DTA measure 3pbupdown3 Date: 2026331:1127 Lower limit = 220.0 C Upper limit = 460.0 C Rate = 10.00 C/min Mtime = 1647.91 s Mass = 959.600 mg data_number = 1025 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 2.5379 -5.2606 463.8667 469.1273 432.7099 4.1311 -5.2663 463.8101 469.0764 432.9940 5.7344 -5.2775 463.7826 469.0602 433.2358 7.3379 -5.2873 463.7463 469.0336 433.4231 8.9465 -5.2990 463.7092 469.0082 433.5354 10.5549 -5.3122 463.6632 468.9754 433.5831 12.1635 -5.3177 463.6316 468.9493 433.5245 13.7823 -5.3258 463.6096 468.9354 433.3864 15.3958 -5.3353 463.5885 468.9238 433.1765 16.9994 -5.3461 463.5383 468.8844 432.8312 18.5978 -5.3520 463.4931 468.8451 432.4684 20.2010 -5.3590 463.4715 468.8305 431.9998 21.8096 -5.3597 463.4056 468.7653 431.5245 23.4131 -5.3620 463.3886 468.7506 431.0429 25.0164 -5.3605 463.3178 468.6783 430.5474 26.6301 -5.3617 463.2803 468.6419 430.0688 28.2336 -5.3588 463.2431 468.6019 429.6229 29.8318 -5.3523 463.1889 468.5413 429.2173 31.4404 -5.3509 463.1951 468.5460 428.8092 33.0388 -5.3538 463.1209 468.4747 428.4737 34.6471 -5.3540 463.0893 468.4432 428.1841 36.2506 -5.3563 463.0169 468.3732 427.9617 37.8591 -5.3565 462.9237 468.2802 427.7884 39.4675 -5.3525 462.7986 468.1511 427.6378 41.0710 -5.3521 462.6827 468.0348 427.5674 42.6794 -5.3498 462.5924 467.9421 427.5333 44.2880 -5.3524 462.5338 467.8862 427.5314 45.8965 -5.3609 462.4848 467.8457 427.5433 47.5049 -5.3588 462.4390 467.7978 427.5264 49.1134 -5.3588 462.3156 467.6743 427.5003 50.7321 -5.3600 462.2318 467.5918 427.4689 52.3406 -5.3615 462.1435 467.5051 427.3663 53.9440 -5.3637 462.0468 467.4104 427.2260 55.5575 -5.3715 461.9660 467.3375 427.0167 57.1610 -5.3797 461.8943 467.2739 426.8332 58.7541 -5.3813 461.8501 467.2315 426.5741 60.3625 -5.3751 461.7731 467.1482 426.3374 61.9455 -5.3736 461.6712 467.0447 426.0002 63.5643 -5.3683 461.5735 466.9418 425.6608 65.1726 -5.3639 461.4620 466.8259 425.3422 66.7761 -5.3627 461.3708 466.7335 425.0063 68.3845 -5.3608 461.2933 466.6541 424.6910 69.9879 -5.3574 461.2413 466.5987 424.3443 71.5965 -5.3547 461.1562 466.5109 424.0044 73.1998 -5.3547 461.0537 466.4084 423.6850 74.8238 -5.3514 460.9570 466.3084 423.4365 76.4169 -5.3464 460.8382 466.1846 423.2282 78.0254 -5.3444 460.7208 466.0652 423.0507 79.6340 -5.3463 460.6347 465.9810 422.8639 81.2371 -5.3472 460.5139 465.8611 422.7167 82.8509 -5.3416 460.3993 465.7409 422.5579 84.4544 -5.3422 460.2555 465.5977 422.3596 86.0628 -5.3413 460.1607 465.5020 422.2327 87.6868 -5.3366 460.0418 465.3784 422.1361 89.2903 -5.3344 459.9308 465.2653 422.0348 90.8730 -5.3335 459.7849 465.1183 421.9175 92.4714 -5.3307 459.6427 464.9734 421.7565 94.0850 -5.3313 459.5128 464.8441 421.5923 95.6833 -5.3303 459.4055 464.7358 421.4335 97.2919 -5.3306 459.2386 464.5692 421.2488 98.8953 -5.3308 459.1219 464.4527 421.0081 100.4934 -5.3370 459.0266 464.3637 420.8040 102.1123 -5.3369 458.9032 464.2401 420.5656 103.7156 -5.3367 458.7707 464.1073 420.3820 105.3241 -5.3337 458.6495 463.9833 420.1230 106.9275 -5.3269 458.5629 463.8898 419.8651 108.5361 -5.3228 458.4059 463.7286 419.5814 110.1395 -5.3242 458.2602 463.5843 419.3006 111.7481 -5.3224 458.1044 463.4268 419.0153 113.3669 -5.3214 457.9532 463.2746 418.7814 114.9805 -5.3199 457.8264 463.1464 418.5236 116.5840 -5.3176 457.7182 463.0358 418.2847 118.1823 -5.3159 457.5929 462.9089 418.0370 119.7855 -5.3156 457.4492 462.7648 417.8051 121.3941 -5.3055 457.3373 462.6428 417.5910 122.9923 -5.3013 457.2104 462.5117 417.3785 124.5956 -5.2988 457.0449 462.3437 417.2077 126.2093 -5.2936 456.8954 462.1890 417.0031 127.8178 -5.2960 456.7585 462.0545 416.8281 129.4109 -5.2936 456.5921 461.8858 416.6564 131.0193 -5.2911 456.4337 461.7249 416.4654 132.6228 -5.2880 456.2583 461.5463 416.2875 134.2314 -5.2903 456.0966 461.3869 416.1459 135.8346 -5.2871 455.9576 461.2447 415.9719 137.4433 -5.2838 455.8046 461.0884 415.8131 139.0621 -5.2828 455.6502 460.9330 415.6353 140.6705 -5.2813 455.5100 460.7913 415.4749 142.2636 -5.2813 455.3463 460.6275 415.2880 143.8773 -5.2717 455.2030 460.4747 415.0702 145.4806 -5.2701 455.0638 460.3338 414.8480 147.0944 -5.2679 454.8916 460.1595 414.6327 148.6978 -5.2651 454.7073 459.9724 414.4125 150.3011 -5.2623 454.5630 459.8252 414.1760 151.9303 -5.2603 454.3750 459.6353 413.9401 153.5284 -5.2558 454.2096 459.4654 413.6697 155.1319 -5.2495 454.0498 459.2994 413.3952 156.7354 -5.2494 453.8920 459.1414 413.1634 158.3336 -5.2480 453.7425 458.9905 412.9436 159.9421 -5.2444 453.5793 458.8237 412.7133 161.5456 -5.2410 453.3749 458.6159 412.4794 163.1695 -5.2380 453.2085 458.4465 412.2204 164.7575 -5.2332 453.0906 458.3239 412.0165 166.3610 -5.2279 452.9368 458.1648 411.8157 167.9694 -5.2228 452.7554 457.9781 411.6273 169.5830 -5.2193 452.5970 457.8163 411.4193 171.1916 -5.2158 452.4547 457.6705 411.2042 172.7951 -5.2143 452.2866 457.5009 411.0336 174.4036 -5.2093 452.0917 457.3009 410.8813 176.0278 -5.1993 451.9159 457.1152 410.6612 177.6361 -5.1989 451.7248 456.9237 410.4603 179.2395 -5.1936 451.5491 456.7428 410.3219 180.8481 -5.1843 451.3980 456.5823 410.1423 182.4516 -5.1818 451.2386 456.4203 409.9360 184.0601 -5.1803 451.0565 456.2368 409.7388 185.6688 -5.1709 450.8612 456.0321 409.5384 187.2669 -5.1657 450.6850 455.8506 409.3422 188.8703 -5.1641 450.5281 455.6923 409.1255 190.4738 -5.1630 450.3348 455.4979 408.9149 192.0769 -5.1625 450.1872 455.3497 408.6886 193.6804 -5.1580 450.0281 455.1861 408.4341 195.2839 -5.1538 449.8811 455.0349 408.1797 196.8768 -5.1476 449.7036 454.8512 407.9626 198.4803 -5.1424 449.4704 454.6128 407.7448 200.0888 -5.1323 449.2671 454.3994 407.5022 201.7074 -5.1281 449.0830 454.2111 407.2635 203.3211 -5.1247 448.9038 454.0284 407.0099 204.9244 -5.1179 448.7146 453.8325 406.7819 206.5278 -5.1135 448.5092 453.6227 406.5596 208.1363 -5.1092 448.3320 453.4412 406.3600 209.7396 -5.1063 448.1925 453.2988 406.1620 211.3533 -5.1029 448.0103 453.1132 405.9480 212.9565 -5.0971 447.8216 452.9187 405.7319 214.5651 -5.0874 447.6420 452.7294 405.5746 216.1686 -5.0823 447.4606 452.5430 405.3658 217.7821 -5.0769 447.2937 452.3706 405.1573 219.3805 -5.0772 447.1241 452.2014 404.9736 220.9789 -5.0716 446.9066 451.9782 404.7970 222.5871 -5.0639 446.7301 451.7940 404.6243 224.1753 -5.0587 446.5752 451.6338 404.4232 225.7838 -5.0493 446.3530 451.4023 404.2429 227.4024 -5.0487 446.1378 451.1865 404.0480 229.0059 -5.0399 445.9584 450.9983 403.8651 230.6145 -5.0354 445.7924 450.8278 403.6861 232.2179 -5.0347 445.6145 450.6493 403.4510 233.8265 -5.0323 445.4441 450.4765 403.2094 235.4299 -5.0261 445.2397 450.2658 402.9799 237.0384 -5.0237 445.0317 450.0554 402.7363 238.6624 -5.0126 444.8395 449.8520 402.4944 240.2710 -5.0105 444.6703 449.6808 402.2874 241.8743 -5.0090 444.4558 449.4648 402.0705 243.4779 -5.0077 444.2708 449.2785 401.8451 245.0916 -5.0029 444.0838 449.0867 401.6137 246.6948 -4.9964 443.9164 448.9128 401.3552 248.3034 -4.9843 443.7298 448.7141 401.1352 249.9221 -4.9760 443.5312 448.5072 400.9266 251.5153 -4.9735 443.3338 448.3073 400.7100 253.1239 -4.9705 443.1250 448.0955 400.5192 254.7273 -4.9625 442.8665 447.8289 400.3218 256.3305 -4.9611 442.6550 447.6161 400.1286 257.9186 -4.9563 442.4688 447.4251 399.8996 259.5270 -4.9525 442.2958 447.2483 399.7018 261.1305 -4.9429 442.0938 447.0366 399.5089 262.7390 -4.9354 441.9114 446.8468 399.2919 264.3576 -4.9330 441.6951 446.6281 399.0792 265.9663 -4.9291 441.5237 446.4528 398.9214 267.5746 -4.9246 441.3157 446.2402 398.7372 269.1830 -4.9150 441.1091 446.0240 398.5348 270.7914 -4.9115 440.8821 445.7937 398.3363 272.4050 -4.9070 440.7340 445.6410 398.1501 273.9983 -4.9008 440.5548 445.4556 397.9188 275.6374 -4.8961 440.3431 445.2392 397.7574 277.2306 -4.8925 440.1423 445.0348 397.5673 278.8391 -4.8853 439.9076 444.7929 397.3297 280.4578 -4.8806 439.6466 444.5272 397.1366 282.0613 -4.8678 439.4654 444.3332 396.9118 283.6648 -4.8623 439.2824 444.1447 396.7133 285.2475 -4.8619 439.0736 443.9355 396.4719 286.8561 -4.8602 438.8467 443.7069 396.2582 288.4749 -4.8549 438.6655 443.5204 396.0236 290.0629 -4.8506 438.4725 443.3231 395.7862 291.6714 -4.8440 438.3071 443.1511 395.5661 293.2749 -4.8352 438.1243 442.9595 395.3157 294.8834 -4.8313 437.9193 442.7506 395.0615 296.4869 -4.8210 437.7043 442.5252 394.8043 298.0954 -4.8066 437.5113 442.3178 394.5360 299.6988 -4.8005 437.3314 442.1319 394.3097 301.3279 -4.7943 437.1354 441.9297 394.1254 302.9313 -4.7831 436.9291 441.7121 393.9312 304.5398 -4.7738 436.7498 441.5237 393.7016 306.1330 -4.7733 436.5432 441.3165 393.5053 307.7415 -4.7654 436.3683 441.1337 393.3373 309.3500 -4.7623 436.2174 440.9797 393.1582 310.9638 -4.7594 435.9941 440.7535 392.9887 312.5671 -4.7503 435.7504 440.5007 392.8438 314.1653 -4.7466 435.4756 440.2221 392.6835 315.7791 -4.7432 435.2630 440.0062 392.4696 317.3823 -4.7383 435.0438 439.7820 392.2851 318.9806 -4.7351 434.8643 439.5995 392.1168 320.5841 -4.7305 434.6827 439.4132 391.9240 322.1823 -4.7244 434.4924 439.2167 391.6820 323.7909 -4.7174 434.3146 439.0320 391.4472 325.3944 -4.7111 434.1124 438.8235 391.2225 326.9823 -4.7053 433.9131 438.6184 390.9904 328.6115 -4.6970 433.7148 438.4118 390.7438 330.2149 -4.6914 433.5157 438.2071 390.5263 331.8231 -4.6853 433.3526 438.0379 390.2780 333.4420 -4.6752 433.1308 437.8060 390.0206 335.0403 -4.6734 432.8915 437.5649 389.8130 336.6436 -4.6679 432.6953 437.3632 389.5812 338.2574 -4.6580 432.4759 437.1339 389.3716 339.8605 -4.6553 432.2991 436.9544 389.1707 341.4690 -4.6518 432.0891 436.7409 388.9303 343.0775 -4.6475 431.8609 436.5084 388.7360 344.6911 -4.6400 431.6378 436.2778 388.5361 346.2995 -4.6294 431.4339 436.0632 388.3299 347.8925 -4.6241 431.2385 435.8626 388.1294 349.5011 -4.6234 431.0353 435.6587 387.9220 351.1045 -4.6167 430.7955 435.4121 387.7060 352.7029 -4.6084 430.6090 435.2173 387.5362 354.3114 -4.5999 430.4128 435.0127 387.3216 355.8994 -4.5939 430.1614 434.7553 387.1270 357.5233 -4.5912 429.9340 434.5252 386.8906 359.1216 -4.5864 429.7207 434.3072 386.7087 360.7249 -4.5772 429.5187 434.0959 386.5339 362.3334 -4.5713 429.3289 433.9002 386.3147 363.9370 -4.5626 429.1275 433.6901 386.0934 365.5455 -4.5604 428.9558 433.5161 385.9055 367.1489 -4.5558 428.7319 433.2877 385.7204 368.7883 -4.5467 428.5308 433.0775 385.5177 370.3916 -4.5386 428.3093 432.8479 385.3053 372.0001 -4.5343 428.0905 432.6248 385.1006 373.6088 -4.5287 427.8717 432.4004 384.9012 375.2171 -4.5237 427.6315 432.1552 384.6835 376.8256 -4.5213 427.4376 431.9589 384.4478 378.4291 -4.5207 427.2458 431.7665 384.2372 380.0324 -4.5152 427.0340 431.5492 383.9624 381.6359 -4.5038 426.8060 431.3098 383.7079 383.2343 -4.4945 426.6005 431.0950 383.4863 384.8375 -4.4912 426.3711 430.8623 383.2589 386.4409 -4.4868 426.1598 430.6465 383.0383 388.0340 -4.4819 425.9437 430.4256 382.8282 389.6374 -4.4724 425.7427 430.2151 382.6224 391.2409 -4.4645 425.5243 429.9888 382.3824 392.8648 -4.4586 425.2943 429.7529 382.1343 394.4681 -4.4516 425.1120 429.5636 381.9116 396.0768 -4.4440 424.9061 429.3501 381.7011 397.6804 -4.4361 424.6986 429.1347 381.5263 399.2939 -4.4294 424.4665 428.8959 381.3199 400.8974 -4.4217 424.2824 428.7041 381.1412 402.5060 -4.4169 424.0853 428.5022 380.9705 404.0990 -4.4091 423.8736 428.2826 380.7675 405.7230 -4.4037 423.6758 428.0795 380.5430 407.3316 -4.3966 423.4661 427.8627 380.3866 408.9400 -4.3919 423.2715 427.6634 380.2056 410.5485 -4.3822 423.0606 427.4428 380.0207 412.1521 -4.3777 422.8487 427.2264 379.8176 413.7553 -4.3700 422.6484 427.0185 379.6012 415.3538 -4.3612 422.3989 426.7601 379.4328 416.9470 -4.3542 422.1913 426.5455 379.2262 418.5656 -4.3527 421.9991 426.3518 378.9979 420.1691 -4.3502 421.7949 426.1452 378.7741 421.7778 -4.3426 421.5571 425.8997 378.5648 423.3810 -4.3346 421.3450 425.6796 378.3575 424.9948 -4.3297 421.1348 425.4646 378.1381 426.5981 -4.3223 420.9721 425.2944 377.9050 428.2065 -4.3179 420.7523 425.0702 377.6468 429.8254 -4.3071 420.5344 424.8414 377.4294 431.4389 -4.3032 420.3215 424.6247 377.2122 433.0269 -4.3019 420.0997 424.4016 376.9933 434.6456 -4.2969 419.8769 424.1738 376.7594 436.2540 -4.2943 419.6951 423.9894 376.5338 437.8625 -4.2875 419.4918 423.7794 376.3024 439.4709 -4.2814 419.2561 423.5375 376.0797 441.0795 -4.2733 419.0049 423.2782 375.8561 442.6984 -4.2688 418.8009 423.0697 375.6192 444.2914 -4.2614 418.6213 422.8827 375.3775 445.8846 -4.2579 418.4142 422.6721 375.1905 447.4879 -4.2549 418.2130 422.4679 375.0344 449.0964 -4.2519 417.9977 422.2496 374.8708 450.6948 -4.2448 417.8043 422.0491 374.6601 452.2981 -4.2391 417.5808 421.8198 374.4687 453.9066 -4.2310 417.3629 421.5939 374.2644 455.5255 -4.2210 417.1395 421.3605 374.0685 457.1391 -4.2114 416.9315 421.1429 373.8539 458.7425 -4.2054 416.6929 420.8983 373.6114 460.3409 -4.1977 416.4635 420.6612 373.4203 461.9595 -4.1914 416.2217 420.4131 373.2023 463.5528 -4.1825 416.0529 420.2354 373.0247 465.1614 -4.1810 415.8640 420.0450 372.8401 466.7800 -4.1798 415.6877 419.8675 372.6401 468.3834 -4.1745 415.4494 419.6239 372.4142 470.0023 -4.1671 415.2099 419.3770 372.2132 471.6156 -4.1610 415.0244 419.1854 371.9869 473.2191 -4.1596 414.8366 418.9962 371.7463 474.8329 -4.1473 414.6411 418.7884 371.5495 476.4361 -4.1360 414.4204 418.5564 371.3201 478.0243 -4.1367 414.2338 418.3705 371.1033 479.6225 -4.1340 413.9684 418.1024 370.8705 481.2258 -4.1314 413.7586 417.8900 370.6421 482.8394 -4.1240 413.5385 417.6625 370.4193 484.4478 -4.1170 413.3503 417.4672 370.1874 486.0511 -4.1088 413.1495 417.2583 369.9922 487.6595 -4.1011 412.9342 417.0353 369.7929 489.2630 -4.0975 412.7196 416.8171 369.5579 490.8714 -4.0909 412.4797 416.5706 369.3103 492.4748 -4.0835 412.2124 416.2960 369.1144 494.0936 -4.0741 412.0370 416.1112 368.8957 495.7021 -4.0625 411.8089 415.8714 368.7022 497.3106 -4.0538 411.6101 415.6639 368.5196 498.9193 -4.0474 411.4020 415.4494 368.3151 500.5276 -4.0463 411.2012 415.2475 368.1590 502.1361 -4.0417 410.9643 415.0060 367.9716 503.7396 -4.0377 410.7402 414.7780 367.7331 505.3633 -4.0294 410.5255 414.5549 367.5134 506.9719 -4.0256 410.3438 414.3694 367.3204 508.5701 -4.0169 410.1607 414.1776 367.1489 510.1735 -4.0064 409.9224 413.9288 366.9387 511.7719 -4.0075 409.7318 413.7393 366.7460 513.3806 -4.0005 409.4814 413.4819 366.5512 514.9839 -3.9975 409.2516 413.2491 366.3519 516.6028 -3.9929 409.0243 413.0172 366.1238 518.2114 -3.9887 408.8332 412.8219 365.8914 519.8146 -3.9852 408.6214 412.6066 365.6814 521.4130 -3.9815 408.4075 412.3891 365.4513 523.0165 -3.9712 408.2135 412.1846 365.2238 524.6249 -3.9629 408.0106 411.9735 364.9791 526.2438 -3.9550 407.7795 411.7344 364.7210 527.8678 -3.9482 407.5832 411.5314 364.5101 529.4761 -3.9409 407.3312 411.2721 364.3119 531.0848 -3.9328 407.1329 411.0657 364.0834 532.6883 -3.9307 406.9748 410.9055 363.8796 534.2966 -3.9206 406.7576 410.6782 363.6297 535.9051 -3.9076 406.5429 410.4505 363.4142 537.5085 -3.9018 406.3234 410.2252 363.1867 539.1375 -3.8959 406.0910 409.9869 362.9676 540.7205 -3.8922 405.8577 409.7500 362.7919 542.3288 -3.8926 405.6310 409.5236 362.5926 543.9220 -3.8868 405.4555 409.3422 362.4048 545.5253 -3.8838 405.2473 409.1311 362.2371 547.1338 -3.8768 405.0095 408.8863 362.0494 548.7424 -3.8704 404.7907 408.6611 361.8391 550.3506 -3.8628 404.5510 408.4138 361.6454 551.9694 -3.8560 404.3617 408.2177 361.4200 553.5779 -3.8505 404.1425 407.9930 361.2395 555.1813 -3.8469 403.8955 407.7424 361.0268 556.7745 -3.8421 403.6585 407.5006 360.7661 558.3830 -3.8396 403.4598 407.2994 360.5461 560.0016 -3.8290 403.2256 407.0545 360.3446 561.6001 -3.8190 403.0033 406.8223 360.1343 563.2035 -3.8133 402.7975 406.6108 359.9145 564.8274 -3.8083 402.5610 406.3693 359.6747 566.4309 -3.8017 402.3846 406.1863 359.4376 568.0445 -3.7935 402.2073 406.0008 359.2409 569.6529 -3.7887 402.0367 405.8254 359.0651 571.2614 -3.7828 401.8185 405.6013 358.8668 572.8698 -3.7765 401.5861 405.3626 358.6582 574.4681 -3.7711 401.3701 405.1411 358.4423 576.0664 -3.7633 401.1516 404.9150 358.2148 577.6903 -3.7624 400.9197 404.6821 358.0266 579.2784 -3.7615 400.7295 404.4910 357.8111 580.8969 -3.7557 400.5502 404.3059 357.6008 582.5004 -3.7483 400.3518 404.1001 357.3623 584.0934 -3.7406 400.1107 403.8513 357.1204 585.6968 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