DTA measure 1lassu Date: 2025218:1149 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 1399.60 s Mass = 957.200 mg data_number = 1736 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1590 0.5884 263.8944 263.3059 251.7610 1.9205 0.5883 263.8540 263.2657 251.6444 2.7735 0.5855 263.7894 263.2040 251.5373 3.5358 0.5793 263.7361 263.1569 251.4240 4.3578 0.5811 263.6786 263.0975 251.3154 5.1800 0.5799 263.6204 263.0405 251.1959 5.9390 0.5817 263.5784 262.9968 251.0740 6.7873 0.5742 263.5083 262.9341 250.9656 7.5453 0.5733 263.4707 262.8974 250.8708 8.3633 0.5897 263.4085 262.8188 250.7580 9.1815 0.5956 263.3507 262.7551 250.6751 9.9395 0.5952 263.2958 262.7006 250.5829 10.7893 0.5919 263.2250 262.6331 250.4933 11.5478 0.5895 263.1790 262.5894 250.4153 12.3675 0.5904 263.1272 262.5368 250.3193 13.1868 0.5948 263.0833 262.4886 250.2653 13.9470 0.5966 263.0271 262.4305 250.1866 14.7985 0.5882 262.9747 262.3866 250.1244 15.5605 0.5903 262.9455 262.3552 250.0574 16.3825 0.5934 262.8981 262.3047 250.0153 17.1745 0.5971 262.8720 262.2749 249.9795 17.9665 0.5986 262.7830 262.1844 249.9069 18.8183 0.5959 262.7267 262.1308 249.8732 19.5805 0.5949 262.6679 262.0730 249.8592 20.4023 0.5963 262.6099 262.0136 249.8357 21.1943 0.5983 262.5824 261.9841 249.8137 21.9855 0.5991 262.5272 261.9281 249.7937 22.8080 0.6039 262.4618 261.8580 249.7807 23.6008 0.6111 262.4044 261.7932 249.7801 24.4248 0.6166 262.3707 261.7542 249.8185 25.2175 0.6162 262.3199 261.7037 249.8334 26.0085 0.6139 262.2806 261.6667 249.8551 26.8313 0.6134 262.2155 261.6021 249.8839 27.6228 0.6119 262.1843 261.5723 249.9091 28.4448 0.6094 262.0990 261.4896 249.9502 29.2370 0.6117 262.0635 261.4518 249.9903 30.0318 0.6263 262.0109 261.3845 250.0355 30.8545 0.6278 261.9461 261.3182 250.1136 31.6155 0.6310 261.9110 261.2800 250.1706 32.4708 0.6253 261.8695 261.2443 250.2353 33.2348 0.6229 261.7973 261.1743 250.3246 34.0568 0.6254 261.7551 261.1297 250.4314 34.8798 0.6182 261.6853 261.0671 250.4914 35.6438 0.6221 261.6548 261.0327 250.6044 36.4968 0.6233 261.6071 260.9838 250.6943 37.2585 0.6084 261.5578 260.9495 250.7944 38.0808 0.6032 261.5101 260.9069 250.8716 38.8985 0.6064 261.4558 260.8494 251.0088 39.6565 0.6053 261.4119 260.8066 251.1064 40.5110 0.6104 261.3611 260.7507 251.2519 41.2690 0.6092 261.2990 260.6898 251.3561 42.0870 0.6001 261.2404 260.6403 251.4875 42.8758 0.5939 261.2286 260.6347 251.6229 43.6655 0.5769 261.1835 260.6066 251.7427 44.5143 0.5855 261.1515 260.5659 251.8929 45.2720 0.5835 261.1009 260.5174 252.0193 46.0908 0.5825 261.0515 260.4691 252.1445 46.8800 0.5845 261.0085 260.4240 252.2858 47.6693 0.5793 260.9848 260.4055 252.4231 48.5228 0.5808 260.9259 260.3450 252.5751 49.2840 0.5789 260.8909 260.3120 252.7379 50.1058 0.5708 260.8355 260.2647 252.8527 50.8990 0.5820 260.7872 260.2052 253.0077 51.6915 0.5787 260.7399 260.1612 253.1409 52.5140 0.5690 260.7216 260.1525 253.2739 53.3058 0.5585 260.6855 260.1270 253.4359 54.1278 0.5585 260.6485 260.0900 253.6013 54.9253 0.5588 260.6143 260.0555 253.7250 55.7193 0.5621 260.5667 260.0046 253.8658 56.5418 0.5520 260.5457 259.9937 254.0087 57.3035 0.5450 260.5178 259.9728 254.1604 58.1558 0.5434 260.4706 259.9272 254.3192 58.9175 0.5397 260.4154 259.8757 254.4601 59.7395 0.5355 260.3791 259.8436 254.5923 60.5615 0.5301 260.3331 259.8031 254.7349 61.3235 0.5310 260.3372 259.8062 254.8569 62.1758 0.5326 260.3083 259.7757 255.0139 62.9375 0.5278 260.2485 259.7207 255.1458 63.7595 0.5203 260.2018 259.6815 255.2752 64.5818 0.5178 260.1778 259.6601 255.4011 65.3435 0.5170 260.1515 259.6345 255.5197 66.1955 0.5091 260.1167 259.6076 255.6665 66.9585 0.5107 260.0906 259.5799 255.7772 67.7805 0.5071 260.0600 259.5530 255.9390 68.6025 0.4983 260.0331 259.5347 256.0495 69.3645 0.4926 260.0159 259.5233 256.1536 70.2150 0.4890 259.9830 259.4939 256.2798 70.9730 0.4853 259.9376 259.4523 256.3841 71.7908 0.4833 259.9026 259.4194 256.5033 72.6088 0.4858 259.8764 259.3906 256.6346 73.3670 0.4819 259.8508 259.3689 256.7464 74.2150 0.4805 259.8319 259.3514 256.8775 74.9730 0.4770 259.7989 259.3219 256.9693 75.7910 0.4715 259.7743 259.3028 257.0749 76.6090 0.4666 259.7578 259.2912 257.1918 77.3670 0.4633 259.7267 259.2634 257.2765 78.2165 0.4613 259.7005 259.2391 257.3762 79.0050 0.4540 259.6709 259.2169 257.4771 79.7950 0.4514 259.6326 259.1812 257.5738 80.6165 0.4533 259.6275 259.1743 257.6570 81.3785 0.4469 259.6035 259.1566 257.7415 82.2305 0.4448 259.5762 259.1314 257.8483 83.0225 0.4397 259.5422 259.1025 257.9127 83.8145 0.4360 259.5213 259.0854 258.0034 84.6368 0.4470 259.5320 259.0850 258.0873 85.3985 0.4423 259.5025 259.0602 258.1742 86.2505 0.4457 259.4840 259.0383 258.2660 87.0133 0.4386 259.4460 259.0074 258.3275 87.8375 0.4223 259.4260 259.0038 258.4065 88.6595 0.3720 259.4142 259.0422 258.4854 89.4215 0.3488 259.3926 259.0438 258.5801 90.2735 0.3385 259.3695 259.0310 258.6588 91.0355 0.3351 259.3487 259.0136 258.7231 91.8575 0.3332 259.3376 259.0044 258.7938 92.6795 0.3309 259.3248 258.9939 258.8758 93.4445 0.3340 259.3294 258.9953 258.9554 94.3005 0.3355 259.3050 258.9694 259.0367 95.0625 0.3299 259.2726 258.9427 259.1045 95.8845 0.3351 259.2633 258.9282 259.1803 96.7065 0.3838 259.2750 258.8912 259.2546 97.4685 0.3868 259.2484 258.8616 259.3144 98.3205 0.3841 259.2326 258.8486 259.4229 99.0825 0.3843 259.2057 258.8214 259.4994 99.9050 0.3905 259.2070 258.8165 259.5667 100.6975 0.3893 259.2143 258.8249 259.6487 101.4895 0.3763 259.1925 258.8162 259.7214 102.3410 0.3693 259.1869 258.8176 259.7992 103.0993 0.3700 259.1672 258.7971 259.8716 103.9178 0.3715 259.1261 258.7546 259.9633 104.7063 0.3662 259.1259 258.7597 260.0647 105.4948 0.3631 259.1169 258.7538 260.1236 106.3425 0.3574 259.1184 258.7611 260.2362 107.1018 0.3556 259.1210 258.7654 260.2803 107.9200 0.3539 259.0979 258.7440 260.3639 108.7383 0.3444 259.0886 258.7442 260.4576 109.4993 0.3353 259.0791 258.7438 260.5416 110.3495 0.3321 259.0560 258.7239 260.6489 111.1083 0.3268 259.0454 258.7186 260.7264 111.9283 0.3232 259.0587 258.7355 260.8255 112.7245 0.3103 259.0453 258.7350 260.9389 113.5165 0.3069 259.0367 258.7298 261.0326 114.3385 0.3031 259.0334 258.7304 261.1256 115.1305 0.2957 259.0303 258.7346 261.2148 115.9525 0.2901 259.0340 258.7438 261.3078 116.7445 0.2859 259.0114 258.7255 261.3938 117.5365 0.2857 259.0135 258.7278 261.4718 118.3585 0.2817 259.0158 258.7341 261.5814 119.1505 0.2828 259.0217 258.7389 261.6728 119.9725 0.2819 259.0112 258.7293 261.7829 120.7645 0.2778 259.0002 258.7223 261.8855 121.5565 0.2732 258.9938 258.7205 261.9727 122.3785 0.2773 258.9981 258.7208 262.0707 123.1405 0.2843 258.9978 258.7135 262.1997 123.9925 0.2803 258.9863 258.7061 262.3019 124.7845 0.2847 258.9843 258.6996 262.3853 125.5758 0.2944 259.0052 258.7108 262.4811 126.3983 0.2934 258.9935 258.7001 262.5865 127.1903 0.2909 259.0044 258.7136 262.6646 128.0118 0.2870 258.9944 258.7074 262.7705 128.8040 0.2862 258.9865 258.7003 262.8683 129.5955 0.2857 258.9769 258.6912 262.9579 130.4180 0.2853 259.0105 258.7252 263.0802 131.2098 0.2834 259.0200 258.7367 263.1909 132.0325 0.2780 258.9946 258.7167 263.3104 132.8250 0.2744 258.9985 258.7241 263.4097 133.6165 0.2697 259.0268 258.7571 263.5207 134.4385 0.2679 259.0297 258.7618 263.6208 135.2270 0.2677 259.0281 258.7604 263.7206 136.0430 0.2643 259.0389 258.7746 263.8374 136.8310 0.2603 259.0313 258.7710 263.9720 137.6203 0.2568 259.0372 258.7804 264.0631 138.4385 0.2537 259.0452 258.7915 264.1849 139.2268 0.2507 259.0542 258.8035 264.2995 140.0453 0.2472 259.0540 258.8068 264.4171 140.8335 0.2423 259.0647 258.8225 264.5216 141.6210 0.2339 259.0896 258.8557 264.6309 142.4700 0.2391 259.1115 258.8724 264.7385 143.2290 0.2342 259.1029 258.8687 264.8629 144.0483 0.2301 259.1072 258.8772 264.9749 144.8698 0.2307 259.1361 258.9054 265.0842 145.6300 0.2292 259.1344 258.9052 265.1991 146.4873 0.2259 259.1413 258.9154 265.3079 147.2493 0.2279 259.1423 258.9145 265.4200 148.0710 0.2251 259.1546 258.9295 265.5504 148.8658 0.2242 259.1675 258.9433 265.6364 149.6590 0.2182 259.1820 258.9637 265.7572 150.5110 0.2137 259.2036 258.9899 265.8875 151.2728 0.2087 259.2299 259.0212 265.9912 152.0948 0.2076 259.2211 259.0135 266.1135 152.8880 0.2023 259.2400 259.0378 266.2213 153.6795 0.2053 259.2641 259.0588 266.3354 154.5020 0.2050 259.2732 259.0682 266.4558 155.2938 0.2020 259.2954 259.0934 266.5741 156.1165 0.1962 259.3194 259.1232 266.7065 156.9090 0.1938 259.3161 259.1223 266.8034 157.7005 0.1897 259.3567 259.1670 266.9011 158.5530 0.1880 259.3581 259.1701 267.0102 159.3148 0.1861 259.3602 259.1741 267.1335 160.1375 0.1856 259.3923 259.2067 267.2356 160.9300 0.1860 259.4045 259.2185 267.3226 161.7215 0.1812 259.4149 259.2337 267.4183 162.5440 0.1767 259.4365 259.2597 267.5176 163.3365 0.1735 259.4715 259.2980 267.6050 164.1595 0.1777 259.4819 259.3042 267.7196 164.9545 0.1776 259.4952 259.3176 267.8165 165.7505 0.1735 259.5151 259.3416 267.9066 166.5725 0.1663 259.5557 259.3894 268.0106 167.3343 0.1617 259.5794 259.4177 268.0888 168.1820 0.1586 259.5966 259.4380 268.1900 168.9710 0.1584 259.6175 259.4591 268.2831 169.7590 0.1537 259.6367 259.4830 268.3683 170.5770 0.1519 259.6353 259.4834 268.4670 171.3350 0.1530 259.6689 259.5159 268.5510 172.1820 0.1565 259.7049 259.5484 268.6357 172.9710 0.1543 259.7285 259.5742 268.7233 173.7600 0.1503 259.7340 259.5837 268.8256 174.5785 0.1472 259.7593 259.6121 268.8960 175.3373 0.1421 259.7965 259.6545 268.9867 176.1888 0.1393 259.8076 259.6683 269.0895 176.9788 0.1396 259.8352 259.6956 269.1798 177.7700 0.1388 259.8668 259.7280 269.2757 178.5930 0.1320 259.8936 259.7615 269.3830 179.3545 0.1271 259.9151 259.7880 269.4529 180.2070 0.1266 259.9531 259.8264 269.5663 180.9688 0.1241 259.9727 259.8486 269.6636 181.7908 0.1223 259.9930 259.8707 269.7280 182.6130 0.1223 260.0244 259.9021 269.8243 183.3745 0.1213 260.0636 259.9423 269.9095 184.2268 0.1183 260.1002 259.9819 270.0042 184.9888 0.1111 260.1057 259.9947 270.0865 185.8108 0.1076 260.1412 260.0335 270.1793 186.6043 0.1071 260.1892 260.0821 270.2882 187.3975 0.1100 260.2123 260.1023 270.3637 188.2498 0.1066 260.2159 260.1094 270.4739 189.0115 0.1035 260.2589 260.1553 270.5736 189.8338 0.0994 260.3039 260.2045 270.6525 190.6255 0.0980 260.3369 260.2388 270.7358 191.4175 0.0967 260.3599 260.2631 270.8275 192.2698 0.0944 260.3638 260.2694 270.9586 193.0315 0.0925 260.4205 260.3280 271.0391 193.8545 0.0885 260.4560 260.3675 271.1388 194.6465 0.0904 260.4929 260.4025 271.2393 195.4385 0.0825 260.5063 260.4238 271.3363 196.2905 0.0827 260.5618 260.4791 271.4541 197.0525 0.0778 260.6004 260.5226 271.5256 197.8745 0.0745 260.6124 260.5379 271.6303 198.6665 0.0684 260.6592 260.5907 271.7475 199.4578 0.0641 260.6918 260.6277 271.8646 200.3053 0.0599 260.7259 260.6660 271.9756 201.0630 0.0564 260.7510 260.6946 272.0861 201.8810 0.0594 260.7920 260.7327 272.1727 202.6690 0.0561 260.8286 260.7725 272.2545 203.4570 0.0580 260.8647 260.8067 272.3535 204.3050 0.0543 260.9160 260.8616 272.4877 205.0630 0.0499 260.9461 260.8962 272.5939 205.8823 0.0476 260.9641 260.9165 272.6775 206.7013 0.0452 261.0208 260.9756 272.7883 207.4603 0.0438 261.0632 261.0194 272.9195 208.3105 0.0394 261.1011 261.0616 273.0287 209.1013 0.0379 261.1211 261.0832 273.1231 209.8923 0.0299 261.1627 261.1328 273.2373 210.7135 0.0226 261.2007 261.1781 273.3527 211.4755 0.0175 261.2657 261.2483 273.4263 212.3278 0.0169 261.2853 261.2684 273.5380 213.0895 0.0246 261.3251 261.3005 273.6482 213.9115 0.0257 261.3612 261.3355 273.7715 214.7338 0.0292 261.4079 261.3787 273.8639 215.4955 0.0267 261.4502 261.4235 273.9612 216.3478 0.0270 261.4964 261.4694 274.0980 217.1398 0.0219 261.5355 261.5136 274.1969 217.9315 0.0200 261.5671 261.5471 274.2738 218.7538 0.0158 261.6224 261.6066 274.4114 219.5155 0.0133 261.6717 261.6584 274.4979 220.3675 0.0130 261.7036 261.6906 274.6166 221.1595 0.0108 261.7325 261.7217 274.7404 221.9525 0.0092 261.8009 261.7916 274.8531 222.7748 0.0068 261.8540 261.8472 274.9234 223.5375 0.0018 261.8899 261.8881 275.0285 224.3895 -0.0049 261.9181 261.9230 275.1341 225.1815 -0.0080 261.9584 261.9665 275.2373 225.9745 -0.0077 262.0114 262.0190 275.3365 226.7965 -0.0110 262.0528 262.0638 275.4394 227.5585 -0.0108 262.0851 262.0959 275.5468 228.4105 -0.0105 262.1376 262.1481 275.6635 229.2025 -0.0170 262.1824 262.1994 275.7660 229.9955 -0.0214 262.2457 262.2670 275.8773 230.8173 -0.0231 262.3019 262.3250 275.9853 231.5778 -0.0225 262.3352 262.3577 276.0791 232.4265 -0.0265 262.3938 262.4203 276.1922 233.2148 -0.0320 262.4333 262.4653 276.2903 234.0025 -0.0348 262.4727 262.5074 276.3802 234.8210 -0.0362 262.5242 262.5605 276.4979 235.5788 -0.0413 262.5681 262.6094 276.5876 236.4270 -0.0456 262.6153 262.6609 276.6908 237.2150 -0.0441 262.6523 262.6965 276.7869 238.0040 -0.0436 262.7031 262.7467 276.8831 238.8228 -0.0404 262.7528 262.7933 276.9840 239.5828 -0.0434 262.8261 262.8695 277.0827 240.4343 -0.0426 262.8831 262.9258 277.1935 241.2255 -0.0443 262.9095 262.9538 277.2990 242.0175 -0.0473 262.9696 263.0170 277.3929 242.8395 -0.0529 263.0038 263.0567 277.4602 243.6015 -0.0537 263.0797 263.1335 277.5639 244.4535 -0.0573 263.1200 263.1773 277.6789 245.2155 -0.0594 263.1552 263.2146 277.7755 246.0375 -0.0608 263.2058 263.2666 277.8709 246.8595 -0.0551 263.2800 263.3351 277.9481 247.6815 -0.0562 263.3342 263.3904 278.0454 248.5945 -0.0605 263.3809 263.4414 278.1792 249.4465 -0.0663 263.4367 263.5030 278.2892 250.2385 -0.0679 263.4831 263.5510 278.3774 251.0305 -0.0695 263.5422 263.6117 278.4617 251.8525 -0.0731 263.6070 263.6801 278.5581 252.6145 -0.0749 263.6586 263.7335 278.6468 253.4665 -0.0776 263.7133 263.7909 278.7497 254.2585 -0.0811 263.7689 263.8500 278.8537 255.0505 -0.0821 263.8402 263.9223 278.9452 255.8723 -0.0854 263.8785 263.9639 279.0305 256.6338 -0.0910 263.9101 264.0011 279.1298 257.4860 -0.0914 263.9517 264.0431 279.2364 258.2780 -0.0931 264.0092 264.1023 279.3427 259.0695 -0.0951 264.0628 264.1579 279.4370 259.8923 -0.0989 264.1568 264.2557 279.5600 260.6545 -0.1012 264.2008 264.3020 279.6485 261.5070 -0.1010 264.2735 264.3745 279.7643 262.2688 -0.1052 264.3159 264.4211 279.8707 263.0908 -0.1065 264.3771 264.4835 279.9769 263.9070 -0.1104 264.4281 264.5385 280.0897 264.6660 -0.1113 264.4761 264.5874 280.1659 265.5140 -0.1122 264.5622 264.6744 280.2845 266.3023 -0.1156 264.6173 264.7329 280.3905 267.0900 -0.1180 264.6551 264.7730 280.5054 267.9135 -0.1156 264.7122 264.8278 280.6089 268.6715 -0.1223 264.7773 264.8996 280.7227 269.5200 -0.1222 264.8307 264.9528 280.8394 270.2783 -0.1254 264.8881 265.0135 280.9446 271.0975 -0.1222 264.9437 265.0658 281.0486 271.9170 -0.1220 265.0174 265.1394 281.1670 272.7983 -0.1354 265.0805 265.2159 281.2806 273.5890 -0.1422 265.1249 265.2671 281.3742 274.3808 -0.1445 265.1858 265.3302 281.4816 275.2033 -0.1486 265.2590 265.4076 281.5785 275.9648 -0.1521 265.3020 265.4541 281.6673 276.8173 -0.1569 265.3795 265.5364 281.8264 277.5793 -0.1579 265.4335 265.5914 281.9165 278.4010 -0.1589 265.4998 265.6587 282.0385 279.1935 -0.1602 265.5534 265.7136 282.1419 279.9850 -0.1635 265.6266 265.7901 282.2558 280.8373 -0.1608 265.6879 265.8487 282.3595 281.5988 -0.1565 265.7386 265.8951 282.4611 282.4208 -0.1553 265.8056 265.9609 282.5596 283.2130 -0.1589 265.8725 266.0314 282.6638 284.0648 -0.1619 265.9442 266.1061 282.7924 284.9775 -0.1635 266.0265 266.1900 282.9379 285.8300 -0.1671 266.0871 266.2541 283.0361 286.5918 -0.1710 266.1344 266.3054 283.1372 287.4138 -0.1706 266.2039 266.3745 283.2497 288.2060 -0.1715 266.2650 266.4366 283.3733 289.0578 -0.1732 266.3340 266.5072 283.4731 289.8495 -0.1852 266.4165 266.6017 283.5629 290.6718 -0.1915 266.4533 266.6448 283.6815 291.4335 -0.1947 266.5156 266.7103 283.7916 292.2858 -0.1970 266.6060 266.8030 283.9227 293.0778 -0.2019 266.6608 266.8627 284.0167 293.8705 -0.2038 266.7309 266.9347 284.1298 294.6930 -0.2088 266.7906 266.9994 284.2216 295.4555 -0.2143 266.8471 267.0614 284.3342 296.3080 -0.2118 266.9155 267.1273 284.4341 297.0970 -0.2158 267.0114 267.2272 284.5530 297.8850 -0.2182 267.0664 267.2846 284.6553 298.7030 -0.2176 267.1115 267.3291 284.7915 299.4610 -0.2232 267.1565 267.3797 284.8817 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