DTA measure 3olom_melegites_1 0.9588 Date: 2026318:936 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1648.35 s Mass = 958.800 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.4096 -5.5727 465.1232 470.6959 432.6765 4.0030 -5.5855 465.0360 470.6216 432.9040 5.6061 -5.6022 464.9771 470.5793 433.1650 7.2045 -5.6097 464.9226 470.5324 433.3956 8.8081 -5.6172 464.8408 470.4581 433.5424 10.4164 -5.6215 464.7835 470.4050 433.6247 12.0301 -5.6273 464.7531 470.3804 433.5885 13.6335 -5.6349 464.7160 470.3509 433.4746 15.2420 -5.6373 464.6637 470.3010 433.2817 16.8455 -5.6431 464.6707 470.3138 432.9990 18.4540 -5.6482 464.6268 470.2750 432.6213 20.0574 -5.6526 464.5715 470.2241 432.2179 21.6609 -5.6540 464.5224 470.1764 431.7443 23.2848 -5.6603 464.4885 470.1488 431.2702 24.8830 -5.6622 464.4303 470.0925 430.7577 26.4916 -5.6631 464.3775 470.0406 430.3046 28.1055 -5.6631 464.3210 469.9841 429.8327 29.7086 -5.6635 464.2862 469.9497 429.3738 31.3224 -5.6662 464.2341 469.9002 428.9314 32.9258 -5.6619 464.1309 469.7927 428.5784 34.5394 -5.6547 464.0370 469.6917 428.2563 36.1429 -5.6513 463.9696 469.6209 428.0090 37.7873 -5.6524 463.8955 469.5479 427.8089 39.3958 -5.6510 463.8220 469.4730 427.6740 40.9890 -5.6497 463.7664 469.4161 427.6039 42.5921 -5.6437 463.6998 469.3435 427.5517 44.1803 -5.6433 463.6013 469.2446 427.5447 45.7989 -5.6462 463.5185 469.1648 427.5496 47.4023 -5.6489 463.4299 469.0789 427.5959 49.0109 -5.6536 463.3218 468.9754 427.6183 50.6140 -5.6538 463.2265 468.8803 427.5636 52.2225 -5.6565 463.1698 468.8262 427.4592 53.8105 -5.6534 463.1033 468.7567 427.3647 55.4241 -5.6573 463.0149 468.6723 427.2364 57.0430 -5.6555 462.9032 468.5586 427.0447 58.6461 -5.6494 462.8205 468.4699 426.8268 60.2394 -5.6521 462.7380 468.3902 426.5704 61.8581 -5.6564 462.6185 468.2749 426.2391 63.4716 -5.6575 462.5624 468.2199 425.8894 65.0751 -5.6497 462.4946 468.1443 425.5670 66.6888 -5.6453 462.3935 468.0388 425.2128 68.2923 -5.6401 462.2758 467.9159 424.8214 69.8956 -5.6368 462.1557 467.7926 424.4958 71.4990 -5.6333 462.0571 467.6904 424.1768 73.0973 -5.6339 461.9705 467.6044 423.8558 74.7059 -5.6335 461.8891 467.5227 423.5290 76.3041 -5.6265 461.7805 467.4070 423.3007 77.9126 -5.6214 461.6698 467.2911 423.0811 79.5213 -5.6146 461.5614 467.1760 422.8212 81.1244 -5.6116 461.4103 467.0219 422.6492 82.7381 -5.6071 461.2966 466.9037 422.4844 84.3416 -5.6055 461.1702 466.7758 422.3551 85.9499 -5.5991 461.0779 466.6770 422.2643 87.5636 -5.5988 460.9509 466.5497 422.1762 89.1720 -5.6030 460.8162 466.4191 422.1151 90.7908 -5.6034 460.6985 466.3019 422.0457 92.4045 -5.6052 460.5681 466.1733 421.9409 94.0076 -5.6006 460.4588 466.0594 421.8223 95.6163 -5.5970 460.3191 465.9161 421.6550 97.2195 -5.5971 460.1815 465.7786 421.4685 98.8331 -5.5971 460.0319 465.6289 421.2982 100.4366 -5.5949 459.8903 465.4852 421.0571 102.0501 -5.5882 459.7440 465.3322 420.8116 103.6538 -5.5829 459.6073 465.1902 420.5351 105.2573 -5.5842 459.4725 465.0567 420.2540 106.8501 -5.5835 459.3894 464.9729 419.9830 108.4535 -5.5810 459.2453 464.8263 419.7049 110.0520 -5.5734 459.0918 464.6652 419.3929 111.6603 -5.5698 458.9539 464.5237 419.0904 113.2638 -5.5638 458.8152 464.3790 418.8307 114.8876 -5.5645 458.6811 464.2456 418.5740 116.4910 -5.5605 458.5478 464.1083 418.3025 118.0998 -5.5553 458.3878 463.9432 418.0126 119.7033 -5.5510 458.2446 463.7957 417.7966 121.3168 -5.5424 458.1091 463.6514 417.6049 122.9203 -5.5397 457.9520 463.4917 417.4529 124.5238 -5.5356 457.8399 463.3755 417.2747 126.1475 -5.5265 457.6954 463.2219 417.1068 127.7561 -5.5237 457.5271 463.0508 416.9373 129.3648 -5.5230 457.3763 462.8994 416.8004 130.9731 -5.5214 457.1685 462.6899 416.6957 132.5664 -5.5230 457.0189 462.5420 416.5304 134.1699 -5.5258 456.8649 462.3907 416.3305 135.7731 -5.5269 456.7112 462.2381 416.1201 137.3766 -5.5199 456.5575 462.0775 415.9714 138.9801 -5.5139 456.3856 461.8996 415.8000 140.5680 -5.5129 456.2288 461.7417 415.6154 142.1920 -5.5068 456.0627 461.5696 415.4236 143.7955 -5.5010 455.9386 461.4395 415.1814 145.3986 -5.4925 455.8107 461.3032 414.9362 146.9919 -5.4867 455.6493 461.1359 414.7100 148.6106 -5.4872 455.4721 460.9593 414.4749 150.2089 -5.4844 455.3297 460.8140 414.2376 151.8175 -5.4764 455.1478 460.6242 413.9619 153.4209 -5.4729 454.9944 460.4672 413.7210 155.0344 -5.4710 454.8637 460.3347 413.4530 156.6533 -5.4684 454.6702 460.1386 413.2146 158.2668 -5.4633 454.4859 459.9492 412.9694 159.8703 -5.4557 454.2806 459.7363 412.7381 161.4790 -5.4486 454.1300 459.5786 412.5157 163.0824 -5.4434 453.9971 459.4404 412.2949 164.6806 -5.4409 453.8107 459.2517 412.0897 166.2841 -5.4359 453.6515 459.0874 411.8896 167.8823 -5.4307 453.5328 458.9635 411.6995 169.5063 -5.4261 453.3926 458.8187 411.4955 171.1046 -5.4216 453.2066 458.6282 411.2822 172.7080 -5.4194 453.0050 458.4244 411.1227 174.3165 -5.4163 452.8309 458.2472 410.9240 175.9200 -5.4113 452.6479 458.0592 410.7406 177.5131 -5.4107 452.4596 457.8703 410.5558 179.1165 -5.4070 452.2597 457.6667 410.3815 180.7303 -5.4028 452.0927 457.4955 410.1654 182.3490 -5.3949 451.8940 457.2888 409.9885 183.9575 -5.3922 451.7483 457.1405 409.8246 185.5610 -5.3898 451.5558 456.9456 409.6481 187.1695 -5.3823 451.3593 456.7416 409.4654 188.7780 -5.3752 451.1962 456.5714 409.2548 190.3815 -5.3746 451.0567 456.4313 409.0455 191.9951 -5.3709 450.8627 456.2336 408.7960 193.6139 -5.3657 450.6761 456.0419 408.5935 195.2225 -5.3655 450.5046 455.8701 408.4068 196.8310 -5.3632 450.3040 455.6672 408.1900 198.4344 -5.3580 450.1417 455.4997 407.9341 200.0379 -5.3526 449.9659 455.3185 407.6673 201.6413 -5.3441 449.7599 455.1040 407.4001 203.2446 -5.3380 449.5356 454.8736 407.1384 204.8328 -5.3302 449.3626 454.6929 406.9242 206.4568 -5.3246 449.2055 454.5302 406.7246 208.0600 -5.3188 449.0279 454.3467 406.5338 209.6686 -5.3145 448.8582 454.1727 406.3160 211.2720 -5.3069 448.6941 454.0010 406.0970 212.8804 -5.3036 448.4721 453.7757 405.8882 214.4890 -5.3004 448.3194 453.6198 405.7212 216.0923 -5.3006 448.1576 453.4582 405.5114 217.7213 -5.2961 447.9503 453.2464 405.2865 219.3245 -5.2879 447.7514 453.0393 405.0726 220.9330 -5.2861 447.5865 452.8726 404.8661 222.5211 -5.2800 447.3992 452.6792 404.6879 224.1345 -5.2747 447.2070 452.4817 404.5176 225.7380 -5.2668 447.0491 452.3159 404.3280 227.3516 -5.2609 446.8392 452.1001 404.0947 228.9549 -5.2551 446.6556 451.9107 403.8714 230.5789 -5.2573 446.4316 451.6889 403.6571 232.1618 -5.2547 446.2910 451.5457 403.4651 233.7651 -5.2475 446.1111 451.3587 403.2335 235.3685 -5.2377 445.8871 451.1248 403.0188 236.9718 -5.2308 445.6956 450.9263 402.8424 238.5804 -5.2231 445.5262 450.7493 402.5955 240.1836 -5.2169 445.3081 450.5251 402.3695 241.7716 -5.2139 445.0981 450.3120 402.1937 243.3803 -5.2048 444.8936 450.0984 401.9243 244.9990 -5.1984 444.7224 449.9209 401.7125 246.6075 -5.1945 444.5436 449.7382 401.5187 248.2111 -5.1930 444.3339 449.5268 401.2941 249.8248 -5.1878 444.1527 449.3405 401.0925 251.4280 -5.1829 443.9162 449.0991 400.8775 253.0366 -5.1730 443.7097 448.8827 400.6744 254.6450 -5.1680 443.5215 448.6895 400.4714 256.2381 -5.1589 443.3538 448.5127 400.2925 257.8570 -5.1560 443.1623 448.3184 400.1051 259.4705 -5.1490 442.9623 448.1113 399.9121 261.0690 -5.1451 442.7867 447.9318 399.6956 262.6825 -5.1416 442.5820 447.7236 399.4687 264.2859 -5.1411 442.4107 447.5518 399.2476 265.8894 -5.1379 442.1678 447.3057 399.0335 267.4875 -5.1345 441.9413 447.0757 398.7952 269.0909 -5.1308 441.7270 446.8578 398.5690 270.6993 -5.1251 441.5279 446.6530 398.3645 272.3026 -5.1216 441.3562 446.4779 398.1428 273.9114 -5.1058 441.1552 446.2611 397.9220 275.5145 -5.0956 440.9673 446.0629 397.6884 277.1179 -5.0881 440.7637 445.8518 397.4760 278.7265 -5.0840 440.5496 445.6335 397.2540 280.3349 -5.0837 440.3284 445.4121 397.0335 281.9435 -5.0816 440.1194 445.2010 396.8247 283.5624 -5.0756 439.9181 444.9936 396.6464 285.1708 -5.0692 439.7250 444.7941 396.4458 286.7793 -5.0631 439.5166 444.5798 396.2134 288.3878 -5.0534 439.3059 444.3593 395.9994 289.9911 -5.0499 439.1051 444.1550 395.8123 291.5996 -5.0469 438.9315 443.9784 395.6041 293.2030 -5.0458 438.7344 443.7802 395.3624 294.8269 -5.0404 438.5265 443.5668 395.1906 296.4304 -5.0320 438.3383 443.3704 394.9868 298.0336 -5.0192 438.1633 443.1825 394.7381 299.6371 -5.0071 437.9497 442.9568 394.5550 301.2406 -5.0017 437.7185 442.7202 394.3503 302.8439 -4.9923 437.5045 442.4968 394.1541 304.4524 -4.9879 437.3407 442.3286 393.9740 306.0556 -4.9842 437.1763 442.1605 393.7746 307.6795 -4.9831 436.9373 441.9204 393.5362 309.2828 -4.9758 436.7521 441.7279 393.3452 310.8759 -4.9721 436.5540 441.5260 393.1548 312.4845 -4.9594 436.3338 441.2932 392.9573 314.0930 -4.9509 436.1241 441.0749 392.7557 315.6964 -4.9458 435.9165 440.8622 392.5529 317.3050 -4.9402 435.6959 440.6361 392.3295 318.9289 -4.9381 435.4985 440.4366 392.0751 320.5321 -4.9285 435.3054 440.2338 391.8170 322.1458 -4.9194 435.0759 439.9953 391.5848 323.7490 -4.9188 434.8807 439.7995 391.3471 325.3576 -4.9156 434.6609 439.5765 391.1097 326.9610 -4.9109 434.4842 439.3951 390.8622 328.5644 -4.9038 434.2410 439.1448 390.6375 330.1525 -4.9018 434.0445 438.9463 390.4192 331.7661 -4.8973 433.8398 438.7371 390.1972 333.3746 -4.8905 433.6499 438.5404 389.9889 334.9629 -4.8836 433.4360 438.3197 389.8070 336.5715 -4.8788 433.2310 438.1098 389.6542 338.1746 -4.8731 433.0377 437.9108 389.4909 339.7781 -4.8625 432.7854 437.6479 389.3143 341.3868 -4.8519 432.5854 437.4372 389.1263 342.9901 -4.8480 432.3964 437.2444 388.9248 344.6140 -4.8449 432.1773 437.0223 388.6905 346.2073 -4.8400 431.9716 436.8116 388.4839 347.8156 -4.8348 431.7767 436.6115 388.3082 349.4243 -4.8270 431.6028 436.4297 388.1036 351.0325 -4.8183 431.3879 436.2063 387.8839 352.6360 -4.8041 431.1308 435.9349 387.6383 354.2498 -4.7979 430.9260 435.7239 387.4642 355.8376 -4.7985 430.7281 435.5266 387.2788 357.4463 -4.7981 430.5318 435.3298 387.0441 359.0700 -4.7906 430.3517 435.1423 386.8486 360.6683 -4.7850 430.1489 434.9339 386.6321 362.2770 -4.7764 429.8854 434.6619 386.4214 363.8651 -4.7718 429.6785 434.4503 386.2078 365.4734 -4.7635 429.4601 434.2236 385.9985 367.0769 -4.7526 429.2698 434.0224 385.7325 368.6853 -4.7488 429.0539 433.8026 385.5324 370.2886 -4.7473 428.8613 433.6086 385.3081 371.9074 -4.7440 428.6687 433.4127 385.0818 373.5158 -4.7338 428.4844 433.2182 384.8395 375.1089 -4.7291 428.2909 433.0200 384.6203 376.7173 -4.7266 428.0378 432.7643 384.4207 378.3258 -4.7193 427.8212 432.5405 384.2143 379.9343 -4.7132 427.6268 432.3399 383.9945 381.5376 -4.7033 427.3671 432.0704 383.7838 383.1514 -4.6934 427.1817 431.8751 383.5431 384.7701 -4.6840 426.9973 431.6813 383.3097 386.3836 -4.6783 426.7530 431.4313 383.1194 387.9871 -4.6753 426.5779 431.2532 382.9462 389.5955 -4.6754 426.3703 431.0457 382.7562 391.1991 -4.6681 426.1305 430.7985 382.5569 392.8026 -4.6632 425.9058 430.5689 382.3659 394.4009 -4.6555 425.7153 430.3708 382.1578 396.0196 -4.6487 425.5176 430.1663 381.9574 397.6180 -4.6365 425.3279 429.9644 381.7620 399.2263 -4.6293 425.1040 429.7332 381.5642 400.8298 -4.6221 424.8851 429.5072 381.3529 402.4230 -4.6155 424.6954 429.3109 381.1415 404.0263 -4.6080 424.4651 429.0731 380.8971 405.6349 -4.6003 424.2387 428.8390 380.6591 407.2743 -4.5924 424.0366 428.6290 380.4394 408.8826 -4.5822 423.8722 428.4544 380.2220 410.4706 -4.5774 423.6621 428.2396 379.9945 412.0843 -4.5696 423.4643 428.0339 379.7600 413.6876 -4.5660 423.2354 427.8013 379.5372 415.2963 -4.5639 423.0065 427.5704 379.3137 416.9046 -4.5607 422.7734 427.3341 379.1004 418.5080 -4.5551 422.5523 427.1074 378.8867 420.1369 -4.5467 422.3182 426.8649 378.6883 421.7403 -4.5437 422.1002 426.6440 378.4883 423.3488 -4.5390 421.8933 426.4323 378.2818 424.9520 -4.5318 421.6733 426.2051 378.0748 426.5554 -4.5244 421.4325 425.9569 377.8785 428.1384 -4.5125 421.2488 425.7614 377.6680 429.7416 -4.5055 421.0814 425.5869 377.4459 431.3503 -4.4997 420.9006 425.4003 377.2633 432.9690 -4.4870 420.6675 425.1545 377.0544 434.5775 -4.4826 420.4372 424.9198 376.8519 436.1810 -4.4825 420.2175 424.7000 376.6716 437.7844 -4.4742 420.0323 424.5065 376.4813 439.3979 -4.4687 419.8350 424.3038 376.2971 441.0014 -4.4662 419.6085 424.0747 376.0557 442.5995 -4.4606 419.3736 423.8342 375.8944 444.2081 -4.4557 419.1537 423.6094 375.6953 445.8321 -4.4476 418.9428 423.3904 375.4866 447.4354 -4.4426 418.7517 423.1942 375.2783 449.0440 -4.4384 418.5673 423.0056 375.0432 450.6525 -4.4260 418.3682 422.7942 374.7943 452.2609 -4.4189 418.1685 422.5874 374.5574 453.8695 -4.4064 417.9278 422.3342 374.3448 455.4780 -4.3967 417.7208 422.1176 374.1316 457.0916 -4.3968 417.5117 421.9085 373.8930 458.6746 -4.3939 417.2902 421.6841 373.6913 460.2831 -4.3881 417.0442 421.4323 373.4664 461.8865 -4.3779 416.8261 421.2040 373.2303 463.4951 -4.3669 416.6319 420.9988 372.9875 465.0985 -4.3620 416.3938 420.7558 372.7685 466.7070 -4.3564 416.1791 420.5355 372.5705 468.3105 -4.3488 415.9740 420.3228 372.3540 469.9190 -4.3393 415.7647 420.1041 372.1390 471.5275 -4.3319 415.5418 419.8737 371.9337 473.1309 -4.3318 415.3078 419.6396 371.7445 474.7393 -4.3227 415.0917 419.4145 371.5367 476.3428 -4.3160 414.8760 419.1920 371.3441 477.9513 -4.3091 414.6853 418.9944 371.1575 479.5598 -4.3000 414.4856 418.7856 370.9801 481.1683 -4.2936 414.2785 418.5721 370.7654 482.7921 -4.2880 414.0410 418.3290 370.5242 484.4006 -4.2842 413.8177 418.1019 370.3251 486.0040 -4.2804 413.5827 417.8631 370.1073 487.6124 -4.2751 413.3660 417.6410 369.9070 489.2108 -4.2662 413.1597 417.4259 369.6944 490.8141 -4.2607 412.9676 417.2283 369.4745 492.4225 -4.2489 412.7560 417.0048 369.2823 494.0363 -4.2466 412.5588 416.8054 369.0805 495.6243 -4.2463 412.3394 416.5857 368.8896 497.2328 -4.2429 412.1057 416.3485 368.6748 498.8516 -4.2347 411.8728 416.1075 368.4808 500.4601 -4.2291 411.6487 415.8778 368.2688 502.0635 -4.2233 411.4406 415.6639 368.0658 503.6618 -4.2189 411.2305 415.4494 367.8607 505.2653 -4.2087 411.0314 415.2401 367.6150 506.8941 -4.2009 410.8466 415.0475 367.3800 508.4976 -4.1974 410.6450 414.8424 367.1383 510.1111 -4.1921 410.3782 414.5703 366.9183 511.7146 -4.1837 410.1807 414.3644 366.7280 513.3284 -4.1762 409.9818 414.1580 366.5007 514.9315 -4.1662 409.7687 413.9349 366.2727 516.5403 -4.1590 409.5730 413.7320 366.0225 518.1591 -4.1532 409.3645 413.5177 365.8306 519.7726 -4.1460 409.1892 413.3353 365.5935 521.3710 -4.1409 408.9630 413.1038 365.3802 522.9745 -4.1378 408.7088 412.8466 365.1804 524.5829 -4.1317 408.4706 412.6024 364.9643 526.1659 -4.1265 408.2715 412.3980 364.7491 527.7694 -4.1155 408.0813 412.1968 364.6000 529.3778 -4.1056 407.8630 411.9685 364.4119 530.9966 -4.1002 407.6445 411.7447 364.1904 532.6053 -4.0867 407.4195 411.5062 364.0076 534.2085 -4.0750 407.1960 411.2710 363.8223 535.8171 -4.0742 406.9873 411.0615 363.5524 537.4205 -4.0680 406.7763 410.8443 363.3633 539.0289 -4.0655 406.5941 410.6595 363.1762 540.6375 -4.0602 406.3953 410.4555 362.9774 542.2614 -4.0575 406.1545 410.2120 362.7409 543.8698 -4.0558 405.9396 409.9953 362.5384 545.4733 -4.0508 405.7443 409.7951 362.3084 547.0866 -4.0481 405.5352 409.5834 362.1071 548.6901 -4.0378 405.3024 409.3402 361.9094 550.3038 -4.0252 405.1156 409.1408 361.7056 551.9071 -4.0177 404.8558 408.8735 361.5005 553.5260 -4.0117 404.5780 408.5897 361.2826 555.1243 -4.0022 404.3716 408.3738 361.0235 556.7224 -3.9977 404.1856 408.1833 360.7832 558.3310 -3.9954 403.9934 407.9888 360.5818 559.9343 -3.9886 403.7725 407.7611 360.3912 561.5428 -3.9784 403.5251 407.5035 360.1723 563.1306 -3.9681 403.3156 407.2838 359.9797 564.7340 -3.9601 403.0997 407.0598 359.7511 566.4605 -3.9543 402.8743 406.8287 359.5356 568.1406 -3.9437 402.6607 406.6044 359.3382 569.7543 -3.9383 402.4373 406.3756 359.1320 571.3730 -3.9331 402.2221 406.1552 358.9185 572.9815 -3.9243 402.0312 405.9555 358.6685 574.5850 -3.9235 401.8292 405.7527 358.4583 576.1985 -3.9230 401.6315 405.5545 358.2556 577.8019 -3.9143 401.4117 405.3260 358.0755 579.4103 -3.9040 401.1914 405.0955 357.8734 581.0188 -3.8981 400.9869 404.8851 357.6656 582.6376 -3.8920 400.7689 404.6609 357.4493 584.2461 -3.8827 400.5507 404.4334 357.2060 585.8495 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