DTA measure 1pbupdown3 Date: 2026331:1058 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1079.69 s Mass = 959.600 mg data_number = 1343 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.2300 1.4227 236.5134 235.0907 275.9389 1.9963 1.4158 236.7736 235.3579 275.8616 2.8233 1.4177 237.0506 235.6329 275.7990 3.6100 1.4187 237.3180 235.8993 275.7129 4.4065 1.4140 237.5863 236.1723 275.6007 5.2338 1.4152 237.8612 236.4459 275.4535 6.0000 1.4128 238.1142 236.7014 275.3329 6.8168 1.4122 238.4067 236.9945 275.1744 7.5928 1.4093 238.6728 237.2636 275.0062 8.4408 1.4057 238.9411 237.5354 274.8311 9.2168 1.4013 239.1922 237.7909 274.6554 10.0340 1.3976 239.4358 238.0382 274.4974 10.8103 1.3974 239.6882 238.2908 274.3094 11.6270 1.3976 239.9642 238.5666 274.1549 12.4240 1.3976 240.2083 238.8107 274.0004 13.2205 1.3964 240.4890 239.0926 273.8898 14.0580 1.3964 240.7456 239.3492 273.7953 14.8240 1.3980 240.9827 239.5847 273.7473 15.6820 1.3958 241.2318 239.8361 273.6961 16.4375 1.3904 241.4863 240.0959 273.6702 17.2755 1.3909 241.7826 240.3917 273.7091 18.0615 1.3906 242.0740 240.6835 273.7973 18.8583 1.3934 242.3410 240.9476 273.9083 19.6858 1.3908 242.5917 241.2009 274.0691 20.4515 1.3881 242.8195 241.4314 274.2684 21.3098 1.3876 243.0735 241.6859 274.5098 22.0653 1.3848 243.2949 241.9102 274.7591 22.9030 1.3865 243.5641 242.1776 275.0690 23.6895 1.3884 243.8221 242.4337 275.3785 24.4860 1.3913 244.0497 242.6584 275.7204 25.3135 1.3871 244.3331 242.9460 276.1008 26.0793 1.3826 244.5644 243.1818 276.4938 26.9375 1.3773 244.8301 243.4527 276.9283 27.7035 1.3720 245.0592 243.6872 277.3318 28.5305 1.3646 245.3366 243.9720 277.7700 29.3273 1.3595 245.5668 244.2073 278.1903 30.1240 1.3538 245.8148 244.4610 278.6072 30.9408 1.3450 246.0643 244.7193 279.0383 31.7173 1.3428 246.3016 244.9588 279.4300 32.5650 1.3389 246.5709 245.2319 279.8342 33.3308 1.3348 246.7815 245.4467 280.1434 34.1585 1.3282 247.0289 245.7008 280.4377 34.9548 1.3195 247.2685 245.9490 280.6996 35.7413 1.3117 247.4993 246.1875 280.9491 36.5685 1.3058 247.7658 246.4600 281.1404 37.3343 1.2980 247.9963 246.6983 281.2974 38.1823 1.2933 248.2351 246.9417 281.4784 38.9483 1.2918 248.4440 247.1522 281.5767 39.7753 1.2850 248.7264 247.4415 281.6708 40.5415 1.2789 248.9564 247.6775 281.7424 41.3585 1.2679 249.1800 247.9121 281.7944 42.1653 1.2550 249.4291 248.1740 281.8187 42.9518 1.2542 249.6892 248.4350 281.8125 43.7790 1.2483 249.9249 248.6767 281.7697 44.5450 1.2475 250.1493 248.9017 281.7088 45.4135 1.2447 250.3848 249.1401 281.6489 46.1688 1.2388 250.5974 249.3585 281.5911 46.9965 1.2307 250.8391 249.6083 281.4870 47.7930 1.2182 251.0669 249.8487 281.3696 48.5895 1.2142 251.2993 250.0851 281.2572 49.4170 1.2098 251.5571 250.3473 281.1264 50.1725 1.2072 251.8060 250.5988 281.0171 51.0410 1.2018 252.0480 250.8461 280.9198 51.8068 1.1947 252.2571 251.0624 280.8362 52.6340 1.1903 252.5243 251.3340 280.7675 53.4205 1.1869 252.7455 251.5586 280.7030 54.2275 1.1833 252.9631 251.7797 280.6709 55.0443 1.1787 253.1695 251.9908 280.6531 55.8103 1.1706 253.3575 252.1869 280.6653 56.6685 1.1605 253.5960 252.4356 280.7470 57.4445 1.1613 253.8180 252.6567 280.8124 58.2618 1.1558 254.0409 252.8850 280.9225 59.0583 1.1527 254.2701 253.1174 281.0254 59.8550 1.1503 254.5020 253.3517 281.1838 60.6825 1.1431 254.7133 253.5702 281.4296 61.4480 1.1420 254.9517 253.8097 281.6299 62.3065 1.1390 255.2067 254.0676 281.8894 63.0723 1.1344 255.4080 254.2736 282.1397 63.8995 1.1274 255.6378 254.5104 282.4281 64.6860 1.1206 255.8421 254.7216 282.7549 65.4825 1.1121 256.0538 254.9417 283.0635 66.3098 1.1022 256.2732 255.1710 283.4323 67.0758 1.0949 256.4931 255.3983 283.8034 67.8928 1.0888 256.7250 255.6362 284.1682 68.6588 1.0803 256.9442 255.8639 284.5080 69.5168 1.0754 257.1670 256.0916 284.8894 70.2723 1.0654 257.3777 256.3122 285.1962 71.1100 1.0576 257.6161 256.5585 285.5807 71.8965 1.0493 257.8492 256.7999 285.9243 72.6928 1.0398 258.0437 257.0039 286.2261 73.5205 1.0343 258.2516 257.2173 286.5016 74.2760 1.0279 258.4450 257.4171 286.7783 75.1343 1.0202 258.6700 257.6498 287.0648 75.9003 1.0106 258.8664 257.8558 287.2826 76.7275 1.0029 259.0918 258.0889 287.4861 77.5243 0.9947 259.2884 258.2937 287.6532 78.3105 0.9877 259.4770 258.4893 287.7795 79.1175 0.9794 259.7099 258.7305 287.8913 79.9143 0.9729 259.9222 258.9493 287.9759 80.7413 0.9633 260.1584 259.1952 288.0488 81.4973 0.9566 260.3809 259.4243 288.0704 82.3655 0.9471 260.6140 259.6669 288.0585 83.1210 0.9385 260.8215 259.8830 288.0643 83.9588 0.9276 261.0650 260.1374 288.0480 84.7450 0.9192 261.3188 260.3996 288.0236 85.5518 0.9125 261.5225 260.6101 287.9857 86.3693 0.9068 261.7346 260.8278 287.9170 87.1450 0.8983 261.8974 260.9990 287.8497 87.9930 0.8947 262.0850 261.1903 287.7780 88.7385 0.8899 262.2857 261.3958 287.7426 89.5860 0.8864 262.5206 261.6342 287.6588 90.3520 0.8801 262.7298 261.8497 287.5648 91.1795 0.8729 262.9262 262.0532 287.5198 91.9860 0.8680 263.1369 262.2689 287.4991 92.7725 0.8635 263.3598 262.4963 287.4907 93.6000 0.8587 263.5852 262.7265 287.4796 94.3655 0.8539 263.7885 262.9346 287.4769 95.2238 0.8474 264.0070 263.1596 287.5279 95.9898 0.8473 264.2052 263.3579 287.5633 96.8170 0.8448 264.3955 263.5506 287.6363 97.6138 0.8396 264.6089 263.7692 287.7408 98.4000 0.8351 264.7997 263.9645 287.8504 99.2173 0.8326 264.9994 264.1669 288.0301 99.9935 0.8325 265.2089 264.3764 288.1909 100.8410 0.8214 265.4559 264.6345 288.4153 101.5663 0.8169 265.6578 264.8409 288.6373 102.4345 0.8185 265.8765 265.0580 288.9286 103.1900 0.8154 266.0550 265.2396 289.1602 104.0175 0.8122 266.2529 265.4407 289.4335 104.8140 0.8023 266.4023 265.6001 289.7302 105.6005 0.7980 266.5869 265.7888 290.0685 106.4280 0.7897 266.8063 266.0166 290.4027 107.1935 0.7847 267.0068 266.2221 290.6902 108.0518 0.7735 267.2215 266.4480 291.0396 108.8178 0.7632 267.4255 266.6623 291.3582 109.6345 0.7503 267.6496 266.8992 291.6838 110.4418 0.7441 267.8479 267.1038 291.9795 111.2280 0.7330 268.0368 267.3038 292.2587 112.0348 0.7170 268.2635 267.5465 292.5142 112.8625 0.7118 268.4760 267.7642 292.7651 113.6383 0.7098 268.6410 267.9312 293.0044 114.4555 0.7044 268.8356 268.1311 293.2311 115.2523 0.6973 269.0444 268.3471 293.4313 116.0485 0.6894 269.2594 268.5700 293.5719 116.8760 0.6863 269.4427 268.7564 293.7588 117.6420 0.6784 269.6388 268.9605 293.8927 118.5000 0.6711 269.8612 269.1901 293.9987 119.2658 0.6621 270.0444 269.3823 294.0708 120.1035 0.6483 270.2749 269.6266 294.1319 120.8898 0.6363 270.4551 269.8188 294.1726 121.6968 0.6274 270.6741 270.0467 294.1782 122.4728 0.6239 270.8507 270.2268 294.2091 123.3000 0.6139 271.0475 270.4336 294.2202 124.0968 0.6079 271.2424 270.6345 294.1713 124.9035 0.6023 271.4344 270.8321 294.1458 125.7205 0.5951 271.6344 271.0393 294.1295 126.4865 0.5880 271.7974 271.2093 294.1068 127.3445 0.5723 271.9895 271.4172 294.0535 128.1208 0.5653 272.1556 271.5903 294.0315 128.9380 0.5623 272.3766 271.8144 294.0129 129.7243 0.5568 272.5672 272.0104 293.9974 130.5313 0.5518 272.7330 272.1813 293.9784 131.3483 0.5459 272.9313 272.3854 294.0069 132.1140 0.5413 273.1386 272.5973 294.0401 132.9210 0.5378 273.3584 272.8206 294.0539 133.7175 0.5311 273.5401 273.0091 294.1065 134.5450 0.5243 273.7243 273.2000 294.1582 135.3110 0.5197 273.9292 273.4095 294.2517 136.1585 0.5115 274.1609 273.6494 294.3761 136.9350 0.5051 274.3360 273.8309 294.5256 137.7520 0.4989 274.5294 274.0305 294.6970 138.5488 0.4937 274.7322 274.2386 294.8783 139.3455 0.4879 274.9202 274.4323 295.0834 140.1725 0.4849 275.1137 274.6289 295.3065 140.9388 0.4749 275.2878 274.8129 295.5109 141.7865 0.4642 275.4677 275.0035 295.7549 142.5420 0.4587 275.6244 275.1657 295.9942 143.4005 0.4541 275.8237 275.3696 296.2691 144.1763 0.4513 275.9985 275.5472 296.5189 144.9935 0.4440 276.1867 275.7427 296.8227 145.7903 0.4349 276.3684 275.9335 297.0958 146.5868 0.4316 276.5653 276.1338 297.3809 147.4143 0.4212 276.7369 276.3157 297.6710 148.1800 0.4133 276.9137 276.5004 297.9296 149.0278 0.4081 277.1334 276.7252 298.2281 149.8040 0.3983 277.2842 276.8858 298.5016 150.6210 0.3948 277.4432 277.0484 298.7479 151.4280 0.3842 277.6592 277.2750 298.9666 152.2143 0.3754 277.8950 277.5195 299.1654 153.0518 0.3694 278.1031 277.7337 299.3850 153.8073 0.3596 278.2623 277.9027 299.5398 154.6760 0.3550 278.4488 278.0938 299.6898 155.4313 0.3483 278.6092 278.2609 299.8208 156.2690 0.3425 278.8080 278.4655 299.9508 157.0555 0.3396 278.9873 278.6478 300.0270 157.8518 0.3334 279.1780 278.8446 300.0821 158.6793 0.3275 279.3552 279.0277 300.1834 159.4555 0.3194 279.5430 279.2235 300.2329 160.3030 0.3051 279.7311 279.4260 300.2757 161.0690 0.3001 279.8956 279.5955 300.2950 161.8965 0.2937 280.0710 279.7774 300.3492 162.6828 0.2880 280.2517 279.9637 300.3846 163.4795 0.2842 280.4169 280.1327 300.4168 164.2760 0.2812 280.6015 280.3203 300.4346 165.0623 0.2767 280.7714 280.4947 300.4507 165.8900 0.2654 280.9272 280.6618 300.4519 166.6555 0.2562 281.1225 280.8663 300.4343 167.5135 0.2497 281.3410 281.0913 300.4414 168.2798 0.2459 281.5196 281.2737 300.4763 169.0965 0.2336 281.7305 281.4969 300.5074 169.8730 0.2254 281.8970 281.6716 300.5441 170.6900 0.2202 282.1046 281.8844 300.5992 171.4865 0.2200 282.2519 282.0319 300.6266 172.2835 0.2174 282.4389 282.2215 300.6920 173.1105 0.2109 282.6405 282.4296 300.7835 173.8765 0.2088 282.8349 282.6261 300.8584 174.7245 0.2039 283.0389 282.8350 300.9759 175.5003 0.2004 283.2144 283.0139 301.1101 176.3178 0.1978 283.3944 283.1966 301.2526 177.1245 0.1935 283.5543 283.3609 301.4247 177.9108 0.1829 283.7481 283.5652 301.5774 178.7485 0.1753 283.9504 283.7751 301.7578 179.5040 0.1716 284.1232 283.9515 301.9617 180.3620 0.1642 284.2976 284.1334 302.2218 181.1283 0.1586 284.4555 284.2969 302.4524 181.9655 0.1530 284.6506 284.4976 302.6836 182.7523 0.1436 284.8205 284.6768 302.9379 183.5488 0.1364 285.0015 284.8651 303.1767 184.3760 0.1340 285.1564 285.0224 303.4431 185.1523 0.1302 285.3127 285.1825 303.6920 185.9693 0.1201 285.4882 285.3680 303.9892 186.7350 0.1136 285.6440 285.5304 304.2235 187.5935 0.1087 285.8292 285.7206 304.4825 188.3693 0.1065 286.0021 285.8956 304.7329 189.1865 0.0998 286.1516 286.0518 304.9718 189.9830 0.0915 286.3408 286.2493 305.1884 190.7795 0.0809 286.5357 286.4547 305.4237 191.6070 0.0731 286.7083 286.6352 305.6703 192.3730 0.0629 286.8833 286.8204 305.8695 193.2205 0.0558 287.0864 287.0306 306.0208 193.9968 0.0517 287.2713 287.2196 306.1755 194.8140 0.0465 287.4593 287.4129 306.3147 195.5693 0.0409 287.6341 287.5931 306.4111 196.4070 0.0363 287.8308 287.7944 306.5187 197.1935 0.0331 287.9951 287.9619 306.5930 197.9900 0.0307 288.1503 288.1195 306.6885 198.8175 0.0288 288.3300 288.3012 306.7508 199.5730 0.0212 288.5083 288.4871 306.8020 200.4313 0.0121 288.6916 288.6794 306.8514 201.1973 0.0044 288.8639 288.8595 306.8834 202.0245 -0.0002 289.0258 289.0261 306.8785 202.7905 -0.0060 289.1791 289.1851 306.8861 203.6178 -0.0147 289.3546 289.3692 306.8736 204.4143 -0.0195 289.5091 289.5285 306.8393 205.2215 -0.0199 289.7064 289.7263 306.8266 206.0178 -0.0225 289.8870 289.9095 306.8323 206.8145 -0.0308 290.0365 290.0673 306.8122 207.6318 -0.0310 290.2025 290.2336 306.8344 208.4075 -0.0339 290.3733 290.4072 306.8642 209.2555 -0.0389 290.5382 290.5771 306.9041 210.0215 -0.0488 290.7159 290.7647 306.9517 210.8488 -0.0552 290.9093 290.9645 307.0481 211.6453 -0.0586 291.1001 291.1588 307.1543 212.4420 -0.0627 291.2733 291.3360 307.2836 213.2590 -0.0605 291.4350 291.4955 307.4060 214.0455 -0.0517 291.6123 291.6640 307.5440 214.8728 -0.0565 291.7900 291.8465 307.7036 215.6490 -0.0634 291.9734 292.0369 307.8399 216.4763 -0.0757 292.1546 292.2304 308.0286 217.2420 -0.0847 292.3184 292.4031 308.2441 218.0900 -0.0888 292.4989 292.5877 308.4714 218.8663 -0.0968 292.6587 292.7555 308.7181 219.6933 -0.1050 292.8210 292.9260 308.9821 220.4900 -0.1088 292.9803 293.0891 309.2111 221.2765 -0.1124 293.1532 293.2657 309.4311 222.1140 -0.1207 293.3421 293.4628 309.6489 222.8800 -0.1258 293.5050 293.6308 309.8705 223.7380 -0.1344 293.7010 293.8354 310.1468 224.4935 -0.1412 293.8713 294.0125 310.3745 225.3313 -0.1445 294.0742 294.2188 310.6071 226.1278 -0.1489 294.2317 294.3806 310.8380 226.9140 -0.1527 294.4023 294.5550 311.0761 227.7415 -0.1549 294.5755 294.7304 311.2975 228.5073 -0.1638 294.7342 294.8980 311.5098 229.3245 -0.1717 294.9168 295.0885 311.6942 230.0905 -0.1766 295.0724 295.2490 311.8658 230.9483 -0.1810 295.2264 295.4074 312.0781 231.7040 -0.1868 295.3533 295.5401 312.2243 232.5315 -0.1910 295.5268 295.7178 312.3697 233.3278 -0.1991 295.6959 295.8951 312.4900 234.1248 -0.2043 295.8559 296.0602 312.6258 234.9213 -0.2097 296.0073 296.2170 312.7458 235.7588 -0.2151 296.1729 296.3880 312.8451 236.5455 -0.2218 296.3521 296.5739 312.9525 237.3418 -0.2260 296.5247 296.7506 313.0273 238.1693 -0.2321 296.6884 296.9205 313.0812 238.9353 -0.2343 296.8561 297.0903 313.1019 239.7930 -0.2410 297.0180 297.2590 313.1352 240.5490 -0.2470 297.1599 297.4069 313.1790 241.3865 -0.2547 297.3566 297.6113 313.2171 242.1728 -0.2579 297.5234 297.7813 313.2044 242.9695 -0.2645 297.7021 297.9666 313.2232 243.7968 -0.2680 297.8948 298.1628 313.2652 244.5730 -0.2705 298.0474 298.3179 313.2831 245.3903 -0.2767 298.2180 298.4947 313.3178 246.1865 -0.2854 298.4086 298.6941 313.3442 247.0143 -0.2858 298.5595 298.8453 313.3866 247.7800 -0.2874 298.7121 298.9995 313.4617 248.6380 -0.2966 298.8904 299.1870 313.4965 249.4040 -0.3005 299.0590 299.3595 313.5464 250.2313 -0.3031 299.2382 299.5413 313.6448 251.0278 -0.3074 299.4231 299.7305 313.7312 251.8245 -0.3127 299.6027 299.9154 313.8503 252.6518 -0.3186 299.7899 300.1085 313.9995 253.4178 -0.3216 299.9491 300.2707 314.1254 254.2760 -0.3237 300.0979 300.4215 314.2875 255.0415 -0.3271 300.2727 300.5998 314.4713 255.8690 -0.3313 300.4517 300.7830 314.6612 256.6658 -0.3395 300.6127 300.9522 314.8752 257.4623 -0.3453 300.7604 301.1058 315.0953 258.2795 -0.3515 300.9309 301.2824 315.3356 259.0555 -0.3588 301.0887 301.4475 315.5735 259.8728 -0.3653 301.2413 301.6067 315.8094 260.6285 -0.3691 301.4079 301.7770 316.0152 261.4965 -0.3747 301.5703 301.9450 316.2949 262.2525 -0.3806 301.7114 302.0921 316.5305 263.0695 -0.3864 301.8845 302.2709 316.7711 263.8763 -0.3915 302.0497 302.4412 317.0094 264.6630 -0.3944 302.1937 302.5880 317.2486 265.4900 -0.4011 302.3837 302.7848 317.4650 266.2560 -0.4079 302.5484 302.9563 317.6702 267.1143 -0.4108 302.7326 303.1434 317.8726 267.8798 -0.4173 302.8782 303.2955 318.0469 268.6970 -0.4231 303.0448 303.4679 318.2201 269.5040 -0.4272 303.2169 303.6441 318.3984 270.2900 -0.4303 303.3846 303.8149 318.5464 271.1178 -0.4327 303.5556 303.9883 318.7019 271.8835 -0.4345 303.6800 304.1146 318.8238 272.7415 -0.4388 303.8268 304.2656 318.9214 273.5078 -0.4467 303.9791 304.4258 319.0155 274.3245 -0.4509 304.1453 304.5963 319.1149 275.1315 -0.4564 304.3062 304.7626 319.1870 275.9180 -0.4645 304.4638 304.9283 319.2409 276.7553 -0.4679 304.6569 305.1249 319.3341 277.5113 -0.4732 304.8141 305.2873 319.3733 278.3795 -0.4787 304.9788 305.4575 319.4314 279.1350 -0.4847 305.1706 305.6553 319.4557 279.9728 -0.4907 305.3422 305.8329 319.5010 280.7590 -0.4951 305.5188 306.0139 319.5162 281.5660 -0.5006 305.6843 306.1849 319.5584 282.3833 -0.5025 305.8538 306.3563 319.6208 283.1590 -0.4975 306.0257 306.5232 319.6516 284.0070 -0.5023 306.1687 306.6710 319.6849 284.7833 -0.5104 306.2940 306.8044 319.7216 285.6000 -0.5140 306.4260 306.9401 319.7630 286.3968 -0.5121 306.5834 307.0955 319.8147 287.1933 -0.5146 306.7722 307.2868 319.8932 288.0205 -0.5191 306.9479 307.4671 319.9813 288.7865 -0.5214 307.1014 307.6228 320.0748 289.6140 -0.5281 307.2862 307.8143 320.1874 290.3795 -0.5316 307.4565 307.9881 320.3013 291.2275 -0.5373 307.6406 308.1779 320.4461 291.9935 -0.5473 307.7676 308.3149 320.6070 292.8208 -0.5558 307.9146 308.4704 320.7741 293.6175 -0.5612 308.0624 308.6236 320.9682 294.4140 -0.5652 308.2176 308.7827 321.1623 295.2003 -0.5696 308.4042 308.9738 321.3560 296.0075 -0.5767 308.5806 309.1574 321.5830 296.8243 -0.5794 308.7525 309.3318 321.8197 297.5800 -0.5840 308.8652 309.4492 322.0273 298.4485 -0.5883 309.0212 309.6094 322.2398 299.2040 -0.5932 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