DTA measure 1Pb Date: 2026428:1555 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1274.16 s Mass = 1157.000 mg data_number = 1585 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1795 0.0154 243.5097 243.4944 250.8461 1.9563 0.0147 243.4891 243.4744 250.8955 2.7740 0.0235 243.4717 243.4482 250.8964 3.5610 0.0150 243.4182 243.4033 250.8262 4.3590 0.0082 243.4658 243.4576 250.8425 5.1770 -0.0044 243.5783 243.5827 250.8140 5.9435 -0.0013 243.6405 243.6419 250.8012 6.7715 -0.0187 243.5203 243.5390 250.8881 7.5380 -0.0221 243.6013 243.6234 250.7870 8.3873 -0.0322 243.6567 243.6889 250.7291 9.1540 -0.0181 243.6869 243.7050 250.7602 9.9820 -0.0153 243.8027 243.8181 250.4518 10.7690 -0.0218 243.8056 243.8274 250.3679 11.5663 -0.0315 243.7522 243.7837 250.2471 12.3640 -0.0250 243.7589 243.7839 250.3188 13.1515 -0.0269 243.7615 243.7883 250.2921 13.9795 -0.0243 243.7897 243.8140 250.2911 14.7460 -0.0054 243.7408 243.7462 250.0893 15.5945 -0.0093 243.6946 243.7038 249.9942 16.3715 -0.0258 243.6038 243.6296 249.9771 17.1900 -0.0347 243.7581 243.7928 250.0028 17.9770 -0.0413 243.7544 243.7956 250.0404 18.7845 -0.0556 243.6731 243.7288 250.0812 19.6023 -0.0586 243.5689 243.6275 250.0992 20.3688 -0.0588 243.6495 243.7083 250.2102 21.2285 -0.0665 243.6359 243.7024 250.0627 21.9643 -0.0679 243.7145 243.7824 250.0993 22.8128 -0.0450 243.9181 243.9631 250.0511 23.5793 -0.0358 243.9230 243.9588 250.0593 24.4073 -0.0528 243.9140 243.9668 250.1299 25.2048 -0.0688 243.9415 244.0103 250.0797 25.9925 -0.0648 244.0410 244.1058 250.0965 26.8308 -0.0876 244.0458 244.1334 250.0606 27.5870 -0.0763 243.9804 244.0567 250.0820 28.4458 -0.0801 244.0918 244.1719 249.9981 29.1815 -0.0715 244.1365 244.2080 249.9973 30.0403 -0.0624 244.1375 244.1998 250.0182 30.8078 -0.0673 244.1454 244.2127 250.0389 31.6255 -0.0567 244.1187 244.1754 250.0850 32.4330 -0.0588 244.2383 244.2970 250.1947 33.2200 -0.0784 244.3279 244.4063 250.1336 34.0480 -0.0931 244.4204 244.5135 250.2542 34.8150 -0.0906 244.4380 244.5286 250.1710 35.6743 -0.0975 244.4827 244.5802 250.2253 36.4408 -0.1043 244.4804 244.5846 250.2016 37.2585 -0.1151 244.3505 244.4655 250.1542 38.0660 -0.1026 244.2706 244.3732 250.1644 38.8538 -0.0929 244.2979 244.3908 250.2962 39.6820 -0.0999 244.2714 244.3714 250.2445 40.4485 -0.1201 244.3700 244.4902 250.2659 41.3073 -0.1118 244.4853 244.5972 250.3123 42.0430 -0.1223 244.4549 244.5772 250.4679 42.9028 -0.1273 244.5751 244.7024 250.5138 43.6693 -0.1269 244.5223 244.6491 250.4193 44.4973 -0.1332 244.4889 244.6221 250.5907 45.2945 -0.1269 244.5115 244.6384 250.6510 46.0815 -0.1318 244.4177 244.5495 250.7097 46.9205 -0.1178 244.3770 244.4948 250.8084 47.6770 -0.1039 244.3980 244.5019 250.8941 48.5358 -0.1031 244.3607 244.4637 251.0036 49.3023 -0.1246 244.3688 244.4934 251.1392 50.1303 -0.1110 244.5279 244.6389 251.1993 50.9283 -0.1131 244.5568 244.6699 251.2932 51.7155 -0.1372 244.5936 244.7308 251.2001 52.5538 -0.1590 244.5486 244.7076 251.1615 53.3100 -0.1602 244.5771 244.7373 251.3091 54.1688 -0.1501 244.5415 244.6915 251.5288 54.9360 -0.1505 244.5322 244.6827 251.7142 55.7643 -0.1612 244.8074 244.9686 251.9520 56.5615 -0.1493 244.9102 245.0595 252.0692 57.3485 -0.1567 245.0342 245.1909 252.2048 58.1868 -0.1578 244.9454 245.1032 252.3601 58.9430 -0.1680 244.8512 245.0192 252.4691 59.8028 -0.1701 245.0133 245.1834 252.5223 60.5693 -0.1594 245.0383 245.1977 252.5874 61.3973 -0.1686 245.0368 245.2054 252.7021 62.1945 -0.1895 245.1183 245.3078 252.7314 62.9815 -0.1928 245.0652 245.2581 252.8251 63.8205 -0.2034 245.0152 245.2186 253.0407 64.5873 -0.1949 245.1107 245.3056 253.1567 65.4460 -0.2008 244.9373 245.1381 253.0951 66.2023 -0.2038 244.8422 245.0460 253.1591 67.0303 -0.2029 245.0062 245.2091 253.3159 67.8178 -0.2030 244.9768 245.1798 253.5420 68.6155 -0.2114 244.9294 245.1408 253.7313 69.4435 -0.2312 244.9915 245.2227 253.8991 70.1998 -0.2375 244.9593 245.1968 254.1263 71.0278 -0.2323 245.0012 245.2335 254.3539 71.7840 -0.2392 245.1589 245.3981 254.5913 72.6335 -0.2332 245.1723 245.4055 254.8970 73.4103 -0.2384 245.0772 245.3156 255.0163 74.2280 -0.2437 245.0265 245.2703 254.9834 75.0253 -0.2570 245.0499 245.3069 255.1527 75.8225 -0.2640 245.0824 245.3465 255.1122 76.6410 -0.2748 245.0256 245.3004 255.1774 77.4078 -0.2674 245.0658 245.3332 255.1766 78.2665 -0.2763 245.2154 245.4918 255.2694 79.0228 -0.2739 245.3830 245.6569 255.4480 79.8513 -0.2602 245.4580 245.7182 255.4603 80.6490 -0.2596 245.6143 245.8739 255.4597 81.4360 -0.2519 245.7642 246.0161 255.8528 82.2640 -0.2482 245.7755 246.0237 255.9450 83.0305 -0.2528 245.8067 246.0596 255.9586 83.8585 -0.2628 245.8181 246.0809 256.0415 84.6260 -0.2769 245.7193 245.9962 256.3205 85.4745 -0.2943 245.6103 245.9046 256.5920 86.2410 -0.2936 245.6905 245.9841 256.8151 87.0690 -0.2909 245.6088 245.8997 257.0159 87.8560 -0.2805 245.6049 245.8853 257.0996 88.6640 -0.2827 245.6124 245.8951 257.2765 89.4823 -0.2854 245.6155 245.9009 257.6166 90.2488 -0.3006 245.6704 245.9710 257.7188 91.1075 -0.2958 245.7803 246.0762 257.7672 91.8740 -0.3066 245.8579 246.1644 257.7357 92.7020 -0.3132 245.7760 246.0891 257.8313 93.4890 -0.3359 245.8257 246.1616 257.9958 94.2970 -0.3358 245.7873 246.1231 258.0215 95.0845 -0.3409 245.8437 246.1846 258.2661 95.8818 -0.3613 245.9143 246.2756 258.4008 96.7098 -0.3520 245.8398 246.1917 258.3966 97.4763 -0.3675 245.7437 246.1112 258.4018 98.3350 -0.3824 245.9277 246.3102 258.5164 99.0918 -0.3952 246.0723 246.4675 258.6220 99.9305 -0.4078 246.1148 246.5226 258.9164 100.7175 -0.4141 246.1632 246.5772 258.9995 101.5148 -0.4273 246.0887 246.5159 259.0391 102.3120 -0.4250 246.3235 246.7485 259.0607 103.1093 -0.4330 246.4906 246.9236 259.0823 103.9380 -0.4518 246.6173 247.0690 259.1206 104.6945 -0.4500 246.6390 247.0890 259.0583 105.5635 -0.4498 246.7620 247.2117 259.1777 106.3198 -0.4555 246.8169 247.2724 259.3593 107.1478 -0.4394 246.7124 247.1518 259.5477 107.9455 -0.4504 246.7218 247.1723 259.6633 108.7433 -0.4547 246.7972 247.2518 259.7425 109.5713 -0.4620 246.6680 247.1300 259.8747 110.3275 -0.4578 246.6384 247.0963 259.8874 111.1965 -0.4749 246.7601 247.2350 260.0110 111.9528 -0.4919 246.7871 247.2790 260.1539 112.7808 -0.5027 246.8714 247.3742 260.4166 113.5790 -0.5163 246.9681 247.4844 260.5241 114.3763 -0.5156 246.9942 247.5098 260.6591 115.2043 -0.5319 247.1198 247.6516 260.6738 115.9605 -0.5241 247.1513 247.6754 260.8268 116.8305 -0.5380 247.2280 247.7660 260.7233 117.5560 -0.5497 247.1740 247.7236 260.9270 118.4148 -0.5599 247.3494 247.9094 261.1267 119.1813 -0.5602 247.4188 247.9790 261.2651 120.0093 -0.5613 247.4275 247.9888 261.3437 120.8070 -0.5581 247.3498 247.9080 261.3260 121.5945 -0.5677 247.3684 247.9361 261.3222 122.4328 -0.5775 247.3047 247.8822 261.6111 123.1890 -0.5743 247.4005 247.9748 261.7559 124.0478 -0.5817 247.4447 248.0264 261.8880 124.8148 -0.5739 247.4089 247.9828 262.0734 125.6433 -0.5783 247.6238 248.2021 262.2987 126.4405 -0.5915 247.7520 248.3435 262.3658 127.2275 -0.5943 248.0269 248.6211 262.4153 128.0658 -0.5945 247.9867 248.5811 262.4412 128.8225 -0.5902 247.9191 248.5093 262.3758 129.6818 -0.5878 247.9394 248.5272 262.4839 130.4483 -0.5887 248.1138 248.7025 262.5481 131.2763 -0.5869 248.1802 248.7672 262.6701 132.0325 -0.5851 248.3592 248.9443 262.8343 132.8608 -0.5871 248.5057 249.0928 262.9998 133.6588 -0.5828 248.5107 249.0935 263.1365 134.4458 -0.5740 248.4967 249.0707 263.0532 135.2738 -0.5823 248.4688 249.0512 262.9387 136.0300 -0.5988 248.4382 249.0370 263.0658 136.8785 -0.6137 248.4586 249.0723 263.1439 137.6563 -0.6160 248.4148 249.0309 263.1854 138.4740 -0.6329 248.4273 249.0603 263.4091 139.2610 -0.6490 248.4486 249.0976 263.4453 140.0685 -0.6280 248.2861 248.9141 263.4872 140.8865 -0.6247 248.4086 249.0334 263.6752 141.6538 -0.6184 248.4969 249.1152 263.7371 142.4818 -0.6023 248.7303 249.3326 263.8421 143.2380 -0.6270 248.8322 249.4592 264.1218 144.0968 -0.6369 248.7866 249.4236 264.3315 144.8635 -0.6416 248.7992 249.4408 264.4010 145.6923 -0.6429 248.7791 249.4220 264.5052 146.4895 -0.6526 248.8187 249.4713 264.5498 147.2765 -0.6641 248.9144 249.5785 264.5143 148.1045 -0.6768 248.8936 249.5705 264.4663 148.8710 -0.6868 249.0728 249.7596 264.4523 149.7205 -0.6893 249.1698 249.8591 264.5044 150.4665 -0.6710 249.1595 249.8305 264.5612 151.3150 -0.6490 249.1890 249.8381 264.8002 152.0815 -0.6649 249.1196 249.7845 265.0174 152.9095 -0.6812 249.2199 249.9011 265.0655 153.7073 -0.6722 249.3353 250.0075 265.0947 154.4948 -0.6818 249.4000 250.0818 265.2827 155.3228 -0.6768 249.3955 250.0723 265.4420 156.0893 -0.6793 249.5047 250.1840 265.5765 156.9480 -0.6816 249.6337 250.3153 265.7787 157.7050 -0.6938 249.6324 250.3263 265.8074 158.5435 -0.7155 249.6604 250.3759 265.9198 159.3305 -0.7094 249.7068 250.4161 265.9094 160.1278 -0.7257 249.9047 250.6304 266.0627 160.9558 -0.7147 249.9435 250.6583 266.1158 161.7230 -0.6970 249.8529 250.5499 266.1838 162.5820 -0.7055 250.0022 250.7077 266.0292 163.3383 -0.7217 250.0037 250.7255 266.0699 164.1765 -0.7294 249.9953 250.7247 266.1491 164.9635 -0.7318 250.1089 250.8407 266.3524 165.7608 -0.7414 250.0517 250.7931 266.5852 166.5898 -0.7461 250.0043 250.7504 266.7299 167.3563 -0.7600 249.9899 250.7499 266.8858 168.2150 -0.7569 250.1530 250.9099 267.0515 168.9713 -0.7695 250.1471 250.9166 267.1094 169.8095 -0.7851 250.1179 250.9030 267.2395 170.6075 -0.7851 250.1387 250.9238 267.3130 171.3948 -0.7903 250.3007 251.0910 267.2835 172.2228 -0.7785 250.3742 251.1527 267.3912 172.9893 -0.7786 250.5952 251.3738 267.6258 173.8483 -0.7795 250.8238 251.6033 267.8057 174.6053 -0.7802 250.9992 251.7794 267.6593 175.4435 -0.7873 251.0796 251.8669 267.6222 176.2305 -0.7668 251.1319 251.8987 267.6935 177.0278 -0.7828 251.1180 251.9008 267.8429 177.8568 -0.7983 251.0958 251.8941 267.8581 178.6233 -0.8123 251.1402 251.9525 268.0088 179.4820 -0.8390 251.2539 252.0929 268.1061 180.2383 -0.8416 251.2270 252.0687 268.1705 181.0770 -0.8410 251.2068 252.0477 268.4243 181.8645 -0.8445 251.1487 251.9932 268.4950 182.6618 -0.8307 251.2342 252.0649 268.6529 183.4898 -0.8266 251.3465 252.1732 268.7572 184.2563 -0.8235 251.3511 252.1746 268.9481 185.1160 -0.8371 251.4024 252.2394 269.2580 185.8723 -0.8314 251.5659 252.3973 269.3421 186.7105 -0.8324 251.5878 252.4201 269.4259 187.4975 -0.8326 251.5467 252.3793 269.3023 188.2950 -0.8447 251.6376 252.4822 269.1966 189.1238 -0.8448 251.6687 252.5135 269.2068 189.8903 -0.8639 251.7593 252.6232 269.2505 190.7490 -0.8513 251.8522 252.7035 269.3155 191.5053 -0.8710 252.0551 252.9261 269.3044 192.3445 -0.8749 252.1519 253.0267 269.4741 193.1315 -0.8699 252.3319 253.2018 269.7121 193.9288 -0.8874 252.4331 253.3205 269.9512 194.7568 -0.8873 252.4499 253.3372 270.0528 195.5130 -0.8787 252.4753 253.3539 269.9954 196.3625 -0.8704 252.3714 253.2417 270.2212 197.1290 -0.8826 252.6190 253.5016 270.2980 197.9570 -0.8831 252.5554 253.4385 270.4905 198.7133 -0.8765 252.6416 253.5181 270.5389 199.5413 -0.8804 252.6826 253.5630 270.7299 200.3293 -0.8818 252.6962 253.5780 270.9484 201.1265 -0.8741 252.6662 253.5403 271.1293 201.9545 -0.8762 252.8207 253.6969 271.1694 202.7108 -0.8964 252.9288 253.8252 271.2868 203.5695 -0.9060 253.0712 253.9772 271.5309 204.3368 -0.9306 253.0455 253.9761 271.7260 205.1548 -0.9569 253.1689 254.1258 271.8876 205.9213 -0.9591 253.4364 254.3955 271.9272 206.7493 -0.9655 253.3603 254.3258 272.0703 207.5465 -0.9652 253.6426 254.6079 272.1861 208.3343 -0.9704 253.7170 254.6874 272.1658 209.1625 -0.9558 253.6776 254.6334 272.3686 209.9290 -0.9645 253.6179 254.5823 272.4271 210.7775 -0.9787 253.7405 254.7192 272.3229 211.5543 -0.9810 253.8525 254.8334 272.4403 212.3720 -0.9755 253.8906 254.8662 272.5585 213.1393 -0.9740 253.9534 254.9274 272.6420 213.9675 -0.9741 253.9591 254.9333 272.6123 214.7648 -0.9695 253.8921 254.8616 272.7478 215.5518 -0.9686 253.8408 254.8094 272.8297 216.3800 -0.9602 253.9432 254.9034 272.9222 217.1575 -0.9697 253.9511 254.9208 272.9754 218.0060 -0.9989 253.8473 254.8462 273.0087 218.7418 -1.0051 253.9212 254.9262 273.0869 219.6005 -1.0064 254.0879 255.0943 273.2490 220.3670 -1.0156 254.2935 255.3091 273.3656 221.1953 -0.9944 254.4078 255.4021 273.4973 221.9830 -0.9946 254.5306 255.5252 273.7331 222.7905 -0.9846 254.7629 255.7476 273.9384 223.6083 -0.9818 254.7332 255.7150 273.9317 224.3748 -0.9787 254.7357 255.7144 273.9704 225.2335 -0.9744 254.7655 255.7399 274.0032 226.0008 -0.9770 254.6720 255.6490 274.2172 226.8290 -0.9722 254.7633 255.7356 274.3794 227.6160 -0.9678 254.9453 255.9131 274.4993 228.4235 -0.9730 255.1413 256.1143 274.4412 229.2105 -0.9823 255.2656 256.2480 274.6887 230.0078 -0.9889 255.3244 256.3133 274.7836 230.8365 -0.9828 255.4621 256.4449 274.7630 231.6033 -0.9942 255.4740 256.4682 274.8738 232.4620 -0.9961 255.5510 256.5471 275.0051 233.2183 -0.9888 255.7469 256.7357 275.1855 234.0565 -0.9790 255.8948 256.8739 275.1407 234.8435 -0.9696 255.7607 256.7303 275.1417 235.6413 -0.9800 255.8529 256.8329 275.3065 236.4698 -0.9949 255.9968 256.9917 275.4118 237.2363 -1.0151 256.0592 257.0743 275.5156 238.0950 -1.0260 256.1685 257.1945 275.5747 238.8513 -1.0286 256.1335 257.1621 275.8125 239.6903 -1.0197 256.1283 257.1479 275.9438 240.4775 -1.0305 256.0433 257.0738 276.0402 241.2748 -1.0315 256.0983 257.1298 276.0954 242.1028 -1.0412 256.1956 257.2367 276.3127 242.8693 -1.0517 256.4001 257.4518 276.4636 243.7288 -1.0486 256.6060 257.6546 276.5324 244.4853 -1.0561 256.6046 257.6608 276.5706 245.3235 -1.0586 256.5363 257.5948 276.6626 246.1105 -1.0524 256.5022 257.5546 276.5857 246.9078 -1.0667 256.4774 257.5440 276.5094 247.7365 -1.0741 256.6737 257.7478 276.5617 248.5033 -1.0785 256.8305 257.9090 276.6322 249.3620 -1.0770 256.9356 258.0127 276.8333 250.0978 -1.0876 256.9198 258.0074 276.9194 250.9565 -1.0992 257.0689 258.1681 277.0774 251.7230 -1.0979 257.1162 258.2141 277.2477 252.5515 -1.1145 257.3053 258.4197 277.3010 253.3390 -1.1296 257.3695 258.4991 277.3371 254.1465 -1.1263 257.2623 258.3885 277.4886 254.9745 -1.1204 257.2868 258.4072 277.5654 255.7410 -1.1066 257.2419 258.3485 277.5949 256.5905 -1.1013 257.3096 258.4109 277.7406 257.3673 -1.0897 257.4616 258.5513 277.9189 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