DTA measure 1olom lassu fel-le Date: 20241210:117 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 10.00 C/min Mtime = 1018.44 s Mass = 959.100 mg data_number = 1267 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 1.1115 0.4875 223.2309 222.7433 265.7792 1.9035 0.4945 223.5035 223.0090 265.7809 2.7560 0.5051 223.7901 223.2851 265.7958 3.4968 0.5086 224.0186 223.5099 265.8069 4.3450 0.5099 224.3069 223.7971 265.8403 5.1330 0.5086 224.5572 224.0486 265.8334 5.9210 0.5099 224.8508 224.3409 265.8527 6.7398 0.5134 225.1208 224.6074 265.8747 7.5290 0.5117 225.3607 224.8490 265.9021 8.3478 0.5509 225.6517 225.1008 265.9577 9.1363 0.5467 225.8840 225.3374 265.9992 9.9260 0.5271 226.1329 225.6059 266.0376 10.7450 0.5315 226.4232 225.8917 266.1172 11.5365 0.5244 226.6875 226.1631 266.1829 12.3585 0.5224 226.9437 226.4213 266.2706 13.1505 0.5233 227.1915 226.6682 266.3536 13.9418 0.5235 227.4312 226.9077 266.4291 14.7635 0.5304 227.7226 227.1922 266.5422 15.5555 0.5242 227.9728 227.4486 266.6513 16.3775 0.5159 228.2310 227.7151 266.7666 17.1695 0.5202 228.4951 227.9748 266.8750 17.9615 0.5221 228.7261 228.2040 267.0103 18.7835 0.5241 228.9822 228.4581 267.1634 19.5755 0.5278 229.2334 228.7056 267.3083 20.3975 0.5284 229.4741 228.9457 267.4717 21.1895 0.5299 229.7473 229.2174 267.6314 21.9815 0.5278 229.9854 229.4575 267.7881 22.8035 0.5262 230.2467 229.7205 267.9601 23.5783 0.5253 230.4855 229.9602 268.1102 24.4133 0.5249 230.7611 230.2362 268.2860 25.2053 0.5253 230.9889 230.4637 268.4517 26.0268 0.5249 231.2369 230.7120 268.6266 26.8190 0.5444 231.4886 230.9442 268.8047 27.6115 0.5255 231.7278 231.2023 268.9633 28.4338 0.5292 231.9816 231.4524 269.1650 29.2255 0.5381 232.2182 231.6801 269.3287 30.0485 0.5216 232.4638 231.9422 269.5068 30.8408 0.5141 232.6950 232.1809 269.6625 31.6325 0.5129 232.9489 232.4360 269.8261 32.4853 0.5141 233.2155 232.7014 269.9752 33.2475 0.5155 233.4462 232.9308 270.1291 34.0705 0.5101 233.6984 233.1883 270.2818 34.8628 0.5062 233.9207 233.4145 270.4441 35.6520 0.5190 234.1604 233.6414 270.5807 36.5000 0.5091 234.4398 233.9307 270.7476 37.2583 0.5025 234.6465 234.1439 270.8764 38.0770 0.4957 234.8797 234.3840 271.0128 38.8655 0.4957 235.1053 234.6096 271.1574 39.6550 0.4901 235.3583 234.8682 271.2788 40.5030 0.4894 235.6167 235.1274 271.4359 41.2613 0.4872 235.8277 235.3405 271.5624 42.0818 0.4830 236.0659 235.5829 271.7093 42.9033 0.4843 236.3132 235.8289 271.8398 43.6645 0.4798 236.5434 236.0636 271.9705 44.5200 0.4808 236.7855 236.3047 272.1090 45.2800 0.4796 237.0102 236.5306 272.2273 46.1018 0.4724 237.2506 236.7782 272.3664 46.8938 0.4687 237.4764 237.0077 272.5076 47.6855 0.4671 237.7049 237.2378 272.6357 48.5378 0.4619 237.9459 237.4840 272.7707 49.2995 0.4789 238.1480 237.6691 272.9010 50.1218 0.4606 238.4117 237.9511 273.0386 50.9138 0.4550 238.6324 238.1774 273.1789 51.7055 0.4502 238.8482 238.3980 273.2999 52.5578 0.4450 239.0977 238.6527 273.4289 53.3195 0.4403 239.3166 238.8763 273.5529 54.1425 0.4378 239.5543 239.1165 273.6808 54.9648 0.4332 239.7889 239.3556 273.8193 55.7265 0.4270 239.9987 239.5718 273.9501 56.5785 0.4212 240.2312 239.8100 274.0869 57.3405 0.4201 240.4420 240.0219 274.2172 58.1625 0.4126 240.6840 240.2715 274.3417 58.9845 0.4122 240.9132 240.5010 274.4657 59.7465 0.4090 241.1330 240.7240 274.5989 60.5985 0.4255 241.3685 240.9430 274.7554 61.3905 0.3919 241.5816 241.1898 274.8702 62.1835 0.3793 241.7852 241.4059 275.0144 63.0058 0.3867 242.0261 241.6394 275.1400 63.7685 0.3885 242.2373 241.8488 275.2684 64.6208 0.3756 242.4521 242.0764 275.4026 65.4135 0.3718 242.7022 242.3303 275.5265 66.2058 0.3666 242.9314 242.5647 275.6715 67.0280 0.3615 243.1427 242.7813 275.7960 67.7873 0.3583 243.3441 242.9858 275.9251 68.6360 0.3565 243.5885 243.2320 276.0698 69.3945 0.3511 243.7924 243.4413 276.1837 70.2128 0.3451 244.0080 243.6629 276.3200 71.0310 0.3377 244.2266 243.8888 276.4545 71.7895 0.3326 244.4258 244.0932 276.5733 72.6385 0.3452 244.6463 244.3010 276.7241 73.3980 0.3458 244.8677 244.5218 276.8377 74.2180 0.3249 245.0919 244.7670 276.9616 75.0380 0.3142 245.3152 245.0010 277.1064 75.7990 0.3121 245.5137 245.2016 277.2141 76.6495 0.3062 245.7394 245.4332 277.3894 77.4115 0.3029 245.9538 245.6509 277.5019 78.2335 0.3013 246.1626 245.8613 277.6326 79.0255 0.2954 246.3958 246.1005 277.7590 79.8170 0.2918 246.5907 246.2989 277.8949 80.6695 0.2824 246.8040 246.5216 278.0346 81.4315 0.2934 247.0127 246.7193 278.1494 82.2533 0.2812 247.2440 246.9628 278.2871 83.0450 0.2734 247.4406 247.1673 278.4060 83.8368 0.2658 247.6422 247.3764 278.5389 84.6590 0.2633 247.8652 247.6018 278.6876 85.4508 0.2641 248.0719 247.8078 278.8040 86.2728 0.2581 248.2763 248.0181 278.9279 87.0650 0.2478 248.4795 248.2317 279.0554 87.8565 0.2445 248.6964 248.4519 279.1896 88.6788 0.2446 248.9185 248.6740 279.3217 89.4705 0.2371 249.1227 248.8856 279.4433 90.2928 0.2292 249.3320 249.1029 279.5830 91.0848 0.2248 249.5527 249.3279 279.7065 91.8775 0.2194 249.7523 249.5328 279.8397 92.6998 0.2138 249.9445 249.7306 279.9606 93.4915 0.2100 250.1668 249.9568 280.0939 94.3145 0.2024 250.3790 250.1767 280.2326 95.1068 0.1982 250.5705 250.3724 280.3609 95.8985 0.1926 250.7861 250.5935 280.4672 96.7205 0.1877 250.9865 250.7988 280.6083 97.4825 0.1810 251.1894 251.0083 280.7395 98.3350 0.1755 251.3729 251.1974 280.8890 99.1278 0.1727 251.5965 251.4237 281.0186 99.9203 0.1671 251.8094 251.6423 281.1270 100.7400 0.1619 252.0056 251.8437 281.2508 101.4980 0.1533 252.1844 252.0312 281.3796 102.3460 0.1444 252.3924 252.2480 281.5267 103.1340 0.1407 252.6029 252.4622 281.6384 103.9230 0.1805 252.8032 252.6227 281.7675 104.7415 0.2855 253.0154 252.7299 281.9108 105.5300 0.1728 253.2059 253.0331 282.0230 106.3490 0.1405 253.4160 253.2755 282.1436 107.1373 0.1267 253.6093 253.4826 282.2777 107.9285 0.1193 253.7968 253.6775 282.3903 108.7505 0.1095 253.9944 253.8849 282.5210 109.5120 0.1086 254.1989 254.0903 282.6240 110.3635 0.1094 254.4132 254.3038 282.7770 111.1558 0.1032 254.6128 254.5097 282.9112 111.9475 0.0943 254.8105 254.7162 283.0413 112.7695 0.0893 255.0102 254.9210 283.1629 113.5315 0.0821 255.1799 255.0978 283.2936 114.3835 0.0790 255.4055 255.3265 283.4509 115.1755 0.0753 255.5973 255.5220 283.5798 115.9675 0.0685 255.7842 255.7157 283.7187 116.7895 0.0599 255.9885 255.9286 283.8619 117.5515 0.0606 256.1698 256.1092 284.0001 118.4035 0.0537 256.3884 256.3348 284.1532 119.1955 0.0463 256.5901 256.5437 284.2996 119.9875 0.0432 256.7601 256.7169 284.4488 120.8095 0.0383 256.9657 256.9274 284.5875 121.5715 0.0370 257.1548 257.1178 284.7321 122.4235 0.0303 257.3663 257.3360 284.8836 123.2153 0.0277 257.5593 257.5315 285.0225 124.0073 0.0204 257.7667 257.7463 285.1693 124.8295 0.0161 257.9461 257.9299 285.3361 125.5915 0.0104 258.1351 258.1247 285.4669 126.4440 0.0062 258.3149 258.3087 285.5924 127.2360 0.0174 258.5098 258.4924 285.7242 128.0285 0.0166 258.6789 258.6623 285.8693 128.8508 -0.0035 258.8950 258.8985 286.0074 129.6425 -0.0143 259.0786 259.0929 286.1321 130.4648 -0.0199 259.2840 259.3040 286.2776 131.2568 -0.0163 259.4810 259.4973 286.4085 132.0493 -0.0251 259.6694 259.6945 286.5292 132.8678 -0.0176 259.8586 259.8762 286.6484 133.6550 0.0039 260.0567 260.0528 286.7789 134.4740 0.0258 260.2410 260.2152 286.8914 135.2628 0.1946 260.4309 260.2363 287.0232 136.0520 0.0930 260.6275 260.5345 287.1603 136.8700 0.0142 260.7925 260.7783 287.2761 137.6580 -0.0101 260.9826 260.9928 287.3924 138.4770 0.0037 261.1877 261.1841 287.5299 139.2658 0.0116 261.3695 261.3579 287.6571 140.0563 -0.0129 261.5576 261.5705 287.7536 140.9070 -0.0340 261.7655 261.7995 287.9034 141.6685 -0.0148 261.9345 261.9493 288.0058 142.4908 -0.0002 262.1407 262.1409 288.1484 143.2828 -0.0103 262.3051 262.3154 288.2618 144.0745 -0.0446 262.4769 262.5215 288.3708 144.9268 -0.0562 262.6679 262.7241 288.5058 145.6885 -0.0398 262.8675 262.9073 288.6296 146.5108 -0.0169 263.0505 263.0674 288.7627 147.3028 -0.0268 263.2394 263.2662 288.8949 148.0945 -0.0481 263.4112 263.4593 289.0050 148.9468 -0.0692 263.6121 263.6813 289.1614 149.7085 -0.1152 263.7948 263.9100 289.2915 150.5308 -0.1519 263.9664 264.1183 289.4294 151.3228 -0.1664 264.1493 264.3157 289.5508 152.1145 -0.1763 264.3376 264.5139 289.6917 152.9668 -0.1807 264.5465 264.7272 289.8256 153.7285 -0.1847 264.7171 264.9018 289.9661 154.5508 -0.1676 264.9166 265.0841 290.1105 155.3728 -0.1671 265.0917 265.2588 290.2632 156.1345 -0.1832 265.2644 265.4476 290.3808 156.9873 -0.2090 265.4597 265.6687 290.5501 157.7495 -0.2212 265.6338 265.8550 290.6781 158.5715 -0.2293 265.8172 266.0465 290.8191 159.3938 -0.2299 265.9970 266.2269 290.9520 160.1565 -0.2309 266.1623 266.3932 291.0956 161.0090 -0.2295 266.3617 266.5912 291.2327 161.7715 -0.2361 266.5458 266.7819 291.3783 162.5935 -0.2436 266.7225 266.9661 291.5433 163.4158 -0.2494 266.9115 267.1609 291.7093 164.1775 -0.2413 267.0893 267.3306 291.8280 165.0255 -0.2384 267.2849 267.5233 291.9801 165.7840 -0.2403 267.4461 267.6864 292.1225 166.6018 -0.2463 267.6408 267.8871 292.2764 167.3898 -0.2515 267.8140 268.0655 292.4063 168.1790 -0.2627 267.9890 268.2517 292.5432 169.0275 -0.2650 268.1813 268.4464 292.6811 169.7860 -0.2711 268.3511 268.6221 292.8159 170.6048 -0.2801 268.5240 268.8041 292.9417 171.4233 -0.2661 268.7173 268.9834 293.0557 172.1845 -0.2079 268.8723 269.0802 293.1759 173.0365 -0.2715 269.0680 269.3394 293.3114 173.7985 -0.2927 269.2481 269.5408 293.4264 174.6205 -0.3055 269.4360 269.7415 293.5519 175.4125 -0.3040 269.6086 269.9126 293.6716 176.2045 -0.3129 269.7897 270.1026 293.7883 177.0265 -0.3234 269.9592 270.2826 293.9254 177.7885 -0.3286 270.1353 270.4638 294.0415 178.6405 -0.3322 270.3221 270.6543 294.1671 179.4325 -0.3418 270.4883 270.8300 294.2709 180.2245 -0.3480 270.6599 271.0078 294.3846 181.0465 -0.3516 270.8556 271.2072 294.5036 181.8083 -0.3570 271.0258 271.3828 294.6032 182.6600 -0.3618 271.2162 271.5780 294.7432 183.4223 -0.3665 271.3845 271.7510 294.8574 184.2438 -0.3687 271.5540 271.9227 294.9831 185.0660 -0.3705 271.7375 272.1080 295.1032 185.8278 -0.3717 271.9146 272.2863 295.2309 186.6800 -0.3798 272.0968 272.4766 295.3715 187.4423 -0.3889 272.2558 272.6447 295.5121 188.2668 -0.3960 272.4379 272.8339 295.6393 189.0890 -0.4034 272.6179 273.0214 295.7913 189.8515 -0.4071 272.7884 273.1955 295.9248 190.7038 -0.4072 272.9683 273.3755 296.0604 191.4655 -0.4089 273.1367 273.5456 296.1852 192.2878 -0.4100 273.3018 273.7118 296.3095 193.0798 -0.4229 273.4828 273.9057 296.4653 193.8715 -0.4301 273.6573 274.0874 296.6006 194.7238 -0.4353 273.8297 274.2650 296.7406 195.4855 -0.4412 273.9854 274.4266 296.8772 196.3070 -0.4482 274.1642 274.6124 296.9997 197.0950 -0.4531 274.3357 274.7888 297.1432 197.8830 -0.4529 274.5040 274.9568 297.2845 198.7310 -0.4582 274.6996 275.1578 297.4215 199.4890 -0.4641 274.8718 275.3360 297.5507 200.3075 -0.4652 275.0444 275.5095 297.6767 201.0963 -0.4716 275.2199 275.6916 297.8117 201.8858 -0.4766 275.3730 275.8496 297.9591 202.7345 -0.4815 275.5386 276.0201 298.0966 203.4940 -0.4891 275.7058 276.1949 298.2330 204.3143 -0.4959 275.8863 276.3822 298.3727 205.1055 -0.4781 276.0690 276.5471 298.4911 205.8968 -0.4742 276.2342 276.7084 298.6311 206.7188 -0.4920 276.4011 276.8932 298.7864 207.5105 -0.5028 276.5744 277.0772 298.9146 208.3328 -0.5090 276.7438 277.2528 299.0557 209.1245 -0.5170 276.9193 277.4363 299.1870 209.9165 -0.5219 277.0828 277.6047 299.3165 210.7388 -0.5282 277.2627 277.7909 299.4435 211.5305 -0.5323 277.4325 277.9648 299.5817 212.3528 -0.5360 277.6268 278.1628 299.7272 213.1448 -0.5427 277.7791 278.3217 299.8477 213.9365 -0.5514 277.9450 278.4964 299.9827 214.7585 -0.5529 278.1208 278.6737 300.1332 215.5205 -0.5559 278.2792 278.8350 300.2699 216.3725 -0.5611 278.4564 279.0175 300.4079 217.1645 -0.5650 278.6290 279.1940 300.5315 217.9578 -0.5692 278.7845 279.3537 300.6805 218.7858 -0.5715 278.9629 279.5344 300.8077 219.5485 -0.5780 279.1131 279.6910 300.9261 220.4005 -0.5850 279.2903 279.8753 301.0709 221.1625 -0.5898 279.4681 280.0579 301.2013 221.9845 -0.5935 279.6370 280.2306 301.3435 222.8068 -0.5988 279.7881 280.3869 301.4870 223.5693 -0.6025 279.9556 280.5581 301.6203 224.4215 -0.6068 280.1445 280.7512 301.7652 225.1840 -0.6059 280.2956 280.9016 301.8880 226.0058 -0.6105 280.4656 281.0761 302.0209 226.8283 -0.6197 280.6410 281.2607 302.1662 227.5905 -0.6229 280.8112 281.4340 302.2806 228.4433 -0.6233 280.9782 281.6015 302.4357 229.2048 -0.6280 281.1378 281.7658 302.5471 230.0233 -0.6321 281.3125 281.9446 302.6863 230.8115 -0.6329 281.4857 282.1187 302.8187 231.5990 -0.6376 281.6562 282.2939 302.9481 232.4470 -0.6459 281.8322 282.4781 303.0763 233.2053 -0.6500 281.9715 282.6215 303.2023 234.0245 -0.6526 282.1284 282.7810 303.3478 234.8433 -0.6578 282.3079 282.9657 303.4832 235.6020 -0.6610 282.4704 283.1313 303.6063 236.4520 -0.6676 282.6366 283.3042 303.7540 237.2120 -0.6722 282.8019 283.4741 303.8889 238.0340 -0.6764 282.9599 283.6362 304.0125 238.8563 -0.6814 283.1320 283.8133 304.1423 239.6178 -0.6870 283.2964 283.9834 304.2657 240.4700 -0.6896 283.4796 284.1692 304.4128 241.2318 -0.6937 283.6360 284.3297 304.5345 242.0538 -0.6951 283.7913 284.4864 304.6596 242.8760 -0.6978 283.9598 284.6576 304.8014 243.6375 -0.7046 284.1238 284.8284 304.9236 244.4898 -0.7091 284.2898 284.9989 305.0765 245.2518 -0.7112 284.4505 285.1617 305.1974 246.0738 -0.7151 284.6018 285.3170 305.3232 246.8958 -0.7230 284.7742 285.4972 305.4492 247.6575 -0.7269 284.9505 285.6773 305.5878 248.5098 -0.7177 285.1154 285.8332 305.7231 249.3018 -0.6793 285.2862 285.9655 305.8479 250.0935 -0.6691 285.4462 286.1153 305.9687 250.9158 -0.6647 285.5983 286.2630 306.1191 251.6775 -0.6763 285.7598 286.4361 306.2567 252.5298 -0.6927 285.9290 286.6217 306.3922 253.3215 -0.6968 286.0914 286.7881 306.5131 254.1135 -0.7082 286.2586 286.9668 306.6259 254.9360 -0.6006 286.4315 287.0321 306.7881 255.6985 -0.4244 286.5971 287.0215 306.9030 256.5505 -0.6448 286.7644 287.4092 307.0414 257.3425 -0.6936 286.9292 287.6228 307.1746 258.1345 -0.7130 287.0913 287.8042 307.2950 258.9565 -0.7163 287.2520 287.9683 307.4288 259.7485 -0.7153 287.4146 288.1299 307.5610 260.5705 -0.7157 287.5802 288.2958 307.6817 261.3613 -0.7174 287.7312 288.4486 307.7985 262.1495 -0.7231 287.8943 288.6174 307.9253 262.9680 -0.7228 288.0670 288.7897 308.0569 263.7560 -0.7250 288.2311 288.9562 308.1890 264.5740 -0.7323 288.4120 289.1444 308.3046 265.3620 -0.7321 288.5687 289.3008 308.4442 266.1510 -0.7379 288.7216 289.4595 308.5631 266.9693 -0.7357 288.8803 289.6160 308.6878 267.7590 -0.7412 289.0314 289.7726 308.8213 268.5785 -0.5469 289.1976 289.7445 308.9545 269.3690 -0.5816 289.3511 289.9326 309.0590 270.1598 -0.7028 289.5172 290.2200 309.1956 270.9815 -0.7362 289.6734 290.4096 309.3354 271.7435 -0.7699 289.8252 290.5951 309.4516 272.5955 -0.7283 289.9917 290.7200 309.5708 273.3875 -0.7484 290.1565 290.9049 309.7031 274.1795 -0.7790 290.3308 291.1098 309.8259 275.0015 -0.7802 290.4876 291.2678 309.9331 275.7635 -0.7333 290.6382 291.3715 310.0604 276.6155 -0.7748 290.8010 291.5758 310.1676 277.3775 -0.7690 290.9611 291.7302 310.2952 278.1995 -0.7689 291.1368 291.9058 310.4259 279.0215 -0.7732 291.2830 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