DTA measure 4őlom gyors fel-le Date: 20241210:1216 Lower limit = 220.0 C Upper limit = 450.0 C Rate = 8.00 C/min Mtime = 132.40 s Mass = 959.100 mg data_number = 659 Time [s] dT [C] Temp_sample. [C] Temp_ref. [C] Temp_f. [C] 0.3330 -4.6268 439.0895 443.7163 424.2941 0.5170 -4.6089 439.0947 443.7036 424.2874 0.6990 -4.6089 439.0918 443.7008 424.2808 0.8820 -4.6096 439.0898 443.6993 424.2828 1.0650 -4.6195 439.1049 443.7244 424.2851 1.2480 -4.6228 439.1112 443.7341 424.2880 1.4310 -4.6301 439.1217 443.7518 424.2944 1.7340 -4.6359 439.1146 443.7505 424.2906 1.9180 -4.6396 439.1268 443.7664 424.2733 2.1000 -4.6413 439.1298 443.7711 424.2801 2.2830 -4.6439 439.1404 443.7842 424.2792 2.4660 -4.6461 439.1335 443.7797 424.2737 2.6490 -4.6487 439.1534 443.8022 424.2660 2.9520 -4.6495 439.1775 443.8270 424.2744 3.1360 -4.6494 439.1779 443.8274 424.2708 3.3180 -4.6518 439.1761 443.8278 424.2888 3.5010 -4.6522 439.1879 443.8401 424.2862 3.6840 -4.6548 439.1865 443.8413 424.2875 3.8670 -4.6561 439.1904 443.8465 424.2756 4.0500 -4.6578 439.2145 443.8723 424.2885 4.3530 -4.6562 439.2085 443.8646 424.2801 4.5370 -4.6553 439.2055 443.8608 424.2809 4.7190 -4.6548 439.2204 443.8753 424.2761 4.9020 -4.6573 439.2346 443.8919 424.2784 5.0850 -4.6579 439.2448 443.9026 424.2810 5.2680 -4.6568 439.2295 443.8863 424.2794 5.4510 -4.6588 439.2273 443.8861 424.2801 5.7540 -4.6566 439.2563 443.9129 424.2897 5.9370 -4.6559 439.2775 443.9335 424.2855 6.1200 -4.6591 439.2953 443.9544 424.2852 6.3030 -4.6615 439.3049 443.9664 424.2841 6.4860 -4.6654 439.2977 443.9630 424.2819 6.6690 -4.6658 439.3021 443.9679 424.2851 6.9720 -4.6688 439.3083 443.9771 424.2789 7.1560 -4.6703 439.3231 443.9934 424.2770 7.3380 -4.6709 439.3226 443.9934 424.2749 7.5210 -4.6705 439.3172 443.9877 424.2760 7.7040 -4.6726 439.3367 444.0093 424.2776 7.8870 -4.6738 439.3387 444.0125 424.2775 8.0700 -4.6731 439.3440 444.0171 424.2760 8.3730 -4.6733 439.3475 444.0208 424.2629 8.5560 -4.6727 439.3498 444.0225 424.2541 8.7390 -4.6751 439.3499 444.0249 424.2501 8.9220 -4.6744 439.3533 444.0277 424.2341 9.1050 -4.6749 439.3500 444.0249 424.2358 9.2880 -4.6761 439.3520 444.0282 424.2225 9.4710 -4.6757 439.3546 444.0303 424.2302 9.7740 -4.6773 439.3652 444.0425 424.2423 9.9570 -4.6787 439.3876 444.0663 424.2329 10.1400 -4.6807 439.3953 444.0760 424.2251 10.3230 -4.6780 439.3859 444.0640 424.2220 10.5060 -4.6810 439.4005 444.0816 424.2233 10.6890 -4.6804 439.3975 444.0779 424.2053 10.8720 -4.6791 439.4032 444.0823 424.1891 11.1750 -4.6797 439.4089 444.0886 424.1749 11.3580 -4.6793 439.4049 444.0842 424.1698 11.5410 -4.6799 439.4229 444.1028 424.1670 11.7240 -4.6798 439.4340 444.1138 424.1610 11.9070 -4.6804 439.4284 444.1088 424.1616 12.0900 -4.6786 439.4396 444.1182 424.1578 12.3930 -4.6779 439.4397 444.1176 424.1480 12.5760 -4.6810 439.4464 444.1274 424.1370 12.7590 -4.6831 439.4473 444.1304 424.1284 12.9420 -4.6843 439.4496 444.1339 424.1207 13.1250 -4.6868 439.4689 444.1557 424.1186 13.3080 -4.6915 439.4772 444.1688 424.1105 13.4910 -4.6945 439.4792 444.1737 424.0928 13.7940 -4.7025 439.4783 444.1808 424.0948 13.9770 -4.7027 439.5007 444.2034 424.0735 14.1600 -4.7029 439.5011 444.2039 424.0579 14.3430 -4.7025 439.5145 444.2170 424.0549 14.5260 -4.7033 439.5007 444.2040 424.0572 14.7090 -4.7041 439.5164 444.2206 424.0433 14.8920 -4.7051 439.5159 444.2210 424.0287 15.1950 -4.7032 439.5361 444.2392 424.0219 15.3780 -4.7046 439.5331 444.2377 424.0088 15.5610 -4.7064 439.5371 444.2434 423.9931 15.7440 -4.7083 439.5645 444.2728 423.9760 15.9270 -4.7098 439.5567 444.2665 423.9640 16.1100 -4.7120 439.5637 444.2757 423.9525 16.4130 -4.7123 439.5765 444.2887 423.9219 16.5960 -4.7123 439.5782 444.2905 423.9189 16.7790 -4.7112 439.5787 444.2900 423.9070 16.9620 -4.7107 439.5718 444.2826 423.9003 17.1440 -4.7127 439.5949 444.3076 423.9039 17.3270 -4.7145 439.5837 444.2982 423.8883 17.5100 -4.7146 439.5821 444.2967 423.8675 17.8140 -4.7151 439.5923 444.3075 423.8365 17.9970 -4.7177 439.6077 444.3254 423.8357 18.1800 -4.7167 439.6049 444.3216 423.8201 18.3620 -4.7165 439.5953 444.3118 423.8116 18.5450 -4.7174 439.6058 444.3232 423.7871 18.7280 -4.7185 439.6150 444.3335 423.7750 18.9110 -4.7191 439.6225 444.3416 423.7438 19.2150 -4.7205 439.6177 444.3382 423.7217 19.3980 -4.7221 439.6231 444.3453 423.7107 19.5800 -4.7231 439.6185 444.3416 423.7041 19.7630 -4.7197 439.6279 444.3477 423.6857 19.9460 -4.7215 439.6352 444.3566 423.6644 20.1290 -4.7227 439.6349 444.3577 423.6664 20.3120 -4.7229 439.6370 444.3599 423.6487 20.6150 -4.7242 439.6592 444.3834 423.6211 20.7990 -4.7236 439.6594 444.3830 423.6211 20.9810 -4.7256 439.6756 444.4012 423.5987 21.1640 -4.7256 439.6818 444.4074 423.5774 21.3470 -4.7258 439.6891 444.4148 423.5630 21.5320 -4.7283 439.6857 444.4140 423.5396 21.8340 -4.7280 439.6935 444.4215 423.5137 22.0180 -4.7275 439.6941 444.4216 423.5001 22.2000 -4.7305 439.7090 444.4395 423.4822 22.3830 -4.7316 439.7077 444.4392 423.4625 22.5660 -4.7301 439.7174 444.4475 423.4383 22.7490 -4.7298 439.7179 444.4477 423.4180 22.9320 -4.7297 439.7125 444.4422 423.4122 23.2350 -4.7306 439.7105 444.4411 423.3777 23.4190 -4.7321 439.7176 444.4497 423.3644 23.6010 -4.7326 439.7143 444.4470 423.3584 23.7840 -4.7346 439.7132 444.4478 423.3474 23.9670 -4.7345 439.7107 444.4452 423.3230 24.1500 -4.7355 439.7420 444.4775 423.2960 24.3330 -4.7346 439.7399 444.4744 423.2779 24.6360 -4.7332 439.7582 444.4914 423.2432 24.8200 -4.7353 439.7574 444.4927 423.2281 25.0020 -4.7353 439.7626 444.4979 423.2187 25.1850 -4.7364 439.7705 444.5069 423.2067 25.3680 -4.7393 439.7662 444.5056 423.1960 25.5510 -4.7394 439.7633 444.5027 423.1764 25.8540 -4.7379 439.7773 444.5151 423.1471 26.0380 -4.7386 439.7772 444.5158 423.1374 26.2200 -4.7384 439.7882 444.5265 423.1210 26.4030 -4.7417 439.7919 444.5336 423.1024 26.5860 -4.7430 439.8032 444.5462 423.0853 26.7690 -4.7447 439.7905 444.5352 423.0741 26.9520 -4.7441 439.7882 444.5322 423.0621 27.2550 -4.7422 439.7830 444.5253 423.0289 27.4390 -4.7436 439.7938 444.5374 422.9973 27.6210 -4.7454 439.8016 444.5470 422.9763 27.8040 -4.7460 439.8116 444.5576 422.9577 27.9870 -4.7476 439.8249 444.5724 422.9343 28.1700 -4.7459 439.8277 444.5736 422.9076 28.4730 -4.7434 439.8223 444.5657 422.8738 28.6570 -4.7458 439.8252 444.5710 422.8720 28.8400 -4.7475 439.8358 444.5833 422.8639 29.0230 -4.7479 439.8437 444.5917 422.8503 29.2060 -4.7482 439.8244 444.5726 422.8426 29.3890 -4.7487 439.8305 444.5792 422.8230 29.5720 -4.7494 439.8352 444.5846 422.7986 29.8750 -4.7468 439.8384 444.5852 422.7651 30.0590 -4.7454 439.8504 444.5959 422.7462 30.2420 -4.7437 439.8547 444.5984 422.7304 30.4250 -4.7497 439.8709 444.6207 422.7027 30.6080 -4.7500 439.8635 444.6135 422.6865 30.7910 -4.7484 439.8719 444.6203 422.6865 30.9740 -4.7467 439.8792 444.6259 422.6635 31.2770 -4.7505 439.8679 444.6184 422.6402 31.4600 -4.7521 439.8734 444.6255 422.6118 31.6430 -4.7522 439.8770 444.6292 422.5966 31.8260 -4.7536 439.8753 444.6290 422.5706 32.0090 -4.7546 439.8899 444.6445 422.5656 32.1920 -4.7557 439.8842 444.6400 422.5443 32.3750 -4.7573 439.8857 444.6430 422.5279 32.6780 -4.7567 439.8874 444.6441 422.4863 32.8610 -4.7567 439.8846 444.6414 422.4651 33.0440 -4.7557 439.8997 444.6554 422.4579 33.2270 -4.7570 439.8969 444.6539 422.4333 33.4100 -4.7569 439.8985 444.6554 422.4084 33.5930 -4.7565 439.9091 444.6656 422.3818 33.8960 -4.7553 439.9308 444.6861 422.3557 34.0790 -4.7528 439.9241 444.6770 422.3365 34.2630 -4.7506 439.9302 444.6808 422.3239 34.4460 -4.7508 439.9516 444.7024 422.3156 34.6290 -4.7491 439.9430 444.6921 422.3098 34.8120 -4.7509 439.9333 444.6841 422.2901 34.9950 -4.7545 439.9347 444.6891 422.2777 35.2980 -4.7562 439.9250 444.6811 422.2424 35.4810 -4.7578 439.9224 444.6802 422.2317 35.6640 -4.7570 439.9404 444.6975 422.2198 35.8470 -4.7554 439.9362 444.6916 422.2050 36.0300 -4.7586 439.9361 444.6947 422.1927 36.2130 -4.7599 439.9243 444.6842 422.1662 36.3960 -4.7617 439.9347 444.6964 422.1533 36.6990 -4.7629 439.9286 444.6915 422.1236 36.8820 -4.7639 439.9375 444.7014 422.1083 37.0650 -4.7649 439.9405 444.7054 422.1029 37.2480 -4.7649 439.9518 444.7166 422.1058 37.4310 -4.7657 439.9627 444.7284 422.0711 37.6140 -4.7657 439.9583 444.7240 422.0544 37.9170 -4.7668 439.9676 444.7344 422.0064 38.1000 -4.7655 439.9675 444.7330 421.9918 38.2840 -4.7628 439.9683 444.7311 421.9667 38.4660 -4.7647 439.9602 444.7249 421.9465 38.6490 -4.7655 439.9687 444.7342 421.9287 38.8330 -4.7671 439.9635 444.7306 421.9006 39.0150 -4.7698 439.9591 444.7289 421.8955 39.3190 -4.7722 439.9684 444.7405 421.8810 39.5020 -4.7729 439.9650 444.7378 421.8696 39.6840 -4.7730 439.9748 444.7478 421.8528 39.8670 -4.7719 439.9793 444.7511 421.8336 40.0500 -4.7715 439.9817 444.7532 421.8229 40.2330 -4.7703 439.9850 444.7553 421.7974 40.4160 -4.7730 439.9760 444.7490 421.7704 40.7190 -4.7733 439.9998 444.7731 421.7447 40.9030 -4.7731 440.0086 444.7818 421.7390 41.0850 -4.7740 440.0041 444.7781 421.7105 41.2680 -4.7780 439.9970 444.7750 421.6973 41.4510 -4.7820 439.9920 444.7739 421.6812 41.6340 -4.7800 439.9909 444.7709 421.6648 41.9370 -4.7793 439.9982 444.7774 421.6425 42.1190 -4.7768 439.9807 444.7575 421.6353 42.3010 -4.7733 439.9882 444.7616 421.6253 42.4830 -4.7753 439.9897 444.7650 421.6021 42.6650 -4.7768 439.9864 444.7632 421.5895 42.8470 -4.7775 439.9910 444.7685 421.5757 43.0340 -4.7770 439.9977 444.7747 421.5578 43.3400 -4.7752 440.0190 444.7942 421.5422 43.5220 -4.7716 440.0118 444.7834 421.5266 43.7040 -4.7688 440.0102 444.7791 421.5110 43.8860 -4.7688 440.0191 444.7880 421.5020 44.0680 -4.7713 440.0168 444.7881 421.4835 44.2500 -4.7648 440.0075 444.7722 421.4824 44.4320 -4.7584 440.0098 444.7682 421.4608 44.7350 -4.7555 440.0249 444.7804 421.4116 44.9170 -4.7498 440.0103 444.7602 421.3973 45.0990 -4.7551 440.0189 444.7740 421.3984 45.2810 -4.7648 440.0390 444.8038 421.3800 45.4630 -4.7663 440.0322 444.7985 421.3755 45.6450 -4.7688 440.0434 444.8121 421.3664 45.8270 -4.7390 440.0314 444.7704 421.3570 46.1290 -4.7197 440.0209 444.7406 421.3526 46.3120 -4.7237 440.0304 444.7540 421.3449 46.4930 -4.7340 440.0231 444.7571 421.3322 46.6750 -4.7388 440.0360 444.7748 421.3226 46.8570 -4.7426 440.0448 444.7874 421.3154 47.0390 -4.7504 440.0376 444.7881 421.2971 47.3420 -4.7578 440.0359 444.7937 421.2691 47.5230 -4.7619 440.0593 444.8212 421.2572 47.7050 -4.7593 440.0353 444.7946 421.2426 47.8870 -4.7609 440.0394 444.8003 421.2342 48.0690 -4.7671 440.0411 444.8082 421.2135 48.2510 -4.7711 440.0400 444.8111 421.2013 48.4330 -4.7731 440.0432 444.8163 421.1791 48.7360 -4.7770 440.0351 444.8121 421.1716 48.9180 -4.7780 440.0318 444.8098 421.1522 49.1000 -4.7787 440.0319 444.8107 421.1387 49.2820 -4.7793 440.0236 444.8029 421.1182 49.4640 -4.7802 440.0247 444.8049 421.1102 49.6460 -4.7818 440.0212 444.8029 421.1044 49.8280 -4.7816 440.0369 444.8185 421.0804 50.1300 -4.7851 440.0386 444.8237 421.0794 50.3120 -4.7836 440.0305 444.8141 421.0841 50.4940 -4.7834 440.0322 444.8156 421.0774 50.6760 -4.7827 440.0344 444.8171 421.0709 50.8580 -4.7844 440.0310 444.8153 421.0595 51.0400 -4.7855 440.0452 444.8307 421.0524 51.3430 -4.7873 440.0520 444.8393 421.0249 51.5260 -4.7888 440.0458 444.8346 421.0091 51.7080 -4.7889 440.0505 444.8394 420.9996 51.8900 -4.7893 440.0499 444.8392 420.9825 52.0720 -4.7879 440.0421 444.8300 420.9585 52.2540 -4.7892 440.0465 444.8357 420.9547 52.4360 -4.7874 440.0478 444.8351 420.9567 52.7380 -4.7828 440.0443 444.8271 420.9357 52.9210 -4.7843 440.0614 444.8457 420.9291 53.1030 -4.7849 440.0520 444.8369 420.9113 53.2850 -4.7850 440.0458 444.8308 420.9098 53.4670 -4.7862 440.0396 444.8257 420.9008 53.6490 -4.7834 440.0431 444.8265 420.8913 53.9510 -4.7868 440.0347 444.8215 420.8644 54.1330 -4.7881 440.0499 444.8380 420.8543 54.3160 -4.7896 440.0512 444.8408 420.8408 54.4990 -4.7849 440.0498 444.8347 420.8372 54.6810 -4.7807 440.0331 444.8139 420.8239 54.8630 -4.7782 440.0325 444.8107 420.8104 55.0450 -4.7754 440.0321 444.8075 420.7900 55.3470 -4.7775 440.0381 444.8156 420.7660 55.5310 -4.7749 440.0355 444.8103 420.7513 55.7130 -4.7770 440.0318 444.8088 420.7348 55.8960 -4.7827 440.0470 444.8297 420.7297 56.0780 -4.7847 440.0342 444.8189 420.7110 56.2610 -4.7877 440.0388 444.8265 420.6906 56.4440 -4.7912 440.0462 444.8374 420.6788 56.7460 -4.7925 440.0419 444.8344 420.6565 56.9290 -4.7934 440.0424 444.8357 420.6380 57.1110 -4.7865 440.0413 444.8277 420.6234 57.2940 -4.7766 440.0335 444.8102 420.6181 57.4770 -4.7758 440.0347 444.8105 420.6035 57.6590 -4.7789 440.0372 444.8161 420.5915 57.9610 -4.7878 440.0445 444.8323 420.5769 58.1440 -4.7898 440.0412 444.8310 420.5919 58.3260 -4.7924 440.0405 444.8328 420.5736 58.5090 -4.7911 440.0434 444.8345 420.5567 58.6920 -4.7792 440.0512 444.8305 420.5364 58.8750 -4.7707 440.0363 444.8070 420.5205 59.0570 -4.7694 440.0300 444.7994 420.5010 59.3600 -4.7793 440.0488 444.8281 420.4796 59.5430 -4.7822 440.0353 444.8175 420.4646 59.7260 -4.7880 440.0461 444.8341 420.4652 59.9090 -4.7918 440.0361 444.8279 420.4546 60.0920 -4.7936 440.0385 444.8321 420.4478 60.2750 -4.7885 440.0422 444.8308 420.4423 60.4580 -4.7892 440.0421 444.8313 420.4152 60.7610 -4.7832 440.0357 444.8189 420.3991 60.9440 -4.7525 440.0249 444.7774 420.3940 61.1270 -4.7564 440.0240 444.7804 420.3689 61.3100 -4.7592 440.0290 444.7882 420.3632 61.4920 -4.7602 440.0150 444.7752 420.3350 61.6750 -4.7699 440.0134 444.7833 420.3233 61.9780 -4.7740 440.0200 444.7940 420.2932 62.1620 -4.7756 440.0155 444.7911 420.2595 62.3440 -4.7793 440.0282 444.8075 420.2516 62.5270 -4.7848 440.0180 444.8028 420.2406 62.7100 -4.7820 440.0224 444.8044 420.2381 62.8930 -4.7845 440.0194 444.8039 420.2354 63.0760 -4.7859 440.0116 444.7975 420.2110 63.3790 -4.7925 440.0232 444.8156 420.1743 63.5620 -4.7943 440.0090 444.8033 420.1561 63.7450 -4.7962 440.0021 444.7984 420.1447 63.9280 -4.7952 439.9977 444.7929 420.1332 64.1110 -4.7884 439.9994 444.7877 420.1146 64.2940 -4.7913 440.0038 444.7951 420.1013 64.4770 -4.7963 440.0136 444.8099 420.1033 64.7800 -4.8004 440.0217 444.8221 420.0641 64.9630 -4.8017 440.0280 444.8297 420.0637 65.1460 -4.8076 440.0124 444.8200 420.0504 65.3290 -4.8088 440.0151 444.8239 420.0296 65.5120 -4.8096 440.0138 444.8234 420.0211 65.6950 -4.8096 440.0081 444.8177 419.9948 65.8780 -4.8105 440.0055 444.8160 419.9816 66.1810 -4.8105 439.9971 444.8076 419.9474 66.3640 -4.8087 439.9944 444.8031 419.9404 66.5470 -4.8100 439.9962 444.8061 419.9323 66.7300 -4.8106 439.9878 444.7984 419.9138 66.9130 -4.8100 439.9904 444.8005 419.9125 67.0960 -4.8112 439.9882 444.7994 419.8987 67.3990 -4.8071 439.9812 444.7883 419.8862 67.5820 -4.8100 439.9859 444.7959 419.8667 67.7650 -4.8095 439.9973 444.8068 419.8587 67.9480 -4.8082 439.9871 444.7953 419.8600 68.1310 -4.8107 439.9901 444.8008 419.8421 68.3140 -4.8102 439.9825 444.7927 419.8219 68.4970 -4.8119 439.9859 444.7978 419.8126 68.8000 -4.8152 439.9816 444.7968 419.7791 68.9830 -4.8170 439.9759 444.7930 419.7722 69.1660 -4.8172 439.9759 444.7931 419.7519 69.3490 -4.8164 439.9694 444.7858 419.7603 69.5320 -4.8150 439.9689 444.7839 419.7262 69.7150 -4.8165 439.9743 444.7907 419.7172 69.8980 -4.8145 439.9897 444.8042 419.7041 70.2010 -4.8141 439.9587 444.7729 419.6783 70.3840 -4.8143 439.9836 444.7979 419.6621 70.5670 -4.8136 439.9866 444.8002 419.6410 70.7500 -4.8165 439.9828 444.7993 419.6423 70.9330 -4.8165 439.9599 444.7764 419.6233 71.1160 -4.8190 439.9627 444.7817 419.6085 71.4190 -4.8165 439.9558 444.7723 419.5739 71.6020 -4.8136 439.9497 444.7633 419.5642 71.7850 -4.8148 439.9430 444.7578 419.5439 71.9680 -4.8117 439.9414 444.7531 419.5181 72.1510 -4.8131 439.9350 444.7480 419.5062 72.3340 -4.8156 439.9314 444.7470 419.4954 72.5170 -4.8166 439.9371 444.7537 419.4876 72.8200 -4.8175 439.9584 444.7759 419.4543 73.0030 -4.8171 439.9341 444.7512 419.4313 73.1860 -4.8198 439.9389 444.7588 419.4144 73.3690 -4.8211 439.9433 444.7644 419.4053 73.5520 -4.8166 439.9408 444.7574 419.3885 73.7350 -4.8147 439.9387 444.7534 419.3713 73.9180 -4.8153 439.9449 444.7602 419.3605 74.2210 -4.8147 439.9161 444.7308 419.3261 74.4040 -4.8171 439.9173 444.7345 419.3116 74.5860 -4.8213 439.9210 444.7423 419.2841 74.7690 -4.8213 439.9195 444.7408 419.2783 74.9520 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