442.1168 400.3698 409.0193 -3.0463 438.9680 442.0143 400.2208 410.6233 -3.0434 438.8260 441.8694 400.1178 412.2485 -3.0379 438.6839 441.7218 400.0067 413.8575 -3.0387 438.5005 441.5392 399.9071 415.4570 -3.0387 438.4282 441.4669 399.7976 417.0663 -3.0379 438.2478 441.2857 399.6836 418.6655 -3.0358 438.1380 441.1738 399.5538 420.2699 -3.0377 438.0457 441.0833 399.4356 421.8689 -3.0344 437.9097 440.9441 399.3473 423.4685 -3.0300 437.7784 440.8084 399.2476 425.0881 -3.0260 437.6721 440.6981 399.1475 426.6719 -3.0259 437.5207 440.5466 399.0272 428.2814 -3.0300 437.4033 440.4333 398.9305 429.8958 -3.0244 437.2860 440.3104 398.8064 431.5005 -3.0215 437.1298 440.1513 398.7318 433.1094 -3.0164 436.9650 439.9813 398.5958 434.7244 -3.0144 436.8504 439.8648 398.4763 436.3180 -3.0112 436.7398 439.7510 398.3058 437.9278 -3.0106 436.6334 439.6441 398.1359 439.5320 -3.0087 436.5206 439.5292 397.9865 441.1260 -3.0056 436.3669 439.3725 397.8540 442.7306 -2.9991 436.2364 439.2355 397.6713 444.3345 -2.9951 436.0966 439.0917 397.5082 445.9598 -2.9915 435.9211 438.9125 397.3485 447.5638 -2.9897 435.7435 438.7332 397.2108 449.1734 -2.9865 435.6567 438.6432 397.0480 450.7778 -2.9851 435.5469 438.5320 396.8553 452.3716 -2.9812 435.4096 438.3908 396.7094 453.9709 -2.9757 435.3216 438.2973 396.5915 455.5801 -2.9783 435.2036 438.1819 396.4540 457.1695 -2.9808 435.0959 438.0767 396.3164 458.7886 -2.9777 434.8847 437.8624 396.1677 460.3934 -2.9716 434.7361 437.7077 396.0689 462.0026 -2.9619 434.5756 437.5375 395.9933 463.6019 -2.9585 434.4447 437.4031 395.9268 465.2118 -2.9615 434.3219 437.2833 395.8879 466.8104 -2.9639 434.2119 437.1758 395.8044 468.4203 -2.9617 434.1211 437.0828 395.6751 470.0291 -2.9621 433.9209 436.8830 395.5825 471.6390 -2.9561 433.8011 436.7573 395.4458 473.2584 -2.9539 433.6797 436.6337 395.2953 474.8526 -2.9492 433.5325 436.4816 395.1640 476.4673 -2.9488 433.4092 436.3580 394.9750 478.0765 -2.9483 433.3113 436.2596 394.8120 479.6864 -2.9466 433.2026 436.1492 394.6500 481.2901 -2.9430 433.0654 436.0083 394.5181 482.8949 -2.9354 432.8780 435.8134 394.3708 484.4889 -2.9327 432.7340 435.6667 394.2562 486.1034 -2.9283 432.6006 435.5288 394.0753 487.6875 -2.9254 432.4895 435.4149 393.8556 489.2863 -2.9239 432.3702 435.2940 393.6513 490.9064 -2.9245 432.2328 435.1573 393.4628 492.5104 -2.9230 432.1654 435.0884 393.3258 494.1149 -2.9173 432.0950 435.0123 393.2216 495.7091 -2.9159 431.9570 434.8730 393.0878 497.3234 -2.9088 431.8319 434.7407 392.9763 498.9281 -2.9084 431.6468 434.5552 392.8631 500.5374 -2.9088 431.4643 434.3731 392.7466 502.1418 -2.9026 431.2909 434.1935 392.6920 503.7463 -2.8973 431.1328 434.0301 392.6575 505.3708 -2.8959 430.9875 433.8835 392.5985 506.9601 -2.8939 430.8740 433.7678 392.5303 508.5743 -2.8871 430.7432 433.6303 392.4623 510.1840 -2.8882 430.6032 433.4914 392.3483 511.7883 -2.8883 430.4722 433.3605 392.2319 513.3976 -2.8810 430.3296 433.2106 392.0573 514.9970 -2.8800 430.2139 433.0939 391.8834 516.6061 -2.8796 430.1257 433.0053 391.7710 518.1955 -2.8788 430.0494 432.9282 391.6594 519.8045 -2.8784 429.9133 432.7917 391.4649 521.4091 -2.8754 429.7728 432.6482 391.2239 523.0288 -2.8745 429.5886 432.4632 391.0550 524.6330 -2.8704 429.4720 432.3423 390.8918 526.2378 -2.8652 429.3754 432.2405 390.7175 527.8313 -2.8613 429.2726 432.1338 390.5398 529.4359 -2.8564 429.1242 431.9806 390.3136 531.0449 -2.8523 428.9903 431.8426 390.1524 532.6496 -2.8486 428.8424 431.6910 390.0456 534.2586 -2.8489 428.7132 431.5621 389.8914 535.8633 -2.8471 428.5556 431.4027 389.7722 537.4881 -2.8471 428.3863 431.2334 389.6623 539.0769 -2.8445 428.2622 431.1067 389.5642 540.6970 -2.8386 428.1316 430.9703 389.5059 542.3061 -2.8394 428.0126 430.8520 389.4034 543.9106 -2.8394 427.8795 430.7189 389.3061 545.5149 -2.8354 427.7602 430.5956 389.2244 547.1243 -2.8327 427.6390 430.4717 389.1469 548.7239 -2.8267 427.5034 430.3302 389.0377 550.3276 -2.8197 427.3729 430.1927 388.9356 551.9324 -2.8174 427.2020 430.0194 388.8546 553.5315 -2.8181 427.0741 429.8921 388.7219 555.1409 -2.8166 426.9577 429.7743 388.6061 556.7456 -2.8146 426.8061 429.6207 388.4641 558.3495 -2.8149 426.6611 429.4759 388.3079 559.9593 -2.8140 426.5472 429.3612 388.1304 561.5481 -2.8062 426.3829 429.1891 387.9705 563.1575 -2.8029 426.2449 429.0478 387.7981 564.7620 -2.8013 426.0924 428.8937 387.6560 566.3865 -2.7953 425.9640 428.7593 387.4408 567.9913 -2.7926 425.7920 428.5845 387.2859 569.5953 -2.7939 425.6817 428.4756 387.1464 571.2049 -2.7910 425.5667 428.3577 386.9678 572.8095 -2.7895 425.4359 428.2254 386.8402 574.4185 -2.7868 425.3266 428.1134 386.6564 576.0233 -2.7850 425.1746 427.9597 386.4822 577.6476 -2.7829 424.9819 427.7648 386.3971 579.2471 -2.7788 424.8292 427.6080 386.2155 580.8514 -2.7786 424.6829 427.4615 386.1262 582.4505 -2.7724 424.5888 427.3612 386.0099 584.0553 -2.7659 424.4585 427.2244 385.9018 585.6488 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