DTA measure 1pbupdown4 Date: 2026331:1159 Lower limit = 20.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1723.48 s Mass = 959.600 mg data_number = 1072 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.3583 -0.2478 251.9926 252.2404 225.4662 3.9666 -0.2427 251.9327 252.1753 225.2143 5.5856 -0.2386 251.8720 252.1106 224.9882 7.1943 -0.2252 251.8029 252.0281 224.7580 8.7975 -0.2180 251.7477 251.9657 224.4891 10.4063 -0.2128 251.6488 251.8615 224.2440 12.0149 -0.2047 251.5976 251.8023 223.9913 13.6184 -0.1960 251.5157 251.7116 223.7418 15.2268 -0.2029 251.4531 251.6560 223.5178 16.8253 -0.2034 251.3909 251.5943 223.2930 18.4390 -0.2016 251.3241 251.5256 223.0162 20.0324 -0.1988 251.2229 251.4217 222.7762 21.6356 -0.1947 251.1290 251.3237 222.5312 23.2444 -0.1940 251.0583 251.2524 222.2644 24.8480 -0.1855 250.9636 251.1492 222.0347 26.4566 -0.1815 250.8609 251.0424 221.8064 28.0601 -0.1855 250.7861 250.9716 221.5680 29.6789 -0.1893 250.6932 250.8825 221.3476 31.2773 -0.1910 250.5688 250.7598 221.0943 32.8859 -0.1906 250.4752 250.6658 220.8727 34.4943 -0.1874 250.3616 250.5489 220.6611 36.1030 -0.1844 250.2752 250.4596 220.4313 37.7116 -0.1742 250.1653 250.3395 220.2453 39.3200 -0.1760 250.0641 250.2401 220.0386 40.9288 -0.1717 249.9512 250.1229 219.8787 42.5476 -0.1707 249.8620 250.0327 219.7840 44.1613 -0.1720 249.7645 249.9365 219.7395 45.7648 -0.1756 249.6543 249.8299 219.7392 47.3683 -0.1852 249.5442 249.7294 219.7842 48.9718 -0.1901 249.4430 249.6331 219.9013 50.5804 -0.1980 249.3567 249.5547 220.0849 52.1633 -0.2081 249.2384 249.4466 220.3262 53.7669 -0.2143 249.1527 249.3670 220.6353 55.3910 -0.2205 249.0211 249.2416 221.0263 56.9944 -0.2225 248.8831 249.1056 221.4222 58.6030 -0.2248 248.7548 248.9796 221.8421 60.2065 -0.2339 248.6274 248.8614 222.3487 61.8203 -0.2406 248.5197 248.7603 222.7875 63.4236 -0.2495 248.4237 248.6732 223.1931 65.0169 -0.2604 248.3048 248.5652 223.5874 66.6255 -0.2701 248.2084 248.4785 223.9885 68.2443 -0.2792 248.1432 248.4224 224.3370 69.8528 -0.2813 248.0547 248.3360 224.6360 71.4614 -0.2880 247.9427 248.2308 224.9138 73.0701 -0.2980 247.8601 248.1580 225.1470 74.6734 -0.3060 247.7698 248.0759 225.3220 76.2820 -0.3092 247.6834 247.9926 225.4377 77.8856 -0.3152 247.5729 247.8880 225.5641 79.4994 -0.3165 247.4616 247.7781 225.6768 81.1079 -0.3237 247.3890 247.7127 225.7261 82.7064 -0.3253 247.3084 247.6338 225.7911 84.2996 -0.3342 247.2079 247.5421 225.8722 85.9033 -0.3480 247.1162 247.4642 225.9160 87.5065 -0.3607 247.0385 247.3992 226.0000 89.1153 -0.3762 246.9608 247.3370 226.0755 90.7188 -0.3863 246.8831 247.2695 226.1637 92.3326 -0.3901 246.7858 247.1759 226.2244 93.9256 -0.3973 246.7122 247.1095 226.3264 95.5446 -0.4062 246.6508 247.0571 226.4631 97.1584 -0.4109 246.5978 247.0087 226.6106 98.7618 -0.4192 246.5194 246.9386 226.8056 100.3703 -0.4257 246.4774 246.9030 227.0736 101.9789 -0.4345 246.3934 246.8279 227.3523 103.5823 -0.4423 246.2929 246.7352 227.6158 105.1908 -0.4431 246.2293 246.6724 227.9286 106.7943 -0.4470 246.1527 246.5997 228.2451 108.4079 -0.4550 246.0903 246.5454 228.5555 110.0266 -0.4626 245.9843 246.4469 228.8905 111.6250 -0.4721 245.9129 246.3850 229.2421 113.2130 -0.4796 245.8749 246.3545 229.5807 114.8164 -0.4840 245.7983 246.2822 229.8656 116.4250 -0.4839 245.7432 246.2270 230.0933 118.0286 -0.4921 245.6973 246.1895 230.3779 119.6319 -0.4962 245.6582 246.1544 230.6254 121.2251 -0.4984 245.6320 246.1304 230.8506 122.8288 -0.5025 245.6002 246.1027 231.0589 124.4526 -0.5001 245.5875 246.0876 231.2093 126.0561 -0.5068 245.5670 246.0737 231.3383 127.6700 -0.5118 245.5223 246.0342 231.4747 129.2736 -0.5174 245.4697 245.9872 231.5988 130.8823 -0.5178 245.4220 245.9399 231.7059 132.4909 -0.5198 245.3413 245.8611 231.7875 134.0994 -0.5263 245.3078 245.8341 231.8800 135.7183 -0.5329 245.2577 245.7906 231.9377 137.3219 -0.5373 245.2332 245.7704 232.0799 138.9355 -0.5394 245.2399 245.7793 232.2129 140.5390 -0.5409 245.2237 245.7646 232.4101 142.1476 -0.5414 245.1818 245.7232 232.6056 143.7513 -0.5364 245.1465 245.6829 232.8235 145.3394 -0.5370 245.1216 245.6585 233.0608 146.9429 -0.5408 245.0716 245.6124 233.2908 148.5618 -0.5451 245.0022 245.5473 233.5587 150.1705 -0.5476 244.9859 245.5335 233.8319 151.7741 -0.5494 245.0048 245.5542 234.1049 153.3825 -0.5521 245.0199 245.5720 234.3818 154.9860 -0.5458 245.0119 245.5577 234.6883 156.5844 -0.5168 245.0226 245.5394 234.9832 158.1876 -0.5194 245.0198 245.5392 235.2917 159.7963 -0.5327 244.9747 245.5073 235.5411 161.4153 -0.5408 244.9868 245.5276 235.8164 163.0184 -0.5414 244.9958 245.5373 236.0435 164.6323 -0.5419 244.9906 245.5326 236.2510 166.2409 -0.5450 244.9947 245.5398 236.4697 167.8494 -0.5484 245.0033 245.5517 236.6626 169.4580 -0.5568 245.0202 245.5770 236.8386 171.0666 -0.5580 245.0320 245.5900 237.0135 172.6855 -0.5566 245.0190 245.5755 237.1773 174.2940 -0.5516 245.0642 245.6158 237.3219 175.8976 -0.5492 245.0751 245.6242 237.4163 177.4960 -0.5530 245.1019 245.6549 237.5228 179.0998 -0.5565 245.1343 245.6907 237.6429 180.6828 -0.5519 245.1097 245.6616 237.7759 182.2911 -0.5534 245.1190 245.6724 237.9555 183.8946 -0.5587 245.1567 245.7154 238.1569 185.5135 -0.5558 245.1582 245.7139 238.3525 187.1221 -0.5492 245.1759 245.7251 238.5539 188.7255 -0.5468 245.2079 245.7546 238.7487 190.3343 -0.5421 245.2494 245.7915 238.9830 191.9376 -0.5385 245.2903 245.8288 239.2574 193.5461 -0.5346 245.3518 245.8864 239.5051 195.1394 -0.5193 245.4328 245.9521 239.7445 196.7480 -0.4927 245.4502 245.9428 240.0275 198.3668 -0.4680 245.4473 245.9152 240.3047 199.9805 -0.4660 245.4653 245.9313 240.5782 201.5840 -0.4718 245.5187 245.9905 240.8507 203.1976 -0.4848 245.5752 246.0600 241.1427 204.8011 -0.4962 245.6273 246.1235 241.3902 206.3995 -0.5003 245.6849 246.1852 241.6001 207.9980 -0.5054 245.7238 246.2293 241.8444 209.6014 -0.5109 245.7999 246.3108 242.0320 211.2203 -0.5169 245.8640 246.3809 242.2301 212.8238 -0.5162 245.9027 246.4189 242.4225 214.4120 -0.5148 245.9700 246.4848 242.5607 216.0205 -0.5118 246.0480 246.5597 242.7156 217.6240 -0.5074 246.1291 246.6365 242.8919 219.2331 -0.5032 246.1657 246.6689 243.0284 220.8379 -0.5018 246.1996 246.7014 243.2070 222.4473 -0.4973 246.2789 246.7762 243.3799 224.0361 -0.4890 246.3415 246.8306 243.5357 225.6665 -0.4763 246.4358 246.9121 243.7229 227.2764 -0.4705 246.4935 246.9639 243.8973 228.8859 -0.4683 246.5424 247.0107 244.0982 230.4746 -0.4598 246.6418 247.1016 244.2871 232.0794 -0.4567 246.7354 247.1921 244.4999 233.7046 -0.4473 246.8050 247.2523 244.7580 235.3086 -0.4469 246.8851 247.3320 244.9999 236.9336 -0.4479 246.9525 247.4004 245.2134 238.5384 -0.4465 247.0363 247.4829 245.4120 240.1431 -0.4486 247.1119 247.5605 245.6804 241.7318 -0.4485 247.1943 247.6429 245.9409 243.3311 -0.4478 247.2672 247.7150 246.1985 244.9359 -0.4423 247.3370 247.7793 246.4941 246.5403 -0.4402 247.4267 247.8669 246.7541 248.1393 -0.4400 247.5499 247.9898 247.0152 249.7645 -0.4324 247.6438 248.0762 247.2661 251.3641 -0.4300 247.7212 248.1512 247.4900 252.9679 -0.4255 247.8110 248.2365 247.7227 254.5778 -0.4205 247.9288 248.3493 247.9346 256.1825 -0.4113 248.0272 248.4385 248.1138 257.7919 -0.4066 248.1044 248.5110 248.2934 259.3961 -0.4058 248.2124 248.6182 248.4527 261.0265 -0.4090 248.3150 248.7240 248.6046 262.6311 -0.4033 248.4343 248.8376 248.7378 264.2350 -0.4011 248.5455 248.9466 248.9137 265.8449 -0.3903 248.6624 249.0527 249.0703 267.4496 -0.3856 248.7643 249.1499 249.1768 269.0595 -0.3833 248.8266 249.2100 249.3123 270.6641 -0.3819 248.9057 249.2876 249.5237 272.2834 -0.3828 249.0177 249.4006 249.6989 273.8728 -0.3792 249.1310 249.5102 249.8854 275.4724 -0.3631 249.2436 249.6067 250.0740 277.0764 -0.3439 249.3459 249.6898 250.3175 278.6809 -0.3410 249.4407 249.7817 250.5565 280.2805 -0.3450 249.5479 249.8929 250.8332 281.8746 -0.3514 249.6713 250.0227 251.1078 283.4788 -0.3525 249.8288 250.1812 251.3942 285.0886 -0.3482 249.9429 250.2911 251.6534 286.7139 -0.3127 250.0480 250.3607 251.9566 288.3178 -0.2846 250.1687 250.4533 252.1774 289.9275 -0.2678 250.2757 250.5435 252.4348 291.5169 -0.2610 250.3722 250.6332 252.6733 293.1268 -0.2648 250.5233 250.7881 252.9287 294.7315 -0.2895 250.6275 250.9170 253.1572 296.3414 -0.3005 250.7548 251.0553 253.3794 297.9451 -0.3115 250.9160 251.2275 253.6066 299.5704 -0.3191 251.0643 251.3833 253.8207 301.1649 -0.3191 251.2069 251.5259 254.0164 302.7696 -0.3161 251.3364 251.6525 254.1987 304.3785 -0.3103 251.4466 251.7569 254.3550 305.9781 -0.3096 251.5827 251.8923 254.5349 307.5726 -0.3131 251.7264 252.0394 254.6673 309.1825 -0.3148 251.8811 252.1960 254.7856 310.7811 -0.3164 252.0302 252.3466 254.9028 312.3705 -0.3180 252.1660 252.4840 255.0740 313.9958 -0.3151 252.2951 252.6101 255.2300 315.6005 -0.3089 252.4384 252.7472 255.4297 317.2098 -0.3026 252.5759 252.8785 255.6277 318.8141 -0.2955 252.7175 253.0130 255.8340 320.4240 -0.2901 252.8893 253.1794 256.0304 322.0285 -0.2877 253.0215 253.3093 256.2441 323.6325 -0.2858 253.1243 253.4100 256.5251 325.2578 -0.2843 253.2574 253.5417 256.7910 326.8625 -0.2808 253.4058 253.6865 257.0424 328.4620 -0.2824 253.5455 253.8279 257.2963 330.0659 -0.2803 253.7017 253.9821 257.5845 331.6758 -0.2781 253.8582 254.1363 257.8763 333.2805 -0.2798 254.0071 254.2869 258.1409 334.8904 -0.2763 254.1635 254.4398 258.4190 336.4950 -0.2719 254.3134 254.5854 258.6895 338.1143 -0.2741 254.4835 254.7576 258.9472 339.7190 -0.2725 254.6368 254.9092 259.1610 341.3238 -0.2716 254.8169 255.0884 259.3674 342.9080 -0.2685 255.0042 255.2727 259.5368 344.5173 -0.2664 255.1487 255.4151 259.6744 346.1216 -0.2620 255.2692 255.5311 259.8428 347.7264 -0.2615 255.4215 255.6830 259.9970 349.3311 -0.2591 255.5821 255.8413 260.1305 350.9505 -0.2557 255.7422 255.9979 260.2675 352.5601 -0.2493 255.8957 256.1450 260.4180 354.1649 -0.2405 256.0400 256.2805 260.5317 355.7746 -0.2390 256.2438 256.4829 260.7081 357.3785 -0.2352 256.4229 256.6580 260.8711 358.9884 -0.2313 256.5994 256.8307 261.1026 360.5931 -0.2355 256.7922 257.0277 261.2934 362.2133 -0.2379 256.9530 257.1909 261.5170 363.8231 -0.2381 257.1083 257.3464 261.7935 365.4270 -0.2359 257.2824 257.5184 262.0679 367.0419 -0.2324 257.4595 257.6920 262.3587 368.6415 -0.2257 257.5784 257.8040 262.6597 370.2308 -0.2256 257.7390 257.9646 262.9545 371.8346 -0.2271 257.8998 258.1269 263.2335 373.4343 -0.2315 258.0716 258.3031 263.4982 375.0595 -0.2335 258.2643 258.4978 263.7652 376.6483 -0.2359 258.4360 258.6719 264.0135 378.2526 -0.2340 258.6275 258.8615 264.2436 379.8625 -0.2302 258.7855 259.0157 264.4534 381.4670 -0.2299 258.9502 259.1802 264.6487 383.0761 -0.2230 259.1326 259.3556 264.8039 384.6809 -0.2222 259.2728 259.4950 264.9419 386.2908 -0.2233 259.4428 259.6661 265.0843 387.8798 -0.2271 259.6541 259.8812 265.2211 389.5044 -0.2250 259.8289 260.0538 265.3961 391.1143 -0.2288 260.0214 260.2502 265.5833 392.7190 -0.2285 260.2040 260.4325 265.7203 394.3280 -0.2174 260.4068 260.6242 265.8540 395.9326 -0.2113 260.5921 260.8034 265.9871 397.5425 -0.2107 260.7627 260.9733 266.1211 399.1366 -0.2084 260.9486 261.1570 266.2941 400.7459 -0.2067 261.1160 261.3226 266.5342 402.3609 -0.2128 261.2667 261.4794 266.7645 403.9603 -0.2080 261.4346 261.6427 267.0400 405.5643 -0.2044 261.6110 261.8154 267.2900 407.1639 -0.2059 261.7773 261.9832 267.5528 408.7686 -0.2081 261.9758 262.1839 267.8374 410.3783 -0.2083 262.1602 262.3685 268.1141 411.9771 -0.2083 262.3572 262.5655 268.3813 413.5973 -0.2069 262.5481 262.7550 268.6916 415.2071 -0.2065 262.7490 262.9555 268.9813 416.8114 -0.2085 262.9313 263.1398 269.2697 418.4105 -0.2138 263.1125 263.3263 269.5162 420.0153 -0.2162 263.3040 263.5203 269.7253 421.6251 -0.2215 263.4866 263.7081 269.9261 423.2299 -0.2221 263.6503 263.8724 270.1277 424.8393 -0.2199 263.8265 264.0464 270.2976 426.4589 -0.2168 264.0315 264.2483 270.4601 428.0636 -0.2067 264.2354 264.4421 270.6012 429.6735 -0.2052 264.4282 264.6334 270.7403 431.2825 -0.2081 264.6282 264.8363 270.8638 432.8923 -0.2072 264.8265 265.0337 270.9839 434.4919 -0.2079 264.9957 265.2036 271.1422 436.0915 -0.2084 265.2199 265.4283 271.3176 437.7109 -0.2097 265.3748 265.5845 271.5069 439.3154 -0.2142 265.5807 265.7949 271.6887 440.9150 -0.2121 265.7815 265.9936 271.8716 442.5249 -0.2092 265.9572 266.1664 272.0816 444.1141 -0.2107 266.1546 266.3654 272.3202 445.7231 -0.2120 266.3167 266.5287 272.5849 447.3279 -0.2142 266.5147 266.7289 272.8605 448.9378 -0.2149 266.7126 266.9274 273.1572 450.5579 -0.2152 266.9290 267.1442 273.4748 452.1616 -0.2174 267.1426 267.3600 273.7574 453.7715 -0.2172 267.3556 267.5729 274.0297 455.3763 -0.2174 267.5516 267.7690 274.3159 456.9861 -0.2207 267.7615 267.9822 274.5757 458.5905 -0.2212 267.9623 268.1835 274.8095 460.1998 -0.2225 268.1618 268.3844 275.0158 461.8096 -0.2240 268.3493 268.5732 275.1884 463.4195 -0.2221 268.5637 268.7859 275.3598 465.0236 -0.2233 268.7865 269.0098 275.5304 466.6229 -0.2250 268.9787 269.2037 275.7046 468.2328 -0.2283 269.1657 269.3940 275.8355 469.8374 -0.2290 269.3943 269.6233 275.9863 471.4361 -0.2281 269.6256 269.8537 276.1309 473.0306 -0.2270 269.8467 270.0737 276.2603 474.6303 -0.2280 270.0207 270.2488 276.4327 476.2549 -0.2301 270.2239 270.4540 276.5775 477.8593 -0.2348 270.4651 270.6999 276.7392 479.4640 -0.2385 270.6741 270.9126 276.9422 481.0736 -0.2360 270.8594 271.0954 277.1592 482.6776 -0.2347 271.0534 271.2881 277.3932 484.2875 -0.2379 271.2517 271.4896 277.6484 485.8923 -0.2392 271.4240 271.6632 277.8862 487.5175 -0.2437 271.6042 271.8479 278.1763 489.1213 -0.2443 271.8186 272.0629 278.4536 490.7260 -0.2437 272.0267 272.2704 278.7208 492.3410 -0.2445 272.2526 272.4970 279.0272 493.9454 -0.2479 272.4370 272.6849 279.3005 495.5546 -0.2505 272.6337 272.8842 279.5968 497.1594 -0.2542 272.8570 273.1112 279.8676 498.7795 -0.2523 273.0965 273.3488 280.0830 500.3680 -0.2559 273.3280 273.5839 280.2908 501.9675 -0.2608 273.5182 273.7790 280.5321 503.5774 -0.2590 273.7308 273.9898 280.7592 505.1766 -0.2602 273.9375 274.1976 280.8833 506.7808 -0.2678 274.1589 274.4267 281.0574 508.3906 -0.2696 274.3638 274.6335 281.1900 509.9954 -0.2700 274.5700 274.8400 281.3357 511.6200 -0.2692 274.7954 275.0646 281.4931 513.2244 -0.2702 275.0024 275.2727 281.5867 514.8343 -0.2722 275.1826 275.4548 281.7316 516.4390 -0.2763 275.3913 275.6676 281.8743 518.0429 -0.2779 275.6071 275.8850 282.0397 519.6526 -0.2794 275.8578 276.1372 282.2229 521.2574 -0.2778 276.1012 276.3791 282.4196 522.8826 -0.2809 276.3215 276.6024 282.6347 524.4874 -0.2815 276.5099 276.7915 282.9004 526.0965 -0.2838 276.7149 276.9987 283.1801 527.7010 -0.2879 276.9175 277.2054 283.4350 529.3058 -0.2863 277.1376 277.4240 283.7336 530.9103 -0.2879 277.3079 277.5958 284.0426 532.5143 -0.2917 277.5320 277.8237 284.3473 534.1293 -0.2935 277.7861 278.0796 284.6557 535.7238 -0.2962 278.0085 278.3048 284.9430 537.3228 -0.2997 278.2548 278.5545 285.2024 538.9323 -0.2989 278.4778 278.7767 285.4689 540.5370 -0.3015 278.6712 278.9727 285.6551 542.1413 -0.3097 278.8754 279.1851 285.8636 543.7506 -0.3114 279.1103 279.4217 286.0571 545.3554 -0.3177 279.3440 279.6617 286.2204 546.9806 -0.3191 279.5982 279.9173 286.3687 548.5848 -0.3216 279.7682 280.0898 286.5131 550.1943 -0.3266 279.9638 280.2903 286.6546 551.7990 -0.3286 280.1693 280.4980 286.7614 553.4035 -0.3284 280.3621 280.6905 286.8837 555.0126 -0.3318 280.6194 280.9512 287.0163 556.6174 -0.3369 280.8798 281.2167 287.1764 558.2426 -0.3393 281.1055 281.4447 287.3668 559.8466 -0.3390 281.3566 281.6956 287.5506 561.4563 -0.3411 281.5518 281.8929 287.7818 563.0559 -0.3417 281.7589 282.1006 288.0328 564.6555 -0.3402 281.9495 282.2897 288.2387 566.2596 -0.3451 282.1711 282.5162 288.5001 567.8640 -0.3562 282.3854 282.7417 288.7821 569.4790 -0.3630 282.6259 282.9888 289.0746 571.0889 -0.3628 282.8427 283.2055 289.3423 572.6926 -0.3651 283.0681 283.4332 289.6527 574.2974 -0.3675 283.2793 283.6468 289.9473 575.9073 -0.3724 283.5317 283.9041 290.2386 577.5115 -0.3713 283.7600 284.1313 290.5039 579.1209 -0.3757 283.9784 284.3541 290.7325 580.7410 -0.3794 284.1802 284.5596 290.9832 582.3509 -0.3809 284.3858 284.7667 291.1899 583.9549 -0.3867 284.6300 285.0167 291.3488 585.5594 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