DTA measure 1fazisat Date: 2025218:110 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1019.01 s Mass = 957.200 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1555 -0.1052 242.2086 242.3138 262.8325 1.9475 -0.1085 242.2982 242.4067 262.8143 2.7695 -0.1038 242.3831 242.4869 262.7955 3.5315 -0.1027 242.4762 242.5789 262.7991 4.3835 -0.1002 242.5492 242.6494 262.7885 5.1755 -0.0997 242.6251 242.7248 262.7944 5.9675 -0.0991 242.7158 242.8148 262.8209 6.7895 -0.0982 242.8206 242.9188 262.8313 7.5515 -0.0964 242.8862 242.9827 262.8177 8.4035 -0.0956 243.0051 243.1007 262.8531 9.1955 -0.0926 243.0972 243.1898 262.8675 9.9875 -0.0907 243.1900 243.2807 262.8907 10.8095 -0.0837 243.2454 243.3291 262.9307 11.5715 -0.0840 243.3282 243.4122 262.9682 12.4235 -0.0872 243.4187 243.5059 263.0160 13.2155 -0.0865 243.5124 243.5989 263.0788 14.0075 -0.0807 243.6045 243.6853 263.1283 14.8295 -0.0815 243.6923 243.7738 263.1939 15.5915 -0.0774 243.7843 243.8617 263.2826 16.4435 -0.0771 243.8598 243.9369 263.3862 17.2053 -0.0792 243.9277 244.0069 263.4664 18.0280 -0.0778 244.0212 244.0990 263.5701 18.8500 -0.0785 244.1058 244.1843 263.6843 19.6115 -0.0756 244.1817 244.2573 263.7546 20.4640 -0.0709 244.2606 244.3314 263.8976 21.2258 -0.0751 244.3675 244.4426 263.9979 22.0478 -0.0715 244.4734 244.5449 264.1266 22.8683 -0.0730 244.5272 244.6002 264.2506 23.6260 -0.0735 244.5911 244.6646 264.3794 24.4748 -0.0693 244.6661 244.7354 264.5100 25.2323 -0.0720 244.7616 244.8336 264.6678 26.0505 -0.0750 244.8739 244.9489 264.8131 26.8690 -0.0738 244.9625 245.0364 265.0057 27.6280 -0.0739 245.0272 245.1011 265.1254 28.4763 -0.0717 245.1717 245.2435 265.3393 29.2648 -0.0731 245.2198 245.2929 265.4927 30.0540 -0.0740 245.2896 245.3635 265.6399 30.8728 -0.0772 245.3760 245.4532 265.8190 31.6628 -0.0786 245.4575 245.5361 266.0001 32.4845 -0.0751 245.5555 245.6307 266.1728 33.2765 -0.0751 245.6309 245.7061 266.3335 34.0685 -0.0789 245.7221 245.8010 266.5283 34.8905 -0.0822 245.7965 245.8787 266.7260 35.6525 -0.0842 245.9025 245.9867 266.8881 36.5045 -0.0853 245.9947 246.0801 267.0920 37.2965 -0.0880 246.0688 246.1568 267.2816 38.0898 -0.0880 246.1452 246.2332 267.4676 38.9175 -0.0920 246.2334 246.3253 267.6563 39.6795 -0.0920 246.3140 246.4061 267.8176 40.5315 -0.0909 246.4134 246.5043 268.0205 41.2933 -0.0940 246.5042 246.5982 268.1725 42.1150 -0.0964 246.6007 246.6971 268.3777 42.9373 -0.0932 246.6671 246.7603 268.5423 43.6990 -0.0961 246.7478 246.8439 268.6886 44.5510 -0.1011 246.8510 246.9521 268.9063 45.3430 -0.1040 246.9237 247.0277 269.0792 46.1345 -0.1032 247.0220 247.1252 269.2417 46.9570 -0.1091 247.1132 247.2223 269.3903 47.7490 -0.1133 247.1880 247.3012 269.5758 48.5728 -0.1134 247.2737 247.3871 269.7489 49.3660 -0.1171 247.3898 247.5069 269.9089 50.1575 -0.1179 247.4643 247.5822 270.0551 50.9800 -0.1210 247.5719 247.6929 270.2051 51.7718 -0.1254 247.6395 247.7649 270.3355 52.5945 -0.1296 247.7379 247.8675 270.5147 53.3868 -0.1324 247.8318 247.9642 270.6419 54.1795 -0.1340 247.9315 248.0655 270.7858 55.0018 -0.1343 248.0149 248.1492 270.9486 55.7913 -0.1305 248.0887 248.2191 271.0759 56.6090 -0.1374 248.1828 248.3202 271.2282 57.3973 -0.1423 248.2770 248.4193 271.3766 58.1850 -0.1423 248.3691 248.5114 271.4973 59.0033 -0.1430 248.4604 248.6034 271.6280 59.7913 -0.1458 248.5625 248.7082 271.7390 60.6093 -0.1500 248.6516 248.8016 271.8595 61.3998 -0.1486 248.7401 248.8887 271.9905 62.1890 -0.1507 248.8284 248.9791 272.1016 63.0093 -0.1544 248.9082 249.0626 272.2344 63.7993 -0.1556 248.9982 249.1538 272.3434 64.6198 -0.1590 249.0960 249.2550 272.4622 65.4120 -0.1677 249.2117 249.3794 272.5703 66.2035 -0.1693 249.3015 249.4708 272.6873 67.0305 -0.1715 249.3983 249.5699 272.7955 67.8218 -0.1737 249.5045 249.6782 272.9157 68.6438 -0.1758 249.5854 249.7611 273.0219 69.4370 -0.1732 249.6646 249.8378 273.1243 70.2285 -0.1795 249.7399 249.9194 273.2223 71.0510 -0.1754 249.8457 250.0211 273.3144 71.8125 -0.1757 249.9499 250.1256 273.4157 72.6650 -0.1771 250.0289 250.2060 273.5453 73.4570 -0.1782 250.1126 250.2907 273.6479 74.2485 -0.1822 250.2066 250.3888 273.7607 75.0710 -0.1827 250.3391 250.5218 273.8603 75.8628 -0.1849 250.4153 250.6002 273.9754 76.6848 -0.1903 250.5064 250.6967 274.0909 77.4770 -0.1900 250.5954 250.7854 274.1936 78.2685 -0.1939 250.6876 250.8815 274.2931 79.0908 -0.1944 250.7864 250.9809 274.3859 79.8825 -0.1957 250.8848 251.0805 274.4835 80.7048 -0.1995 250.9818 251.1813 274.6118 81.4968 -0.2012 251.0867 251.2879 274.7239 82.2885 -0.2043 251.1875 251.3918 274.8243 83.1110 -0.2046 251.2606 251.4652 274.9255 83.9035 -0.2060 251.3474 251.5534 275.0447 84.7273 -0.2092 251.4407 251.6498 275.1495 85.5195 -0.2121 251.5362 251.7483 275.2900 86.3115 -0.2126 251.6350 251.8475 275.4034 87.1335 -0.2168 251.7427 251.9596 275.5266 87.9230 -0.2204 251.8379 252.0583 275.6480 88.7400 -0.2195 251.9535 252.1730 275.7669 89.5280 -0.2186 252.0386 252.2572 275.8938 90.3160 -0.2227 252.1188 252.3416 276.0114 91.1340 -0.2229 252.2303 252.4532 276.1250 91.9220 -0.2255 252.3179 252.5434 276.2481 92.7410 -0.2269 252.4009 252.6278 276.3694 93.5290 -0.2303 252.4955 252.7257 276.4819 94.3180 -0.2322 252.5903 252.8226 276.5972 95.1383 -0.2344 252.6924 252.9268 276.7467 95.9285 -0.2367 252.7900 253.0266 276.8696 96.7495 -0.2395 252.8802 253.1198 276.9802 97.5418 -0.2434 252.9610 253.2045 277.1085 98.3335 -0.2452 253.0746 253.3198 277.2320 99.1553 -0.2439 253.1828 253.4267 277.3503 99.9165 -0.2467 253.2973 253.5440 277.4899 100.7690 -0.2499 253.3939 253.6439 277.6243 101.5308 -0.2550 253.4873 253.7423 277.7462 102.3525 -0.2608 253.5752 253.8361 277.8816 103.1748 -0.2627 253.6920 253.9547 278.0334 103.9365 -0.2621 253.7550 254.0171 278.1599 104.7888 -0.2619 253.8607 254.1226 278.3184 105.5505 -0.2653 253.9455 254.2108 278.4572 106.3725 -0.2689 254.0593 254.3282 278.5956 107.1645 -0.2711 254.1702 254.4413 278.7191 107.9565 -0.2774 254.2445 254.5219 278.8588 108.8088 -0.2791 254.3645 254.6436 279.0312 109.5705 -0.2814 254.4600 254.7414 279.1456 110.3928 -0.2796 254.5306 254.8103 279.3078 111.1845 -0.2849 254.6633 254.9482 279.4411 111.9765 -0.2897 254.7484 255.0381 279.5799 112.8285 -0.2924 254.8628 255.1553 279.7086 113.5905 -0.2952 254.9403 255.2355 279.8431 114.4133 -0.2970 255.0441 255.3411 280.0097 115.2055 -0.3008 255.1361 255.4368 280.1623 115.9975 -0.3057 255.2425 255.5482 280.3103 116.8495 -0.3062 255.3471 255.6533 280.4504 117.6115 -0.3049 255.4379 255.7428 280.5830 118.4335 -0.3035 255.5466 255.8501 280.7448 119.2253 -0.3103 255.6534 255.9637 280.8778 120.0148 -0.3172 255.7496 256.0668 281.0221 120.8615 -0.3186 255.8618 256.1804 281.1594 121.6220 -0.3187 255.9540 256.2727 281.3067 122.4400 -0.3206 256.0430 256.3636 281.4506 123.2285 -0.3271 256.1577 256.4848 281.5860 124.0170 -0.3282 256.2630 256.5912 281.7214 124.8650 -0.3268 256.3733 256.7002 281.8758 125.6230 -0.3329 256.4793 256.8122 282.0120 126.4433 -0.3389 256.5980 256.9369 282.1446 127.2328 -0.3382 256.6832 257.0214 282.2756 128.0220 -0.3356 256.7656 257.1012 282.4172 128.8725 -0.3398 256.8716 257.2114 282.5424 129.6345 -0.3433 256.9832 257.3265 282.6769 130.4565 -0.3473 257.0708 257.4181 282.7845 131.2488 -0.3506 257.1749 257.5256 282.9214 132.0405 -0.3563 257.2757 257.6320 283.0518 132.8925 -0.3562 257.3818 257.7380 283.1798 133.6545 -0.3575 257.5051 257.8625 283.3110 134.4765 -0.3595 257.5963 257.9558 283.4391 135.2685 -0.3656 257.6800 258.0456 283.5572 136.0605 -0.3718 257.7818 258.1536 283.6752 136.9125 -0.3712 257.9048 258.2760 283.8352 137.6745 -0.3724 258.0094 258.3818 283.9334 138.4965 -0.3738 258.0984 258.4722 284.0473 139.2885 -0.3796 258.1963 258.5759 284.1536 140.0805 -0.3794 258.3175 258.6969 284.2905 140.9325 -0.3814 258.4390 258.8204 284.4099 141.6945 -0.3847 258.5302 258.9149 284.5247 142.5165 -0.3870 258.6221 259.0091 284.6522 143.3085 -0.3892 258.7468 259.1360 284.7717 144.1005 -0.3914 258.8421 259.2335 284.8924 144.9530 -0.3958 258.9604 259.3562 285.0001 145.7155 -0.3984 259.0535 259.4519 285.1232 146.5383 -0.3995 259.1502 259.5497 285.2340 147.3305 -0.4007 259.2568 259.6575 285.3451 148.1223 -0.4023 259.3748 259.7770 285.4706 148.9745 -0.4077 259.4811 259.8889 285.5886 149.7370 -0.4104 259.5912 260.0016 285.7220 150.5588 -0.4089 259.6783 260.0873 285.8617 151.3600 -0.4132 259.7985 260.2116 285.9842 152.1483 -0.4177 259.9000 260.3177 286.1127 152.9663 -0.4203 260.0133 260.4336 286.2137 153.7545 -0.4210 260.1130 260.5340 286.3282 154.5728 -0.4230 260.1905 260.6135 286.4685 155.3608 -0.4285 260.3121 260.7406 286.5841 156.1488 -0.4294 260.4380 260.8674 286.7266 156.9985 -0.4323 260.5625 260.9948 286.8505 157.7570 -0.4351 260.6381 261.0732 286.9768 158.5775 -0.4393 260.7648 261.2040 287.1045 159.3973 -0.4400 260.8659 261.3059 287.2410 160.1583 -0.4440 260.9709 261.4148 287.3781 161.0123 -0.4446 261.1019 261.5465 287.4793 161.7775 -0.4457 261.1962 261.6419 287.6278 162.5995 -0.4491 261.2955 261.7447 287.7463 163.3915 -0.4536 261.3904 261.8441 287.8859 164.1835 -0.4547 261.5176 261.9723 288.0027 165.0355 -0.4571 261.6287 262.0858 288.1299 165.7975 -0.4642 261.7357 262.1999 288.2548 166.6195 -0.4635 261.8450 262.3086 288.3940 167.4115 -0.4664 261.9507 262.4171 288.5224 168.2035 -0.4726 262.0661 262.5387 288.6508 169.0555 -0.4727 262.1302 262.6029 288.7873 169.8175 -0.4745 262.2765 262.7510 288.8936 170.6393 -0.4770 262.3902 262.8671 289.0218 171.4613 -0.4785 262.4970 262.9755 289.1179 172.2233 -0.4807 262.6007 263.0815 289.2452 173.0753 -0.4787 262.7065 263.1852 289.4087 173.8675 -0.4837 262.8242 263.3079 289.5465 174.6585 -0.4860 262.9266 263.4126 289.6647 175.4810 -0.4914 263.0480 263.5394 289.7940 176.2425 -0.4929 263.1456 263.6385 289.9269 177.0950 -0.4938 263.2824 263.7762 290.0384 177.8870 -0.4942 263.3749 263.8690 290.1955 178.6795 -0.5005 263.4752 263.9757 290.3049 179.5023 -0.5025 263.5825 264.0850 290.4143 180.2645 -0.5048 263.7127 264.2175 290.5599 181.1175 -0.5079 263.8606 264.3686 290.7026 181.9100 -0.5096 263.9264 264.4359 290.8284 182.7015 -0.5124 264.0449 264.5573 290.9270 183.5238 -0.5123 264.1602 264.6725 291.0828 184.3143 -0.5147 264.2615 264.7762 291.2218 185.1320 -0.5136 264.3630 264.8766 291.3711 185.9210 -0.5191 264.4669 264.9860 291.5141 186.7090 -0.5241 264.5886 265.1127 291.6523 187.5273 -0.5246 264.7020 265.2266 291.8150 188.3153 -0.5263 264.8035 265.3299 291.9139 189.1340 -0.5304 264.9095 265.4399 292.0526 189.9225 -0.5316 265.0321 265.5636 292.1851 190.7110 -0.5341 265.1240 265.6581 292.3325 191.5298 -0.5371 265.2540 265.7911 292.4942 192.3183 -0.5409 265.3641 265.9050 292.6389 193.1380 -0.5441 265.4939 266.0381 292.7905 193.9290 -0.5463 265.6011 266.1474 292.9336 194.7208 -0.5505 265.7075 266.2580 293.0708 195.5430 -0.5529 265.8092 266.3621 293.2125 196.3045 -0.5554 265.9306 266.4860 293.3436 197.1570 -0.5593 266.0508 266.6101 293.5181 197.9188 -0.5597 266.1625 266.7221 293.6567 198.7408 -0.5639 266.2758 266.8397 293.8160 199.5635 -0.5659 266.4001 266.9660 293.9688 200.3255 -0.5693 266.5178 267.0871 294.1024 201.1780 -0.5779 266.6082 267.1861 294.2179 201.9398 -0.5757 266.7252 267.3009 294.3434 202.7618 -0.5713 266.8645 267.4359 294.5204 203.5540 -0.5754 266.9989 267.5743 294.6467 204.3455 -0.5808 267.0764 267.6573 294.7878 205.1980 -0.5700 267.1979 267.7679 294.9236 205.9598 -0.5688 267.2847 267.8535 295.0606 206.7818 -0.5700 267.4004 267.9704 295.1858 207.5740 -0.5720 267.5249 268.0969 295.3145 208.3655 -0.5786 267.6473 268.2259 295.4459 209.2180 -0.5803 267.7692 268.3494 295.5399 209.9795 -0.5855 267.8769 268.4623 295.6825 210.8015 -0.5895 267.9973 268.5869 295.8072 211.5938 -0.5932 268.0928 268.6860 295.9492 212.3855 -0.5953 268.2332 268.8284 296.0543 213.2078 -0.5994 268.3501 268.9496 296.1823 213.9995 -0.6027 268.4681 269.0707 296.3215 214.8218 -0.6021 268.5863 269.1883 296.4751 215.6135 -0.6052 268.6990 269.3042 296.5807 216.4048 -0.6075 268.8121 269.4196 296.7080 217.2495 -0.6094 268.9337 269.5431 296.8262 218.0088 -0.6150 269.0595 269.6745 296.9456 218.8278 -0.6149 269.1729 269.7878 297.0552 219.6160 -0.6164 269.2869 269.9033 297.1705 220.4040 -0.6182 269.3989 270.0171 297.2916 221.2520 -0.6299 269.5073 270.1372 297.4145 222.0103 -0.6525 269.6345 270.2870 297.5305 222.8300 -0.6663 269.7686 270.4348 297.6331 223.6483 -0.6645 269.8570 270.5214 297.7635 224.4088 -0.6600 269.9809 270.6408 297.8662 225.2588 -0.6630 270.1154 270.7784 297.9809 226.0198 -0.6765 270.2203 270.8969 298.1022 226.8418 -0.6679 270.3390 271.0069 298.2549 227.6638 -0.6602 270.4678 271.1281 298.3504 228.4255 -0.6600 270.5622 271.2222 298.4586 229.2780 -0.6627 270.6881 271.3508 298.5939 230.0398 -0.6629 270.8039 271.4668 298.7437 230.8618 -0.6563 270.9345 271.5908 298.8586 231.6535 -0.6555 271.0389 271.6943 298.9430 232.4455 -0.6538 271.1536 271.8074 299.0625 233.2978 -0.6560 271.2965 271.9525 299.2048 234.0595 -0.6575 271.4089 272.0664 299.3207 234.8818 -0.6559 271.5268 272.1827 299.4424 235.6738 -0.6620 271.6449 272.3069 299.5474 236.4655 -0.6651 271.7398 272.4049 299.6846 237.3188 -0.6689 271.8477 272.5166 299.8138 238.0805 -0.6718 271.9748 272.6466 299.9162 238.9028 -0.6747 272.0849 272.7596 300.0475 239.6945 -0.6760 272.2155 272.8915 300.1709 240.4865 -0.6767 272.3098 272.9865 300.2791 241.3385 -0.6755 272.4813 273.1568 300.4147 242.1005 -0.6780 272.5594 273.2374 300.5290 242.9233 -0.6920 272.7157 273.4077 300.6482 243.7173 -0.7066 272.8346 273.5412 300.7849 244.5105 -0.6948 272.9361 273.6309 300.9027 245.3325 -0.6917 273.0523 273.7440 301.0348 246.1245 -0.6927 273.1715 273.8642 301.1520 246.9465 -0.6961 273.2990 273.9951 301.2945 247.7385 -0.6965 273.4252 274.1217 301.4017 248.5290 -0.6993 273.5317 274.2310 301.5186 249.3458 -0.7031 273.6572 274.3603 301.6630 250.1345 -0.7039 273.7888 274.4927 301.7963 250.9530 -0.7048 273.8966 274.6014 301.9373 251.7410 -0.7103 273.9890 274.6993 302.0823 252.5290 -0.7105 274.1424 274.8529 302.2090 253.3470 -0.7151 274.2683 274.9834 302.3708 254.1355 -0.7121 274.3824 275.0945 302.4747 254.9548 -0.7087 274.4985 275.2071 302.6058 255.7433 -0.7091 274.6048 275.3139 302.7639 256.5333 -0.7145 274.7382 275.4527 302.8948 257.3835 -0.7203 274.8676 275.5879 302.9982 258.1755 -0.7231 274.9848 275.7080 303.1332 258.9675 -0.7298 275.1044 275.8341 303.2939 259.7895 -0.7342 275.2226 275.9568 303.4426 260.5515 -0.7370 275.3521 276.0891 303.5696 261.4035 -0.7550 275.4689 276.2238 303.7137 262.1655 -0.7609 275.5977 276.3586 303.8465 262.9878 -0.7458 275.6964 276.4422 303.9965 263.8395 -0.7458 275.8249 276.5706 304.1487 264.6015 -0.7508 275.9426 276.6934 304.2786 265.4235 -0.7518 276.0875 276.8394 304.4116 266.2155 -0.7567 276.2149 276.9716 304.5718 267.0075 -0.7597 276.3133 277.0730 304.7057 267.8595 -0.7591 276.4385 277.1977 304.8413 268.6215 -0.7636 276.5481 277.3117 304.9995 269.4435 -0.7661 276.6646 277.4307 305.1305 270.2355 -0.7686 276.8094 277.5780 305.2868 271.0275 -0.7732 276.9357 277.7089 305.4362 271.8795 -0.7738 277.0495 277.8233 305.5733 272.6415 -0.7776 277.1685 277.9461 305.6800 273.4635 -0.7780 277.2973 278.0753 305.8187 274.2663 -0.7791 277.4205 278.1996 305.9917 275.0585 -0.7852 277.5412 278.3264 306.1364 275.8805 -0.7861 277.6669 278.4530 306.2824 276.7035 -0.7944 277.7793 278.5737 306.4323 277.4950 -0.7979 277.9091 278.7070 306.5552 278.3173 -0.7988 278.0274 278.8261 306.7030 279.1090 -0.8010 278.1424 278.9434 306.8267 279.9315 -0.7995 278.2839 279.0834 306.9773 280.7208 -0.8058 278.4196 279.2254 307.0941 281.5090 -0.8124 278.5363 279.3487 307.2532 282.3270 -0.8106 278.6497 279.4603 307.3787 283.0858 -0.8103 278.7881 279.5984 307.4938 283.9355 -0.8156 278.9159 279.7314 307.6441 284.7238 -0.8174 279.0279 279.8453 307.7660 285.5118 -0.8195 279.1515 279.9711 307.8771 286.3308 -0.8246 279.2799 280.1045 307.9981 287.1203 -0.8258 279.3959 280.2218 308.1299 287.9400 -0.8346 279.5238 280.3584 308.2465 288.7295 -0.8511 279.6486 280.4997 308.3792 289.5205 -0.8522 279.7738 280.6260 308.5008 290.3425 -0.8525 279.8691 280.7217 308.6290 291.1345 -0.8552 280.0042 280.8594 308.7406 291.9565 -0.8613 280.1276 280.9889 308.8393 292.7485 -0.8646 280.2452 281.1098 308.9750 293.5405 -0.8670 280.3857 281.2527 309.0863 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403.8090 424.5071 1002.7175 -3.4905 400.4749 403.9654 424.6306 1003.5400 -3.4907 400.6304 404.1210 424.7625 1004.3318 -3.4923 400.7534 404.2456 424.8759 1005.1538 -3.4874 400.8820 404.3694 425.0379 1005.9460 -3.4914 401.0202 404.5116 425.1779 1006.7978 -3.4944 401.2016 404.6960 425.3313 1007.7105 -3.5055 401.3391 404.8447 425.4630 1008.5628 -3.5099 401.4857 404.9956 425.6232 1009.3245 -3.5166 401.6156 405.1322 425.7512 1010.1468 -3.5172 401.7590 405.2762 425.8845 1010.9385 -3.5132 401.9048 405.4180 426.0403 1011.7305 -3.5158 402.0465 405.5623 426.2007 1012.5828 -3.5289 402.1907 405.7196 426.3292 1013.3445 -3.5349 402.3320 405.8668 426.4455 1014.1668 -3.5377 402.4661 406.0038 426.5818 1014.9888 -3.5386 402.5983 406.1369 426.7160 1015.7505 -3.5409 402.7448 406.2857 426.8616 1016.6025 -3.5483 402.8911 406.4395 427.0197 1017.3645 -3.5541 403.0176 406.5717 427.1367 1018.1865 -3.5562 403.1579 406.7141 427.2552 1019.0085 -3.5614 403.2922 406.8536 427.4012