DTA measure 1Pb Date: 2026428:154 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1010.26 s Mass = 1157.000 mg data_number = 1257 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1590 -2.3782 206.7931 209.1713 247.3884 1.9568 -2.3794 206.9419 209.3213 247.2549 2.7545 -2.3958 207.1412 209.5369 247.2272 3.5518 -2.3963 207.2977 209.6940 247.2117 4.3490 -2.3775 207.4805 209.8579 247.1744 5.1668 -2.3848 207.5998 209.9846 247.0718 5.9435 -2.3886 207.7070 210.0956 247.0588 6.7930 -2.3696 207.7103 210.0799 247.1108 7.5595 -2.3765 207.9249 210.3014 247.0905 8.3875 -2.3626 207.9834 210.3460 247.0690 9.1848 -2.3504 208.0306 210.3810 246.8676 9.9820 -2.3496 208.1830 210.5326 246.7916 10.8005 -2.3522 208.2845 210.6367 246.7944 11.5775 -2.3565 208.4399 210.7963 246.7406 12.4260 -2.3443 208.6861 211.0304 246.6515 13.1925 -2.3371 208.9356 211.2727 246.7281 14.0205 -2.3362 209.0987 211.4350 246.6862 14.8180 -2.3342 209.2459 211.5801 246.5544 15.6160 -2.3432 209.4523 211.7955 246.5020 16.4133 -2.3301 209.5189 211.8490 246.3515 17.2105 -2.3343 209.6959 212.0301 246.4073 18.0385 -2.3208 209.7937 212.1145 246.2895 18.8050 -2.3204 209.9834 212.3038 246.3068 19.6540 -2.2998 210.2051 212.5049 246.3346 20.4313 -2.3084 210.4956 212.8039 246.2063 21.2490 -2.3029 210.6521 212.9550 246.2904 22.0360 -2.2901 210.7008 212.9908 246.3915 22.8333 -2.2900 210.8700 213.1600 246.3102 23.6203 -2.2793 211.0276 213.3069 246.2903 24.4185 -2.2791 211.0717 213.3508 246.3456 25.2465 -2.2611 211.1903 213.4515 246.3554 26.0028 -2.2437 211.3432 213.5869 246.3209 26.8615 -2.2305 211.3702 213.6008 246.3911 27.6178 -2.2398 211.4718 213.7116 246.3260 28.4463 -2.2286 211.6435 213.8721 246.2714 29.2440 -2.2252 211.8063 214.0315 246.4910 30.0310 -2.2053 211.9377 214.1430 246.6826 30.8488 -2.2328 212.1489 214.3817 246.5645 31.6255 -2.2351 212.2584 214.4935 246.5482 32.4743 -2.2310 212.2918 214.5228 246.5279 33.2108 -2.2162 212.5338 214.7499 246.6431 34.0695 -2.2021 212.8401 215.0422 246.7067 34.8360 -2.1881 212.7978 214.9859 246.7720 35.6538 -2.1775 212.8498 215.0273 246.8162 36.4510 -2.1703 213.0563 215.2266 246.9264 37.2490 -2.1648 213.1395 215.3043 247.1075 38.0773 -2.1608 213.3445 215.5053 247.1787 38.8335 -2.1670 213.5325 215.6995 247.1799 39.7025 -2.1429 213.7043 215.8472 247.3666 40.4588 -2.1397 213.7795 215.9192 247.3473 41.2868 -2.1296 213.8352 215.9648 247.4749 42.0850 -2.1453 213.9249 216.0702 247.7533 42.8720 -2.1612 214.0531 216.2143 248.0119 43.7000 -2.1601 214.1086 216.2686 248.2359 44.4665 -2.1412 214.2197 216.3609 248.2987 45.2948 -2.1175 214.3485 216.4660 248.5241 46.0620 -2.1337 214.4156 216.5493 248.7115 46.9105 -2.1243 214.5351 216.6594 248.7767 47.6873 -2.1052 214.7496 216.8548 249.0166 48.5050 -2.1225 214.9710 217.0935 249.3279 49.3023 -2.1127 215.0739 217.1867 249.5979 50.1005 -2.1115 215.2950 217.4064 249.7623 50.9285 -2.1143 215.3553 217.4696 249.9150 51.6950 -2.1123 215.4383 217.5506 250.0354 52.5435 -2.1051 215.6660 217.7711 250.1919 53.3203 -2.0987 215.8333 217.9320 250.2696 54.1380 -2.0735 216.0001 218.0736 250.5498 54.9358 -2.0704 216.0624 218.1328 250.6247 55.7335 -2.0804 216.2947 218.3751 250.8503 56.5615 -2.0700 216.5784 218.6484 250.9858 57.3280 -2.0535 216.7337 218.7871 251.1711 58.1765 -2.0466 217.0023 219.0489 251.4392 58.9533 -2.0321 217.1660 219.1982 251.5677 59.7715 -2.0259 217.2992 219.3251 251.7134 60.5693 -2.0461 217.4992 219.5453 251.9786 61.3665 -2.0592 217.5705 219.6297 252.2522 62.1945 -2.0587 217.6579 219.7166 252.5079 62.9610 -2.0584 217.8373 219.8957 252.6463 63.8095 -2.0815 217.9943 220.0758 252.8725 64.5873 -2.0782 218.2350 220.3132 252.9696 65.4050 -2.0835 218.2655 220.3490 253.1029 66.2023 -2.0844 218.4552 220.5396 253.1927 66.9995 -2.0992 218.5843 220.6836 253.3219 67.8070 -2.0941 218.8923 220.9864 253.3402 68.5940 -2.0691 219.0847 221.1538 253.4404 69.4128 -2.0567 219.1027 221.1594 253.7787 70.2203 -2.0375 219.1091 221.1466 253.9966 71.0380 -2.0301 219.1910 221.2211 254.2307 71.8353 -2.0382 219.2665 221.3047 254.4962 72.6330 -2.0456 219.3333 221.3788 254.7884 73.4615 -2.0273 219.4141 221.4415 254.9740 74.2280 -2.0454 219.5322 221.5775 255.1936 75.0765 -2.0496 219.6651 221.7147 255.2147 75.8533 -2.0471 219.7017 221.7488 255.2438 76.6713 -2.0595 219.8578 221.9173 255.4213 77.4693 -2.0518 220.1680 222.2198 255.5213 78.2665 -2.0668 220.2920 222.3587 255.5089 79.0945 -2.0782 220.4744 222.5526 255.7303 79.8610 -2.0901 220.5466 222.6366 255.9882 80.7100 -2.1033 220.5173 222.6206 256.2773 81.4873 -2.0733 220.6568 222.7300 256.4705 82.3050 -2.0732 220.7154 222.7886 256.7225 83.1023 -2.0724 220.8989 222.9713 256.8361 83.8995 -2.0865 221.0306 223.1172 256.9346 84.7283 -2.0740 221.1344 223.2084 257.1182 85.4848 -2.0683 221.3466 223.4149 257.2695 86.3435 -2.0605 221.6393 223.6998 257.3518 87.0690 -2.0561 221.7374 223.7935 257.6143 87.9175 -2.0455 221.8851 223.9307 257.6933 88.6943 -2.0365 222.0181 224.0546 257.8181 89.5130 -2.0478 222.2622 224.3100 257.9427 90.3000 -2.0566 222.5172 224.5738 257.9473 91.0973 -2.0427 222.7414 224.7841 258.0949 91.9150 -2.0341 222.8841 224.9182 258.3628 92.6815 -2.0437 222.9875 225.0312 258.4206 93.5413 -2.0482 223.0988 225.1471 258.5721 94.2975 -2.0428 223.2293 225.2721 258.7463 95.1255 -2.0360 223.4745 225.5105 258.7589 95.9228 -2.0397 223.6367 225.6764 258.9464 96.7200 -2.0329 223.6162 225.6491 259.0456 97.5383 -2.0320 223.8348 225.8667 259.2142 98.3053 -2.0304 223.9750 226.0054 259.3829 99.1640 -2.0225 224.0123 226.0348 259.5649 99.9203 -2.0344 224.1953 226.2296 259.6252 100.7585 -2.0376 224.2762 226.3138 259.7827 101.5150 -2.0295 224.3899 226.4194 260.1102 102.3438 -2.0205 224.4316 226.4521 260.3988 103.1410 -2.0220 224.5314 226.5533 260.5431 103.9383 -2.0156 224.7396 226.7552 260.6284 104.7663 -2.0165 224.8905 226.9069 260.6593 105.5225 -2.0237 224.9714 226.9951 260.6724 106.3823 -2.0271 225.1581 227.1852 260.8105 107.1488 -2.0194 225.1982 227.2176 261.0470 107.9665 -2.0123 225.4569 227.4692 261.1564 108.7740 -2.0193 225.3266 227.3459 261.2308 109.5610 -2.0323 225.2247 227.2570 261.4253 110.3890 -2.0415 225.3171 227.3586 261.5598 111.1565 -2.0448 225.5508 227.5956 261.7522 111.9845 -2.0366 225.5712 227.6078 261.9394 112.7510 -2.0310 225.7500 227.7810 262.0271 113.5995 -2.0391 225.9879 228.0270 262.2323 114.3765 -2.0304 226.1962 228.2266 262.4581 115.1948 -2.0155 226.3858 228.4013 262.5622 115.9923 -2.0217 226.6042 228.6259 262.6732 116.7895 -2.0373 226.6246 228.6619 262.8743 117.6175 -2.0506 226.8126 228.8631 262.9996 118.3840 -2.0337 227.0143 229.0479 262.9943 119.2325 -2.0413 227.3002 229.3416 262.9114 120.0095 -2.0430 227.5026 229.5456 263.0290 120.8280 -2.0694 227.4865 229.5558 263.2525 121.6253 -2.0880 227.5972 229.6852 263.2685 122.4225 -2.0977 227.9227 230.0204 263.1840 123.2198 -2.0727 228.1776 230.2504 263.1888 124.0170 -2.0622 228.3895 230.4517 263.3311 124.8348 -2.0678 228.4570 230.5249 263.5568 125.6115 -2.0701 228.5933 230.6634 263.7213 126.4713 -2.0776 228.5972 230.6748 263.8880 127.2378 -2.0917 228.7353 230.8270 264.1061 128.0555 -2.0790 228.8226 230.9016 264.2429 128.8630 -2.0820 228.9796 231.0616 264.4444 129.6500 -2.0807 229.0138 231.0946 264.4645 130.4780 -2.0694 229.2624 231.3319 264.5906 131.2453 -2.0521 229.4947 231.5468 264.6885 132.1043 -2.0494 229.7083 231.7577 264.8187 132.8708 -2.0535 229.8413 231.8948 264.9514 133.6885 -2.0339 230.0173 232.0512 265.0264 134.4960 -2.0173 230.0718 232.0891 265.1103 135.2830 -2.0243 230.1528 232.1771 265.1613 136.0808 -2.0307 230.3404 232.3711 265.2471 136.8785 -2.0166 230.4521 232.4687 265.4697 137.7373 -2.0189 230.6427 232.6616 265.6365 138.4730 -2.0136 230.8141 232.8277 265.8110 139.3215 -2.0248 230.8778 232.9027 265.8317 140.0985 -2.0331 230.9686 233.0017 265.9954 140.9170 -2.0213 231.0392 233.0605 266.2372 141.7143 -2.0330 231.1063 233.1393 266.3541 142.5115 -2.0306 231.1682 233.1989 266.4266 143.3395 -2.0220 231.2378 233.2598 266.4448 144.1060 -2.0186 231.3883 233.4069 266.6637 144.9553 -2.0238 231.6265 233.6503 266.8233 145.7323 -2.0270 231.8540 233.8810 266.8590 146.5500 -2.0377 231.9761 234.0138 267.0187 147.3473 -2.0394 232.1558 234.1952 267.1171 148.1445 -2.0297 232.2905 234.3202 267.1987 148.9725 -2.0479 232.5609 234.6088 267.1406 149.7290 -2.0493 232.7378 234.7870 267.3368 150.5885 -2.0352 232.7732 234.8084 267.3949 151.3448 -2.0172 232.8158 234.8330 267.4872 152.1625 -2.0320 232.9277 234.9596 267.6148 152.9598 -2.0409 233.1015 235.1424 267.8212 153.7570 -2.0511 233.2824 235.3335 267.8612 154.5755 -2.0382 233.4612 235.4994 267.8810 155.3423 -2.0281 233.5379 235.5659 267.8854 156.1908 -2.0080 233.7473 235.7553 268.1022 156.9265 -2.0123 233.6446 235.6569 267.9751 157.7853 -2.0293 233.9978 236.0271 268.2760 158.5723 -2.0372 234.1579 236.1952 268.5477 159.3705 -2.0349 234.2972 236.3321 268.7059 160.1678 -2.0376 234.4167 236.4543 268.8589 160.9650 -2.0377 234.4685 236.5061 268.9015 161.7828 -2.0290 234.5374 236.5665 269.0659 162.5493 -2.0261 234.7412 236.7673 269.1433 163.4080 -2.0214 234.8743 236.8957 269.2698 164.1645 -2.0196 234.9637 236.9834 269.2857 164.9933 -2.0307 235.0890 237.1197 269.3431 165.7905 -2.0167 235.1923 237.2090 269.3237 166.5775 -2.0216 235.2823 237.3038 269.2932 167.4158 -2.0317 235.3878 237.4195 269.3036 168.1720 -2.0217 235.6119 237.6336 269.5008 169.0308 -2.0144 235.6777 237.6921 269.9148 169.7983 -2.0141 235.8452 237.8593 270.1528 170.6263 -2.0167 236.1329 238.1496 270.4043 171.4235 -2.0266 236.2858 238.3124 270.7063 172.2105 -2.0233 236.3079 238.3313 270.8313 173.0385 -2.0313 236.4252 238.4565 270.8823 173.8050 -2.0246 236.6038 238.6284 270.9557 174.6545 -2.0392 236.8265 238.8658 271.0423 175.4313 -2.0324 237.0014 239.0337 271.1597 176.2490 -2.0480 237.1115 239.1595 271.3456 177.0463 -2.0440 237.3274 239.3715 271.6451 177.8435 -2.0260 237.5694 239.5954 271.6854 178.6723 -1.9890 237.6749 239.6640 271.9442 179.4390 -1.9765 237.6821 239.6586 272.1380 180.2875 -1.9849 237.7297 239.7146 272.1631 181.0643 -1.9772 237.8036 239.7808 272.1654 181.8820 -1.9627 238.0280 239.9907 272.2889 182.6793 -1.9778 238.1514 240.1292 272.4154 183.4768 -1.9750 238.1990 240.1740 272.3726 184.3050 -1.9723 238.4106 240.3830 272.4745 185.0720 -1.9962 238.4988 240.4950 272.7507 185.9205 -2.0089 238.6917 240.7007 272.8367 186.6973 -2.0189 238.9929 241.0118 273.0474 187.5150 -2.0302 239.0319 241.0622 273.2250 188.3123 -2.0366 239.0481 241.0847 273.3652 189.1100 -2.0372 239.0946 241.1318 273.4432 189.9385 -2.0499 239.2202 241.2701 273.5520 190.7050 -2.0439 239.2255 241.2695 273.6187 191.5535 -2.0299 239.2995 241.3294 273.8606 192.3303 -2.0393 239.5954 241.6347 274.0369 193.1480 -2.0550 239.6209 241.6759 274.2054 193.9455 -2.0437 239.7959 241.8396 274.3183 194.7435 -2.0334 239.8912 241.9246 274.3638 195.5715 -2.0267 240.2975 242.3241 274.6451 196.3380 -2.0260 240.6513 242.6773 274.8302 197.1865 -2.0246 240.8070 242.8316 275.0944 197.9633 -2.0409 241.0137 243.0545 275.2185 198.7810 -2.0505 241.1220 243.1726 275.3457 199.5788 -2.0455 241.2129 243.2584 275.6168 200.3765 -2.0319 241.4204 243.4523 275.7514 201.2045 -2.0390 241.5186 243.5576 275.7458 201.9710 -2.0432 241.6509 243.6941 275.8875 202.8195 -2.0404 241.7757 243.8161 275.9830 203.5963 -2.0453 241.7926 243.8378 276.1031 204.4148 -2.0303 241.8577 243.8880 276.3101 205.2225 -2.0213 242.0022 244.0235 276.6199 206.0095 -2.0151 242.1979 244.2130 276.8112 206.8478 -2.0252 242.2328 244.2580 276.8861 207.6040 -2.0104 242.5216 244.5320 276.9168 208.4630 -2.0104 242.7077 244.7181 277.0792 209.1995 -2.0081 242.7679 244.7760 277.2160 210.0583 -2.0280 242.8839 244.9119 277.4987 210.8248 -2.0226 242.9031 244.9257 277.4993 211.6425 -2.0091 242.8727 244.8818 277.5536 212.4398 -2.0175 243.0925 245.1100 277.5870 213.2370 -2.0373 243.2889 245.3262 277.7241 214.0555 -2.0053 243.4220 245.4273 277.8029 214.8223 -1.9882 243.6240 245.6121 277.9702 215.6708 -1.9885 243.6120 245.6005 278.0743 216.4065 -1.9967 243.5896 245.5863 278.3890 217.2653 -1.9960 243.7441 245.7401 278.5726 218.0215 -1.9983 243.9380 245.9363 278.6079 218.8505 -2.0061 244.1505 246.1566 278.7598 219.6478 -2.0116 244.1986 246.2103 278.8298 220.4450 -2.0270 244.3841 246.4111 278.9765 221.2320 -2.0391 244.5211 246.5602 279.0674 222.0293 -2.0266 244.5992 246.6258 279.1523 222.8785 -2.0070 244.7163 246.7233 279.2865 223.6453 -2.0012 244.7625 246.7636 279.2886 224.4733 -1.9902 244.7594 246.7496 279.3764 225.2295 -2.0037 244.9382 246.9418 279.5072 226.0575 -2.0093 245.2551 247.2644 279.6511 226.8553 -2.0167 245.4120 247.4287 279.6952 227.6530 -2.0262 245.6200 247.6463 279.8700 228.4708 -2.0224 245.7975 247.8199 279.9903 229.2475 -2.0247 245.9229 247.9476 280.0019 230.0960 -2.0087 246.1033 248.1120 280.2106 230.8628 -2.0126 246.2504 248.2630 280.3507 231.6915 -2.0266 246.4121 248.4387 280.3919 232.4580 -2.0335 246.5982 248.6317 280.4770 233.2860 -2.0286 246.8123 248.8410 280.5383 234.0730 -2.0277 247.0938 249.1214 280.7794 234.8703 -2.0139 247.2102 249.2241 281.1199 235.6990 -2.0305 247.3941 249.4246 281.3142 236.4555 -2.0405 247.6138 249.6543 281.3562 237.3245 -2.0332 247.7895 249.8227 281.4776 238.0808 -2.0453 247.8802 249.9256 281.6920 238.9088 -2.0450 248.0861 250.1312 281.8052 239.7065 -2.0451 248.2789 250.3240 281.8838 240.5043 -2.0681 248.2837 250.3518 281.9369 241.3015 -2.0747 248.3879 250.4626 282.1781 242.0885 -2.0806 248.5917 250.6723 282.1526 242.9268 -2.0672 248.5631 250.6303 282.2342 243.6830 -2.0618 248.6558 250.7176 282.3814 244.5320 -2.0630 248.7280 250.7909 282.5923 245.3093 -2.0747 248.8883 250.9630 282.7473 246.1270 -2.0785 248.9322 251.0106 282.8612 246.9243 -2.0717 249.0681 251.1398 282.9364 247.7215 -2.0676 249.2932 251.3609 283.2120 248.5495 -2.0732 249.4452 251.5184 283.4584 249.3160 -2.0658 249.5134 251.5792 283.6632 250.1650 -2.0761 249.6567 251.7328 283.7314 250.9423 -2.0829 249.6406 251.7235 283.7632 251.7600 -2.0791 249.7497 251.8288 283.8020 252.5573 -2.0747 250.0015 252.0762 283.8670 253.3545 -2.0641 250.2438 252.3079 283.9127 254.1828 -2.0539 250.3406 252.3945 284.1373 254.9500 -2.0777 250.4523 252.5300 284.2395 255.7985 -2.0970 250.7015 252.7986 284.2960 256.5753 -2.0908 250.7841 252.8749 284.3948 257.3930 -2.0713 251.1305 253.2018 284.6341 258.1903 -2.0734 251.2762 253.3496 284.7028 258.9875 -2.0767 251.3658 253.4425 284.8226 259.7853 -2.0598 251.3495 253.4093 284.8380 260.5830 -2.0586 251.4814 253.5400 285.0556 261.4008 -2.0514 251.7132 253.7645 285.2447 262.1775 -2.0575 251.9192 253.9768 285.3606 263.0260 -2.0651 251.8627 253.9278 285.4647 263.7925 -2.0599 252.0254 254.0853 285.5187 264.6215 -2.0555 252.2198 254.2753 285.7832 265.4188 -2.0575 252.3703 254.4279 286.0303 266.2160 -2.0563 252.4806 254.5369 286.1824 267.0645 -2.0767 252.5709 254.6476 286.2151 267.8105 -2.0776 252.5662 254.6439 286.3321 268.6590 -2.0788 252.6701 254.7489 286.3754 269.4563 -2.0636 252.7222 254.7858 286.4862 270.2545 -2.0579 252.9339 254.9918 286.6171 271.0825 -2.0584 253.0677 255.1260 286.7081 271.8490 -2.0581 253.1581 255.2162 286.9853 272.6975 -2.0469 253.3232 255.3701 287.2269 273.4743 -2.0445 253.4238 255.4683 287.3123 274.2920 -2.0537 253.6105 255.6641 287.2788 275.0898 -2.0249 253.6124 255.6373 287.4575 275.8875 -2.0243 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